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HomeMy WebLinkAboutSB-0244 Appendix T - Lab DataJune 06, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5063325 5063325 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5063325 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5063325 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5063325001 SBI068:AMW6I:S040053 Solid 05/21/12 09:07 05/23/12 07:30 5063325002 SBI068:AMW6I:S200213 Solid 05/21/12 09:44 05/23/12 07:30 5063325003 SBI068:AMW6I:S200213A Solid 05/21/12 09:44 05/23/12 07:30 5063325004 SBI068:AMW7I:S040055 Solid 05/22/12 07:52 05/23/12 07:30 5063325005 SBI068:AMW7I:S200211 Solid 05/22/12 08:33 05/23/12 07:30 5063325006 SBI068:AMW7I:S200211A Solid 05/22/12 08:33 05/23/12 07:30 5063325007 SBI068:FB1:W052112 Water 05/21/12 12:00 05/23/12 07:30 5063325008 SBI068:FB2:W052212 Water 05/21/12 08:00 05/23/12 07:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5063325 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5063325001 SBI068:AMW6I:S040053 EPA 8260 73GRM ASTM D2974-87 1DAE 5063325002 SBI068:AMW6I:S200213 EPA 8260 73GRM ASTM D2974-87 1DAE 5063325003 SBI068:AMW6I:S200213A EPA 8260 73GRM ASTM D2974-87 1DAE 5063325004 SBI068:AMW7I:S040055 EPA 8260 73GRM ASTM D2974-87 1DAE 5063325005 SBI068:AMW7I:S200211 EPA 8260 73GRM ASTM D2974-87 1DAE 5063325006 SBI068:AMW7I:S200211A EPA 8260 73GRM ASTM D2974-87 1DAE 5063325007 SBI068:FB1:W052112 EPA 8260 73GRM 5063325008 SBI068:FB2:W052212 EPA 8260 73GRM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S040053 Lab ID:5063325001 Collected:05/21/12 09:07 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/24/12 20:31 67-64-187.9 Acrolein ND ug/kg 1 05/24/12 20:31 107-02-887.9 Acrylonitrile ND ug/kg 1 05/24/12 20:31 107-13-187.9 Benzene ND ug/kg 1 05/24/12 20:31 71-43-24.4 Bromobenzene ND ug/kg 1 05/24/12 20:31 108-86-14.4 Bromochloromethane ND ug/kg 1 05/24/12 20:31 74-97-54.4 Bromodichloromethane ND ug/kg 1 05/24/12 20:31 75-27-44.4 Bromoform ND ug/kg 1 05/24/12 20:31 75-25-24.4 Bromomethane ND ug/kg 1 05/24/12 20:31 74-83-94.4 2-Butanone (MEK)ND ug/kg 1 05/24/12 20:31 78-93-322.0 n-Butylbenzene ND ug/kg 1 05/24/12 20:31 104-51-84.4 sec-Butylbenzene ND ug/kg 1 05/24/12 20:31 135-98-84.4 tert-Butylbenzene ND ug/kg 1 05/24/12 20:31 98-06-64.4 Carbon disulfide ND ug/kg 1 05/24/12 20:31 75-15-08.8 Carbon tetrachloride ND ug/kg 1 05/24/12 20:31 56-23-54.4 Chlorobenzene ND ug/kg 1 05/24/12 20:31 108-90-74.4 Chloroethane ND ug/kg 1 05/24/12 20:31 75-00-34.4 Chloroform ND ug/kg 1 05/24/12 20:31 67-66-34.4 Chloromethane ND ug/kg 1 05/24/12 20:31 74-87-34.4 2-Chlorotoluene ND ug/kg 1 05/24/12 20:31 95-49-84.4 4-Chlorotoluene ND ug/kg 1 05/24/12 20:31 106-43-44.4 Dibromochloromethane ND ug/kg 1 05/24/12 20:31 124-48-14.4 1,2-Dibromoethane (EDB)ND ug/kg 1 05/24/12 20:31 106-93-44.4 Dibromomethane ND ug/kg 1 05/24/12 20:31 74-95-34.4 1,2-Dichlorobenzene ND ug/kg 1 05/24/12 20:31 95-50-14.4 1,3-Dichlorobenzene ND ug/kg 1 05/24/12 20:31 541-73-14.4 1,4-Dichlorobenzene ND ug/kg 1 05/24/12 20:31 106-46-74.4 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/24/12 20:31 110-57-687.9 Dichlorodifluoromethane ND ug/kg 1 05/24/12 20:31 75-71-84.4 1,1-Dichloroethane ND ug/kg 1 05/24/12 20:31 75-34-34.4 1,2-Dichloroethane ND ug/kg 1 05/24/12 20:31 107-06-24.4 1,1-Dichloroethene ND ug/kg 1 05/24/12 20:31 75-35-44.4 cis-1,2-Dichloroethene ND ug/kg 1 05/24/12 20:31 156-59-24.4 trans-1,2-Dichloroethene ND ug/kg 1 05/24/12 20:31 156-60-54.4 1,2-Dichloropropane ND ug/kg 1 05/24/12 20:31 78-87-54.4 1,3-Dichloropropane ND ug/kg 1 05/24/12 20:31 142-28-94.4 2,2-Dichloropropane ND ug/kg 1 05/24/12 20:31 594-20-74.4 1,1-Dichloropropene ND ug/kg 1 05/24/12 20:31 563-58-64.4 cis-1,3-Dichloropropene ND ug/kg 1 05/24/12 20:31 10061-01-54.4 trans-1,3-Dichloropropene ND ug/kg 1 05/24/12 20:31 10061-02-64.4 Ethylbenzene ND ug/kg 1 05/24/12 20:31 100-41-44.4 Ethyl methacrylate ND ug/kg 1 05/24/12 20:31 97-63-287.9 Hexachloro-1,3-butadiene ND ug/kg 1 05/24/12 20:31 87-68-34.4 n-Hexane ND ug/kg 1 05/24/12 20:31 110-54-34.4 2-Hexanone ND ug/kg 1 05/24/12 20:31 591-78-687.9 Iodomethane ND ug/kg 1 05/24/12 20:31 74-88-487.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 5 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S040053 Lab ID:5063325001 Collected:05/21/12 09:07 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/24/12 20:31 98-82-84.4 p-Isopropyltoluene ND ug/kg 1 05/24/12 20:31 99-87-64.4 Methylene Chloride ND ug/kg 1 05/24/12 20:31 75-09-217.6 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/24/12 20:31 108-10-122.0 Methyl-tert-butyl ether ND ug/kg 1 05/24/12 20:31 1634-04-44.4 Naphthalene ND ug/kg 1 05/24/12 20:31 91-20-34.4 n-Propylbenzene ND ug/kg 1 05/24/12 20:31 103-65-14.4 Styrene ND ug/kg 1 05/24/12 20:31 100-42-54.4 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/24/12 20:31 630-20-64.4 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/24/12 20:31 79-34-54.4 Tetrachloroethene ND ug/kg 1 05/24/12 20:31 127-18-44.4 Toluene ND ug/kg 1 05/24/12 20:31 108-88-34.4 1,2,3-Trichlorobenzene ND ug/kg 1 05/24/12 20:31 87-61-64.4 1,2,4-Trichlorobenzene ND ug/kg 1 05/24/12 20:31 120-82-14.4 1,1,1-Trichloroethane ND ug/kg 1 05/24/12 20:31 71-55-64.4 1,1,2-Trichloroethane ND ug/kg 1 05/24/12 20:31 79-00-54.4 Trichloroethene ND ug/kg 1 05/24/12 20:31 79-01-64.4 Trichlorofluoromethane ND ug/kg 1 05/24/12 20:31 75-69-44.4 1,2,3-Trichloropropane ND ug/kg 1 05/24/12 20:31 96-18-44.4 1,2,4-Trimethylbenzene ND ug/kg 1 05/24/12 20:31 95-63-64.4 1,3,5-Trimethylbenzene ND ug/kg 1 05/24/12 20:31 108-67-84.4 Vinyl acetate ND ug/kg 1 05/24/12 20:31 108-05-487.9 Vinyl chloride ND ug/kg 1 05/24/12 20:31 75-01-44.4 Xylene (Total)ND ug/kg 1 05/24/12 20:31 1330-20-78.8 Surrogates Dibromofluoromethane (S)91 %.1 05/24/12 20:31 1868-53-771-125 Toluene-d8 (S)99 %.1 05/24/12 20:31 2037-26-576-124 4-Bromofluorobenzene (S)97 %.1 05/24/12 20:31 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 05/30/12 18:070.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 6 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S200213 Lab ID:5063325002 Collected:05/21/12 09:44 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/24/12 22:09 67-64-189.8 Acrolein ND ug/kg 1 05/24/12 22:09 107-02-889.8 Acrylonitrile ND ug/kg 1 05/24/12 22:09 107-13-189.8 Benzene ND ug/kg 1 05/24/12 22:09 71-43-24.5 Bromobenzene ND ug/kg 1 05/24/12 22:09 108-86-14.5 Bromochloromethane ND ug/kg 1 05/24/12 22:09 74-97-54.5 Bromodichloromethane ND ug/kg 1 05/24/12 22:09 75-27-44.5 Bromoform ND ug/kg 1 05/24/12 22:09 75-25-24.5 Bromomethane ND ug/kg 1 05/24/12 22:09 74-83-94.5 2-Butanone (MEK)ND ug/kg 1 05/24/12 22:09 78-93-322.5 n-Butylbenzene ND ug/kg 1 05/24/12 22:09 104-51-84.5 sec-Butylbenzene ND ug/kg 1 05/24/12 22:09 135-98-84.5 tert-Butylbenzene ND ug/kg 1 05/24/12 22:09 98-06-64.5 Carbon disulfide ND ug/kg 1 05/24/12 22:09 75-15-09.0 Carbon tetrachloride ND ug/kg 1 05/24/12 22:09 56-23-54.5 Chlorobenzene ND ug/kg 1 05/24/12 22:09 108-90-74.5 Chloroethane ND ug/kg 1 05/24/12 22:09 75-00-34.5 Chloroform ND ug/kg 1 05/24/12 22:09 67-66-34.5 Chloromethane ND ug/kg 1 05/24/12 22:09 74-87-34.5 2-Chlorotoluene ND ug/kg 1 05/24/12 22:09 95-49-84.5 4-Chlorotoluene ND ug/kg 1 05/24/12 22:09 106-43-44.5 Dibromochloromethane ND ug/kg 1 05/24/12 22:09 124-48-14.5 1,2-Dibromoethane (EDB)ND ug/kg 1 05/24/12 22:09 106-93-44.5 Dibromomethane ND ug/kg 1 05/24/12 22:09 74-95-34.5 1,2-Dichlorobenzene ND ug/kg 1 05/24/12 22:09 95-50-14.5 1,3-Dichlorobenzene ND ug/kg 1 05/24/12 22:09 541-73-14.5 1,4-Dichlorobenzene ND ug/kg 1 05/24/12 22:09 106-46-74.5 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/24/12 22:09 110-57-689.8 Dichlorodifluoromethane ND ug/kg 1 05/24/12 22:09 75-71-84.5 1,1-Dichloroethane ND ug/kg 1 05/24/12 22:09 75-34-34.5 1,2-Dichloroethane ND ug/kg 1 05/24/12 22:09 107-06-24.5 1,1-Dichloroethene ND ug/kg 1 05/24/12 22:09 75-35-44.5 cis-1,2-Dichloroethene ND ug/kg 1 05/24/12 22:09 156-59-24.5 trans-1,2-Dichloroethene ND ug/kg 1 05/24/12 22:09 156-60-54.5 1,2-Dichloropropane ND ug/kg 1 05/24/12 22:09 78-87-54.5 1,3-Dichloropropane ND ug/kg 1 05/24/12 22:09 142-28-94.5 2,2-Dichloropropane ND ug/kg 1 05/24/12 22:09 594-20-74.5 1,1-Dichloropropene ND ug/kg 1 05/24/12 22:09 563-58-64.5 cis-1,3-Dichloropropene ND ug/kg 1 05/24/12 22:09 10061-01-54.5 trans-1,3-Dichloropropene ND ug/kg 1 05/24/12 22:09 10061-02-64.5 Ethylbenzene ND ug/kg 1 05/24/12 22:09 100-41-44.5 Ethyl methacrylate ND ug/kg 1 05/24/12 22:09 97-63-289.8 Hexachloro-1,3-butadiene ND ug/kg 1 05/24/12 22:09 87-68-34.5 n-Hexane ND ug/kg 1 05/24/12 22:09 110-54-34.5 2-Hexanone ND ug/kg 1 05/24/12 22:09 591-78-689.8 Iodomethane ND ug/kg 1 05/24/12 22:09 74-88-489.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 7 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S200213 Lab ID:5063325002 Collected:05/21/12 09:44 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/24/12 22:09 98-82-84.5 p-Isopropyltoluene ND ug/kg 1 05/24/12 22:09 99-87-64.5 Methylene Chloride ND ug/kg 1 05/24/12 22:09 75-09-218.0 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/24/12 22:09 108-10-122.5 Methyl-tert-butyl ether ND ug/kg 1 05/24/12 22:09 1634-04-44.5 Naphthalene ND ug/kg 1 05/24/12 22:09 91-20-34.5 n-Propylbenzene ND ug/kg 1 05/24/12 22:09 103-65-14.5 Styrene ND ug/kg 1 05/24/12 22:09 100-42-54.5 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/24/12 22:09 630-20-64.5 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/24/12 22:09 79-34-54.5 Tetrachloroethene ND ug/kg 1 05/24/12 22:09 127-18-44.5 Toluene ND ug/kg 1 05/24/12 22:09 108-88-34.5 1,2,3-Trichlorobenzene ND ug/kg 1 05/24/12 22:09 87-61-64.5 1,2,4-Trichlorobenzene ND ug/kg 1 05/24/12 22:09 120-82-14.5 1,1,1-Trichloroethane ND ug/kg 1 05/24/12 22:09 71-55-64.5 1,1,2-Trichloroethane ND ug/kg 1 05/24/12 22:09 79-00-54.5 Trichloroethene ND ug/kg 1 05/24/12 22:09 79-01-64.5 Trichlorofluoromethane ND ug/kg 1 05/24/12 22:09 75-69-44.5 1,2,3-Trichloropropane ND ug/kg 1 05/24/12 22:09 96-18-44.5 1,2,4-Trimethylbenzene ND ug/kg 1 05/24/12 22:09 95-63-64.5 1,3,5-Trimethylbenzene ND ug/kg 1 05/24/12 22:09 108-67-84.5 Vinyl acetate ND ug/kg 1 05/24/12 22:09 108-05-489.8 Vinyl chloride ND ug/kg 1 05/24/12 22:09 75-01-44.5 Xylene (Total)ND ug/kg 1 05/24/12 22:09 1330-20-79.0 Surrogates Dibromofluoromethane (S)94 %.1 05/24/12 22:09 1868-53-771-125 Toluene-d8 (S)99 %.1 05/24/12 22:09 2037-26-576-124 4-Bromofluorobenzene (S)99 %.1 05/24/12 22:09 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.1 %1 05/30/12 18:080.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 8 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S200213A Lab ID:5063325003 Collected:05/21/12 09:44 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/24/12 22:41 67-64-183.5 Acrolein ND ug/kg 1 05/24/12 22:41 107-02-883.5 Acrylonitrile ND ug/kg 1 05/24/12 22:41 107-13-183.5 Benzene ND ug/kg 1 05/24/12 22:41 71-43-24.2 Bromobenzene ND ug/kg 1 05/24/12 22:41 108-86-14.2 Bromochloromethane ND ug/kg 1 05/24/12 22:41 74-97-54.2 Bromodichloromethane ND ug/kg 1 05/24/12 22:41 75-27-44.2 Bromoform ND ug/kg 1 05/24/12 22:41 75-25-24.2 Bromomethane ND ug/kg 1 05/24/12 22:41 74-83-94.2 2-Butanone (MEK)ND ug/kg 1 05/24/12 22:41 78-93-320.9 n-Butylbenzene ND ug/kg 1 05/24/12 22:41 104-51-84.2 sec-Butylbenzene ND ug/kg 1 05/24/12 22:41 135-98-84.2 tert-Butylbenzene ND ug/kg 1 05/24/12 22:41 98-06-64.2 Carbon disulfide ND ug/kg 1 05/24/12 22:41 75-15-08.3 Carbon tetrachloride ND ug/kg 1 05/24/12 22:41 56-23-54.2 Chlorobenzene ND ug/kg 1 05/24/12 22:41 108-90-74.2 Chloroethane ND ug/kg 1 05/24/12 22:41 75-00-34.2 Chloroform ND ug/kg 1 05/24/12 22:41 67-66-34.2 Chloromethane ND ug/kg 1 05/24/12 22:41 74-87-34.2 2-Chlorotoluene ND ug/kg 1 05/24/12 22:41 95-49-84.2 4-Chlorotoluene ND ug/kg 1 05/24/12 22:41 106-43-44.2 Dibromochloromethane ND ug/kg 1 05/24/12 22:41 124-48-14.2 1,2-Dibromoethane (EDB)ND ug/kg 1 05/24/12 22:41 106-93-44.2 Dibromomethane ND ug/kg 1 05/24/12 22:41 74-95-34.2 1,2-Dichlorobenzene ND ug/kg 1 05/24/12 22:41 95-50-14.2 1,3-Dichlorobenzene ND ug/kg 1 05/24/12 22:41 541-73-14.2 1,4-Dichlorobenzene ND ug/kg 1 05/24/12 22:41 106-46-74.2 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/24/12 22:41 110-57-683.5 Dichlorodifluoromethane ND ug/kg 1 05/24/12 22:41 75-71-84.2 1,1-Dichloroethane ND ug/kg 1 05/24/12 22:41 75-34-34.2 1,2-Dichloroethane ND ug/kg 1 05/24/12 22:41 107-06-24.2 1,1-Dichloroethene ND ug/kg 1 05/24/12 22:41 75-35-44.2 cis-1,2-Dichloroethene ND ug/kg 1 05/24/12 22:41 156-59-24.2 trans-1,2-Dichloroethene ND ug/kg 1 05/24/12 22:41 156-60-54.2 1,2-Dichloropropane ND ug/kg 1 05/24/12 22:41 78-87-54.2 1,3-Dichloropropane ND ug/kg 1 05/24/12 22:41 142-28-94.2 2,2-Dichloropropane ND ug/kg 1 05/24/12 22:41 594-20-74.2 1,1-Dichloropropene ND ug/kg 1 05/24/12 22:41 563-58-64.2 cis-1,3-Dichloropropene ND ug/kg 1 05/24/12 22:41 10061-01-54.2 trans-1,3-Dichloropropene ND ug/kg 1 05/24/12 22:41 10061-02-64.2 Ethylbenzene ND ug/kg 1 05/24/12 22:41 100-41-44.2 Ethyl methacrylate ND ug/kg 1 05/24/12 22:41 97-63-283.5 Hexachloro-1,3-butadiene ND ug/kg 1 05/24/12 22:41 87-68-34.2 n-Hexane ND ug/kg 1 05/24/12 22:41 110-54-34.2 2-Hexanone ND ug/kg 1 05/24/12 22:41 591-78-683.5 Iodomethane ND ug/kg 1 05/24/12 22:41 74-88-483.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 9 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW6I:S200213A Lab ID:5063325003 Collected:05/21/12 09:44 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/24/12 22:41 98-82-84.2 p-Isopropyltoluene ND ug/kg 1 05/24/12 22:41 99-87-64.2 Methylene Chloride ND ug/kg 1 05/24/12 22:41 75-09-216.7 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/24/12 22:41 108-10-120.9 Methyl-tert-butyl ether ND ug/kg 1 05/24/12 22:41 1634-04-44.2 Naphthalene ND ug/kg 1 05/24/12 22:41 91-20-34.2 n-Propylbenzene ND ug/kg 1 05/24/12 22:41 103-65-14.2 Styrene ND ug/kg 1 05/24/12 22:41 100-42-54.2 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/24/12 22:41 630-20-64.2 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/24/12 22:41 79-34-54.2 Tetrachloroethene ND ug/kg 1 05/24/12 22:41 127-18-44.2 Toluene ND ug/kg 1 05/24/12 22:41 108-88-34.2 1,2,3-Trichlorobenzene ND ug/kg 1 05/24/12 22:41 87-61-64.2 1,2,4-Trichlorobenzene ND ug/kg 1 05/24/12 22:41 120-82-14.2 1,1,1-Trichloroethane ND ug/kg 1 05/24/12 22:41 71-55-64.2 1,1,2-Trichloroethane ND ug/kg 1 05/24/12 22:41 79-00-54.2 Trichloroethene ND ug/kg 1 05/24/12 22:41 79-01-64.2 Trichlorofluoromethane ND ug/kg 1 05/24/12 22:41 75-69-44.2 1,2,3-Trichloropropane ND ug/kg 1 05/24/12 22:41 96-18-44.2 1,2,4-Trimethylbenzene ND ug/kg 1 05/24/12 22:41 95-63-64.2 1,3,5-Trimethylbenzene ND ug/kg 1 05/24/12 22:41 108-67-84.2 Vinyl acetate ND ug/kg 1 05/24/12 22:41 108-05-483.5 Vinyl chloride ND ug/kg 1 05/24/12 22:41 75-01-44.2 Xylene (Total)ND ug/kg 1 05/24/12 22:41 1330-20-78.3 Surrogates Dibromofluoromethane (S)93 %.1 05/24/12 22:41 1868-53-771-125 Toluene-d8 (S)99 %.1 05/24/12 22:41 2037-26-576-124 4-Bromofluorobenzene (S)99 %.1 05/24/12 22:41 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.9 %1 05/30/12 18:080.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 10 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S040055 Lab ID:5063325004 Collected:05/22/12 07:52 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/24/12 23:14 67-64-178.8 Acrolein ND ug/kg 1 05/24/12 23:14 107-02-878.8 Acrylonitrile ND ug/kg 1 05/24/12 23:14 107-13-178.8 Benzene ND ug/kg 1 05/24/12 23:14 71-43-23.9 Bromobenzene ND ug/kg 1 05/24/12 23:14 108-86-13.9 Bromochloromethane ND ug/kg 1 05/24/12 23:14 74-97-53.9 Bromodichloromethane ND ug/kg 1 05/24/12 23:14 75-27-43.9 Bromoform ND ug/kg 1 05/24/12 23:14 75-25-23.9 Bromomethane ND ug/kg 1 05/24/12 23:14 74-83-93.9 2-Butanone (MEK)ND ug/kg 1 05/24/12 23:14 78-93-319.7 n-Butylbenzene ND ug/kg 1 05/24/12 23:14 104-51-83.9 sec-Butylbenzene ND ug/kg 1 05/24/12 23:14 135-98-83.9 tert-Butylbenzene ND ug/kg 1 05/24/12 23:14 98-06-63.9 Carbon disulfide ND ug/kg 1 05/24/12 23:14 75-15-07.9 Carbon tetrachloride ND ug/kg 1 05/24/12 23:14 56-23-53.9 Chlorobenzene ND ug/kg 1 05/24/12 23:14 108-90-73.9 Chloroethane ND ug/kg 1 05/24/12 23:14 75-00-33.9 Chloroform ND ug/kg 1 05/24/12 23:14 67-66-33.9 Chloromethane ND ug/kg 1 05/24/12 23:14 74-87-33.9 2-Chlorotoluene ND ug/kg 1 05/24/12 23:14 95-49-83.9 4-Chlorotoluene ND ug/kg 1 05/24/12 23:14 106-43-43.9 Dibromochloromethane ND ug/kg 1 05/24/12 23:14 124-48-13.9 1,2-Dibromoethane (EDB)ND ug/kg 1 05/24/12 23:14 106-93-43.9 Dibromomethane ND ug/kg 1 05/24/12 23:14 74-95-33.9 1,2-Dichlorobenzene ND ug/kg 1 05/24/12 23:14 95-50-13.9 1,3-Dichlorobenzene ND ug/kg 1 05/24/12 23:14 541-73-13.9 1,4-Dichlorobenzene ND ug/kg 1 05/24/12 23:14 106-46-73.9 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/24/12 23:14 110-57-678.8 Dichlorodifluoromethane ND ug/kg 1 05/24/12 23:14 75-71-83.9 1,1-Dichloroethane ND ug/kg 1 05/24/12 23:14 75-34-33.9 1,2-Dichloroethane ND ug/kg 1 05/24/12 23:14 107-06-23.9 1,1-Dichloroethene ND ug/kg 1 05/24/12 23:14 75-35-43.9 cis-1,2-Dichloroethene ND ug/kg 1 05/24/12 23:14 156-59-23.9 trans-1,2-Dichloroethene ND ug/kg 1 05/24/12 23:14 156-60-53.9 1,2-Dichloropropane ND ug/kg 1 05/24/12 23:14 78-87-53.9 1,3-Dichloropropane ND ug/kg 1 05/24/12 23:14 142-28-93.9 2,2-Dichloropropane ND ug/kg 1 05/24/12 23:14 594-20-73.9 1,1-Dichloropropene ND ug/kg 1 05/24/12 23:14 563-58-63.9 cis-1,3-Dichloropropene ND ug/kg 1 05/24/12 23:14 10061-01-53.9 trans-1,3-Dichloropropene ND ug/kg 1 05/24/12 23:14 10061-02-63.9 Ethylbenzene ND ug/kg 1 05/24/12 23:14 100-41-43.9 Ethyl methacrylate ND ug/kg 1 05/24/12 23:14 97-63-278.8 Hexachloro-1,3-butadiene ND ug/kg 1 05/24/12 23:14 87-68-33.9 n-Hexane ND ug/kg 1 05/24/12 23:14 110-54-33.9 2-Hexanone ND ug/kg 1 05/24/12 23:14 591-78-678.8 Iodomethane ND ug/kg 1 05/24/12 23:14 74-88-478.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 11 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S040055 Lab ID:5063325004 Collected:05/22/12 07:52 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/24/12 23:14 98-82-83.9 p-Isopropyltoluene ND ug/kg 1 05/24/12 23:14 99-87-63.9 Methylene Chloride ND ug/kg 1 05/24/12 23:14 75-09-215.8 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/24/12 23:14 108-10-119.7 Methyl-tert-butyl ether ND ug/kg 1 05/24/12 23:14 1634-04-43.9 Naphthalene ND ug/kg 1 05/24/12 23:14 91-20-33.9 n-Propylbenzene ND ug/kg 1 05/24/12 23:14 103-65-13.9 Styrene ND ug/kg 1 05/24/12 23:14 100-42-53.9 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/24/12 23:14 630-20-63.9 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/24/12 23:14 79-34-53.9 Tetrachloroethene ND ug/kg 1 05/24/12 23:14 127-18-43.9 Toluene ND ug/kg 1 05/24/12 23:14 108-88-33.9 1,2,3-Trichlorobenzene ND ug/kg 1 05/24/12 23:14 87-61-63.9 1,2,4-Trichlorobenzene ND ug/kg 1 05/24/12 23:14 120-82-13.9 1,1,1-Trichloroethane ND ug/kg 1 05/24/12 23:14 71-55-63.9 1,1,2-Trichloroethane ND ug/kg 1 05/24/12 23:14 79-00-53.9 Trichloroethene ND ug/kg 1 05/24/12 23:14 79-01-63.9 Trichlorofluoromethane ND ug/kg 1 05/24/12 23:14 75-69-43.9 1,2,3-Trichloropropane ND ug/kg 1 05/24/12 23:14 96-18-43.9 1,2,4-Trimethylbenzene ND ug/kg 1 05/24/12 23:14 95-63-63.9 1,3,5-Trimethylbenzene ND ug/kg 1 05/24/12 23:14 108-67-83.9 Vinyl acetate ND ug/kg 1 05/24/12 23:14 108-05-478.8 Vinyl chloride ND ug/kg 1 05/24/12 23:14 75-01-43.9 Xylene (Total)ND ug/kg 1 05/24/12 23:14 1330-20-77.9 Surrogates Dibromofluoromethane (S)93 %.1 05/24/12 23:14 1868-53-771-125 Toluene-d8 (S)99 %.1 05/24/12 23:14 2037-26-576-124 4-Bromofluorobenzene (S)97 %.1 05/24/12 23:14 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.6 %1 05/30/12 18:080.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 12 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S200211 Lab ID:5063325005 Collected:05/22/12 08:33 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/25/12 03:00 67-64-185.2 Acrolein ND ug/kg 1 05/25/12 03:00 107-02-885.2 Acrylonitrile ND ug/kg 1 05/25/12 03:00 107-13-185.2 Benzene ND ug/kg 1 05/25/12 03:00 71-43-24.3 Bromobenzene ND ug/kg 1 05/25/12 03:00 108-86-14.3 Bromochloromethane ND ug/kg 1 05/25/12 03:00 74-97-54.3 Bromodichloromethane ND ug/kg 1 05/25/12 03:00 75-27-44.3 Bromoform ND ug/kg 1 05/25/12 03:00 75-25-24.3 Bromomethane ND ug/kg 1 05/25/12 03:00 74-83-94.3 2-Butanone (MEK)ND ug/kg 1 05/25/12 03:00 78-93-321.3 n-Butylbenzene ND ug/kg 1 05/25/12 03:00 104-51-84.3 sec-Butylbenzene ND ug/kg 1 05/25/12 03:00 135-98-84.3 tert-Butylbenzene ND ug/kg 1 05/25/12 03:00 98-06-64.3 Carbon disulfide ND ug/kg 1 05/25/12 03:00 75-15-08.5 Carbon tetrachloride ND ug/kg 1 05/25/12 03:00 56-23-54.3 Chlorobenzene ND ug/kg 1 05/25/12 03:00 108-90-74.3 Chloroethane ND ug/kg 1 05/25/12 03:00 75-00-34.3 Chloroform ND ug/kg 1 05/25/12 03:00 67-66-34.3 Chloromethane ND ug/kg 1 05/25/12 03:00 74-87-34.3 2-Chlorotoluene ND ug/kg 1 05/25/12 03:00 95-49-84.3 4-Chlorotoluene ND ug/kg 1 05/25/12 03:00 106-43-44.3 Dibromochloromethane ND ug/kg 1 05/25/12 03:00 124-48-14.3 1,2-Dibromoethane (EDB)ND ug/kg 1 05/25/12 03:00 106-93-44.3 Dibromomethane ND ug/kg 1 05/25/12 03:00 74-95-34.3 1,2-Dichlorobenzene ND ug/kg 1 05/25/12 03:00 95-50-14.3 1,3-Dichlorobenzene ND ug/kg 1 05/25/12 03:00 541-73-14.3 1,4-Dichlorobenzene ND ug/kg 1 05/25/12 03:00 106-46-74.3 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/25/12 03:00 110-57-685.2 Dichlorodifluoromethane ND ug/kg 1 05/25/12 03:00 75-71-84.3 1,1-Dichloroethane ND ug/kg 1 05/25/12 03:00 75-34-34.3 1,2-Dichloroethane ND ug/kg 1 05/25/12 03:00 107-06-24.3 1,1-Dichloroethene ND ug/kg 1 05/25/12 03:00 75-35-44.3 cis-1,2-Dichloroethene ND ug/kg 1 05/25/12 03:00 156-59-24.3 trans-1,2-Dichloroethene ND ug/kg 1 05/25/12 03:00 156-60-54.3 1,2-Dichloropropane ND ug/kg 1 05/25/12 03:00 78-87-54.3 1,3-Dichloropropane ND ug/kg 1 05/25/12 03:00 142-28-94.3 2,2-Dichloropropane ND ug/kg 1 05/25/12 03:00 594-20-74.3 1,1-Dichloropropene ND ug/kg 1 05/25/12 03:00 563-58-64.3 cis-1,3-Dichloropropene ND ug/kg 1 05/25/12 03:00 10061-01-54.3 trans-1,3-Dichloropropene ND ug/kg 1 05/25/12 03:00 10061-02-64.3 Ethylbenzene ND ug/kg 1 05/25/12 03:00 100-41-44.3 Ethyl methacrylate ND ug/kg 1 05/25/12 03:00 97-63-285.2 Hexachloro-1,3-butadiene ND ug/kg 1 05/25/12 03:00 87-68-34.3 n-Hexane ND ug/kg 1 05/25/12 03:00 110-54-34.3 2-Hexanone ND ug/kg 1 05/25/12 03:00 591-78-685.2 Iodomethane ND ug/kg 1 05/25/12 03:00 74-88-485.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 13 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S200211 Lab ID:5063325005 Collected:05/22/12 08:33 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/25/12 03:00 98-82-84.3 p-Isopropyltoluene ND ug/kg 1 05/25/12 03:00 99-87-64.3 Methylene Chloride ND ug/kg 1 05/25/12 03:00 75-09-217.0 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/25/12 03:00 108-10-121.3 Methyl-tert-butyl ether ND ug/kg 1 05/25/12 03:00 1634-04-44.3 Naphthalene ND ug/kg 1 05/25/12 03:00 91-20-34.3 n-Propylbenzene ND ug/kg 1 05/25/12 03:00 103-65-14.3 Styrene ND ug/kg 1 05/25/12 03:00 100-42-54.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/25/12 03:00 630-20-64.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/25/12 03:00 79-34-54.3 Tetrachloroethene ND ug/kg 1 05/25/12 03:00 127-18-44.3 Toluene ND ug/kg 1 05/25/12 03:00 108-88-34.3 1,2,3-Trichlorobenzene ND ug/kg 1 05/25/12 03:00 87-61-64.3 1,2,4-Trichlorobenzene ND ug/kg 1 05/25/12 03:00 120-82-14.3 1,1,1-Trichloroethane ND ug/kg 1 05/25/12 03:00 71-55-64.3 1,1,2-Trichloroethane ND ug/kg 1 05/25/12 03:00 79-00-54.3 Trichloroethene ND ug/kg 1 05/25/12 03:00 79-01-64.3 Trichlorofluoromethane ND ug/kg 1 05/25/12 03:00 75-69-44.3 1,2,3-Trichloropropane ND ug/kg 1 05/25/12 03:00 96-18-44.3 1,2,4-Trimethylbenzene ND ug/kg 1 05/25/12 03:00 95-63-64.3 1,3,5-Trimethylbenzene ND ug/kg 1 05/25/12 03:00 108-67-84.3 Vinyl acetate ND ug/kg 1 05/25/12 03:00 108-05-485.2 Vinyl chloride ND ug/kg 1 05/25/12 03:00 75-01-44.3 Xylene (Total)ND ug/kg 1 05/25/12 03:00 1330-20-78.5 Surrogates Dibromofluoromethane (S)94 %.1 05/25/12 03:00 1868-53-771-125 Toluene-d8 (S)101 %.1 05/25/12 03:00 2037-26-576-124 4-Bromofluorobenzene (S)96 %.1 05/25/12 03:00 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.9 %1 05/30/12 18:080.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 14 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S200211A Lab ID:5063325006 Collected:05/22/12 08:33 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/25/12 03:33 67-64-186.5 Acrolein ND ug/kg 1 05/25/12 03:33 107-02-886.5 Acrylonitrile ND ug/kg 1 05/25/12 03:33 107-13-186.5 Benzene ND ug/kg 1 05/25/12 03:33 71-43-24.3 Bromobenzene ND ug/kg 1 05/25/12 03:33 108-86-14.3 Bromochloromethane ND ug/kg 1 05/25/12 03:33 74-97-54.3 Bromodichloromethane ND ug/kg 1 05/25/12 03:33 75-27-44.3 Bromoform ND ug/kg 1 05/25/12 03:33 75-25-24.3 Bromomethane ND ug/kg 1 05/25/12 03:33 74-83-94.3 2-Butanone (MEK)ND ug/kg 1 05/25/12 03:33 78-93-321.6 n-Butylbenzene ND ug/kg 1 05/25/12 03:33 104-51-84.3 sec-Butylbenzene ND ug/kg 1 05/25/12 03:33 135-98-84.3 tert-Butylbenzene ND ug/kg 1 05/25/12 03:33 98-06-64.3 Carbon disulfide ND ug/kg 1 05/25/12 03:33 75-15-08.6 Carbon tetrachloride ND ug/kg 1 05/25/12 03:33 56-23-54.3 Chlorobenzene ND ug/kg 1 05/25/12 03:33 108-90-74.3 Chloroethane ND ug/kg 1 05/25/12 03:33 75-00-34.3 Chloroform ND ug/kg 1 05/25/12 03:33 67-66-34.3 Chloromethane ND ug/kg 1 05/25/12 03:33 74-87-34.3 2-Chlorotoluene ND ug/kg 1 05/25/12 03:33 95-49-84.3 4-Chlorotoluene ND ug/kg 1 05/25/12 03:33 106-43-44.3 Dibromochloromethane ND ug/kg 1 05/25/12 03:33 124-48-14.3 1,2-Dibromoethane (EDB)ND ug/kg 1 05/25/12 03:33 106-93-44.3 Dibromomethane ND ug/kg 1 05/25/12 03:33 74-95-34.3 1,2-Dichlorobenzene ND ug/kg 1 05/25/12 03:33 95-50-14.3 1,3-Dichlorobenzene ND ug/kg 1 05/25/12 03:33 541-73-14.3 1,4-Dichlorobenzene ND ug/kg 1 05/25/12 03:33 106-46-74.3 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/25/12 03:33 110-57-686.5 Dichlorodifluoromethane ND ug/kg 1 05/25/12 03:33 75-71-84.3 1,1-Dichloroethane ND ug/kg 1 05/25/12 03:33 75-34-34.3 1,2-Dichloroethane ND ug/kg 1 05/25/12 03:33 107-06-24.3 1,1-Dichloroethene ND ug/kg 1 05/25/12 03:33 75-35-44.3 cis-1,2-Dichloroethene ND ug/kg 1 05/25/12 03:33 156-59-24.3 trans-1,2-Dichloroethene ND ug/kg 1 05/25/12 03:33 156-60-54.3 1,2-Dichloropropane ND ug/kg 1 05/25/12 03:33 78-87-54.3 1,3-Dichloropropane ND ug/kg 1 05/25/12 03:33 142-28-94.3 2,2-Dichloropropane ND ug/kg 1 05/25/12 03:33 594-20-74.3 1,1-Dichloropropene ND ug/kg 1 05/25/12 03:33 563-58-64.3 cis-1,3-Dichloropropene ND ug/kg 1 05/25/12 03:33 10061-01-54.3 trans-1,3-Dichloropropene ND ug/kg 1 05/25/12 03:33 10061-02-64.3 Ethylbenzene ND ug/kg 1 05/25/12 03:33 100-41-44.3 Ethyl methacrylate ND ug/kg 1 05/25/12 03:33 97-63-286.5 Hexachloro-1,3-butadiene ND ug/kg 1 05/25/12 03:33 87-68-34.3 n-Hexane ND ug/kg 1 05/25/12 03:33 110-54-34.3 2-Hexanone ND ug/kg 1 05/25/12 03:33 591-78-686.5 Iodomethane ND ug/kg 1 05/25/12 03:33 74-88-486.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 15 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:AMW7I:S200211A Lab ID:5063325006 Collected:05/22/12 08:33 Received:05/23/12 07:30 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/25/12 03:33 98-82-84.3 p-Isopropyltoluene ND ug/kg 1 05/25/12 03:33 99-87-64.3 Methylene Chloride ND ug/kg 1 05/25/12 03:33 75-09-217.3 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/25/12 03:33 108-10-121.6 Methyl-tert-butyl ether ND ug/kg 1 05/25/12 03:33 1634-04-44.3 Naphthalene ND ug/kg 1 05/25/12 03:33 91-20-34.3 n-Propylbenzene ND ug/kg 1 05/25/12 03:33 103-65-14.3 Styrene ND ug/kg 1 05/25/12 03:33 100-42-54.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/25/12 03:33 630-20-64.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/25/12 03:33 79-34-54.3 Tetrachloroethene ND ug/kg 1 05/25/12 03:33 127-18-44.3 Toluene ND ug/kg 1 05/25/12 03:33 108-88-34.3 1,2,3-Trichlorobenzene ND ug/kg 1 05/25/12 03:33 87-61-64.3 1,2,4-Trichlorobenzene ND ug/kg 1 05/25/12 03:33 120-82-14.3 1,1,1-Trichloroethane ND ug/kg 1 05/25/12 03:33 71-55-64.3 1,1,2-Trichloroethane ND ug/kg 1 05/25/12 03:33 79-00-54.3 Trichloroethene ND ug/kg 1 05/25/12 03:33 79-01-64.3 Trichlorofluoromethane ND ug/kg 1 05/25/12 03:33 75-69-44.3 1,2,3-Trichloropropane ND ug/kg 1 05/25/12 03:33 96-18-44.3 1,2,4-Trimethylbenzene ND ug/kg 1 05/25/12 03:33 95-63-64.3 1,3,5-Trimethylbenzene ND ug/kg 1 05/25/12 03:33 108-67-84.3 Vinyl acetate ND ug/kg 1 05/25/12 03:33 108-05-486.5 Vinyl chloride ND ug/kg 1 05/25/12 03:33 75-01-44.3 Xylene (Total)ND ug/kg 1 05/25/12 03:33 1330-20-78.6 Surrogates Dibromofluoromethane (S)94 %.1 05/25/12 03:33 1868-53-771-125 Toluene-d8 (S)98 %.1 05/25/12 03:33 2037-26-576-124 4-Bromofluorobenzene (S)97 %.1 05/25/12 03:33 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.6 %1 05/30/12 18:080.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 16 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:FB1:W052112 Lab ID:5063325007 Collected:05/21/12 12:00 Received:05/23/12 07:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 05/24/12 19:26 67-64-1100 Acrolein ND ug/L 1 05/24/12 19:26 107-02-8100 Acrylonitrile ND ug/L 1 05/24/12 19:26 107-13-1100 Benzene ND ug/L 1 05/24/12 19:26 71-43-25.0 Bromobenzene ND ug/L 1 05/24/12 19:26 108-86-15.0 Bromochloromethane ND ug/L 1 05/24/12 19:26 74-97-55.0 Bromodichloromethane ND ug/L 1 05/24/12 19:26 75-27-45.0 Bromoform ND ug/L 1 05/24/12 19:26 75-25-25.0 Bromomethane ND ug/L 1 05/24/12 19:26 74-83-95.0 2-Butanone (MEK)ND ug/L 1 05/24/12 19:26 78-93-325.0 n-Butylbenzene ND ug/L 1 05/24/12 19:26 104-51-85.0 sec-Butylbenzene ND ug/L 1 05/24/12 19:26 135-98-85.0 tert-Butylbenzene ND ug/L 1 05/24/12 19:26 98-06-65.0 Carbon disulfide ND ug/L 1 05/24/12 19:26 75-15-010.0 Carbon tetrachloride ND ug/L 1 05/24/12 19:26 56-23-55.0 Chlorobenzene ND ug/L 1 05/24/12 19:26 108-90-75.0 Chloroethane ND ug/L 1 05/24/12 19:26 75-00-35.0 Chloroform 9.1 ug/L 1 05/24/12 19:26 67-66-3 1d5.0 Chloromethane ND ug/L 1 05/24/12 19:26 74-87-35.0 2-Chlorotoluene ND ug/L 1 05/24/12 19:26 95-49-85.0 4-Chlorotoluene ND ug/L 1 05/24/12 19:26 106-43-45.0 Dibromochloromethane ND ug/L 1 05/24/12 19:26 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 05/24/12 19:26 106-93-45.0 Dibromomethane ND ug/L 1 05/24/12 19:26 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 05/24/12 19:26 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 05/24/12 19:26 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 05/24/12 19:26 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 05/24/12 19:26 110-57-6100 Dichlorodifluoromethane ND ug/L 1 05/24/12 19:26 75-71-85.0 1,1-Dichloroethane ND ug/L 1 05/24/12 19:26 75-34-35.0 1,2-Dichloroethane ND ug/L 1 05/24/12 19:26 107-06-25.0 1,1-Dichloroethene ND ug/L 1 05/24/12 19:26 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 05/24/12 19:26 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 05/24/12 19:26 156-60-55.0 1,2-Dichloropropane ND ug/L 1 05/24/12 19:26 78-87-55.0 1,3-Dichloropropane ND ug/L 1 05/24/12 19:26 142-28-95.0 2,2-Dichloropropane ND ug/L 1 05/24/12 19:26 594-20-75.0 1,1-Dichloropropene ND ug/L 1 05/24/12 19:26 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 05/24/12 19:26 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 05/24/12 19:26 10061-02-65.0 Ethylbenzene ND ug/L 1 05/24/12 19:26 100-41-45.0 Ethyl methacrylate ND ug/L 1 05/24/12 19:26 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 05/24/12 19:26 87-68-35.0 n-Hexane ND ug/L 1 05/24/12 19:26 110-54-3 N25.0 2-Hexanone ND ug/L 1 05/24/12 19:26 591-78-625.0 Iodomethane ND ug/L 1 05/24/12 19:26 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 05/24/12 19:26 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 17 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:FB1:W052112 Lab ID:5063325007 Collected:05/21/12 12:00 Received:05/23/12 07:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 05/24/12 19:26 99-87-65.0 Methylene Chloride ND ug/L 1 05/24/12 19:26 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/24/12 19:26 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 05/24/12 19:26 1634-04-44.0 Naphthalene ND ug/L 1 05/24/12 19:26 91-20-35.0 n-Propylbenzene ND ug/L 1 05/24/12 19:26 103-65-15.0 Styrene ND ug/L 1 05/24/12 19:26 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 05/24/12 19:26 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 05/24/12 19:26 79-34-55.0 Tetrachloroethene ND ug/L 1 05/24/12 19:26 127-18-45.0 Toluene ND ug/L 1 05/24/12 19:26 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 05/24/12 19:26 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 05/24/12 19:26 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 05/24/12 19:26 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 05/24/12 19:26 79-00-55.0 Trichloroethene ND ug/L 1 05/24/12 19:26 79-01-65.0 Trichlorofluoromethane ND ug/L 1 05/24/12 19:26 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 05/24/12 19:26 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 05/24/12 19:26 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 05/24/12 19:26 108-67-85.0 Vinyl acetate ND ug/L 1 05/24/12 19:26 108-05-450.0 Vinyl chloride ND ug/L 1 05/24/12 19:26 75-01-42.0 Xylene (Total)ND ug/L 1 05/24/12 19:26 1330-20-710.0 Surrogates Dibromofluoromethane (S)93 %.1 05/24/12 19:26 1868-53-783-123 4-Bromofluorobenzene (S)97 %.1 05/24/12 19:26 460-00-472-125 Toluene-d8 (S)100 %.1 05/24/12 19:26 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 18 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:FB2:W052212 Lab ID:5063325008 Collected:05/21/12 08:00 Received:05/23/12 07:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 05/24/12 19:59 67-64-1100 Acrolein ND ug/L 1 05/24/12 19:59 107-02-8100 Acrylonitrile ND ug/L 1 05/24/12 19:59 107-13-1100 Benzene ND ug/L 1 05/24/12 19:59 71-43-25.0 Bromobenzene ND ug/L 1 05/24/12 19:59 108-86-15.0 Bromochloromethane ND ug/L 1 05/24/12 19:59 74-97-55.0 Bromodichloromethane ND ug/L 1 05/24/12 19:59 75-27-45.0 Bromoform ND ug/L 1 05/24/12 19:59 75-25-25.0 Bromomethane ND ug/L 1 05/24/12 19:59 74-83-95.0 2-Butanone (MEK)ND ug/L 1 05/24/12 19:59 78-93-325.0 n-Butylbenzene ND ug/L 1 05/24/12 19:59 104-51-85.0 sec-Butylbenzene ND ug/L 1 05/24/12 19:59 135-98-85.0 tert-Butylbenzene ND ug/L 1 05/24/12 19:59 98-06-65.0 Carbon disulfide ND ug/L 1 05/24/12 19:59 75-15-010.0 Carbon tetrachloride ND ug/L 1 05/24/12 19:59 56-23-55.0 Chlorobenzene ND ug/L 1 05/24/12 19:59 108-90-75.0 Chloroethane ND ug/L 1 05/24/12 19:59 75-00-35.0 Chloroform 11.5 ug/L 1 05/24/12 19:59 67-66-3 1d5.0 Chloromethane ND ug/L 1 05/24/12 19:59 74-87-35.0 2-Chlorotoluene ND ug/L 1 05/24/12 19:59 95-49-85.0 4-Chlorotoluene ND ug/L 1 05/24/12 19:59 106-43-45.0 Dibromochloromethane ND ug/L 1 05/24/12 19:59 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 05/24/12 19:59 106-93-45.0 Dibromomethane ND ug/L 1 05/24/12 19:59 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 05/24/12 19:59 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 05/24/12 19:59 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 05/24/12 19:59 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 05/24/12 19:59 110-57-6100 Dichlorodifluoromethane ND ug/L 1 05/24/12 19:59 75-71-85.0 1,1-Dichloroethane ND ug/L 1 05/24/12 19:59 75-34-35.0 1,2-Dichloroethane ND ug/L 1 05/24/12 19:59 107-06-25.0 1,1-Dichloroethene ND ug/L 1 05/24/12 19:59 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 05/24/12 19:59 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 05/24/12 19:59 156-60-55.0 1,2-Dichloropropane ND ug/L 1 05/24/12 19:59 78-87-55.0 1,3-Dichloropropane ND ug/L 1 05/24/12 19:59 142-28-95.0 2,2-Dichloropropane ND ug/L 1 05/24/12 19:59 594-20-75.0 1,1-Dichloropropene ND ug/L 1 05/24/12 19:59 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 05/24/12 19:59 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 05/24/12 19:59 10061-02-65.0 Ethylbenzene ND ug/L 1 05/24/12 19:59 100-41-45.0 Ethyl methacrylate ND ug/L 1 05/24/12 19:59 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 05/24/12 19:59 87-68-35.0 n-Hexane ND ug/L 1 05/24/12 19:59 110-54-3 N25.0 2-Hexanone ND ug/L 1 05/24/12 19:59 591-78-625.0 Iodomethane ND ug/L 1 05/24/12 19:59 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 05/24/12 19:59 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 19 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063325 SBI068 Sample:SBI068:FB2:W052212 Lab ID:5063325008 Collected:05/21/12 08:00 Received:05/23/12 07:30 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 05/24/12 19:59 99-87-65.0 Methylene Chloride ND ug/L 1 05/24/12 19:59 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/24/12 19:59 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 05/24/12 19:59 1634-04-44.0 Naphthalene ND ug/L 1 05/24/12 19:59 91-20-35.0 n-Propylbenzene ND ug/L 1 05/24/12 19:59 103-65-15.0 Styrene ND ug/L 1 05/24/12 19:59 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 05/24/12 19:59 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 05/24/12 19:59 79-34-55.0 Tetrachloroethene ND ug/L 1 05/24/12 19:59 127-18-45.0 Toluene ND ug/L 1 05/24/12 19:59 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 05/24/12 19:59 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 05/24/12 19:59 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 05/24/12 19:59 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 05/24/12 19:59 79-00-55.0 Trichloroethene ND ug/L 1 05/24/12 19:59 79-01-65.0 Trichlorofluoromethane ND ug/L 1 05/24/12 19:59 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 05/24/12 19:59 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 05/24/12 19:59 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 05/24/12 19:59 108-67-85.0 Vinyl acetate ND ug/L 1 05/24/12 19:59 108-05-450.0 Vinyl chloride ND ug/L 1 05/24/12 19:59 75-01-42.0 Xylene (Total)ND ug/L 1 05/24/12 19:59 1330-20-710.0 Surrogates Dibromofluoromethane (S)90 %.1 05/24/12 19:59 1868-53-783-123 4-Bromofluorobenzene (S)97 %.1 05/24/12 19:59 460-00-472-125 Toluene-d8 (S)101 %.1 05/24/12 19:59 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 20 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42482 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5063325007, 5063325008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740136 Associated Lab Samples:5063325007, 5063325008 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/24/12 14:34 1,1,1-Trichloroethane ug/L ND 5.0 05/24/12 14:34 1,1,2,2-Tetrachloroethane ug/L ND 5.0 05/24/12 14:34 1,1,2-Trichloroethane ug/L ND 5.0 05/24/12 14:34 1,1-Dichloroethane ug/L ND 5.0 05/24/12 14:34 1,1-Dichloroethene ug/L ND 5.0 05/24/12 14:34 1,1-Dichloropropene ug/L ND 5.0 05/24/12 14:34 1,2,3-Trichlorobenzene ug/L ND 5.0 05/24/12 14:34 1,2,3-Trichloropropane ug/L ND 5.0 05/24/12 14:34 1,2,4-Trichlorobenzene ug/L ND 5.0 05/24/12 14:34 1,2,4-Trimethylbenzene ug/L ND 5.0 05/24/12 14:34 1,2-Dibromoethane (EDB)ug/L ND 5.0 05/24/12 14:34 1,2-Dichlorobenzene ug/L ND 5.0 05/24/12 14:34 1,2-Dichloroethane ug/L ND 5.0 05/24/12 14:34 1,2-Dichloropropane ug/L ND 5.0 05/24/12 14:34 1,3,5-Trimethylbenzene ug/L ND 5.0 05/24/12 14:34 1,3-Dichlorobenzene ug/L ND 5.0 05/24/12 14:34 1,3-Dichloropropane ug/L ND 5.0 05/24/12 14:34 1,4-Dichlorobenzene ug/L ND 5.0 05/24/12 14:34 2,2-Dichloropropane ug/L ND 5.0 05/24/12 14:34 2-Butanone (MEK)ug/L ND 25.0 05/24/12 14:34 2-Chlorotoluene ug/L ND 5.0 05/24/12 14:34 2-Hexanone ug/L ND 25.0 05/24/12 14:34 4-Chlorotoluene ug/L ND 5.0 05/24/12 14:34 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 05/24/12 14:34 Acetone ug/L ND 100 05/24/12 14:34 Acrolein ug/L ND 100 05/24/12 14:34 Acrylonitrile ug/L ND 100 05/24/12 14:34 Benzene ug/L ND 5.0 05/24/12 14:34 Bromobenzene ug/L ND 5.0 05/24/12 14:34 Bromochloromethane ug/L ND 5.0 05/24/12 14:34 Bromodichloromethane ug/L ND 5.0 05/24/12 14:34 Bromoform ug/L ND 5.0 05/24/12 14:34 Bromomethane ug/L ND 5.0 05/24/12 14:34 Carbon disulfide ug/L ND 10.0 05/24/12 14:34 Carbon tetrachloride ug/L ND 5.0 05/24/12 14:34 Chlorobenzene ug/L ND 5.0 05/24/12 14:34 Chloroethane ug/L ND 5.0 05/24/12 14:34 Chloroform ug/L ND 5.0 05/24/12 14:34 Chloromethane ug/L ND 5.0 05/24/12 14:34 cis-1,2-Dichloroethene ug/L ND 5.0 05/24/12 14:34 cis-1,3-Dichloropropene ug/L ND 5.0 05/24/12 14:34 Dibromochloromethane ug/L ND 5.0 05/24/12 14:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 21 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740136 Associated Lab Samples:5063325007, 5063325008 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 05/24/12 14:34 Dichlorodifluoromethane ug/L ND 5.0 05/24/12 14:34 Ethyl methacrylate ug/L ND 100 05/24/12 14:34 Ethylbenzene ug/L ND 5.0 05/24/12 14:34 Hexachloro-1,3-butadiene ug/L ND 5.0 05/24/12 14:34 Iodomethane ug/L ND 10.0 05/24/12 14:34 Isopropylbenzene (Cumene)ug/L ND 5.0 05/24/12 14:34 Methyl-tert-butyl ether ug/L ND 4.0 05/24/12 14:34 Methylene Chloride ug/L ND 5.0 05/24/12 14:34 n-Butylbenzene ug/L ND 5.0 05/24/12 14:34 n-Hexane ug/L ND 5.0 N205/24/12 14:34 n-Propylbenzene ug/L ND 5.0 05/24/12 14:34 Naphthalene ug/L ND 5.0 05/24/12 14:34 p-Isopropyltoluene ug/L ND 5.0 05/24/12 14:34 sec-Butylbenzene ug/L ND 5.0 05/24/12 14:34 Styrene ug/L ND 5.0 05/24/12 14:34 tert-Butylbenzene ug/L ND 5.0 05/24/12 14:34 Tetrachloroethene ug/L ND 5.0 05/24/12 14:34 Toluene ug/L ND 5.0 05/24/12 14:34 trans-1,2-Dichloroethene ug/L ND 5.0 05/24/12 14:34 trans-1,3-Dichloropropene ug/L ND 5.0 05/24/12 14:34 trans-1,4-Dichloro-2-butene ug/L ND 100 05/24/12 14:34 Trichloroethene ug/L ND 5.0 05/24/12 14:34 Trichlorofluoromethane ug/L ND 5.0 05/24/12 14:34 Vinyl acetate ug/L ND 50.0 05/24/12 14:34 Vinyl chloride ug/L ND 2.0 05/24/12 14:34 Xylene (Total)ug/L ND 10.0 05/24/12 14:34 4-Bromofluorobenzene (S)%.98 72-125 05/24/12 14:34 Dibromofluoromethane (S)%.89 83-123 05/24/12 14:34 Toluene-d8 (S)%.99 81-114 05/24/12 14:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740137LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 43.750 87 69-122 1,1,1-Trichloroethane ug/L 51.850 104 69-126 1,1,2,2-Tetrachloroethane ug/L 54.650 109 68-134 1,1,2-Trichloroethane ug/L 61.050 122 77-129 1,1-Dichloroethane ug/L 51.250 102 70-127 1,1-Dichloroethene ug/L 49.950 100 75-145 1,1-Dichloropropene ug/L 57.650 115 75-126 1,2,3-Trichlorobenzene ug/L 55.550 111 63-130 1,2,3-Trichloropropane ug/L 88.1 L35017645-121 1,2,4-Trichlorobenzene ug/L 55.150 110 64-122 1,2,4-Trimethylbenzene ug/L 54.050 108 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 22 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740137LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 53.450 107 77-123 1,2-Dichlorobenzene ug/L 50.850 102 74-123 1,2-Dichloroethane ug/L 55.950 112 71-127 1,2-Dichloropropane ug/L 56.350 113 75-126 1,3,5-Trimethylbenzene ug/L 53.150 106 69-129 1,3-Dichlorobenzene ug/L 52.050 104 76-123 1,3-Dichloropropane ug/L 53.250 106 77-126 1,4-Dichlorobenzene ug/L 50.850 102 77-121 2,2-Dichloropropane ug/L 49.950 100 45-138 2-Butanone (MEK)ug/L 299250 120 42-177 2-Chlorotoluene ug/L 51.950 104 74-129 2-Hexanone ug/L 294250 118 57-162 4-Chlorotoluene ug/L 51.650 103 70-125 4-Methyl-2-pentanone (MIBK)ug/L 275250 110 64-135 Acetone ug/L 381250 152 10-200 Acrolein ug/L 14901000 149 10-200 Acrylonitrile ug/L 10801000 108 59-144 Benzene ug/L 52.350 105 76-123 Bromobenzene ug/L 52.750 105 67-130 Bromochloromethane ug/L 55.450 111 58-153 Bromodichloromethane ug/L 55.050 110 71-124 Bromoform ug/L 39.050 78 64-116 Bromomethane ug/L 74.750 149 23-197 Carbon disulfide ug/L 90.5100 90 55-146 Carbon tetrachloride ug/L 41.950 84 65-125 Chlorobenzene ug/L 51.050 102 78-120 Chloroethane ug/L 46.450 93 56-163 Chloroform ug/L 55.850 112 73-122 Chloromethane ug/L 52.550 105 46-146 cis-1,2-Dichloroethene ug/L 53.850 108 79-129 cis-1,3-Dichloropropene ug/L 52.050 104 66-123 Dibromochloromethane ug/L 43.350 87 70-123 Dibromomethane ug/L 54.950 110 73-123 Dichlorodifluoromethane ug/L 62.250 124 19-200 Ethyl methacrylate ug/L 216200 108 70-127 Ethylbenzene ug/L 52.850 106 75-120 Hexachloro-1,3-butadiene ug/L 51.250 102 64-131 Iodomethane ug/L 69.2100 69 16-181 Isopropylbenzene (Cumene)ug/L 50.650 101 73-123 Methyl-tert-butyl ether ug/L 103100 103 66-128 Methylene Chloride ug/L 49.050 98 61-138 n-Butylbenzene ug/L 56.850 114 69-130 n-Hexane ug/L 47.7 N2509567-142 n-Propylbenzene ug/L 53.350 107 71-132 Naphthalene ug/L 54.050 108 62-130 p-Isopropyltoluene ug/L 56.050 112 71-126 sec-Butylbenzene ug/L 53.650 107 69-130 Styrene ug/L 53.250 106 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 23 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740137LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 49.150 98 49-114 Tetrachloroethene ug/L 44.850 90 57-125 Toluene ug/L 50.150 100 72-124 trans-1,2-Dichloroethene ug/L 51.950 104 71-145 trans-1,3-Dichloropropene ug/L 54.350 109 58-118 trans-1,4-Dichloro-2-butene ug/L 175200 88 50-121 Trichloroethene ug/L 55.050 110 77-122 Trichlorofluoromethane ug/L 55.250 110 56-159 Vinyl acetate ug/L 181200 91 27-119 Vinyl chloride ug/L 53.350 107 61-146 Xylene (Total)ug/L 156150 104 72-126 4-Bromofluorobenzene (S)%.100 72-125 Dibromofluoromethane (S)%.97 83-123 Toluene-d8 (S)%.99 81-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 24 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42484 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063325001, 5063325002, 5063325003, 5063325004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740142 Associated Lab Samples:5063325001, 5063325002, 5063325003, 5063325004 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/24/12 15:06 1,1,1-Trichloroethane ug/kg ND 5.0 05/24/12 15:06 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/24/12 15:06 1,1,2-Trichloroethane ug/kg ND 5.0 05/24/12 15:06 1,1-Dichloroethane ug/kg ND 5.0 05/24/12 15:06 1,1-Dichloroethene ug/kg ND 5.0 05/24/12 15:06 1,1-Dichloropropene ug/kg ND 5.0 05/24/12 15:06 1,2,3-Trichlorobenzene ug/kg ND 5.0 05/24/12 15:06 1,2,3-Trichloropropane ug/kg ND 5.0 05/24/12 15:06 1,2,4-Trichlorobenzene ug/kg ND 5.0 05/24/12 15:06 1,2,4-Trimethylbenzene ug/kg ND 5.0 05/24/12 15:06 1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/24/12 15:06 1,2-Dichlorobenzene ug/kg ND 5.0 05/24/12 15:06 1,2-Dichloroethane ug/kg ND 5.0 05/24/12 15:06 1,2-Dichloropropane ug/kg ND 5.0 05/24/12 15:06 1,3,5-Trimethylbenzene ug/kg ND 5.0 05/24/12 15:06 1,3-Dichlorobenzene ug/kg ND 5.0 05/24/12 15:06 1,3-Dichloropropane ug/kg ND 5.0 05/24/12 15:06 1,4-Dichlorobenzene ug/kg ND 5.0 05/24/12 15:06 2,2-Dichloropropane ug/kg ND 5.0 05/24/12 15:06 2-Butanone (MEK)ug/kg ND 25.0 05/24/12 15:06 2-Chlorotoluene ug/kg ND 5.0 05/24/12 15:06 2-Hexanone ug/kg ND 100 05/24/12 15:06 4-Chlorotoluene ug/kg ND 5.0 05/24/12 15:06 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 05/24/12 15:06 Acetone ug/kg ND 100 05/24/12 15:06 Acrolein ug/kg ND 100 05/24/12 15:06 Acrylonitrile ug/kg ND 100 05/24/12 15:06 Benzene ug/kg ND 5.0 05/24/12 15:06 Bromobenzene ug/kg ND 5.0 05/24/12 15:06 Bromochloromethane ug/kg ND 5.0 05/24/12 15:06 Bromodichloromethane ug/kg ND 5.0 05/24/12 15:06 Bromoform ug/kg ND 5.0 05/24/12 15:06 Bromomethane ug/kg ND 5.0 05/24/12 15:06 Carbon disulfide ug/kg ND 10.0 05/24/12 15:06 Carbon tetrachloride ug/kg ND 5.0 05/24/12 15:06 Chlorobenzene ug/kg ND 5.0 05/24/12 15:06 Chloroethane ug/kg ND 5.0 05/24/12 15:06 Chloroform ug/kg ND 5.0 05/24/12 15:06 Chloromethane ug/kg ND 5.0 05/24/12 15:06 cis-1,2-Dichloroethene ug/kg ND 5.0 05/24/12 15:06 cis-1,3-Dichloropropene ug/kg ND 5.0 05/24/12 15:06 Dibromochloromethane ug/kg ND 5.0 05/24/12 15:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 25 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740142 Associated Lab Samples:5063325001, 5063325002, 5063325003, 5063325004 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 05/24/12 15:06 Dichlorodifluoromethane ug/kg ND 5.0 05/24/12 15:06 Ethyl methacrylate ug/kg ND 100 05/24/12 15:06 Ethylbenzene ug/kg ND 5.0 05/24/12 15:06 Hexachloro-1,3-butadiene ug/kg ND 5.0 05/24/12 15:06 Iodomethane ug/kg ND 100 05/24/12 15:06 Isopropylbenzene (Cumene)ug/kg ND 5.0 05/24/12 15:06 Methyl-tert-butyl ether ug/kg ND 5.0 05/24/12 15:06 Methylene Chloride ug/kg ND 20.0 05/24/12 15:06 n-Butylbenzene ug/kg ND 5.0 05/24/12 15:06 n-Hexane ug/kg ND 5.0 05/24/12 15:06 n-Propylbenzene ug/kg ND 5.0 05/24/12 15:06 Naphthalene ug/kg ND 5.0 05/24/12 15:06 p-Isopropyltoluene ug/kg ND 5.0 05/24/12 15:06 sec-Butylbenzene ug/kg ND 5.0 05/24/12 15:06 Styrene ug/kg ND 5.0 05/24/12 15:06 tert-Butylbenzene ug/kg ND 5.0 05/24/12 15:06 Tetrachloroethene ug/kg ND 5.0 05/24/12 15:06 Toluene ug/kg ND 5.0 05/24/12 15:06 trans-1,2-Dichloroethene ug/kg ND 5.0 05/24/12 15:06 trans-1,3-Dichloropropene ug/kg ND 5.0 05/24/12 15:06 trans-1,4-Dichloro-2-butene ug/kg ND 100 05/24/12 15:06 Trichloroethene ug/kg ND 5.0 05/24/12 15:06 Trichlorofluoromethane ug/kg ND 5.0 05/24/12 15:06 Vinyl acetate ug/kg ND 100 05/24/12 15:06 Vinyl chloride ug/kg ND 5.0 05/24/12 15:06 Xylene (Total)ug/kg ND 10.0 05/24/12 15:06 4-Bromofluorobenzene (S)%.97 67-134 05/24/12 15:06 Dibromofluoromethane (S)%.93 71-125 05/24/12 15:06 Toluene-d8 (S)%.99 76-124 05/24/12 15:06 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740143LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 42.950 86 68-125 1,1,1-Trichloroethane ug/kg 50.350 101 63-124 1,1,2,2-Tetrachloroethane ug/kg 53.450 107 73-123 1,1,2-Trichloroethane ug/kg 58.750 117 70-124 1,1-Dichloroethane ug/kg 49.250 98 63-122 1,1-Dichloroethene ug/kg 48.450 97 71-129 1,1-Dichloropropene ug/kg 55.150 110 71-122 1,2,3-Trichlorobenzene ug/kg 53.050 106 68-123 1,2,3-Trichloropropane ug/kg 86.8 L35017447-117 1,2,4-Trichlorobenzene ug/kg 53.150 106 68-125 1,2,4-Trimethylbenzene ug/kg 51.950 104 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 26 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740143LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 51.050 102 67-121 1,2-Dichlorobenzene ug/kg 49.650 99 71-121 1,2-Dichloroethane ug/kg 53.850 108 74-120 1,2-Dichloropropane ug/kg 54.350 109 71-117 1,3,5-Trimethylbenzene ug/kg 50.950 102 64-119 1,3-Dichlorobenzene ug/kg 50.050 100 70-122 1,3-Dichloropropane ug/kg 51.250 102 68-118 1,4-Dichlorobenzene ug/kg 49.350 99 71-118 2,2-Dichloropropane ug/kg 48.050 96 62-119 2-Butanone (MEK)ug/kg 263250 105 38-154 2-Chlorotoluene ug/kg 49.750 99 71-120 2-Hexanone ug/kg 272250 109 50-134 4-Chlorotoluene ug/kg 49.750 99 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 266250 106 66-122 Acetone ug/kg 286250 114 10-200 Acrolein ug/kg 14101000 141 11-200 Acrylonitrile ug/kg 10201000 102 66-120 Benzene ug/kg 50.450 101 73-115 Bromobenzene ug/kg 50.850 102 64-130 Bromochloromethane ug/kg 53.750 107 71-127 Bromodichloromethane ug/kg 53.450 107 60-121 Bromoform ug/kg 39.650 79 44-130 Bromomethane ug/kg 72.550 145 48-175 Carbon disulfide ug/kg 87.5100 88 71-126 Carbon tetrachloride ug/kg 41.250 82 57-127 Chlorobenzene ug/kg 48.950 98 72-121 Chloroethane ug/kg 44.150 88 72-141 Chloroform ug/kg 53.750 107 74-114 Chloromethane ug/kg 50.950 102 51-126 cis-1,2-Dichloroethene ug/kg 51.750 103 72-115 cis-1,3-Dichloropropene ug/kg 50.450 101 64-115 Dibromochloromethane ug/kg 42.850 86 58-114 Dibromomethane ug/kg 52.850 106 73-120 Dichlorodifluoromethane ug/kg 60.550 121 32-167 Ethyl methacrylate ug/kg 210200 105 65-117 Ethylbenzene ug/kg 50.450 101 73-120 Hexachloro-1,3-butadiene ug/kg 49.550 99 65-121 Iodomethane ug/kg 65.5J100 65 45-156 Isopropylbenzene (Cumene)ug/kg 48.550 97 74-123 Methyl-tert-butyl ether ug/kg 99.2100 99 69-123 Methylene Chloride ug/kg 46.950 94 58-124 n-Butylbenzene ug/kg 54.550 109 71-118 n-Hexane ug/kg 45.750 91 50-106 n-Propylbenzene ug/kg 51.050 102 70-120 Naphthalene ug/kg 51.950 104 67-124 p-Isopropyltoluene ug/kg 53.250 106 71-123 sec-Butylbenzene ug/kg 51.650 103 66-122 Styrene ug/kg 51.350 103 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 27 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740143LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 46.950 94 54-124 Tetrachloroethene ug/kg 42.750 85 66-126 Toluene ug/kg 48.150 96 69-115 trans-1,2-Dichloroethene ug/kg 50.050 100 69-120 trans-1,3-Dichloropropene ug/kg 52.750 105 61-116 trans-1,4-Dichloro-2-butene ug/kg 173200 86 59-130 Trichloroethene ug/kg 52.850 106 71-117 Trichlorofluoromethane ug/kg 52.850 106 67-138 Vinyl acetate ug/kg 174200 87 35-134 Vinyl chloride ug/kg 51.350 103 64-127 Xylene (Total)ug/kg 150150 100 69-117 4-Bromofluorobenzene (S)%.100 67-134 Dibromofluoromethane (S)%.98 71-125 Toluene-d8 (S)%.99 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 740144MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063325001 740145 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 46.7 75 10-11155 32 2045.8ND 34.9 25.3 1,1,1-Trichloroethane ug/kg 46.7 92 36-12874 23 2045.8ND 42.9 34.1 1,1,2,2-Tetrachloroethane ug/kg 46.7 102 10-13085 19 2045.8ND 47.5 39.1 1,1,2-Trichloroethane ug/kg 46.7 111 10-126101 10 2045.8ND 51.6 46.5 1,1-Dichloroethane ug/kg 46.7 95 39-12684 15 2045.8ND 44.4 38.3 1,1-Dichloroethene ug/kg 46.7 92 42-14782 13 2045.8ND 42.7 37.4 1,1-Dichloropropene ug/kg 46.7 104 29-12988 18 2045.8ND 48.4 40.4 1,2,3-Trichlorobenzene ug/kg 46.7 76 10-9153 37 2045.8ND 35.2 24.1 1,2,3-Trichloropropane ug/kg M046.7 143 10-99111 27 2045.8ND 66.6 50.7 1,2,4-Trichlorobenzene ug/kg 46.7 76 10-8853 36 2045.8ND 35.2 24.4 1,2,4-Trimethylbenzene ug/kg 46.7 90 10-10973 22 2045.8ND 41.9 33.6 1,2-Dibromoethane (EDB)ug/kg 46.7 92 10-11985 10 2045.8ND 43.1 38.9 1,2-Dichlorobenzene ug/kg 46.7 83 10-10466 25 2045.8ND 38.8 30.1 1,2-Dichloroethane ug/kg 46.7 104 19-12692 14 2045.8ND 48.3 42.0 1,2-Dichloropropane ug/kg 46.7 104 24-12394 12 2045.8ND 48.4 43.1 1,3,5-Trimethylbenzene ug/kg 46.7 89 10-11872 23 2045.8ND 41.6 33.1 1,3-Dichlorobenzene ug/kg 46.7 84 10-10865 27 2045.8ND 39.0 29.7 1,3-Dichloropropane ug/kg 46.7 95 12-12186 12 2045.8ND 44.3 39.5 1,4-Dichlorobenzene ug/kg 46.7 82 10-10464 27 2045.8ND 38.2 29.1 2,2-Dichloropropane ug/kg 46.7 88 32-12475 18 2045.8ND 41.2 34.4 2-Butanone (MEK)ug/kg 233 136 10-183124 11 20229ND316284 2-Chlorotoluene ug/kg 46.7 90 10-12870 26 2045.8ND 41.8 32.0 2-Hexanone ug/kg 233 122 10-158111 11 20229ND284255 4-Chlorotoluene ug/kg 46.7 86 10-11969 24 2045.8ND 40.0 31.5 4-Methyl-2-pentanone (MIBK)ug/kg 233 99 12-13091 10 20229ND231208 Acetone ug/kg M023324410-200196 23 20229ND569450 Acrolein ug/kg 932 127 10-200123 5 20916ND11801130 Acrylonitrile ug/kg 932 97 19-13090 9 20916ND907828 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 28 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 740144MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063325001 740145 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 46.7 96 23-13885 13 2045.8ND 44.6 39.1 Bromobenzene ug/kg 46.7 93 10-11174 24 2045.8ND 43.3 34.0 Bromochloromethane ug/kg 46.7 96 26-12688 10 2045.8ND 44.7 40.4 Bromodichloromethane ug/kg 46.7 96 10-12071 32 2045.8ND 44.9 32.7 Bromoform ug/kg 46.7 65 10-10643 42 2045.8ND 30.1 19.7 Bromomethane ug/kg 46.7 95 10-190154 46 2045.8ND 44.3 70.4 Carbon disulfide ug/kg 93.2 83 31-12866 26 2091.6ND 77.8 60.2 Carbon tetrachloride ug/kg 46.7 69 26-12649 36 2045.8ND 32.2 22.3 Chlorobenzene ug/kg 46.7 90 10-12077 17 2045.8ND 41.8 35.1 Chloroethane ug/kg 46.7 85 18-18675 14 2045.8ND 39.5 34.2 Chloroform ug/kg 46.7 103 29-12690 15 2045.8ND 48.0 41.4 Chloromethane ug/kg 46.7 104 34-13182 26 2045.8ND 48.7 37.5 cis-1,2-Dichloroethene ug/kg 46.7 97 28-13288 12 2045.8ND 45.4 40.5 cis-1,3-Dichloropropene ug/kg 46.7 87 10-10868 26 2045.8ND 40.5 31.3 Dibromochloromethane ug/kg 46.7 73 10-10849 40 2045.8ND 33.9 22.6 Dibromomethane ug/kg 46.7 99 13-12290 11 2045.8ND 46.2 41.3 Dichlorodifluoromethane ug/kg 46.7 121 10-197100 21 2045.8ND 56.5 45.7 Ethyl methacrylate ug/kg 186 91 10-13052 56 20183ND17096.1 Ethylbenzene ug/kg 46.7 92 10-13579 17 2045.8ND 42.8 36.3 Hexachloro-1,3-butadiene ug/kg 46.7 64 10-10542 44 2045.8ND 29.9 19.1 Iodomethane ug/kg 93.2 39 10-16330 2091.6ND ND ND Isopropylbenzene (Cumene)ug/kg 46.7 86 10-12173 19 2045.8ND 40.3 33.3 Methyl-tert-butyl ether ug/kg 93.2 94 20-14094 1 2091.6ND 87.2 86.1 Methylene Chloride ug/kg 46.7 86 28-13179 10 2045.8ND 39.9 36.0 n-Butylbenzene ug/kg 46.7 83 10-11063 30 2045.8ND 38.9 28.7 n-Hexane ug/kg 46.7 83 21-15061 32 2045.8ND 38.5 27.9 n-Propylbenzene ug/kg 46.7 89 10-12370 25 2045.8ND 41.7 32.3 Naphthalene ug/kg 46.7 81 10-10670 17 2045.8ND 38.0 31.9 p-Isopropyltoluene ug/kg 46.7 88 10-11770 25 2045.8ND 41.2 32.1 sec-Butylbenzene ug/kg 46.7 87 10-12367 28 2045.8ND 40.4 30.6 Styrene ug/kg 46.7 92 10-11977 19 2045.8ND 42.8 35.4 tert-Butylbenzene ug/kg 46.7 82 10-10568 21 2045.8ND 38.3 31.1 Tetrachloroethene ug/kg 46.7 77 10-12268 15 2045.8ND 36.0 31.0 Toluene ug/kg 46.7 90 10-13177 18 2045.8ND 42.1 35.1 trans-1,2-Dichloroethene ug/kg 46.7 95 32-13683 15 2045.8ND 44.0 38.1 trans-1,3-Dichloropropene ug/kg 46.7 88 10-10168 28 2045.8ND 40.9 30.9 trans-1,4-Dichloro-2-butene ug/kg 186 69 10-10458 20 20183ND129106 Trichloroethene ug/kg 46.7 98 15-13387 14 2045.8ND 45.9 39.7 Trichlorofluoromethane ug/kg 46.7 102 37-15288 17 2045.8ND 47.7 40.3 Vinyl acetate ug/kg 186 54 10-10310 20183ND99.9 ND Vinyl chloride ug/kg 46.7 101 41-14784 19 2045.8ND 46.9 38.7 Xylene (Total)ug/kg 140 91 10-13178 16 20137ND127108 4-Bromofluorobenzene (S)%.99 67-13499 20 Dibromofluoromethane (S)%.2d9771-12595 20 Toluene-d8 (S)%.99 76-12497 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 29 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 740146MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063325004 740147 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 39 72 10-11179 11 2039.9ND 28.3 31.5 1,1,1-Trichloroethane ug/kg 39 89 36-12895 9 2039.9ND 34.7 38.0 1,1,2,2-Tetrachloroethane ug/kg 39 94 10-130101 9 2039.9ND 36.6 40.2 1,1,2-Trichloroethane ug/kg 39 105 10-126113 10 2039.9ND 40.9 45.1 1,1-Dichloroethane ug/kg 39 92 39-12697 7 2039.9ND 35.9 38.6 1,1-Dichloroethene ug/kg 39 91 42-14795 6 2039.9ND 35.5 37.9 1,1-Dichloropropene ug/kg 39 102 29-129108 8 2039.9ND 39.8 43.0 1,2,3-Trichlorobenzene ug/kg 39 77 10-9184 11 2039.9ND 30.0 33.6 1,2,3-Trichloropropane ug/kg M03913310-99147 12 2039.9ND 52.0 58.5 1,2,4-Trichlorobenzene ug/kg 39 78 10-8884 10 2039.9ND 30.5 33.6 1,2,4-Trimethylbenzene ug/kg 39 89 10-10997 10 2039.9ND 34.8 38.6 1,2-Dibromoethane (EDB)ug/kg 39 88 10-11992 7 2039.9ND 34.3 36.9 1,2-Dichlorobenzene ug/kg 39 84 10-10490 10 2039.9ND 32.6 35.9 1,2-Dichloroethane ug/kg 39 99 19-126105 8 2039.9ND 38.7 41.7 1,2-Dichloropropane ug/kg 39 100 24-123106 7 2039.9ND 39.2 42.1 1,3,5-Trimethylbenzene ug/kg 39 88 10-11897 12 2039.9ND 34.4 38.7 1,3-Dichlorobenzene ug/kg 39 84 10-10892 11 2039.9ND 32.9 36.6 1,3-Dichloropropane ug/kg 39 91 12-12197 9 2039.9ND 35.5 38.9 1,4-Dichlorobenzene ug/kg 39 82 10-10489 10 2039.9ND 31.9 35.4 2,2-Dichloropropane ug/kg 39 83 32-12490 10 2039.9ND 32.5 35.9 2-Butanone (MEK)ug/kg 195 126 10-183132 6 20199ND247263 2-Chlorotoluene ug/kg 39 88 10-12895 10 2039.9ND 34.4 38.0 2-Hexanone ug/kg 195 117 10-158123 7 20199ND228245 4-Chlorotoluene ug/kg 39 86 10-11993 11 2039.9ND 33.4 37.1 4-Methyl-2-pentanone (MIBK)ug/kg 195 94 12-13099 7 20199ND184198 Acetone ug/kg M019523310-200233 2 20199ND455466 Acrolein ug/kg 780 120 10-200126 7 20798ND9401010 Acrylonitrile ug/kg 780 92 19-13096 7 20798ND718769 Benzene ug/kg 39 93 23-13899 9 2039.9ND 36.3 39.5 Bromobenzene ug/kg 39 93 10-11196 6 2039.9ND 36.3 38.4 Bromochloromethane ug/kg 39 88 26-12691 5 2039.9ND 34.5 36.2 Bromodichloromethane ug/kg 39 93 10-12099 9 2039.9ND 36.2 39.6 Bromoform ug/kg 39 62 10-10668 11 2039.9ND 24.3 27.1 Bromomethane ug/kg 39 99 10-190100 3 2039.9ND 38.7 40.0 Carbon disulfide ug/kg 78 82 31-12887 8 2079.8ND 64.0 69.7 Carbon tetrachloride ug/kg 39 68 26-12674 11 2039.9ND 26.5 29.5 Chlorobenzene ug/kg 39 88 10-12094 8 2039.9ND 34.4 37.3 Chloroethane ug/kg 39 85 18-18686 4 2039.9ND 33.0 34.3 Chloroform ug/kg 39 99 29-126106 8 2039.9ND 38.8 42.2 Chloromethane ug/kg 39 89 34-13196 10 2039.9ND 34.5 38.3 cis-1,2-Dichloroethene ug/kg 39 95 28-132100 8 2039.9ND 36.9 40.0 cis-1,3-Dichloropropene ug/kg 39 82 10-10889 10 2039.9ND 32.1 35.6 Dibromochloromethane ug/kg 39 69 10-10877 14 2039.9ND 27.0 30.9 Dibromomethane ug/kg 39 95 13-12296 3 2039.9ND 37.1 38.3 Dichlorodifluoromethane ug/kg 39 117 10-197123 8 2039.9ND 45.5 49.2 Ethyl methacrylate ug/kg 156 84 10-13091 11 20160ND130146 Ethylbenzene ug/kg 39 90 10-13597 10 2039.9ND 35.2 38.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 30 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 740146MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063325004 740147 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Hexachloro-1,3-butadiene ug/kg 39 72 10-10583 16 2039.9ND 28.2 33.1 Iodomethane ug/kg 78 41 10-16349 2079.8ND ND ND Isopropylbenzene (Cumene)ug/kg 39 87 10-12194 10 2039.9ND 34.0 37.6 Methyl-tert-butyl ether ug/kg 78 89 20-14094 8 2079.8ND 69.4 74.8 Methylene Chloride ug/kg 39 83 28-13188 8 2039.9ND 32.3 35.2 n-Butylbenzene ug/kg 39 88 10-11097 12 2039.9ND 34.5 38.7 n-Hexane ug/kg 39 84 21-15089 8 2039.9ND 32.9 35.6 n-Propylbenzene ug/kg 39 89 10-12397 11 2039.9ND 34.8 38.6 Naphthalene ug/kg 39 80 10-10688 12 2039.9ND 31.1 35.1 p-Isopropyltoluene ug/kg 39 91 10-117100 12 2039.9ND 35.4 39.9 sec-Butylbenzene ug/kg 39 89 10-12398 12 2039.9ND 34.7 39.0 Styrene ug/kg 39 90 10-11997 9 2039.9ND 35.2 38.7 tert-Butylbenzene ug/kg 39 83 10-10590 11 2039.9ND 32.2 36.1 Tetrachloroethene ug/kg 39 77 10-12282 8 2039.9ND 30.1 32.8 Toluene ug/kg 39 87 10-13193 8 2039.9ND 34.0 37.0 trans-1,2-Dichloroethene ug/kg 39 92 32-13697 7 2039.9ND 35.8 38.5 trans-1,3-Dichloropropene ug/kg 39 83 10-10191 11 2039.9ND 32.6 36.3 trans-1,4-Dichloro-2-butene ug/kg 156 68 10-10472 7 20160ND106114 Trichloroethene ug/kg 39 99 15-133105 8 2039.9ND 38.4 41.7 Trichlorofluoromethane ug/kg 39 102 37-152105 5 2039.9ND 39.8 41.9 Vinyl acetate ug/kg 156 22 10-10320 20160NDNDND Vinyl chloride ug/kg 39 99 41-147102 6 2039.9ND 38.5 40.8 Xylene (Total)ug/kg 117 89 10-13196 9 20119ND105115 4-Bromofluorobenzene (S)%.101 67-134101 20 Dibromofluoromethane (S)%.98 71-12596 20 Toluene-d8 (S)%.98 76-12498 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 31 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42486 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063325005, 5063325006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740152 Associated Lab Samples:5063325005, 5063325006 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/25/12 02:28 1,1,1-Trichloroethane ug/kg ND 5.0 05/25/12 02:28 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/25/12 02:28 1,1,2-Trichloroethane ug/kg ND 5.0 05/25/12 02:28 1,1-Dichloroethane ug/kg ND 5.0 05/25/12 02:28 1,1-Dichloroethene ug/kg ND 5.0 05/25/12 02:28 1,1-Dichloropropene ug/kg ND 5.0 05/25/12 02:28 1,2,3-Trichlorobenzene ug/kg ND 5.0 05/25/12 02:28 1,2,3-Trichloropropane ug/kg ND 5.0 05/25/12 02:28 1,2,4-Trichlorobenzene ug/kg ND 5.0 05/25/12 02:28 1,2,4-Trimethylbenzene ug/kg ND 5.0 05/25/12 02:28 1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/25/12 02:28 1,2-Dichlorobenzene ug/kg ND 5.0 05/25/12 02:28 1,2-Dichloroethane ug/kg ND 5.0 05/25/12 02:28 1,2-Dichloropropane ug/kg ND 5.0 05/25/12 02:28 1,3,5-Trimethylbenzene ug/kg ND 5.0 05/25/12 02:28 1,3-Dichlorobenzene ug/kg ND 5.0 05/25/12 02:28 1,3-Dichloropropane ug/kg ND 5.0 05/25/12 02:28 1,4-Dichlorobenzene ug/kg ND 5.0 05/25/12 02:28 2,2-Dichloropropane ug/kg ND 5.0 05/25/12 02:28 2-Butanone (MEK)ug/kg ND 25.0 05/25/12 02:28 2-Chlorotoluene ug/kg ND 5.0 05/25/12 02:28 2-Hexanone ug/kg ND 100 05/25/12 02:28 4-Chlorotoluene ug/kg ND 5.0 05/25/12 02:28 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 05/25/12 02:28 Acetone ug/kg ND 100 05/25/12 02:28 Acrolein ug/kg ND 100 05/25/12 02:28 Acrylonitrile ug/kg ND 100 05/25/12 02:28 Benzene ug/kg ND 5.0 05/25/12 02:28 Bromobenzene ug/kg ND 5.0 05/25/12 02:28 Bromochloromethane ug/kg ND 5.0 05/25/12 02:28 Bromodichloromethane ug/kg ND 5.0 05/25/12 02:28 Bromoform ug/kg ND 5.0 05/25/12 02:28 Bromomethane ug/kg ND 5.0 05/25/12 02:28 Carbon disulfide ug/kg ND 10.0 05/25/12 02:28 Carbon tetrachloride ug/kg ND 5.0 05/25/12 02:28 Chlorobenzene ug/kg ND 5.0 05/25/12 02:28 Chloroethane ug/kg ND 5.0 05/25/12 02:28 Chloroform ug/kg ND 5.0 05/25/12 02:28 Chloromethane ug/kg ND 5.0 05/25/12 02:28 cis-1,2-Dichloroethene ug/kg ND 5.0 05/25/12 02:28 cis-1,3-Dichloropropene ug/kg ND 5.0 05/25/12 02:28 Dibromochloromethane ug/kg ND 5.0 05/25/12 02:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 32 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:740152 Associated Lab Samples:5063325005, 5063325006 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 05/25/12 02:28 Dichlorodifluoromethane ug/kg ND 5.0 05/25/12 02:28 Ethyl methacrylate ug/kg ND 100 05/25/12 02:28 Ethylbenzene ug/kg ND 5.0 05/25/12 02:28 Hexachloro-1,3-butadiene ug/kg ND 5.0 05/25/12 02:28 Iodomethane ug/kg ND 100 05/25/12 02:28 Isopropylbenzene (Cumene)ug/kg ND 5.0 05/25/12 02:28 Methyl-tert-butyl ether ug/kg ND 5.0 05/25/12 02:28 Methylene Chloride ug/kg ND 20.0 05/25/12 02:28 n-Butylbenzene ug/kg ND 5.0 05/25/12 02:28 n-Hexane ug/kg ND 5.0 05/25/12 02:28 n-Propylbenzene ug/kg ND 5.0 05/25/12 02:28 Naphthalene ug/kg ND 5.0 05/25/12 02:28 p-Isopropyltoluene ug/kg ND 5.0 05/25/12 02:28 sec-Butylbenzene ug/kg ND 5.0 05/25/12 02:28 Styrene ug/kg ND 5.0 05/25/12 02:28 tert-Butylbenzene ug/kg ND 5.0 05/25/12 02:28 Tetrachloroethene ug/kg ND 5.0 05/25/12 02:28 Toluene ug/kg ND 5.0 05/25/12 02:28 trans-1,2-Dichloroethene ug/kg ND 5.0 05/25/12 02:28 trans-1,3-Dichloropropene ug/kg ND 5.0 05/25/12 02:28 trans-1,4-Dichloro-2-butene ug/kg ND 100 05/25/12 02:28 Trichloroethene ug/kg ND 5.0 05/25/12 02:28 Trichlorofluoromethane ug/kg ND 5.0 05/25/12 02:28 Vinyl acetate ug/kg ND 100 05/25/12 02:28 Vinyl chloride ug/kg ND 5.0 05/25/12 02:28 Xylene (Total)ug/kg ND 10.0 05/25/12 02:28 4-Bromofluorobenzene (S)%.98 67-134 05/25/12 02:28 Dibromofluoromethane (S)%.95 71-125 05/25/12 02:28 Toluene-d8 (S)%.100 76-124 05/25/12 02:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740153LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 44.350 89 68-125 1,1,1-Trichloroethane ug/kg 53.650 107 63-124 1,1,2,2-Tetrachloroethane ug/kg 55.350 111 73-123 1,1,2-Trichloroethane ug/kg 60.450 121 70-124 1,1-Dichloroethane ug/kg 52.150 104 63-122 1,1-Dichloroethene ug/kg 52.250 104 71-129 1,1-Dichloropropene ug/kg 57.950 116 71-122 1,2,3-Trichlorobenzene ug/kg 51.550 103 68-123 1,2,3-Trichloropropane ug/kg 81.7 L35016347-117 1,2,4-Trichlorobenzene ug/kg 50.750 101 68-125 1,2,4-Trimethylbenzene ug/kg 52.950 106 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 33 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740153LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 51.050 102 67-121 1,2-Dichlorobenzene ug/kg 49.750 99 71-121 1,2-Dichloroethane ug/kg 56.050 112 74-120 1,2-Dichloropropane ug/kg 57.150 114 71-117 1,3,5-Trimethylbenzene ug/kg 52.750 105 64-119 1,3-Dichlorobenzene ug/kg 50.350 101 70-122 1,3-Dichloropropane ug/kg 52.050 104 68-118 1,4-Dichlorobenzene ug/kg 49.450 99 71-118 2,2-Dichloropropane ug/kg 49.250 98 62-119 2-Butanone (MEK)ug/kg 257250 103 38-154 2-Chlorotoluene ug/kg 51.650 103 71-120 2-Hexanone ug/kg 260250 104 50-134 4-Chlorotoluene ug/kg 51.050 102 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 263250 105 66-122 Acetone ug/kg 266250 107 10-200 Acrolein ug/kg 13701000 137 11-200 Acrylonitrile ug/kg 10501000 105 66-120 Benzene ug/kg 52.950 106 73-115 Bromobenzene ug/kg 53.050 106 64-130 Bromochloromethane ug/kg 48.350 97 71-127 Bromodichloromethane ug/kg 55.850 112 60-121 Bromoform ug/kg 39.150 78 44-130 Bromomethane ug/kg 55.450 111 48-175 Carbon disulfide ug/kg 94.6100 95 71-126 Carbon tetrachloride ug/kg 42.950 86 57-127 Chlorobenzene ug/kg 51.150 102 72-121 Chloroethane ug/kg 46.350 93 72-141 Chloroform ug/kg 56.450 113 74-114 Chloromethane ug/kg 49.050 98 51-126 cis-1,2-Dichloroethene ug/kg 53.450 107 72-115 cis-1,3-Dichloropropene ug/kg 50.350 101 64-115 Dibromochloromethane ug/kg 43.750 87 58-114 Dibromomethane ug/kg 51.450 103 73-120 Dichlorodifluoromethane ug/kg 68.350 137 32-167 Ethyl methacrylate ug/kg 210200 105 65-117 Ethylbenzene ug/kg 52.850 106 73-120 Hexachloro-1,3-butadiene ug/kg 49.150 98 65-121 Iodomethane ug/kg 56.3J100 56 45-156 Isopropylbenzene (Cumene)ug/kg 50.950 102 74-123 Methyl-tert-butyl ether ug/kg 102100 102 69-123 Methylene Chloride ug/kg 48.150 96 58-124 n-Butylbenzene ug/kg 55.050 110 71-118 n-Hexane ug/kg 48.550 97 50-106 n-Propylbenzene ug/kg 53.050 106 70-120 Naphthalene ug/kg 51.550 103 67-124 p-Isopropyltoluene ug/kg 54.550 109 71-123 sec-Butylbenzene ug/kg 53.250 106 66-122 Styrene ug/kg 53.450 107 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 34 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 740153LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 48.950 98 54-124 Tetrachloroethene ug/kg 44.850 90 66-126 Toluene ug/kg 50.550 101 69-115 trans-1,2-Dichloroethene ug/kg 52.650 105 69-120 trans-1,3-Dichloropropene ug/kg 51.850 104 61-116 trans-1,4-Dichloro-2-butene ug/kg 156200 78 59-130 Trichloroethene ug/kg 55.650 111 71-117 Trichlorofluoromethane ug/kg 57.550 115 67-138 Vinyl acetate ug/kg 167200 84 35-134 Vinyl chloride ug/kg 56.050 112 64-127 Xylene (Total)ug/kg 156150 104 69-117 4-Bromofluorobenzene (S)%.100 67-134 Dibromofluoromethane (S)%.98 71-125 Toluene-d8 (S)%.99 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 740154MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063364004 740155 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 41.4 50 10-11151 14 2046.4ND 20.5 23.6 1,1,1-Trichloroethane ug/kg 41.4 76 36-12880 17 2046.4ND 31.3 37.0 1,1,2,2-Tetrachloroethane ug/kg 41.4 68 10-13067 9 2046.4ND 28.2 31.0 1,1,2-Trichloroethane ug/kg 41.4 87 10-12687 13 2046.4ND 35.8 40.6 1,1-Dichloroethane ug/kg 41.4 81 39-12684 14 2046.4ND 33.6 38.8 1,1-Dichloroethene ug/kg 41.4 80 42-14784 16 2046.4ND 33.0 38.8 1,1-Dichloropropene ug/kg 41.4 80 29-12981 12 2046.4ND 33.2 37.5 1,2,3-Trichlorobenzene ug/kg 41.4 26 10-9126 9 2046.4ND 10.9 11.9 1,2,3-Trichloropropane ug/kg 41.4 96 10-9997 13 2046.4ND 39.5 44.9 1,2,4-Trichlorobenzene ug/kg 41.4 25 10-8824 6 2046.4ND 10.4 11.1 1,2,4-Trimethylbenzene ug/kg 41.4 36 10-10934 8 2046.4ND 14.8 16.0 1,2-Dibromoethane (EDB)ug/kg 41.4 71 10-11972 13 2046.4ND 29.3 33.4 1,2-Dichlorobenzene ug/kg 41.4 36 10-10435 8 2046.4ND 14.8 16.0 1,2-Dichloroethane ug/kg 41.4 88 19-12689 13 2046.4ND 36.2 41.4 1,2-Dichloropropane ug/kg 41.4 83 24-12383 12 2046.4ND 34.2 38.5 1,3,5-Trimethylbenzene ug/kg 41.4 36 10-11835 7 2046.4ND 15.0 16.1 1,3-Dichlorobenzene ug/kg 41.4 33 10-10832 9 2046.4ND 13.6 15.0 1,3-Dichloropropane ug/kg 41.4 74 12-12175 13 2046.4ND 30.6 34.8 1,4-Dichlorobenzene ug/kg 41.4 33 10-10431 7 2046.4ND 13.6 14.6 2,2-Dichloropropane ug/kg 41.4 68 32-12472 18 2046.4ND 27.9 33.5 2-Butanone (MEK)ug/kg 206 106 10-183110 16 20232ND219257 2-Chlorotoluene ug/kg 41.4 39 10-12838 8 2046.4ND 16.2 17.5 2-Hexanone ug/kg 206 104 10-158107 15 20232ND214249 4-Chlorotoluene ug/kg 41.4 35 10-11933 6 2046.4ND 14.5 15.4 4-Methyl-2-pentanone (MIBK)ug/kg 206 91 12-13092 14 20232ND187214 Acetone ug/kg R120614010-200167 29 20232ND289389 Acrolein ug/kg 826 115 10-200121 17 20929ND9471120 Acrylonitrile ug/kg 826 91 19-13094 15 20929ND749870 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 35 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 740154MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063364004 740155 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 41.4 76 23-13878 14 2046.4ND 31.5 36.1 Bromobenzene ug/kg 41.4 48 10-11146 7 2046.4ND 20.0 21.4 Bromochloromethane ug/kg 41.4 85 26-12688 15 2046.4ND 35.3 40.9 Bromodichloromethane ug/kg 41.4 74 10-12076 14 2046.4ND 30.7 35.4 Bromoform ug/kg 41.4 47 10-10649 15 2046.4ND 19.4 22.5 Bromomethane ug/kg 41.4 147 10-190144 9 2046.4ND 60.7 66.8 Carbon disulfide ug/kg 82.6 69 31-12869 12 2092.9ND 56.9 64.0 Carbon tetrachloride ug/kg 41.4 56 26-12659 18 2046.4ND 23.0 27.5 Chlorobenzene ug/kg 41.4 52 10-12051 10 2046.4ND 21.3 23.5 Chloroethane ug/kg 41.4 77 18-18681 16 2046.4ND 32.0 37.5 Chloroform ug/kg 41.4 85 29-12688 14 2046.4ND 35.2 40.7 Chloromethane ug/kg 41.4 91 34-13194 16 2046.4ND 37.4 43.9 cis-1,2-Dichloroethene ug/kg 41.4 80 28-13280 12 2046.4ND 32.9 37.2 cis-1,3-Dichloropropene ug/kg 41.4 63 10-10865 15 2046.4ND 25.9 30.2 Dibromochloromethane ug/kg 41.4 54 10-10856 15 2046.4ND 22.4 26.1 Dibromomethane ug/kg 41.4 82 13-12283 13 2046.4ND 33.9 38.5 Dichlorodifluoromethane ug/kg 41.4 115 10-197119 15 2046.4ND 47.5 55.3 Ethyl methacrylate ug/kg 165 71 10-13074 16 20186ND118138 Ethylbenzene ug/kg 41.4 50 10-13548 8 2046.4ND 20.5 22.3 Hexachloro-1,3-butadiene ug/kg 41.4 15 10-10514 4 2046.4ND 6.2 6.4 Iodomethane ug/kg 82.6 30 10-16347 2092.9ND ND ND Isopropylbenzene (Cumene)ug/kg 41.4 41 10-12139 7 2046.4ND 16.9 18.2 Methyl-tert-butyl ether ug/kg 82.6 86 20-14089 15 2092.9ND 70.8 82.3 Methylene Chloride ug/kg 41.4 75 28-13178 16 2046.4ND 30.9 36.2 n-Butylbenzene ug/kg 41.4 23 10-11021 6 2046.4ND 9.4 10 n-Hexane ug/kg 41.4 69 21-15071 15 2046.4ND 28.4 32.9 n-Propylbenzene ug/kg 41.4 35 10-12333 6 2046.4ND 14.5 15.4 Naphthalene ug/kg 41.4 40 10-10639 11 2046.4ND 16.5 18.3 p-Isopropyltoluene ug/kg 41.4 29 10-11727 6 2046.4ND 11.9 12.6 sec-Butylbenzene ug/kg 41.4 31 10-12329 7 2046.4ND 12.8 13.7 Styrene ug/kg 41.4 48 10-11946 8 2046.4ND 19.8 21.5 tert-Butylbenzene ug/kg 41.4 35 10-10533 7 2046.4ND 14.3 15.4 Tetrachloroethene ug/kg 41.4 47 10-12245 8 2046.4ND 19.4 20.9 Toluene ug/kg 41.4 60 10-13160 11 2046.4ND 25.3 28.3 trans-1,2-Dichloroethene ug/kg 41.4 78 32-13679 13 2046.4ND 32.3 36.8 trans-1,3-Dichloropropene ug/kg 41.4 62 10-10163 13 2046.4ND 25.6 29.2 trans-1,4-Dichloro-2-butene ug/kg 165 48 10-10448 20186ND80J89.8J Trichloroethene ug/kg 41.4 75 15-13375 13 2046.4ND 30.9 35.1 Trichlorofluoromethane ug/kg 41.4 94 37-15298 16 2046.4ND 39.0 45.6 Vinyl acetate ug/kg 165 14 10-10320 20186NDNDND Vinyl chloride ug/kg 41.4 92 41-14796 15 2046.4ND 38.1 44.5 Xylene (Total)ug/kg 124 48 10-13146 8 20139ND58.9 64.0 4-Bromofluorobenzene (S)%.100 67-13499 20 Dibromofluoromethane (S)%.98 71-12598 20 Toluene-d8 (S)%.100 76-124100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 36 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063325 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/7089 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5063325001, 5063325002, 5063325003, 5063325004, 5063325005, 5063325006 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063325001 741896SAMPLE DUPLICATE: Percent Moisture %6.2 5 56.6 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063325004 741897SAMPLE DUPLICATE: Percent Moisture %9.0 5 58.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 37 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5063325 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Presence of this compound indicates the possible use of commercially purchased DI water. grm 5-25-121d Several compounds are outside of acceptance limits for RPD value. Refer to the LCS for system control. grm 5-29-122d Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 38 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5063325 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5063325007 MSV/42482SBI068:FB1:W052112 EPA 8260 5063325008 MSV/42482SBI068:FB2:W052212 EPA 8260 5063325001 MSV/42484SBI068:AMW6I:S040053 EPA 8260 5063325002 MSV/42484SBI068:AMW6I:S200213 EPA 8260 5063325003 MSV/42484SBI068:AMW6I:S200213A EPA 8260 5063325004 MSV/42484SBI068:AMW7I:S040055 EPA 8260 5063325005 MSV/42486SBI068:AMW7I:S200211 EPA 8260 5063325006 MSV/42486SBI068:AMW7I:S200211A EPA 8260 5063325001 PMST/7089SBI068:AMW6I:S040053 ASTM D2974-87 5063325002 PMST/7089SBI068:AMW6I:S200213 ASTM D2974-87 5063325003 PMST/7089SBI068:AMW6I:S200213A ASTM D2974-87 5063325004 PMST/7089SBI068:AMW7I:S040055 ASTM D2974-87 5063325005 PMST/7089SBI068:AMW7I:S200211 ASTM D2974-87 5063325006 PMST/7089SBI068:AMW7I:S200211A ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:40 PM Page 39 of 39 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 June 19, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 10194400 10194400 Project: Pace Project No.: RE: Doug Stuart Hull and Associates, Inc. 8470 Allison Pointe Boulevard Suite 120 Indianapolis, IN 46250 SBI068 Dear Doug Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on June 06, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Aaron Fredrikson aaron.fredrikson@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 1 of 29 CERTIFICATIONS Pace Project No.: Project: 10194400 SBI068 Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01 Alaska Certification #: UST-078Alaska Certification #MN00064Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680California Certification #: 01155CA EPA Region 8 Certification #: PaceFlorida/NELAP Certification #: E87605Georgia Certification #: 959Idaho Certification #: MN00064Illinois Certification #: 200011 Iowa Certification #: 368Kansas Certification #: E-10167Louisiana Certification #: 03086Louisiana Certification #: LA080009Maine Certification #: 2007029 Maryland Certification #: 322Michigan DEQ Certification #: 9909Minnesota Certification #: 027-053-137 Mississippi Certification #: PaceMontana Certification #: MT CERT0092 Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New Mexico Certification #: PaceNew York Certification #: 11647 North Carolina Certification #: 530North Dakota Certification #: R-036North Dakota Certification #: R-036AOhio VAP Certification #: CL101Oklahoma Certification #: D9921 Oklahoma Certification #: 9507Oregon Certification #: MN200001Pennsylvania Certification #: 68-00563Puerto Rico CertificationTennessee Certification #: 02818 Texas Certification #: T104704192Washington Certification #: C754Wisconsin Certification #: 999407970 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 2 of 29 SAMPLE SUMMARY Pace Project No.: Project: 10194400 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 10194400001 ASGP1D:A060512 Air 06/05/12 09:57 06/06/12 09:25 10194400002 ASGP1S:A060512 Air 06/05/12 10:00 06/06/12 09:25 10194400003 ASGP2D:A060512 Air 06/05/12 10:53 06/06/12 09:25 10194400004 ASGP2S:A060512 Air 06/05/12 10:50 06/06/12 09:25 10194400005 ASGP3S:A060512 Air 06/05/12 11:50 06/06/12 09:25 10194400006 ASGP3D:A060512 Air 06/05/12 12:00 06/06/12 09:25 10194400007 ASGP4D:A060512 Air 06/05/12 13:46 06/06/12 09:25 10194400008 ASGP4S:A060512 Air 06/05/12 13:51 06/06/12 09:25 10194400009 ASGP3D:A060512A Air 06/05/12 12:06 06/06/12 09:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 3 of 29 SAMPLE ANALYTE COUNT Pace Project No.: Project: 10194400 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 10194400001 ASGP1D:A060512 TO-15 61DR1 10194400002 ASGP1S:A060512 TO-15 61DR1 10194400003 ASGP2D:A060512 TO-15 61DR1 10194400004 ASGP2S:A060512 TO-15 61DR1 10194400005 ASGP3S:A060512 TO-15 61DR1 10194400006 ASGP3D:A060512 TO-15 61DR1 10194400007 ASGP4D:A060512 TO-15 61DR1 10194400008 ASGP4S:A060512 TO-15 61DR1 10194400009 ASGP3D:A060512A TO-15 61DR1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 4 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP1D:A060512 Lab ID:10194400001 Collected:06/05/12 09:57 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 681 ug/m3 18 06/18/12 21:12 67-64-18.6 Benzene ND ug/m3 18 06/18/12 21:12 71-43-25.8 Benzyl chloride ND ug/m3 18 06/18/12 21:12 100-44-718.9 Bromodichloromethane ND ug/m3 18 06/18/12 21:12 75-27-424.5 Bromoform ND ug/m3 18 06/18/12 21:12 75-25-237.8 Bromomethane ND ug/m3 18 06/18/12 21:12 74-83-914.2 1,3-Butadiene ND ug/m3 18 06/18/12 21:12 106-99-08.1 2-Butanone (MEK)ND ug/m3 18 06/18/12 21:12 78-93-310.8 Carbon disulfide ND ug/m3 18 06/18/12 21:12 75-15-011.3 Carbon tetrachloride ND ug/m3 18 06/18/12 21:12 56-23-511.5 Chlorobenzene ND ug/m3 18 06/18/12 21:12 108-90-716.9 Chloroethane ND ug/m3 18 06/18/12 21:12 75-00-39.7 Chloroform ND ug/m3 18 06/18/12 21:12 67-66-317.8 Chloromethane ND ug/m3 18 06/18/12 21:12 74-87-37.6 Cyclohexane ND ug/m3 18 06/18/12 21:12 110-82-712.2 Dibromochloromethane ND ug/m3 18 06/18/12 21:12 124-48-131.1 1,2-Dibromoethane (EDB)ND ug/m3 18 06/18/12 21:12 106-93-428.1 1,2-Dichlorobenzene ND ug/m3 18 06/18/12 21:12 95-50-122.0 1,3-Dichlorobenzene ND ug/m3 18 06/18/12 21:12 541-73-122.0 1,4-Dichlorobenzene ND ug/m3 18 06/18/12 21:12 106-46-722.0 Dichlorodifluoromethane ND ug/m3 18 06/18/12 21:12 75-71-818.2 1,1-Dichloroethane ND ug/m3 18 06/18/12 21:12 75-34-314.8 1,2-Dichloroethane ND ug/m3 18 06/18/12 21:12 107-06-27.4 1,1-Dichloroethene ND ug/m3 18 06/18/12 21:12 75-35-414.6 cis-1,2-Dichloroethene ND ug/m3 18 06/18/12 21:12 156-59-214.6 trans-1,2-Dichloroethene ND ug/m3 18 06/18/12 21:12 156-60-514.6 1,2-Dichloropropane ND ug/m3 18 06/18/12 21:12 78-87-516.9 cis-1,3-Dichloropropene ND ug/m3 18 06/18/12 21:12 10061-01-516.6 trans-1,3-Dichloropropene ND ug/m3 18 06/18/12 21:12 10061-02-616.6 Dichlorotetrafluoroethane ND ug/m3 18 06/18/12 21:12 76-14-225.6 Ethanol 210 ug/m3 18 06/18/12 21:12 64-17-5 SS6.8 Ethyl acetate ND ug/m3 18 06/18/12 21:12 141-78-613.1 Ethylbenzene 33.0 ug/m3 18 06/18/12 21:12 100-41-415.8 4-Ethyltoluene ND ug/m3 18 06/18/12 21:12 622-96-818.0 n-Heptane ND ug/m3 18 06/18/12 21:12 142-82-514.9 Hexachloro-1,3-butadiene ND ug/m3 18 06/18/12 21:12 87-68-339.6 n-Hexane 42.4 ug/m3 18 06/18/12 21:12 110-54-313.0 2-Hexanone ND ug/m3 18 06/18/12 21:12 591-78-614.9 Methylene Chloride ND ug/m3 18 06/18/12 21:12 75-09-212.8 4-Methyl-2-pentanone (MIBK)ND ug/m3 18 06/18/12 21:12 108-10-114.9 Methyl-tert-butyl ether ND ug/m3 18 06/18/12 21:12 1634-04-413.1 Naphthalene ND ug/m3 18 06/18/12 21:12 91-20-319.3 2-Propanol ND ug/m3 18 06/18/12 21:12 67-63-045.0 Propylene ND ug/m3 18 06/18/12 21:12 115-07-16.3 Styrene ND ug/m3 18 06/18/12 21:12 100-42-515.7 1,1,2,2-Tetrachloroethane ND ug/m3 18 06/18/12 21:12 79-34-512.6 Tetrachloroethene ND ug/m3 18 06/18/12 21:12 127-18-412.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 5 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 5 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP1D:A060512 Lab ID:10194400001 Collected:06/05/12 09:57 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 18 06/18/12 21:12 109-99-910.8 Toluene 354 ug/m3 18 06/18/12 21:12 108-88-313.9 1,2,4-Trichlorobenzene ND ug/m3 18 06/18/12 21:12 120-82-117.8 1,1,1-Trichloroethane 1710 ug/m3 18 06/18/12 21:12 71-55-620.0 1,1,2-Trichloroethane ND ug/m3 18 06/18/12 21:12 79-00-59.9 Trichloroethene ND ug/m3 18 06/18/12 21:12 79-01-69.9 Trichlorofluoromethane 1280 ug/m3 18 06/18/12 21:12 75-69-420.5 1,1,2-Trichlorotrifluoroethane ND ug/m3 18 06/18/12 21:12 76-13-128.8 1,2,4-Trimethylbenzene ND ug/m3 18 06/18/12 21:12 95-63-618.0 1,3,5-Trimethylbenzene ND ug/m3 18 06/18/12 21:12 108-67-818.0 Vinyl acetate ND ug/m3 18 06/18/12 21:12 108-05-412.8 Vinyl chloride ND ug/m3 18 06/18/12 21:12 75-01-44.7 m&p-Xylene 145 ug/m3 18 06/18/12 21:12 179601-23-131.7 o-Xylene ND ug/m3 18 06/18/12 21:12 95-47-615.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 6 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 6 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP1S:A060512 Lab ID:10194400002 Collected:06/05/12 10:00 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 149 ug/m3 30.24 06/18/12 23:33 67-64-114.5 Benzene ND ug/m3 30.24 06/18/12 23:33 71-43-29.8 Benzyl chloride ND ug/m3 30.24 06/18/12 23:33 100-44-731.8 Bromodichloromethane ND ug/m3 30.24 06/18/12 23:33 75-27-441.1 Bromoform ND ug/m3 30.24 06/18/12 23:33 75-25-263.5 Bromomethane ND ug/m3 30.24 06/18/12 23:33 74-83-923.9 1,3-Butadiene ND ug/m3 30.24 06/18/12 23:33 106-99-013.6 2-Butanone (MEK)ND ug/m3 30.24 06/18/12 23:33 78-93-318.1 Carbon disulfide 20.9 ug/m3 30.24 06/18/12 23:33 75-15-0 SS19.1 Carbon tetrachloride ND ug/m3 30.24 06/18/12 23:33 56-23-519.4 Chlorobenzene ND ug/m3 30.24 06/18/12 23:33 108-90-728.4 Chloroethane ND ug/m3 30.24 06/18/12 23:33 75-00-316.3 Chloroform ND ug/m3 30.24 06/18/12 23:33 67-66-329.9 Chloromethane ND ug/m3 30.24 06/18/12 23:33 74-87-312.7 Cyclohexane ND ug/m3 30.24 06/18/12 23:33 110-82-720.6 Dibromochloromethane ND ug/m3 30.24 06/18/12 23:33 124-48-152.3 1,2-Dibromoethane (EDB)ND ug/m3 30.24 06/18/12 23:33 106-93-447.2 1,2-Dichlorobenzene ND ug/m3 30.24 06/18/12 23:33 95-50-136.9 1,3-Dichlorobenzene ND ug/m3 30.24 06/18/12 23:33 541-73-136.9 1,4-Dichlorobenzene ND ug/m3 30.24 06/18/12 23:33 106-46-736.9 Dichlorodifluoromethane ND ug/m3 30.24 06/18/12 23:33 75-71-830.5 1,1-Dichloroethane ND ug/m3 30.24 06/18/12 23:33 75-34-324.8 1,2-Dichloroethane ND ug/m3 30.24 06/18/12 23:33 107-06-212.4 1,1-Dichloroethene ND ug/m3 30.24 06/18/12 23:33 75-35-424.5 cis-1,2-Dichloroethene ND ug/m3 30.24 06/18/12 23:33 156-59-224.5 trans-1,2-Dichloroethene ND ug/m3 30.24 06/18/12 23:33 156-60-524.5 1,2-Dichloropropane ND ug/m3 30.24 06/18/12 23:33 78-87-528.4 cis-1,3-Dichloropropene ND ug/m3 30.24 06/18/12 23:33 10061-01-527.8 trans-1,3-Dichloropropene ND ug/m3 30.24 06/18/12 23:33 10061-02-627.8 Dichlorotetrafluoroethane ND ug/m3 30.24 06/18/12 23:33 76-14-242.9 Ethanol ND ug/m3 30.24 06/18/12 23:33 64-17-511.5 Ethyl acetate ND ug/m3 30.24 06/18/12 23:33 141-78-622.1 Ethylbenzene 29.4 ug/m3 30.24 06/18/12 23:33 100-41-426.6 4-Ethyltoluene ND ug/m3 30.24 06/18/12 23:33 622-96-830.2 n-Heptane ND ug/m3 30.24 06/18/12 23:33 142-82-525.1 Hexachloro-1,3-butadiene ND ug/m3 30.24 06/18/12 23:33 87-68-366.5 n-Hexane ND ug/m3 30.24 06/18/12 23:33 110-54-321.8 2-Hexanone ND ug/m3 30.24 06/18/12 23:33 591-78-625.1 Methylene Chloride ND ug/m3 30.24 06/18/12 23:33 75-09-221.5 4-Methyl-2-pentanone (MIBK)ND ug/m3 30.24 06/18/12 23:33 108-10-125.1 Methyl-tert-butyl ether ND ug/m3 30.24 06/18/12 23:33 1634-04-422.1 Naphthalene ND ug/m3 30.24 06/18/12 23:33 91-20-332.4 2-Propanol ND ug/m3 30.24 06/18/12 23:33 67-63-075.6 Propylene ND ug/m3 30.24 06/18/12 23:33 115-07-110.6 Styrene ND ug/m3 30.24 06/18/12 23:33 100-42-526.3 1,1,2,2-Tetrachloroethane ND ug/m3 30.24 06/18/12 23:33 79-34-521.1 Tetrachloroethene ND ug/m3 30.24 06/18/12 23:33 127-18-420.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 7 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 7 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP1S:A060512 Lab ID:10194400002 Collected:06/05/12 10:00 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 30.24 06/18/12 23:33 109-99-918.1 Toluene 483 ug/m3 30.24 06/18/12 23:33 108-88-323.3 1,2,4-Trichlorobenzene ND ug/m3 30.24 06/18/12 23:33 120-82-129.9 1,1,1-Trichloroethane 2310 ug/m3 30.24 06/18/12 23:33 71-55-633.6 1,1,2-Trichloroethane ND ug/m3 30.24 06/18/12 23:33 79-00-516.6 Trichloroethene ND ug/m3 30.24 06/18/12 23:33 79-01-616.6 Trichlorofluoromethane 1090 ug/m3 30.24 06/18/12 23:33 75-69-434.5 1,1,2-Trichlorotrifluoroethane ND ug/m3 30.24 06/18/12 23:33 76-13-148.4 1,2,4-Trimethylbenzene ND ug/m3 30.24 06/18/12 23:33 95-63-630.2 1,3,5-Trimethylbenzene ND ug/m3 30.24 06/18/12 23:33 108-67-830.2 Vinyl acetate ND ug/m3 30.24 06/18/12 23:33 108-05-421.5 Vinyl chloride ND ug/m3 30.24 06/18/12 23:33 75-01-47.9 m&p-Xylene 133 ug/m3 30.24 06/18/12 23:33 179601-23-153.2 o-Xylene ND ug/m3 30.24 06/18/12 23:33 95-47-626.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 8 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 8 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP2D:A060512 Lab ID:10194400003 Collected:06/05/12 10:53 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 69.3 ug/m3 1.8 06/18/12 22:37 67-64-10.86 Benzene ND ug/m3 1.8 06/18/12 22:37 71-43-20.58 Benzyl chloride ND ug/m3 1.8 06/18/12 22:37 100-44-71.9 Bromodichloromethane 7.1 ug/m3 1.8 06/18/12 22:37 75-27-42.4 Bromoform ND ug/m3 1.8 06/18/12 22:37 75-25-23.8 Bromomethane ND ug/m3 1.8 06/18/12 22:37 74-83-91.4 1,3-Butadiene ND ug/m3 1.8 06/18/12 22:37 106-99-00.81 2-Butanone (MEK)16.6 ug/m3 1.8 06/18/12 22:37 78-93-3 CH,L11.1 Carbon disulfide 20.0 ug/m3 1.8 06/18/12 22:37 75-15-0 SS1.1 Carbon tetrachloride 1.6 ug/m3 1.8 06/18/12 22:37 56-23-51.2 Chlorobenzene ND ug/m3 1.8 06/18/12 22:37 108-90-71.7 Chloroethane ND ug/m3 1.8 06/18/12 22:37 75-00-30.97 Chloroform 12.5 ug/m3 1.8 06/18/12 22:37 67-66-31.8 Chloromethane ND ug/m3 1.8 06/18/12 22:37 74-87-30.76 Cyclohexane ND ug/m3 1.8 06/18/12 22:37 110-82-71.2 Dibromochloromethane ND ug/m3 1.8 06/18/12 22:37 124-48-13.1 1,2-Dibromoethane (EDB)ND ug/m3 1.8 06/18/12 22:37 106-93-42.8 1,2-Dichlorobenzene ND ug/m3 1.8 06/18/12 22:37 95-50-12.2 1,3-Dichlorobenzene ND ug/m3 1.8 06/18/12 22:37 541-73-12.2 1,4-Dichlorobenzene ND ug/m3 1.8 06/18/12 22:37 106-46-72.2 Dichlorodifluoromethane ND ug/m3 1.8 06/18/12 22:37 75-71-81.8 1,1-Dichloroethane ND ug/m3 1.8 06/18/12 22:37 75-34-31.5 1,2-Dichloroethane ND ug/m3 1.8 06/18/12 22:37 107-06-20.74 1,1-Dichloroethene ND ug/m3 1.8 06/18/12 22:37 75-35-41.5 cis-1,2-Dichloroethene ND ug/m3 1.8 06/18/12 22:37 156-59-21.5 trans-1,2-Dichloroethene ND ug/m3 1.8 06/18/12 22:37 156-60-51.5 1,2-Dichloropropane ND ug/m3 1.8 06/18/12 22:37 78-87-51.7 cis-1,3-Dichloropropene ND ug/m3 1.8 06/18/12 22:37 10061-01-51.7 trans-1,3-Dichloropropene ND ug/m3 1.8 06/18/12 22:37 10061-02-61.7 Dichlorotetrafluoroethane ND ug/m3 1.8 06/18/12 22:37 76-14-22.6 Ethanol ND ug/m3 1.8 06/18/12 22:37 64-17-50.68 Ethyl acetate ND ug/m3 1.8 06/18/12 22:37 141-78-61.3 Ethylbenzene 3.3 ug/m3 1.8 06/18/12 22:37 100-41-41.6 4-Ethyltoluene ND ug/m3 1.8 06/18/12 22:37 622-96-81.8 n-Heptane ND ug/m3 1.8 06/18/12 22:37 142-82-51.5 Hexachloro-1,3-butadiene ND ug/m3 1.8 06/18/12 22:37 87-68-34.0 n-Hexane 9.9 ug/m3 1.8 06/18/12 22:37 110-54-31.3 2-Hexanone ND ug/m3 1.8 06/18/12 22:37 591-78-61.5 Methylene Chloride ND ug/m3 1.8 06/18/12 22:37 75-09-21.3 4-Methyl-2-pentanone (MIBK)ND ug/m3 1.8 06/18/12 22:37 108-10-11.5 Methyl-tert-butyl ether ND ug/m3 1.8 06/18/12 22:37 1634-04-41.3 Naphthalene ND ug/m3 1.8 06/18/12 22:37 91-20-31.9 2-Propanol ND ug/m3 1.8 06/18/12 22:37 67-63-04.5 Propylene ND ug/m3 1.8 06/18/12 22:37 115-07-10.63 Styrene ND ug/m3 1.8 06/18/12 22:37 100-42-51.6 1,1,2,2-Tetrachloroethane ND ug/m3 1.8 06/18/12 22:37 79-34-51.3 Tetrachloroethene 167 ug/m3 1.8 06/18/12 22:37 127-18-41.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 9 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 9 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP2D:A060512 Lab ID:10194400003 Collected:06/05/12 10:53 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 1.8 06/18/12 22:37 109-99-91.1 Toluene 85.6 ug/m3 1.8 06/18/12 22:37 108-88-31.4 1,2,4-Trichlorobenzene ND ug/m3 1.8 06/18/12 22:37 120-82-11.8 1,1,1-Trichloroethane 64.2 ug/m3 1.8 06/18/12 22:37 71-55-62.0 1,1,2-Trichloroethane ND ug/m3 1.8 06/18/12 22:37 79-00-50.99 Trichloroethene ND ug/m3 1.8 06/18/12 22:37 79-01-60.99 Trichlorofluoromethane 165 ug/m3 1.8 06/18/12 22:37 75-69-42.1 1,1,2-Trichlorotrifluoroethane ND ug/m3 1.8 06/18/12 22:37 76-13-12.9 1,2,4-Trimethylbenzene 4.1 ug/m3 1.8 06/18/12 22:37 95-63-61.8 1,3,5-Trimethylbenzene ND ug/m3 1.8 06/18/12 22:37 108-67-81.8 Vinyl acetate ND ug/m3 1.8 06/18/12 22:37 108-05-41.3 Vinyl chloride ND ug/m3 1.8 06/18/12 22:37 75-01-40.47 m&p-Xylene 16.3 ug/m3 1.8 06/18/12 22:37 179601-23-13.2 o-Xylene 1.6 ug/m3 1.8 06/18/12 22:37 95-47-61.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 10 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 10 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP2S:A060512 Lab ID:10194400004 Collected:06/05/12 10:50 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 75.2 ug/m3 9 06/18/12 22:09 67-64-14.3 Benzene ND ug/m3 9 06/18/12 22:09 71-43-22.9 Benzyl chloride ND ug/m3 9 06/18/12 22:09 100-44-79.4 Bromodichloromethane ND ug/m3 9 06/18/12 22:09 75-27-412.2 Bromoform ND ug/m3 9 06/18/12 22:09 75-25-218.9 Bromomethane ND ug/m3 9 06/18/12 22:09 74-83-97.1 1,3-Butadiene ND ug/m3 9 06/18/12 22:09 106-99-04.0 2-Butanone (MEK)9.0 ug/m3 9 06/18/12 22:09 78-93-3 CH,L15.4 Carbon disulfide 82.6 ug/m3 9 06/18/12 22:09 75-15-0 SS5.7 Carbon tetrachloride ND ug/m3 9 06/18/12 22:09 56-23-55.8 Chlorobenzene ND ug/m3 9 06/18/12 22:09 108-90-78.5 Chloroethane ND ug/m3 9 06/18/12 22:09 75-00-34.9 Chloroform ND ug/m3 9 06/18/12 22:09 67-66-38.9 Chloromethane ND ug/m3 9 06/18/12 22:09 74-87-33.8 Cyclohexane ND ug/m3 9 06/18/12 22:09 110-82-76.1 Dibromochloromethane ND ug/m3 9 06/18/12 22:09 124-48-115.6 1,2-Dibromoethane (EDB)ND ug/m3 9 06/18/12 22:09 106-93-414.0 1,2-Dichlorobenzene ND ug/m3 9 06/18/12 22:09 95-50-111.0 1,3-Dichlorobenzene ND ug/m3 9 06/18/12 22:09 541-73-111.0 1,4-Dichlorobenzene ND ug/m3 9 06/18/12 22:09 106-46-711.0 Dichlorodifluoromethane ND ug/m3 9 06/18/12 22:09 75-71-89.1 1,1-Dichloroethane ND ug/m3 9 06/18/12 22:09 75-34-37.4 1,2-Dichloroethane ND ug/m3 9 06/18/12 22:09 107-06-23.7 1,1-Dichloroethene ND ug/m3 9 06/18/12 22:09 75-35-47.3 cis-1,2-Dichloroethene ND ug/m3 9 06/18/12 22:09 156-59-27.3 trans-1,2-Dichloroethene ND ug/m3 9 06/18/12 22:09 156-60-57.3 1,2-Dichloropropane ND ug/m3 9 06/18/12 22:09 78-87-58.5 cis-1,3-Dichloropropene ND ug/m3 9 06/18/12 22:09 10061-01-58.3 trans-1,3-Dichloropropene ND ug/m3 9 06/18/12 22:09 10061-02-68.3 Dichlorotetrafluoroethane ND ug/m3 9 06/18/12 22:09 76-14-212.8 Ethanol ND ug/m3 9 06/18/12 22:09 64-17-53.4 Ethyl acetate ND ug/m3 9 06/18/12 22:09 141-78-66.6 Ethylbenzene ND ug/m3 9 06/18/12 22:09 100-41-47.9 4-Ethyltoluene ND ug/m3 9 06/18/12 22:09 622-96-89.0 n-Heptane ND ug/m3 9 06/18/12 22:09 142-82-57.5 Hexachloro-1,3-butadiene ND ug/m3 9 06/18/12 22:09 87-68-319.8 n-Hexane ND ug/m3 9 06/18/12 22:09 110-54-36.5 2-Hexanone ND ug/m3 9 06/18/12 22:09 591-78-67.5 Methylene Chloride ND ug/m3 9 06/18/12 22:09 75-09-26.4 4-Methyl-2-pentanone (MIBK)ND ug/m3 9 06/18/12 22:09 108-10-17.5 Methyl-tert-butyl ether ND ug/m3 9 06/18/12 22:09 1634-04-46.6 Naphthalene ND ug/m3 9 06/18/12 22:09 91-20-39.6 2-Propanol ND ug/m3 9 06/18/12 22:09 67-63-022.5 Propylene ND ug/m3 9 06/18/12 22:09 115-07-13.2 Styrene ND ug/m3 9 06/18/12 22:09 100-42-57.8 1,1,2,2-Tetrachloroethane ND ug/m3 9 06/18/12 22:09 79-34-56.3 Tetrachloroethene 477 ug/m3 9 06/18/12 22:09 127-18-46.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 11 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 11 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP2S:A060512 Lab ID:10194400004 Collected:06/05/12 10:50 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 9 06/18/12 22:09 109-99-95.4 Toluene 145 ug/m3 9 06/18/12 22:09 108-88-36.9 1,2,4-Trichlorobenzene ND ug/m3 9 06/18/12 22:09 120-82-18.9 1,1,1-Trichloroethane 58.4 ug/m3 9 06/18/12 22:09 71-55-610 1,1,2-Trichloroethane ND ug/m3 9 06/18/12 22:09 79-00-55.0 Trichloroethene ND ug/m3 9 06/18/12 22:09 79-01-65.0 Trichlorofluoromethane 197 ug/m3 9 06/18/12 22:09 75-69-410.3 1,1,2-Trichlorotrifluoroethane ND ug/m3 9 06/18/12 22:09 76-13-114.4 1,2,4-Trimethylbenzene ND ug/m3 9 06/18/12 22:09 95-63-69.0 1,3,5-Trimethylbenzene ND ug/m3 9 06/18/12 22:09 108-67-89.0 Vinyl acetate ND ug/m3 9 06/18/12 22:09 108-05-46.4 Vinyl chloride ND ug/m3 9 06/18/12 22:09 75-01-42.3 m&p-Xylene ND ug/m3 9 06/18/12 22:09 179601-23-115.8 o-Xylene ND ug/m3 9 06/18/12 22:09 95-47-67.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 12 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 12 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3S:A060512 Lab ID:10194400005 Collected:06/05/12 11:50 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 6660 ug/m3 144 06/19/12 00:30 67-64-169.1 Benzene ND ug/m3 144 06/19/12 00:30 71-43-246.8 Benzyl chloride ND ug/m3 144 06/19/12 00:30 100-44-7151 Bromodichloromethane ND ug/m3 144 06/19/12 00:30 75-27-4196 Bromoform ND ug/m3 144 06/19/12 00:30 75-25-2302 Bromomethane ND ug/m3 144 06/19/12 00:30 74-83-9114 1,3-Butadiene ND ug/m3 144 06/19/12 00:30 106-99-064.8 2-Butanone (MEK)227 ug/m3 144 06/19/12 00:30 78-93-3 CH,L186.4 Carbon disulfide ND ug/m3 144 06/19/12 00:30 75-15-090.7 Carbon tetrachloride ND ug/m3 144 06/19/12 00:30 56-23-592.2 Chlorobenzene ND ug/m3 144 06/19/12 00:30 108-90-7135 Chloroethane ND ug/m3 144 06/19/12 00:30 75-00-377.8 Chloroform ND ug/m3 144 06/19/12 00:30 67-66-3143 Chloromethane ND ug/m3 144 06/19/12 00:30 74-87-360.5 Cyclohexane ND ug/m3 144 06/19/12 00:30 110-82-797.9 Dibromochloromethane ND ug/m3 144 06/19/12 00:30 124-48-1249 1,2-Dibromoethane (EDB)ND ug/m3 144 06/19/12 00:30 106-93-4225 1,2-Dichlorobenzene ND ug/m3 144 06/19/12 00:30 95-50-1176 1,3-Dichlorobenzene ND ug/m3 144 06/19/12 00:30 541-73-1176 1,4-Dichlorobenzene ND ug/m3 144 06/19/12 00:30 106-46-7176 Dichlorodifluoromethane ND ug/m3 144 06/19/12 00:30 75-71-8145 1,1-Dichloroethane ND ug/m3 144 06/19/12 00:30 75-34-3118 1,2-Dichloroethane ND ug/m3 144 06/19/12 00:30 107-06-259.0 1,1-Dichloroethene ND ug/m3 144 06/19/12 00:30 75-35-4117 cis-1,2-Dichloroethene ND ug/m3 144 06/19/12 00:30 156-59-2117 trans-1,2-Dichloroethene ND ug/m3 144 06/19/12 00:30 156-60-5117 1,2-Dichloropropane ND ug/m3 144 06/19/12 00:30 78-87-5135 cis-1,3-Dichloropropene ND ug/m3 144 06/19/12 00:30 10061-01-5132 trans-1,3-Dichloropropene ND ug/m3 144 06/19/12 00:30 10061-02-6132 Dichlorotetrafluoroethane ND ug/m3 144 06/19/12 00:30 76-14-2204 Ethanol 1190 ug/m3 144 06/19/12 00:30 64-17-5 SS54.7 Ethyl acetate ND ug/m3 144 06/19/12 00:30 141-78-6105 Ethylbenzene ND ug/m3 144 06/19/12 00:30 100-41-4127 4-Ethyltoluene ND ug/m3 144 06/19/12 00:30 622-96-8144 n-Heptane ND ug/m3 144 06/19/12 00:30 142-82-5120 Hexachloro-1,3-butadiene ND ug/m3 144 06/19/12 00:30 87-68-3317 n-Hexane 121 ug/m3 144 06/19/12 00:30 110-54-3104 2-Hexanone ND ug/m3 144 06/19/12 00:30 591-78-6120 Methylene Chloride ND ug/m3 144 06/19/12 00:30 75-09-2102 4-Methyl-2-pentanone (MIBK)ND ug/m3 144 06/19/12 00:30 108-10-1120 Methyl-tert-butyl ether ND ug/m3 144 06/19/12 00:30 1634-04-4105 Naphthalene ND ug/m3 144 06/19/12 00:30 91-20-3154 2-Propanol ND ug/m3 144 06/19/12 00:30 67-63-0360 Propylene ND ug/m3 144 06/19/12 00:30 115-07-150.4 Styrene ND ug/m3 144 06/19/12 00:30 100-42-5125 1,1,2,2-Tetrachloroethane ND ug/m3 144 06/19/12 00:30 79-34-5101 Tetrachloroethene 19700 ug/m3 144 06/19/12 00:30 127-18-499.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 13 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 13 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3S:A060512 Lab ID:10194400005 Collected:06/05/12 11:50 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 144 06/19/12 00:30 109-99-986.4 Toluene 188 ug/m3 144 06/19/12 00:30 108-88-3111 1,2,4-Trichlorobenzene ND ug/m3 144 06/19/12 00:30 120-82-1143 1,1,1-Trichloroethane ND ug/m3 144 06/19/12 00:30 71-55-6160 1,1,2-Trichloroethane ND ug/m3 144 06/19/12 00:30 79-00-579.2 Trichloroethene 820 ug/m3 144 06/19/12 00:30 79-01-679.2 Trichlorofluoromethane 320 ug/m3 144 06/19/12 00:30 75-69-4164 1,1,2-Trichlorotrifluoroethane ND ug/m3 144 06/19/12 00:30 76-13-1230 1,2,4-Trimethylbenzene ND ug/m3 144 06/19/12 00:30 95-63-6144 1,3,5-Trimethylbenzene ND ug/m3 144 06/19/12 00:30 108-67-8144 Vinyl acetate ND ug/m3 144 06/19/12 00:30 108-05-4102 Vinyl chloride ND ug/m3 144 06/19/12 00:30 75-01-437.4 m&p-Xylene ND ug/m3 144 06/19/12 00:30 179601-23-1253 o-Xylene ND ug/m3 144 06/19/12 00:30 95-47-6127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 14 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 14 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3D:A060512 Lab ID:10194400006 Collected:06/05/12 12:00 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 92.2 ug/m3 30.24 06/19/12 00:02 67-64-114.5 Benzene ND ug/m3 30.24 06/19/12 00:02 71-43-29.8 Benzyl chloride ND ug/m3 30.24 06/19/12 00:02 100-44-731.8 Bromodichloromethane ND ug/m3 30.24 06/19/12 00:02 75-27-441.1 Bromoform ND ug/m3 30.24 06/19/12 00:02 75-25-263.5 Bromomethane ND ug/m3 30.24 06/19/12 00:02 74-83-923.9 1,3-Butadiene ND ug/m3 30.24 06/19/12 00:02 106-99-013.6 2-Butanone (MEK)ND ug/m3 30.24 06/19/12 00:02 78-93-318.1 Carbon disulfide ND ug/m3 30.24 06/19/12 00:02 75-15-019.1 Carbon tetrachloride ND ug/m3 30.24 06/19/12 00:02 56-23-519.4 Chlorobenzene ND ug/m3 30.24 06/19/12 00:02 108-90-728.4 Chloroethane ND ug/m3 30.24 06/19/12 00:02 75-00-316.3 Chloroform ND ug/m3 30.24 06/19/12 00:02 67-66-329.9 Chloromethane ND ug/m3 30.24 06/19/12 00:02 74-87-312.7 Cyclohexane ND ug/m3 30.24 06/19/12 00:02 110-82-720.6 Dibromochloromethane ND ug/m3 30.24 06/19/12 00:02 124-48-152.3 1,2-Dibromoethane (EDB)ND ug/m3 30.24 06/19/12 00:02 106-93-447.2 1,2-Dichlorobenzene ND ug/m3 30.24 06/19/12 00:02 95-50-136.9 1,3-Dichlorobenzene ND ug/m3 30.24 06/19/12 00:02 541-73-136.9 1,4-Dichlorobenzene ND ug/m3 30.24 06/19/12 00:02 106-46-736.9 Dichlorodifluoromethane ND ug/m3 30.24 06/19/12 00:02 75-71-830.5 1,1-Dichloroethane ND ug/m3 30.24 06/19/12 00:02 75-34-324.8 1,2-Dichloroethane ND ug/m3 30.24 06/19/12 00:02 107-06-212.4 1,1-Dichloroethene ND ug/m3 30.24 06/19/12 00:02 75-35-424.5 cis-1,2-Dichloroethene ND ug/m3 30.24 06/19/12 00:02 156-59-224.5 trans-1,2-Dichloroethene ND ug/m3 30.24 06/19/12 00:02 156-60-524.5 1,2-Dichloropropane ND ug/m3 30.24 06/19/12 00:02 78-87-528.4 cis-1,3-Dichloropropene ND ug/m3 30.24 06/19/12 00:02 10061-01-527.8 trans-1,3-Dichloropropene ND ug/m3 30.24 06/19/12 00:02 10061-02-627.8 Dichlorotetrafluoroethane ND ug/m3 30.24 06/19/12 00:02 76-14-242.9 Ethanol 55.4 ug/m3 30.24 06/19/12 00:02 64-17-5 SS11.5 Ethyl acetate ND ug/m3 30.24 06/19/12 00:02 141-78-622.1 Ethylbenzene ND ug/m3 30.24 06/19/12 00:02 100-41-426.6 4-Ethyltoluene ND ug/m3 30.24 06/19/12 00:02 622-96-830.2 n-Heptane ND ug/m3 30.24 06/19/12 00:02 142-82-525.1 Hexachloro-1,3-butadiene ND ug/m3 30.24 06/19/12 00:02 87-68-366.5 n-Hexane ND ug/m3 30.24 06/19/12 00:02 110-54-321.8 2-Hexanone ND ug/m3 30.24 06/19/12 00:02 591-78-625.1 Methylene Chloride 360 ug/m3 30.24 06/19/12 00:02 75-09-221.5 4-Methyl-2-pentanone (MIBK)ND ug/m3 30.24 06/19/12 00:02 108-10-125.1 Methyl-tert-butyl ether ND ug/m3 30.24 06/19/12 00:02 1634-04-422.1 Naphthalene ND ug/m3 30.24 06/19/12 00:02 91-20-332.4 2-Propanol ND ug/m3 30.24 06/19/12 00:02 67-63-075.6 Propylene ND ug/m3 30.24 06/19/12 00:02 115-07-110.6 Styrene ND ug/m3 30.24 06/19/12 00:02 100-42-526.3 1,1,2,2-Tetrachloroethane ND ug/m3 30.24 06/19/12 00:02 79-34-521.1 Tetrachloroethene 2610 ug/m3 30.24 06/19/12 00:02 127-18-420.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 15 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 15 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3D:A060512 Lab ID:10194400006 Collected:06/05/12 12:00 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 30.24 06/19/12 00:02 109-99-918.1 Toluene 265 ug/m3 30.24 06/19/12 00:02 108-88-323.3 1,2,4-Trichlorobenzene ND ug/m3 30.24 06/19/12 00:02 120-82-129.9 1,1,1-Trichloroethane ND ug/m3 30.24 06/19/12 00:02 71-55-633.6 1,1,2-Trichloroethane ND ug/m3 30.24 06/19/12 00:02 79-00-516.6 Trichloroethene 206 ug/m3 30.24 06/19/12 00:02 79-01-616.6 Trichlorofluoromethane 120 ug/m3 30.24 06/19/12 00:02 75-69-434.5 1,1,2-Trichlorotrifluoroethane ND ug/m3 30.24 06/19/12 00:02 76-13-148.4 1,2,4-Trimethylbenzene ND ug/m3 30.24 06/19/12 00:02 95-63-630.2 1,3,5-Trimethylbenzene ND ug/m3 30.24 06/19/12 00:02 108-67-830.2 Vinyl acetate ND ug/m3 30.24 06/19/12 00:02 108-05-421.5 Vinyl chloride ND ug/m3 30.24 06/19/12 00:02 75-01-47.9 m&p-Xylene ND ug/m3 30.24 06/19/12 00:02 179601-23-153.2 o-Xylene ND ug/m3 30.24 06/19/12 00:02 95-47-626.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 16 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 16 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP4D:A060512 Lab ID:10194400007 Collected:06/05/12 13:46 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 34.4 ug/m3 9.35 06/18/12 21:40 67-64-14.5 Benzene ND ug/m3 9.35 06/18/12 21:40 71-43-23.0 Benzyl chloride ND ug/m3 9.35 06/18/12 21:40 100-44-79.8 Bromodichloromethane ND ug/m3 9.35 06/18/12 21:40 75-27-412.7 Bromoform ND ug/m3 9.35 06/18/12 21:40 75-25-219.6 Bromomethane ND ug/m3 9.35 06/18/12 21:40 74-83-97.4 1,3-Butadiene ND ug/m3 9.35 06/18/12 21:40 106-99-04.2 2-Butanone (MEK)ND ug/m3 9.35 06/18/12 21:40 78-93-35.6 Carbon disulfide ND ug/m3 9.35 06/18/12 21:40 75-15-05.9 Carbon tetrachloride 6.6 ug/m3 9.35 06/18/12 21:40 56-23-56.0 Chlorobenzene ND ug/m3 9.35 06/18/12 21:40 108-90-78.8 Chloroethane ND ug/m3 9.35 06/18/12 21:40 75-00-35.0 Chloroform ND ug/m3 9.35 06/18/12 21:40 67-66-39.3 Chloromethane ND ug/m3 9.35 06/18/12 21:40 74-87-33.9 Cyclohexane ND ug/m3 9.35 06/18/12 21:40 110-82-76.4 Dibromochloromethane ND ug/m3 9.35 06/18/12 21:40 124-48-116.2 1,2-Dibromoethane (EDB)ND ug/m3 9.35 06/18/12 21:40 106-93-414.6 1,2-Dichlorobenzene ND ug/m3 9.35 06/18/12 21:40 95-50-111.4 1,3-Dichlorobenzene ND ug/m3 9.35 06/18/12 21:40 541-73-111.4 1,4-Dichlorobenzene ND ug/m3 9.35 06/18/12 21:40 106-46-711.4 Dichlorodifluoromethane ND ug/m3 9.35 06/18/12 21:40 75-71-89.4 1,1-Dichloroethane ND ug/m3 9.35 06/18/12 21:40 75-34-37.7 1,2-Dichloroethane ND ug/m3 9.35 06/18/12 21:40 107-06-23.8 1,1-Dichloroethene ND ug/m3 9.35 06/18/12 21:40 75-35-47.6 cis-1,2-Dichloroethene ND ug/m3 9.35 06/18/12 21:40 156-59-27.6 trans-1,2-Dichloroethene ND ug/m3 9.35 06/18/12 21:40 156-60-57.6 1,2-Dichloropropane ND ug/m3 9.35 06/18/12 21:40 78-87-58.8 cis-1,3-Dichloropropene ND ug/m3 9.35 06/18/12 21:40 10061-01-58.6 trans-1,3-Dichloropropene ND ug/m3 9.35 06/18/12 21:40 10061-02-68.6 Dichlorotetrafluoroethane ND ug/m3 9.35 06/18/12 21:40 76-14-213.3 Ethanol ND ug/m3 9.35 06/18/12 21:40 64-17-53.6 Ethyl acetate ND ug/m3 9.35 06/18/12 21:40 141-78-66.8 Ethylbenzene ND ug/m3 9.35 06/18/12 21:40 100-41-48.2 4-Ethyltoluene ND ug/m3 9.35 06/18/12 21:40 622-96-89.4 n-Heptane ND ug/m3 9.35 06/18/12 21:40 142-82-57.8 Hexachloro-1,3-butadiene ND ug/m3 9.35 06/18/12 21:40 87-68-320.6 n-Hexane ND ug/m3 9.35 06/18/12 21:40 110-54-36.7 2-Hexanone ND ug/m3 9.35 06/18/12 21:40 591-78-67.8 Methylene Chloride ND ug/m3 9.35 06/18/12 21:40 75-09-26.6 4-Methyl-2-pentanone (MIBK)ND ug/m3 9.35 06/18/12 21:40 108-10-17.8 Methyl-tert-butyl ether ND ug/m3 9.35 06/18/12 21:40 1634-04-46.8 Naphthalene ND ug/m3 9.35 06/18/12 21:40 91-20-310.0 2-Propanol ND ug/m3 9.35 06/18/12 21:40 67-63-023.4 Propylene ND ug/m3 9.35 06/18/12 21:40 115-07-13.3 Styrene ND ug/m3 9.35 06/18/12 21:40 100-42-58.1 1,1,2,2-Tetrachloroethane ND ug/m3 9.35 06/18/12 21:40 79-34-56.5 Tetrachloroethene 168 ug/m3 9.35 06/18/12 21:40 127-18-46.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 17 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 17 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP4D:A060512 Lab ID:10194400007 Collected:06/05/12 13:46 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 9.35 06/18/12 21:40 109-99-95.6 Toluene 107 ug/m3 9.35 06/18/12 21:40 108-88-37.2 1,2,4-Trichlorobenzene ND ug/m3 9.35 06/18/12 21:40 120-82-19.3 1,1,1-Trichloroethane 16.7 ug/m3 9.35 06/18/12 21:40 71-55-610.4 1,1,2-Trichloroethane ND ug/m3 9.35 06/18/12 21:40 79-00-55.1 Trichloroethene ND ug/m3 9.35 06/18/12 21:40 79-01-65.1 Trichlorofluoromethane 508 ug/m3 9.35 06/18/12 21:40 75-69-410.7 1,1,2-Trichlorotrifluoroethane ND ug/m3 9.35 06/18/12 21:40 76-13-115.0 1,2,4-Trimethylbenzene ND ug/m3 9.35 06/18/12 21:40 95-63-69.3 1,3,5-Trimethylbenzene ND ug/m3 9.35 06/18/12 21:40 108-67-89.3 Vinyl acetate ND ug/m3 9.35 06/18/12 21:40 108-05-46.6 Vinyl chloride ND ug/m3 9.35 06/18/12 21:40 75-01-42.4 m&p-Xylene ND ug/m3 9.35 06/18/12 21:40 179601-23-116.5 o-Xylene ND ug/m3 9.35 06/18/12 21:40 95-47-68.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 18 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 18 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP4S:A060512 Lab ID:10194400008 Collected:06/05/12 13:51 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 524 ug/m3 36 06/18/12 23:05 67-64-117.3 Benzene ND ug/m3 36 06/18/12 23:05 71-43-211.7 Benzyl chloride ND ug/m3 36 06/18/12 23:05 100-44-737.8 Bromodichloromethane ND ug/m3 36 06/18/12 23:05 75-27-449.0 Bromoform ND ug/m3 36 06/18/12 23:05 75-25-275.6 Bromomethane ND ug/m3 36 06/18/12 23:05 74-83-928.4 1,3-Butadiene ND ug/m3 36 06/18/12 23:05 106-99-016.2 2-Butanone (MEK)129 ug/m3 36 06/18/12 23:05 78-93-3 CH,L121.6 Carbon disulfide ND ug/m3 36 06/18/12 23:05 75-15-022.7 Carbon tetrachloride ND ug/m3 36 06/18/12 23:05 56-23-523.0 Chlorobenzene ND ug/m3 36 06/18/12 23:05 108-90-733.8 Chloroethane ND ug/m3 36 06/18/12 23:05 75-00-319.4 Chloroform ND ug/m3 36 06/18/12 23:05 67-66-335.6 Chloromethane ND ug/m3 36 06/18/12 23:05 74-87-315.1 Cyclohexane ND ug/m3 36 06/18/12 23:05 110-82-724.5 Dibromochloromethane ND ug/m3 36 06/18/12 23:05 124-48-162.3 1,2-Dibromoethane (EDB)ND ug/m3 36 06/18/12 23:05 106-93-456.2 1,2-Dichlorobenzene ND ug/m3 36 06/18/12 23:05 95-50-143.9 1,3-Dichlorobenzene ND ug/m3 36 06/18/12 23:05 541-73-143.9 1,4-Dichlorobenzene ND ug/m3 36 06/18/12 23:05 106-46-743.9 Dichlorodifluoromethane ND ug/m3 36 06/18/12 23:05 75-71-836.4 1,1-Dichloroethane ND ug/m3 36 06/18/12 23:05 75-34-329.5 1,2-Dichloroethane ND ug/m3 36 06/18/12 23:05 107-06-214.8 1,1-Dichloroethene ND ug/m3 36 06/18/12 23:05 75-35-429.2 cis-1,2-Dichloroethene ND ug/m3 36 06/18/12 23:05 156-59-229.2 trans-1,2-Dichloroethene ND ug/m3 36 06/18/12 23:05 156-60-529.2 1,2-Dichloropropane ND ug/m3 36 06/18/12 23:05 78-87-533.8 cis-1,3-Dichloropropene ND ug/m3 36 06/18/12 23:05 10061-01-533.1 trans-1,3-Dichloropropene ND ug/m3 36 06/18/12 23:05 10061-02-633.1 Dichlorotetrafluoroethane ND ug/m3 36 06/18/12 23:05 76-14-251.1 Ethanol ND ug/m3 36 06/18/12 23:05 64-17-513.7 Ethyl acetate ND ug/m3 36 06/18/12 23:05 141-78-626.3 Ethylbenzene ND ug/m3 36 06/18/12 23:05 100-41-431.7 4-Ethyltoluene ND ug/m3 36 06/18/12 23:05 622-96-836.0 n-Heptane ND ug/m3 36 06/18/12 23:05 142-82-529.9 Hexachloro-1,3-butadiene ND ug/m3 36 06/18/12 23:05 87-68-379.2 n-Hexane 45.5 ug/m3 36 06/18/12 23:05 110-54-325.9 2-Hexanone ND ug/m3 36 06/18/12 23:05 591-78-629.9 Methylene Chloride ND ug/m3 36 06/18/12 23:05 75-09-225.6 4-Methyl-2-pentanone (MIBK)ND ug/m3 36 06/18/12 23:05 108-10-129.9 Methyl-tert-butyl ether ND ug/m3 36 06/18/12 23:05 1634-04-426.3 Naphthalene ND ug/m3 36 06/18/12 23:05 91-20-338.5 2-Propanol ND ug/m3 36 06/18/12 23:05 67-63-090.0 Propylene ND ug/m3 36 06/18/12 23:05 115-07-112.6 Styrene ND ug/m3 36 06/18/12 23:05 100-42-531.3 1,1,2,2-Tetrachloroethane ND ug/m3 36 06/18/12 23:05 79-34-525.1 Tetrachloroethene 34.8 ug/m3 36 06/18/12 23:05 127-18-424.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 19 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 19 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP4S:A060512 Lab ID:10194400008 Collected:06/05/12 13:51 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 36 06/18/12 23:05 109-99-921.6 Toluene 3340 ug/m3 36 06/18/12 23:05 108-88-327.7 1,2,4-Trichlorobenzene ND ug/m3 36 06/18/12 23:05 120-82-135.6 1,1,1-Trichloroethane ND ug/m3 36 06/18/12 23:05 71-55-640.0 1,1,2-Trichloroethane ND ug/m3 36 06/18/12 23:05 79-00-519.8 Trichloroethene ND ug/m3 36 06/18/12 23:05 79-01-619.8 Trichlorofluoromethane 935 ug/m3 36 06/18/12 23:05 75-69-441.0 1,1,2-Trichlorotrifluoroethane ND ug/m3 36 06/18/12 23:05 76-13-157.6 1,2,4-Trimethylbenzene ND ug/m3 36 06/18/12 23:05 95-63-636.0 1,3,5-Trimethylbenzene ND ug/m3 36 06/18/12 23:05 108-67-836.0 Vinyl acetate ND ug/m3 36 06/18/12 23:05 108-05-425.6 Vinyl chloride ND ug/m3 36 06/18/12 23:05 75-01-49.4 m&p-Xylene ND ug/m3 36 06/18/12 23:05 179601-23-163.4 o-Xylene ND ug/m3 36 06/18/12 23:05 95-47-631.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 20 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 20 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3D:A060512A Lab ID:10194400009 Collected:06/05/12 12:06 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone ND ug/m3 37.4 06/18/12 20:15 67-64-118.0 Benzene ND ug/m3 37.4 06/18/12 20:15 71-43-212.2 Benzyl chloride ND ug/m3 37.4 06/18/12 20:15 100-44-739.3 Bromodichloromethane ND ug/m3 37.4 06/18/12 20:15 75-27-450.9 Bromoform ND ug/m3 37.4 06/18/12 20:15 75-25-278.5 Bromomethane ND ug/m3 37.4 06/18/12 20:15 74-83-929.5 1,3-Butadiene ND ug/m3 37.4 06/18/12 20:15 106-99-016.8 2-Butanone (MEK)ND ug/m3 37.4 06/18/12 20:15 78-93-322.4 Carbon disulfide ND ug/m3 37.4 06/18/12 20:15 75-15-023.6 Carbon tetrachloride ND ug/m3 37.4 06/18/12 20:15 56-23-523.9 Chlorobenzene ND ug/m3 37.4 06/18/12 20:15 108-90-735.2 Chloroethane ND ug/m3 37.4 06/18/12 20:15 75-00-320.2 Chloroform ND ug/m3 37.4 06/18/12 20:15 67-66-337.0 Chloromethane ND ug/m3 37.4 06/18/12 20:15 74-87-315.7 Cyclohexane ND ug/m3 37.4 06/18/12 20:15 110-82-725.4 Dibromochloromethane ND ug/m3 37.4 06/18/12 20:15 124-48-164.7 1,2-Dibromoethane (EDB)ND ug/m3 37.4 06/18/12 20:15 106-93-458.3 1,2-Dichlorobenzene ND ug/m3 37.4 06/18/12 20:15 95-50-145.6 1,3-Dichlorobenzene ND ug/m3 37.4 06/18/12 20:15 541-73-145.6 1,4-Dichlorobenzene ND ug/m3 37.4 06/18/12 20:15 106-46-745.6 Dichlorodifluoromethane ND ug/m3 37.4 06/18/12 20:15 75-71-837.8 1,1-Dichloroethane ND ug/m3 37.4 06/18/12 20:15 75-34-330.7 1,2-Dichloroethane ND ug/m3 37.4 06/18/12 20:15 107-06-215.3 1,1-Dichloroethene ND ug/m3 37.4 06/18/12 20:15 75-35-430.3 cis-1,2-Dichloroethene ND ug/m3 37.4 06/18/12 20:15 156-59-230.3 trans-1,2-Dichloroethene ND ug/m3 37.4 06/18/12 20:15 156-60-530.3 1,2-Dichloropropane ND ug/m3 37.4 06/18/12 20:15 78-87-535.2 cis-1,3-Dichloropropene ND ug/m3 37.4 06/18/12 20:15 10061-01-534.4 trans-1,3-Dichloropropene ND ug/m3 37.4 06/18/12 20:15 10061-02-634.4 Dichlorotetrafluoroethane ND ug/m3 37.4 06/18/12 20:15 76-14-253.1 Ethanol ND ug/m3 37.4 06/18/12 20:15 64-17-514.2 Ethyl acetate ND ug/m3 37.4 06/18/12 20:15 141-78-627.3 Ethylbenzene ND ug/m3 37.4 06/18/12 20:15 100-41-432.9 4-Ethyltoluene ND ug/m3 37.4 06/18/12 20:15 622-96-837.4 n-Heptane ND ug/m3 37.4 06/18/12 20:15 142-82-531.0 Hexachloro-1,3-butadiene ND ug/m3 37.4 06/18/12 20:15 87-68-382.3 n-Hexane ND ug/m3 37.4 06/18/12 20:15 110-54-326.9 2-Hexanone ND ug/m3 37.4 06/18/12 20:15 591-78-631.0 Methylene Chloride ND ug/m3 37.4 06/18/12 20:15 75-09-226.6 4-Methyl-2-pentanone (MIBK)ND ug/m3 37.4 06/18/12 20:15 108-10-131.0 Methyl-tert-butyl ether ND ug/m3 37.4 06/18/12 20:15 1634-04-427.3 Naphthalene ND ug/m3 37.4 06/18/12 20:15 91-20-340.0 2-Propanol ND ug/m3 37.4 06/18/12 20:15 67-63-093.5 Propylene ND ug/m3 37.4 06/18/12 20:15 115-07-113.1 Styrene ND ug/m3 37.4 06/18/12 20:15 100-42-532.5 1,1,2,2-Tetrachloroethane ND ug/m3 37.4 06/18/12 20:15 79-34-526.1 Tetrachloroethene 7100 ug/m3 37.4 06/18/12 20:15 127-18-425.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 21 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 21 of 29 ANALYTICAL RESULTS Pace Project No.: Project: 10194400 SBI068 Sample:ASGP3D:A060512A Lab ID:10194400009 Collected:06/05/12 12:06 Received:06/06/12 09:25 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 37.4 06/18/12 20:15 109-99-922.4 Toluene 218 ug/m3 37.4 06/18/12 20:15 108-88-328.8 1,2,4-Trichlorobenzene ND ug/m3 37.4 06/18/12 20:15 120-82-137.0 1,1,1-Trichloroethane ND ug/m3 37.4 06/18/12 20:15 71-55-641.5 1,1,2-Trichloroethane ND ug/m3 37.4 06/18/12 20:15 79-00-520.6 Trichloroethene 775 ug/m3 37.4 06/18/12 20:15 79-01-620.6 Trichlorofluoromethane 261 ug/m3 37.4 06/18/12 20:15 75-69-442.6 1,1,2-Trichlorotrifluoroethane ND ug/m3 37.4 06/18/12 20:15 76-13-159.8 1,2,4-Trimethylbenzene ND ug/m3 37.4 06/18/12 20:15 95-63-637.4 1,3,5-Trimethylbenzene ND ug/m3 37.4 06/18/12 20:15 108-67-837.4 Vinyl acetate ND ug/m3 37.4 06/18/12 20:15 108-05-426.6 Vinyl chloride ND ug/m3 37.4 06/18/12 20:15 75-01-49.7 m&p-Xylene ND ug/m3 37.4 06/18/12 20:15 179601-23-165.8 o-Xylene ND ug/m3 37.4 06/18/12 20:15 95-47-632.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 22 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 22 of 29 QUALITY CONTROL DATA Pace Project No.: Project: 10194400 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/15120 TO-15 TO-15 TO15 MSV AIR Low Level Associated Lab Samples:10194400001, 10194400002, 10194400003, 10194400004, 10194400005, 10194400006, 10194400007, 10194400008, 10194400009 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1219377 Associated Lab Samples:10194400001, 10194400002, 10194400003, 10194400004, 10194400005, 10194400006, 10194400007, 10194400008, 10194400009 Matrix:Air Analyzed 1,1,1-Trichloroethane ug/m3 ND 1.1 06/18/12 09:14 1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 06/18/12 09:14 1,1,2-Trichloroethane ug/m3 ND 0.55 06/18/12 09:14 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 06/18/12 09:14 1,1-Dichloroethane ug/m3 ND 0.82 06/18/12 09:14 1,1-Dichloroethene ug/m3 ND 0.81 06/18/12 09:14 1,2,4-Trichlorobenzene ug/m3 ND 0.99 06/18/12 09:14 1,2,4-Trimethylbenzene ug/m3 ND 1.0 06/18/12 09:14 1,2-Dibromoethane (EDB)ug/m3 ND 1.6 06/18/12 09:14 1,2-Dichlorobenzene ug/m3 ND 1.2 06/18/12 09:14 1,2-Dichloroethane ug/m3 ND 0.41 06/18/12 09:14 1,2-Dichloropropane ug/m3 ND 0.94 06/18/12 09:14 1,3,5-Trimethylbenzene ug/m3 ND 1.0 06/18/12 09:14 1,3-Butadiene ug/m3 ND 0.45 06/18/12 09:14 1,3-Dichlorobenzene ug/m3 ND 1.2 06/18/12 09:14 1,4-Dichlorobenzene ug/m3 ND 1.2 06/18/12 09:14 2-Butanone (MEK)ug/m3 ND 0.60 06/18/12 09:14 2-Hexanone ug/m3 ND 0.83 06/18/12 09:14 2-Propanol ug/m3 ND 2.5 06/18/12 09:14 4-Ethyltoluene ug/m3 ND 1.0 06/18/12 09:14 4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 06/18/12 09:14 Acetone ug/m3 ND 0.48 06/18/12 09:14 Benzene ug/m3 ND 0.32 06/18/12 09:14 Benzyl chloride ug/m3 ND 1.0 06/18/12 09:14 Bromodichloromethane ug/m3 ND 1.4 06/18/12 09:14 Bromoform ug/m3 ND 2.1 06/18/12 09:14 Bromomethane ug/m3 ND 0.79 06/18/12 09:14 Carbon disulfide ug/m3 ND 0.63 06/18/12 09:14 Carbon tetrachloride ug/m3 ND 0.64 06/18/12 09:14 Chlorobenzene ug/m3 ND 0.94 06/18/12 09:14 Chloroethane ug/m3 ND 0.54 06/18/12 09:14 Chloroform ug/m3 ND 0.99 06/18/12 09:14 Chloromethane ug/m3 ND 0.42 06/18/12 09:14 cis-1,2-Dichloroethene ug/m3 ND 0.81 06/18/12 09:14 cis-1,3-Dichloropropene ug/m3 ND 0.92 06/18/12 09:14 Cyclohexane ug/m3 ND 0.68 06/18/12 09:14 Dibromochloromethane ug/m3 ND 1.7 06/18/12 09:14 Dichlorodifluoromethane ug/m3 ND 1.0 06/18/12 09:14 Dichlorotetrafluoroethane ug/m3 ND 1.4 06/18/12 09:14 Ethanol ug/m3 ND 0.38 06/18/12 09:14 Ethyl acetate ug/m3 ND 0.73 06/18/12 09:14 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 23 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 23 of 29 QUALITY CONTROL DATA Pace Project No.: Project: 10194400 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1219377 Associated Lab Samples:10194400001, 10194400002, 10194400003, 10194400004, 10194400005, 10194400006, 10194400007, 10194400008, 10194400009 Matrix:Air Analyzed Ethylbenzene ug/m3 ND 0.88 06/18/12 09:14 Hexachloro-1,3-butadiene ug/m3 ND 2.2 06/18/12 09:14 m&p-Xylene ug/m3 ND 1.8 06/18/12 09:14 Methyl-tert-butyl ether ug/m3 ND 0.73 06/18/12 09:14 Methylene Chloride ug/m3 ND 0.71 06/18/12 09:14 n-Heptane ug/m3 ND 0.83 06/18/12 09:14 n-Hexane ug/m3 ND 0.72 06/18/12 09:14 Naphthalene ug/m3 ND 1.1 06/18/12 09:14 o-Xylene ug/m3 ND 0.88 06/18/12 09:14 Propylene ug/m3 ND 0.35 06/18/12 09:14 Styrene ug/m3 ND 0.87 06/18/12 09:14 Tetrachloroethene ug/m3 ND 0.69 06/18/12 09:14 Tetrahydrofuran ug/m3 ND 0.60 06/18/12 09:14 Toluene ug/m3 ND 0.77 06/18/12 09:14 trans-1,2-Dichloroethene ug/m3 ND 0.81 06/18/12 09:14 trans-1,3-Dichloropropene ug/m3 ND 0.92 06/18/12 09:14 Trichloroethene ug/m3 ND 0.55 06/18/12 09:14 Trichlorofluoromethane ug/m3 ND 1.1 06/18/12 09:14 Vinyl acetate ug/m3 ND 0.71 06/18/12 09:14 Vinyl chloride ug/m3 ND 0.26 06/18/12 09:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1219378LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/m3 62.355.5 112 72-129 1,1,2,2-Tetrachloroethane ug/m3 65.169.8 93 73-131 1,1,2-Trichloroethane ug/m3 60.955.5 110 71-128 1,1,2-Trichlorotrifluoroethane ug/m3 78.277.9 100 65-132 1,1-Dichloroethane ug/m3 49.941.2 121 67-132 1,1-Dichloroethene ug/m3 49.240.3 122 68-134 1,2,4-Trichlorobenzene ug/m3 125 CH,L375.5 166 48-150 1,2,4-Trimethylbenzene ug/m3 53.850 108 72-127 1,2-Dibromoethane (EDB)ug/m3 82.378.1 105 75-130 1,2-Dichlorobenzene ug/m3 69.961.2 114 71-132 1,2-Dichloroethane ug/m3 46.741.2 113 70-131 1,2-Dichloropropane ug/m3 44.047 94 73-130 1,3,5-Trimethylbenzene ug/m3 46.050 92 70-133 1,3-Butadiene ug/m3 22.722.5 101 69-132 1,3-Dichlorobenzene ug/m3 54.561.2 89 71-128 1,4-Dichlorobenzene ug/m3 61.961.2 101 72-131 2-Butanone (MEK)ug/m3 49.7 CH,L13016669-131 2-Hexanone ug/m3 43.941.7 105 71-134 2-Propanol ug/m3 26.525 106 72-132 4-Ethyltoluene ug/m3 54.250 108 71-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 24 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 24 of 29 QUALITY CONTROL DATA Pace Project No.: Project: 10194400 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1219378LABORATORY CONTROL SAMPLE: LCSSpike 4-Methyl-2-pentanone (MIBK)ug/m3 45.541.7 109 69-135 Acetone ug/m3 19.324.2 80 61-139 Benzene ug/m3 30.332.5 93 69-134 Benzyl chloride ug/m3 52.952.5 101 70-129 Bromodichloromethane ug/m3 65.268.2 96 71-130 Bromoform ug/m3 111105 106 70-130 Bromomethane ug/m3 42.6 SS39.5 108 69-125 Carbon disulfide ug/m3 36.6 SS31.7 116 66-131 Carbon tetrachloride ug/m3 60.664 95 68-128 Chlorobenzene ug/m3 51.046.8 109 75-128 Chloroethane ug/m3 29.626.8 110 66-131 Chloroform ug/m3 54.749.7 110 68-132 Chloromethane ug/m3 20.421 97 60-139 cis-1,2-Dichloroethene ug/m3 44.240.3 110 73-130 cis-1,3-Dichloropropene ug/m3 50.246.2 109 74-134 Cyclohexane ug/m3 32.935 94 67-136 Dibromochloromethane ug/m3 91.986.6 106 69-131 Dichlorodifluoromethane ug/m3 56.350.3 112 67-131 Dichlorotetrafluoroethane ug/m3 68.071.1 96 66-130 Ethanol ug/m3 19.7 SS19.2 103 69-131 Ethyl acetate ug/m3 41.836.6 114 71-131 Ethylbenzene ug/m3 41.744.2 94 69-139 Hexachloro-1,3-butadiene ug/m3 161 CH10814941-150 m&p-Xylene ug/m3 82.988.3 94 66-137 Methyl-tert-butyl ether ug/m3 43.536.7 119 70-132 Methylene Chloride ug/m3 40.635.3 115 73-134 n-Heptane ug/m3 38.841.7 93 70-134 n-Hexane ug/m3 41.435.8 115 65-133 Naphthalene ug/m3 89.7 CH,L153.3 168 57-150 o-Xylene ug/m3 47.944.2 109 69-138 Propylene ug/m3 18.317.5 105 70-134 Styrene ug/m3 40.043.3 92 72-132 Tetrachloroethene ug/m3 72.069 104 70-130 Tetrahydrofuran ug/m3 31.830 106 74-128 Toluene ug/m3 36.538.3 95 71-132 trans-1,2-Dichloroethene ug/m3 45.540.3 113 72-128 trans-1,3-Dichloropropene ug/m3 48.846.2 106 73-130 Trichloroethene ug/m3 58.454.6 107 72-131 Trichlorofluoromethane ug/m3 55.557.1 97 66-129 Vinyl acetate ug/m3 43.235.8 121 71-131 Vinyl chloride ug/m3 26.726 103 70-131 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 25 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 25 of 29 QUALIFIERS Pace Project No.: Project: 10194400 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.CH Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results may be biased high.L1 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be considered an estimated value.SS REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 26 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 26 of 29 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 10194400 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 10194400001 AIR/15120ASGP1D:A060512 TO-15 10194400002 AIR/15120ASGP1S:A060512 TO-15 10194400003 AIR/15120ASGP2D:A060512 TO-15 10194400004 AIR/15120ASGP2S:A060512 TO-15 10194400005 AIR/15120ASGP3S:A060512 TO-15 10194400006 AIR/15120ASGP3D:A060512 TO-15 10194400007 AIR/15120ASGP4D:A060512 TO-15 10194400008 AIR/15120ASGP4S:A060512 TO-15 10194400009 AIR/15120ASGP3D:A060512A TO-15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/19/2012 07:28 PM Page 27 of 27 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 27 of 29 28 of 29 29 of 29 August 30, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 10202694 10202694 Project: Pace Project No.: RE: Doug Stuart Hull and Associates, Inc. 8470 Allison Pointe Boulevard Suite 120 Indianapolis, IN 46250 SBI068 Dear Doug Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Aaron Fredrikson aaron.fredrikson@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 1 of 36 CERTIFICATIONS Pace Project No.: Project: 10202694 SBI068 Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414A2LA Certification #: 2926.01 Alaska Certification #: UST-078Alaska Certification #MN00064Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680California Certification #: 01155CA EPA Region 8 Certification #: PaceFlorida/NELAP Certification #: E87605Georgia Certification #: 959Idaho Certification #: MN00064Illinois Certification #: 200011 Iowa Certification #: 368Kansas Certification #: E-10167Louisiana Certification #: 03086Louisiana Certification #: LA080009Maine Certification #: 2007029 Maryland Certification #: 322Michigan DEQ Certification #: 9909Minnesota Certification #: 027-053-137Mississippi Certification #: Pace Montana Certification #: MT CERT0092Nevada Certification #: MN_00064 Nebraska Certification #: PaceNew Jersey Certification #: MN-002New Mexico Certification #: PaceNew York Certification #: 11647North Carolina Certification #: 530 North Dakota Certification #: R-036North Dakota Certification #: R-036AOhio VAP Certification #: CL101Oklahoma Certification #: D9921Oklahoma Certification #: 9507 Oregon Certification #: MN200001Pennsylvania Certification #: 68-00563Puerto Rico CertificationTennessee Certification #: 02818Texas Certification #: T104704192 Virginia/DCLS Certification #: 002521Virginia/VELAP Certification #: 460163Washington Certification #: C754Wisconsin Certification #: 999407970 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 2 of 36 SAMPLE SUMMARY Pace Project No.: Project: 10202694 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 10202694001 ASGP8D:A081612 Air 08/16/12 16:23 08/17/12 09:35 10202694002 ASGP8S:A081612 Air 08/16/12 16:18 08/17/12 09:35 10202694003 ASGP7D:A081612 Air 08/16/12 16:42 08/17/12 09:35 10202694004 ASGP7S:A081612 Air 08/16/12 16:44 08/17/12 09:35 10202694005 ASGP6D:A081612 Air 08/16/12 16:55 08/17/12 09:35 10202694006 ASGP6S:A081612 Air 08/16/12 16:58 08/17/12 09:35 10202694007 ASGP5D:A081612 Air 08/16/12 17:15 08/17/12 09:35 10202694008 ASGP5S:A081612 Air 08/16/12 17:18 08/17/12 09:35 10202694009 ASGP6D:A081612A Air 08/16/12 17:02 08/17/12 09:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 3 of 36 SAMPLE ANALYTE COUNT Pace Project No.: Project: 10202694 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 10202694001 ASGP8D:A081612 TO-15 61DR1 10202694002 ASGP8S:A081612 TO-15 61DR1 10202694003 ASGP7D:A081612 TO-15 61DR1 10202694004 ASGP7S:A081612 TO-15 61DR1 10202694005 ASGP6D:A081612 TO-15 61DR1 10202694006 ASGP6S:A081612 TO-15 61DR1 10202694007 ASGP5D:A081612 TO-15 61DR1 10202694008 ASGP5S:A081612 TO-15 61DR1 10202694009 ASGP6D:A081612A TO-15 61DR1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 4 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP8D:A081612 Lab ID:10202694001 Collected:08/16/12 16:23 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 701 ug/m3 18 08/22/12 00:30 67-64-18.6 Benzene 6.4 ug/m3 18 08/22/12 00:30 71-43-25.8 Benzyl chloride ND ug/m3 18 08/22/12 00:30 100-44-718.9 Bromodichloromethane ND ug/m3 18 08/22/12 00:30 75-27-424.5 Bromoform ND ug/m3 18 08/22/12 00:30 75-25-237.8 Bromomethane ND ug/m3 18 08/22/12 00:30 74-83-914.2 1,3-Butadiene ND ug/m3 18 08/22/12 00:30 106-99-08.1 2-Butanone (MEK)44.5 ug/m3 18 08/22/12 00:30 78-93-310.8 Carbon disulfide 22.6 ug/m3 18 08/22/12 00:30 75-15-011.3 Carbon tetrachloride 12.9 ug/m3 18 08/22/12 00:30 56-23-511.5 Chlorobenzene ND ug/m3 18 08/22/12 00:30 108-90-716.9 Chloroethane ND ug/m3 18 08/22/12 00:30 75-00-39.7 Chloroform ND ug/m3 18 08/22/12 00:30 67-66-317.8 Chloromethane ND ug/m3 18 08/22/12 00:30 74-87-37.6 Cyclohexane ND ug/m3 18 08/22/12 00:30 110-82-712.6 Dibromochloromethane ND ug/m3 18 08/22/12 00:30 124-48-131.1 1,2-Dibromoethane (EDB)ND ug/m3 18 08/22/12 00:30 106-93-428.1 1,2-Dichlorobenzene ND ug/m3 18 08/22/12 00:30 95-50-122.0 1,3-Dichlorobenzene ND ug/m3 18 08/22/12 00:30 541-73-122.0 1,4-Dichlorobenzene ND ug/m3 18 08/22/12 00:30 106-46-722.0 Dichlorodifluoromethane ND ug/m3 18 08/22/12 00:30 75-71-818.2 1,1-Dichloroethane ND ug/m3 18 08/22/12 00:30 75-34-314.8 1,2-Dichloroethane ND ug/m3 18 08/22/12 00:30 107-06-27.4 1,1-Dichloroethene ND ug/m3 18 08/22/12 00:30 75-35-414.6 cis-1,2-Dichloroethene ND ug/m3 18 08/22/12 00:30 156-59-214.6 trans-1,2-Dichloroethene ND ug/m3 18 08/22/12 00:30 156-60-514.6 1,2-Dichloropropane ND ug/m3 18 08/22/12 00:30 78-87-516.9 cis-1,3-Dichloropropene ND ug/m3 18 08/22/12 00:30 10061-01-516.6 trans-1,3-Dichloropropene ND ug/m3 18 08/22/12 00:30 10061-02-616.6 Dichlorotetrafluoroethane ND ug/m3 18 08/22/12 00:30 76-14-225.6 Ethanol 316 ug/m3 18 08/22/12 00:30 64-17-56.8 Ethyl acetate ND ug/m3 18 08/22/12 00:30 141-78-613.1 Ethylbenzene 16.5 ug/m3 18 08/22/12 00:30 100-41-415.8 4-Ethyltoluene ND ug/m3 18 08/22/12 00:30 622-96-818.0 n-Heptane ND ug/m3 18 08/22/12 00:30 142-82-514.9 Hexachloro-1,3-butadiene ND ug/m3 18 08/22/12 00:30 87-68-339.6 n-Hexane 33.4 ug/m3 18 08/22/12 00:30 110-54-313.0 2-Hexanone ND ug/m3 18 08/22/12 00:30 591-78-614.9 Methylene Chloride ND ug/m3 18 08/22/12 00:30 75-09-212.8 4-Methyl-2-pentanone (MIBK)18.0 ug/m3 18 08/22/12 00:30 108-10-114.9 Methyl-tert-butyl ether ND ug/m3 18 08/22/12 00:30 1634-04-413.1 Naphthalene ND ug/m3 18 08/22/12 00:30 91-20-319.3 2-Propanol ND ug/m3 18 08/22/12 00:30 67-63-09.0 Propylene ND ug/m3 18 08/22/12 00:30 115-07-16.3 Styrene ND ug/m3 18 08/22/12 00:30 100-42-515.7 1,1,2,2-Tetrachloroethane ND ug/m3 18 08/22/12 00:30 79-34-512.6 Tetrachloroethene ND ug/m3 18 08/22/12 00:30 127-18-412.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 5 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 5 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP8D:A081612 Lab ID:10202694001 Collected:08/16/12 16:23 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 18 08/22/12 00:30 109-99-910.8 Toluene 1430 ug/m3 18 08/22/12 00:30 108-88-313.9 1,2,4-Trichlorobenzene ND ug/m3 18 08/22/12 00:30 120-82-127.2 1,1,1-Trichloroethane ND ug/m3 18 08/22/12 00:30 71-55-620.0 1,1,2-Trichloroethane ND ug/m3 18 08/22/12 00:30 79-00-59.9 Trichloroethene ND ug/m3 18 08/22/12 00:30 79-01-69.9 Trichlorofluoromethane ND ug/m3 18 08/22/12 00:30 75-69-420.5 1,1,2-Trichlorotrifluoroethane ND ug/m3 18 08/22/12 00:30 76-13-128.8 1,2,4-Trimethylbenzene 22.3 ug/m3 18 08/22/12 00:30 95-63-618.0 1,3,5-Trimethylbenzene ND ug/m3 18 08/22/12 00:30 108-67-818.0 Vinyl acetate ND ug/m3 18 08/22/12 00:30 108-05-412.9 Vinyl chloride ND ug/m3 18 08/22/12 00:30 75-01-44.7 m&p-Xylene 54.1 ug/m3 18 08/22/12 00:30 179601-23-131.7 o-Xylene ND ug/m3 18 08/22/12 00:30 95-47-615.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 6 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 6 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP8S:A081612 Lab ID:10202694002 Collected:08/16/12 16:18 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 759 ug/m3 18.7 08/21/12 23:33 67-64-19.0 Benzene ND ug/m3 18.7 08/21/12 23:33 71-43-26.1 Benzyl chloride ND ug/m3 18.7 08/21/12 23:33 100-44-719.6 Bromodichloromethane ND ug/m3 18.7 08/21/12 23:33 75-27-425.4 Bromoform ND ug/m3 18.7 08/21/12 23:33 75-25-239.3 Bromomethane ND ug/m3 18.7 08/21/12 23:33 74-83-914.8 1,3-Butadiene ND ug/m3 18.7 08/21/12 23:33 106-99-08.4 2-Butanone (MEK)66.2 ug/m3 18.7 08/21/12 23:33 78-93-311.2 Carbon disulfide 30.6 ug/m3 18.7 08/21/12 23:33 75-15-011.8 Carbon tetrachloride 63.7 ug/m3 18.7 08/21/12 23:33 56-23-512.0 Chlorobenzene ND ug/m3 18.7 08/21/12 23:33 108-90-717.6 Chloroethane ND ug/m3 18.7 08/21/12 23:33 75-00-310.1 Chloroform ND ug/m3 18.7 08/21/12 23:33 67-66-318.5 Chloromethane ND ug/m3 18.7 08/21/12 23:33 74-87-37.9 Cyclohexane ND ug/m3 18.7 08/21/12 23:33 110-82-713.1 Dibromochloromethane ND ug/m3 18.7 08/21/12 23:33 124-48-132.4 1,2-Dibromoethane (EDB)ND ug/m3 18.7 08/21/12 23:33 106-93-429.2 1,2-Dichlorobenzene ND ug/m3 18.7 08/21/12 23:33 95-50-122.8 1,3-Dichlorobenzene ND ug/m3 18.7 08/21/12 23:33 541-73-122.8 1,4-Dichlorobenzene ND ug/m3 18.7 08/21/12 23:33 106-46-722.8 Dichlorodifluoromethane ND ug/m3 18.7 08/21/12 23:33 75-71-818.9 1,1-Dichloroethane ND ug/m3 18.7 08/21/12 23:33 75-34-315.3 1,2-Dichloroethane ND ug/m3 18.7 08/21/12 23:33 107-06-27.7 1,1-Dichloroethene ND ug/m3 18.7 08/21/12 23:33 75-35-415.1 cis-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 23:33 156-59-215.1 trans-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 23:33 156-60-515.1 1,2-Dichloropropane ND ug/m3 18.7 08/21/12 23:33 78-87-517.6 cis-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 23:33 10061-01-517.2 trans-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 23:33 10061-02-617.2 Dichlorotetrafluoroethane ND ug/m3 18.7 08/21/12 23:33 76-14-226.6 Ethanol 300 ug/m3 18.7 08/21/12 23:33 64-17-57.1 Ethyl acetate ND ug/m3 18.7 08/21/12 23:33 141-78-613.7 Ethylbenzene ND ug/m3 18.7 08/21/12 23:33 100-41-416.5 4-Ethyltoluene ND ug/m3 18.7 08/21/12 23:33 622-96-818.7 n-Heptane ND ug/m3 18.7 08/21/12 23:33 142-82-515.5 Hexachloro-1,3-butadiene ND ug/m3 18.7 08/21/12 23:33 87-68-341.1 n-Hexane 45.7 ug/m3 18.7 08/21/12 23:33 110-54-313.5 2-Hexanone ND ug/m3 18.7 08/21/12 23:33 591-78-615.5 Methylene Chloride ND ug/m3 18.7 08/21/12 23:33 75-09-213.3 4-Methyl-2-pentanone (MIBK)ND ug/m3 18.7 08/21/12 23:33 108-10-115.5 Methyl-tert-butyl ether ND ug/m3 18.7 08/21/12 23:33 1634-04-413.7 Naphthalene ND ug/m3 18.7 08/21/12 23:33 91-20-320.0 2-Propanol 20.8 ug/m3 18.7 08/21/12 23:33 67-63-09.4 Propylene ND ug/m3 18.7 08/21/12 23:33 115-07-16.5 Styrene ND ug/m3 18.7 08/21/12 23:33 100-42-516.3 1,1,2,2-Tetrachloroethane ND ug/m3 18.7 08/21/12 23:33 79-34-513.1 Tetrachloroethene ND ug/m3 18.7 08/21/12 23:33 127-18-412.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 7 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 7 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP8S:A081612 Lab ID:10202694002 Collected:08/16/12 16:18 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 18.7 08/21/12 23:33 109-99-911.2 Toluene 2310 ug/m3 18.7 08/21/12 23:33 108-88-314.4 1,2,4-Trichlorobenzene ND ug/m3 18.7 08/21/12 23:33 120-82-128.2 1,1,1-Trichloroethane ND ug/m3 18.7 08/21/12 23:33 71-55-620.8 1,1,2-Trichloroethane ND ug/m3 18.7 08/21/12 23:33 79-00-510.3 Trichloroethene ND ug/m3 18.7 08/21/12 23:33 79-01-610.3 Trichlorofluoromethane ND ug/m3 18.7 08/21/12 23:33 75-69-421.3 1,1,2-Trichlorotrifluoroethane ND ug/m3 18.7 08/21/12 23:33 76-13-129.9 1,2,4-Trimethylbenzene ND ug/m3 18.7 08/21/12 23:33 95-63-618.7 1,3,5-Trimethylbenzene ND ug/m3 18.7 08/21/12 23:33 108-67-818.7 Vinyl acetate ND ug/m3 18.7 08/21/12 23:33 108-05-413.4 Vinyl chloride ND ug/m3 18.7 08/21/12 23:33 75-01-44.9 m&p-Xylene 44.3 ug/m3 18.7 08/21/12 23:33 179601-23-132.9 o-Xylene 18.1 ug/m3 18.7 08/21/12 23:33 95-47-616.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 8 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 8 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP7D:A081612 Lab ID:10202694003 Collected:08/16/12 16:42 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 129 ug/m3 19.4 08/21/12 23:04 67-64-19.3 Benzene ND ug/m3 19.4 08/21/12 23:04 71-43-26.3 Benzyl chloride ND ug/m3 19.4 08/21/12 23:04 100-44-720.4 Bromodichloromethane ND ug/m3 19.4 08/21/12 23:04 75-27-426.4 Bromoform ND ug/m3 19.4 08/21/12 23:04 75-25-240.7 Bromomethane ND ug/m3 19.4 08/21/12 23:04 74-83-915.3 1,3-Butadiene ND ug/m3 19.4 08/21/12 23:04 106-99-08.7 2-Butanone (MEK)22.9 ug/m3 19.4 08/21/12 23:04 78-93-311.6 Carbon disulfide ND ug/m3 19.4 08/21/12 23:04 75-15-012.2 Carbon tetrachloride ND ug/m3 19.4 08/21/12 23:04 56-23-512.4 Chlorobenzene ND ug/m3 19.4 08/21/12 23:04 108-90-718.2 Chloroethane ND ug/m3 19.4 08/21/12 23:04 75-00-310.5 Chloroform ND ug/m3 19.4 08/21/12 23:04 67-66-319.2 Chloromethane ND ug/m3 19.4 08/21/12 23:04 74-87-38.1 Cyclohexane ND ug/m3 19.4 08/21/12 23:04 110-82-713.6 Dibromochloromethane ND ug/m3 19.4 08/21/12 23:04 124-48-133.6 1,2-Dibromoethane (EDB)ND ug/m3 19.4 08/21/12 23:04 106-93-430.3 1,2-Dichlorobenzene ND ug/m3 19.4 08/21/12 23:04 95-50-123.7 1,3-Dichlorobenzene ND ug/m3 19.4 08/21/12 23:04 541-73-123.7 1,4-Dichlorobenzene ND ug/m3 19.4 08/21/12 23:04 106-46-723.7 Dichlorodifluoromethane ND ug/m3 19.4 08/21/12 23:04 75-71-819.6 1,1-Dichloroethane ND ug/m3 19.4 08/21/12 23:04 75-34-315.9 1,2-Dichloroethane ND ug/m3 19.4 08/21/12 23:04 107-06-28.0 1,1-Dichloroethene ND ug/m3 19.4 08/21/12 23:04 75-35-415.7 cis-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 23:04 156-59-215.7 trans-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 23:04 156-60-515.7 1,2-Dichloropropane ND ug/m3 19.4 08/21/12 23:04 78-87-518.2 cis-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 23:04 10061-01-517.8 trans-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 23:04 10061-02-617.8 Dichlorotetrafluoroethane ND ug/m3 19.4 08/21/12 23:04 76-14-227.5 Ethanol 165 ug/m3 19.4 08/21/12 23:04 64-17-57.4 Ethyl acetate ND ug/m3 19.4 08/21/12 23:04 141-78-614.2 Ethylbenzene ND ug/m3 19.4 08/21/12 23:04 100-41-417.1 4-Ethyltoluene ND ug/m3 19.4 08/21/12 23:04 622-96-819.4 n-Heptane ND ug/m3 19.4 08/21/12 23:04 142-82-516.1 Hexachloro-1,3-butadiene ND ug/m3 19.4 08/21/12 23:04 87-68-342.7 n-Hexane ND ug/m3 19.4 08/21/12 23:04 110-54-314.0 2-Hexanone ND ug/m3 19.4 08/21/12 23:04 591-78-616.1 Methylene Chloride ND ug/m3 19.4 08/21/12 23:04 75-09-213.8 4-Methyl-2-pentanone (MIBK)ND ug/m3 19.4 08/21/12 23:04 108-10-116.1 Methyl-tert-butyl ether ND ug/m3 19.4 08/21/12 23:04 1634-04-414.2 Naphthalene ND ug/m3 19.4 08/21/12 23:04 91-20-320.8 2-Propanol 17.4 ug/m3 19.4 08/21/12 23:04 67-63-09.7 Propylene ND ug/m3 19.4 08/21/12 23:04 115-07-16.8 Styrene ND ug/m3 19.4 08/21/12 23:04 100-42-516.9 1,1,2,2-Tetrachloroethane ND ug/m3 19.4 08/21/12 23:04 79-34-513.5 Tetrachloroethene 14.7 ug/m3 19.4 08/21/12 23:04 127-18-413.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 9 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 9 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP7D:A081612 Lab ID:10202694003 Collected:08/16/12 16:42 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 19.4 08/21/12 23:04 109-99-911.6 Toluene 437 ug/m3 19.4 08/21/12 23:04 108-88-314.9 1,2,4-Trichlorobenzene ND ug/m3 19.4 08/21/12 23:04 120-82-129.3 1,1,1-Trichloroethane ND ug/m3 19.4 08/21/12 23:04 71-55-621.5 1,1,2-Trichloroethane ND ug/m3 19.4 08/21/12 23:04 79-00-510.7 Trichloroethene ND ug/m3 19.4 08/21/12 23:04 79-01-610.7 Trichlorofluoromethane ND ug/m3 19.4 08/21/12 23:04 75-69-422.1 1,1,2-Trichlorotrifluoroethane ND ug/m3 19.4 08/21/12 23:04 76-13-131.0 1,2,4-Trimethylbenzene ND ug/m3 19.4 08/21/12 23:04 95-63-619.4 1,3,5-Trimethylbenzene ND ug/m3 19.4 08/21/12 23:04 108-67-819.4 Vinyl acetate ND ug/m3 19.4 08/21/12 23:04 108-05-413.9 Vinyl chloride ND ug/m3 19.4 08/21/12 23:04 75-01-45.0 m&p-Xylene ND ug/m3 19.4 08/21/12 23:04 179601-23-134.1 o-Xylene ND ug/m3 19.4 08/21/12 23:04 95-47-617.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 10 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 10 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP7S:A081612 Lab ID:10202694004 Collected:08/16/12 16:44 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 228 ug/m3 18.7 08/21/12 22:35 67-64-19.0 Benzene ND ug/m3 18.7 08/21/12 22:35 71-43-26.1 Benzyl chloride ND ug/m3 18.7 08/21/12 22:35 100-44-719.6 Bromodichloromethane ND ug/m3 18.7 08/21/12 22:35 75-27-425.4 Bromoform ND ug/m3 18.7 08/21/12 22:35 75-25-239.3 Bromomethane ND ug/m3 18.7 08/21/12 22:35 74-83-914.8 1,3-Butadiene ND ug/m3 18.7 08/21/12 22:35 106-99-08.4 2-Butanone (MEK)28.9 ug/m3 18.7 08/21/12 22:35 78-93-311.2 Carbon disulfide ND ug/m3 18.7 08/21/12 22:35 75-15-011.8 Carbon tetrachloride ND ug/m3 18.7 08/21/12 22:35 56-23-512.0 Chlorobenzene ND ug/m3 18.7 08/21/12 22:35 108-90-717.6 Chloroethane ND ug/m3 18.7 08/21/12 22:35 75-00-310.1 Chloroform ND ug/m3 18.7 08/21/12 22:35 67-66-318.5 Chloromethane ND ug/m3 18.7 08/21/12 22:35 74-87-37.9 Cyclohexane ND ug/m3 18.7 08/21/12 22:35 110-82-713.1 Dibromochloromethane ND ug/m3 18.7 08/21/12 22:35 124-48-132.4 1,2-Dibromoethane (EDB)ND ug/m3 18.7 08/21/12 22:35 106-93-429.2 1,2-Dichlorobenzene ND ug/m3 18.7 08/21/12 22:35 95-50-122.8 1,3-Dichlorobenzene ND ug/m3 18.7 08/21/12 22:35 541-73-122.8 1,4-Dichlorobenzene ND ug/m3 18.7 08/21/12 22:35 106-46-722.8 Dichlorodifluoromethane ND ug/m3 18.7 08/21/12 22:35 75-71-818.9 1,1-Dichloroethane ND ug/m3 18.7 08/21/12 22:35 75-34-315.3 1,2-Dichloroethane ND ug/m3 18.7 08/21/12 22:35 107-06-27.7 1,1-Dichloroethene ND ug/m3 18.7 08/21/12 22:35 75-35-415.1 cis-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 22:35 156-59-215.1 trans-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 22:35 156-60-515.1 1,2-Dichloropropane ND ug/m3 18.7 08/21/12 22:35 78-87-517.6 cis-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 22:35 10061-01-517.2 trans-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 22:35 10061-02-617.2 Dichlorotetrafluoroethane ND ug/m3 18.7 08/21/12 22:35 76-14-226.6 Ethanol 73.3 ug/m3 18.7 08/21/12 22:35 64-17-57.1 Ethyl acetate ND ug/m3 18.7 08/21/12 22:35 141-78-613.7 Ethylbenzene ND ug/m3 18.7 08/21/12 22:35 100-41-416.5 4-Ethyltoluene ND ug/m3 18.7 08/21/12 22:35 622-96-818.7 n-Heptane ND ug/m3 18.7 08/21/12 22:35 142-82-515.5 Hexachloro-1,3-butadiene ND ug/m3 18.7 08/21/12 22:35 87-68-341.1 n-Hexane ND ug/m3 18.7 08/21/12 22:35 110-54-313.5 2-Hexanone ND ug/m3 18.7 08/21/12 22:35 591-78-615.5 Methylene Chloride ND ug/m3 18.7 08/21/12 22:35 75-09-213.3 4-Methyl-2-pentanone (MIBK)ND ug/m3 18.7 08/21/12 22:35 108-10-115.5 Methyl-tert-butyl ether ND ug/m3 18.7 08/21/12 22:35 1634-04-413.7 Naphthalene ND ug/m3 18.7 08/21/12 22:35 91-20-320.0 2-Propanol ND ug/m3 18.7 08/21/12 22:35 67-63-09.4 Propylene ND ug/m3 18.7 08/21/12 22:35 115-07-16.5 Styrene ND ug/m3 18.7 08/21/12 22:35 100-42-516.3 1,1,2,2-Tetrachloroethane ND ug/m3 18.7 08/21/12 22:35 79-34-513.1 Tetrachloroethene 25.2 ug/m3 18.7 08/21/12 22:35 127-18-412.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 11 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 11 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP7S:A081612 Lab ID:10202694004 Collected:08/16/12 16:44 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 18.7 08/21/12 22:35 109-99-911.2 Toluene 756 ug/m3 18.7 08/21/12 22:35 108-88-314.4 1,2,4-Trichlorobenzene ND ug/m3 18.7 08/21/12 22:35 120-82-128.2 1,1,1-Trichloroethane ND ug/m3 18.7 08/21/12 22:35 71-55-620.8 1,1,2-Trichloroethane ND ug/m3 18.7 08/21/12 22:35 79-00-510.3 Trichloroethene ND ug/m3 18.7 08/21/12 22:35 79-01-610.3 Trichlorofluoromethane ND ug/m3 18.7 08/21/12 22:35 75-69-421.3 1,1,2-Trichlorotrifluoroethane ND ug/m3 18.7 08/21/12 22:35 76-13-129.9 1,2,4-Trimethylbenzene 19.1 ug/m3 18.7 08/21/12 22:35 95-63-618.7 1,3,5-Trimethylbenzene ND ug/m3 18.7 08/21/12 22:35 108-67-818.7 Vinyl acetate ND ug/m3 18.7 08/21/12 22:35 108-05-413.4 Vinyl chloride ND ug/m3 18.7 08/21/12 22:35 75-01-44.9 m&p-Xylene 43.0 ug/m3 18.7 08/21/12 22:35 179601-23-132.9 o-Xylene 17.7 ug/m3 18.7 08/21/12 22:35 95-47-616.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 12 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 12 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6D:A081612 Lab ID:10202694005 Collected:08/16/12 16:55 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 429 ug/m3 19.4 08/21/12 22:06 67-64-19.3 Benzene ND ug/m3 19.4 08/21/12 22:06 71-43-26.3 Benzyl chloride ND ug/m3 19.4 08/21/12 22:06 100-44-720.4 Bromodichloromethane ND ug/m3 19.4 08/21/12 22:06 75-27-426.4 Bromoform ND ug/m3 19.4 08/21/12 22:06 75-25-240.7 Bromomethane ND ug/m3 19.4 08/21/12 22:06 74-83-915.3 1,3-Butadiene ND ug/m3 19.4 08/21/12 22:06 106-99-08.7 2-Butanone (MEK)32.4 ug/m3 19.4 08/21/12 22:06 78-93-311.6 Carbon disulfide 18.3 ug/m3 19.4 08/21/12 22:06 75-15-012.2 Carbon tetrachloride ND ug/m3 19.4 08/21/12 22:06 56-23-512.4 Chlorobenzene ND ug/m3 19.4 08/21/12 22:06 108-90-718.2 Chloroethane ND ug/m3 19.4 08/21/12 22:06 75-00-310.5 Chloroform ND ug/m3 19.4 08/21/12 22:06 67-66-319.2 Chloromethane ND ug/m3 19.4 08/21/12 22:06 74-87-38.1 Cyclohexane ND ug/m3 19.4 08/21/12 22:06 110-82-713.6 Dibromochloromethane ND ug/m3 19.4 08/21/12 22:06 124-48-133.6 1,2-Dibromoethane (EDB)ND ug/m3 19.4 08/21/12 22:06 106-93-430.3 1,2-Dichlorobenzene ND ug/m3 19.4 08/21/12 22:06 95-50-123.7 1,3-Dichlorobenzene ND ug/m3 19.4 08/21/12 22:06 541-73-123.7 1,4-Dichlorobenzene ND ug/m3 19.4 08/21/12 22:06 106-46-723.7 Dichlorodifluoromethane ND ug/m3 19.4 08/21/12 22:06 75-71-819.6 1,1-Dichloroethane ND ug/m3 19.4 08/21/12 22:06 75-34-315.9 1,2-Dichloroethane ND ug/m3 19.4 08/21/12 22:06 107-06-28.0 1,1-Dichloroethene ND ug/m3 19.4 08/21/12 22:06 75-35-415.7 cis-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 22:06 156-59-215.7 trans-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 22:06 156-60-515.7 1,2-Dichloropropane ND ug/m3 19.4 08/21/12 22:06 78-87-518.2 cis-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 22:06 10061-01-517.8 trans-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 22:06 10061-02-617.8 Dichlorotetrafluoroethane ND ug/m3 19.4 08/21/12 22:06 76-14-227.5 Ethanol 187 ug/m3 19.4 08/21/12 22:06 64-17-57.4 Ethyl acetate ND ug/m3 19.4 08/21/12 22:06 141-78-614.2 Ethylbenzene ND ug/m3 19.4 08/21/12 22:06 100-41-417.1 4-Ethyltoluene ND ug/m3 19.4 08/21/12 22:06 622-96-819.4 n-Heptane ND ug/m3 19.4 08/21/12 22:06 142-82-516.1 Hexachloro-1,3-butadiene ND ug/m3 19.4 08/21/12 22:06 87-68-342.7 n-Hexane 16.2 ug/m3 19.4 08/21/12 22:06 110-54-314.0 2-Hexanone ND ug/m3 19.4 08/21/12 22:06 591-78-616.1 Methylene Chloride ND ug/m3 19.4 08/21/12 22:06 75-09-213.8 4-Methyl-2-pentanone (MIBK)ND ug/m3 19.4 08/21/12 22:06 108-10-116.1 Methyl-tert-butyl ether ND ug/m3 19.4 08/21/12 22:06 1634-04-414.2 Naphthalene ND ug/m3 19.4 08/21/12 22:06 91-20-320.8 2-Propanol 12.6 ug/m3 19.4 08/21/12 22:06 67-63-09.7 Propylene ND ug/m3 19.4 08/21/12 22:06 115-07-16.8 Styrene ND ug/m3 19.4 08/21/12 22:06 100-42-516.9 1,1,2,2-Tetrachloroethane ND ug/m3 19.4 08/21/12 22:06 79-34-513.5 Tetrachloroethene 14.6 ug/m3 19.4 08/21/12 22:06 127-18-413.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 13 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 13 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6D:A081612 Lab ID:10202694005 Collected:08/16/12 16:55 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 19.4 08/21/12 22:06 109-99-911.6 Toluene 827 ug/m3 19.4 08/21/12 22:06 108-88-314.9 1,2,4-Trichlorobenzene ND ug/m3 19.4 08/21/12 22:06 120-82-129.3 1,1,1-Trichloroethane ND ug/m3 19.4 08/21/12 22:06 71-55-621.5 1,1,2-Trichloroethane ND ug/m3 19.4 08/21/12 22:06 79-00-510.7 Trichloroethene ND ug/m3 19.4 08/21/12 22:06 79-01-610.7 Trichlorofluoromethane ND ug/m3 19.4 08/21/12 22:06 75-69-422.1 1,1,2-Trichlorotrifluoroethane ND ug/m3 19.4 08/21/12 22:06 76-13-131.0 1,2,4-Trimethylbenzene ND ug/m3 19.4 08/21/12 22:06 95-63-619.4 1,3,5-Trimethylbenzene ND ug/m3 19.4 08/21/12 22:06 108-67-819.4 Vinyl acetate ND ug/m3 19.4 08/21/12 22:06 108-05-413.9 Vinyl chloride ND ug/m3 19.4 08/21/12 22:06 75-01-45.0 m&p-Xylene ND ug/m3 19.4 08/21/12 22:06 179601-23-134.1 o-Xylene ND ug/m3 19.4 08/21/12 22:06 95-47-617.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 14 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 14 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6S:A081612 Lab ID:10202694006 Collected:08/16/12 16:58 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 407 ug/m3 18.7 08/21/12 21:38 67-64-19.0 Benzene ND ug/m3 18.7 08/21/12 21:38 71-43-26.1 Benzyl chloride ND ug/m3 18.7 08/21/12 21:38 100-44-719.6 Bromodichloromethane ND ug/m3 18.7 08/21/12 21:38 75-27-425.4 Bromoform ND ug/m3 18.7 08/21/12 21:38 75-25-239.3 Bromomethane ND ug/m3 18.7 08/21/12 21:38 74-83-914.8 1,3-Butadiene ND ug/m3 18.7 08/21/12 21:38 106-99-08.4 2-Butanone (MEK)17.7 ug/m3 18.7 08/21/12 21:38 78-93-311.2 Carbon disulfide 26.8 ug/m3 18.7 08/21/12 21:38 75-15-011.8 Carbon tetrachloride ND ug/m3 18.7 08/21/12 21:38 56-23-512.0 Chlorobenzene ND ug/m3 18.7 08/21/12 21:38 108-90-717.6 Chloroethane ND ug/m3 18.7 08/21/12 21:38 75-00-310.1 Chloroform ND ug/m3 18.7 08/21/12 21:38 67-66-318.5 Chloromethane ND ug/m3 18.7 08/21/12 21:38 74-87-37.9 Cyclohexane ND ug/m3 18.7 08/21/12 21:38 110-82-713.1 Dibromochloromethane ND ug/m3 18.7 08/21/12 21:38 124-48-132.4 1,2-Dibromoethane (EDB)ND ug/m3 18.7 08/21/12 21:38 106-93-429.2 1,2-Dichlorobenzene ND ug/m3 18.7 08/21/12 21:38 95-50-122.8 1,3-Dichlorobenzene ND ug/m3 18.7 08/21/12 21:38 541-73-122.8 1,4-Dichlorobenzene ND ug/m3 18.7 08/21/12 21:38 106-46-722.8 Dichlorodifluoromethane ND ug/m3 18.7 08/21/12 21:38 75-71-818.9 1,1-Dichloroethane ND ug/m3 18.7 08/21/12 21:38 75-34-315.3 1,2-Dichloroethane ND ug/m3 18.7 08/21/12 21:38 107-06-27.7 1,1-Dichloroethene ND ug/m3 18.7 08/21/12 21:38 75-35-415.1 cis-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 21:38 156-59-215.1 trans-1,2-Dichloroethene ND ug/m3 18.7 08/21/12 21:38 156-60-515.1 1,2-Dichloropropane ND ug/m3 18.7 08/21/12 21:38 78-87-517.6 cis-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 21:38 10061-01-517.2 trans-1,3-Dichloropropene ND ug/m3 18.7 08/21/12 21:38 10061-02-617.2 Dichlorotetrafluoroethane ND ug/m3 18.7 08/21/12 21:38 76-14-226.6 Ethanol 90.8 ug/m3 18.7 08/21/12 21:38 64-17-57.1 Ethyl acetate ND ug/m3 18.7 08/21/12 21:38 141-78-613.7 Ethylbenzene ND ug/m3 18.7 08/21/12 21:38 100-41-416.5 4-Ethyltoluene ND ug/m3 18.7 08/21/12 21:38 622-96-818.7 n-Heptane ND ug/m3 18.7 08/21/12 21:38 142-82-515.5 Hexachloro-1,3-butadiene ND ug/m3 18.7 08/21/12 21:38 87-68-341.1 n-Hexane 20.3 ug/m3 18.7 08/21/12 21:38 110-54-313.5 2-Hexanone ND ug/m3 18.7 08/21/12 21:38 591-78-615.5 Methylene Chloride ND ug/m3 18.7 08/21/12 21:38 75-09-213.3 4-Methyl-2-pentanone (MIBK)ND ug/m3 18.7 08/21/12 21:38 108-10-115.5 Methyl-tert-butyl ether ND ug/m3 18.7 08/21/12 21:38 1634-04-413.7 Naphthalene ND ug/m3 18.7 08/21/12 21:38 91-20-320.0 2-Propanol ND ug/m3 18.7 08/21/12 21:38 67-63-09.4 Propylene ND ug/m3 18.7 08/21/12 21:38 115-07-16.5 Styrene ND ug/m3 18.7 08/21/12 21:38 100-42-516.3 1,1,2,2-Tetrachloroethane ND ug/m3 18.7 08/21/12 21:38 79-34-513.1 Tetrachloroethene 60.0 ug/m3 18.7 08/21/12 21:38 127-18-412.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 15 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 15 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6S:A081612 Lab ID:10202694006 Collected:08/16/12 16:58 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 18.7 08/21/12 21:38 109-99-911.2 Toluene 688 ug/m3 18.7 08/21/12 21:38 108-88-314.4 1,2,4-Trichlorobenzene ND ug/m3 18.7 08/21/12 21:38 120-82-128.2 1,1,1-Trichloroethane ND ug/m3 18.7 08/21/12 21:38 71-55-620.8 1,1,2-Trichloroethane ND ug/m3 18.7 08/21/12 21:38 79-00-510.3 Trichloroethene ND ug/m3 18.7 08/21/12 21:38 79-01-610.3 Trichlorofluoromethane ND ug/m3 18.7 08/21/12 21:38 75-69-421.3 1,1,2-Trichlorotrifluoroethane ND ug/m3 18.7 08/21/12 21:38 76-13-129.9 1,2,4-Trimethylbenzene 35.8 ug/m3 18.7 08/21/12 21:38 95-63-618.7 1,3,5-Trimethylbenzene ND ug/m3 18.7 08/21/12 21:38 108-67-818.7 Vinyl acetate ND ug/m3 18.7 08/21/12 21:38 108-05-413.4 Vinyl chloride ND ug/m3 18.7 08/21/12 21:38 75-01-44.9 m&p-Xylene 41.5 ug/m3 18.7 08/21/12 21:38 179601-23-132.9 o-Xylene 19.5 ug/m3 18.7 08/21/12 21:38 95-47-616.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 16 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 16 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP5D:A081612 Lab ID:10202694007 Collected:08/16/12 17:15 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 174 ug/m3 20.2 08/22/12 00:02 67-64-19.7 Benzene ND ug/m3 20.2 08/22/12 00:02 71-43-26.6 Benzyl chloride ND ug/m3 20.2 08/22/12 00:02 100-44-721.2 Bromodichloromethane ND ug/m3 20.2 08/22/12 00:02 75-27-427.5 Bromoform ND ug/m3 20.2 08/22/12 00:02 75-25-242.4 Bromomethane ND ug/m3 20.2 08/22/12 00:02 74-83-916.0 1,3-Butadiene ND ug/m3 20.2 08/22/12 00:02 106-99-09.1 2-Butanone (MEK)27.0 ug/m3 20.2 08/22/12 00:02 78-93-312.1 Carbon disulfide 21.0 ug/m3 20.2 08/22/12 00:02 75-15-012.7 Carbon tetrachloride 13.0 ug/m3 20.2 08/22/12 00:02 56-23-512.9 Chlorobenzene ND ug/m3 20.2 08/22/12 00:02 108-90-719.0 Chloroethane ND ug/m3 20.2 08/22/12 00:02 75-00-310.9 Chloroform ND ug/m3 20.2 08/22/12 00:02 67-66-320.0 Chloromethane 26.5 ug/m3 20.2 08/22/12 00:02 74-87-38.5 Cyclohexane ND ug/m3 20.2 08/22/12 00:02 110-82-714.1 Dibromochloromethane ND ug/m3 20.2 08/22/12 00:02 124-48-134.9 1,2-Dibromoethane (EDB)ND ug/m3 20.2 08/22/12 00:02 106-93-431.5 1,2-Dichlorobenzene ND ug/m3 20.2 08/22/12 00:02 95-50-124.6 1,3-Dichlorobenzene ND ug/m3 20.2 08/22/12 00:02 541-73-124.6 1,4-Dichlorobenzene ND ug/m3 20.2 08/22/12 00:02 106-46-724.6 Dichlorodifluoromethane ND ug/m3 20.2 08/22/12 00:02 75-71-820.4 1,1-Dichloroethane ND ug/m3 20.2 08/22/12 00:02 75-34-316.6 1,2-Dichloroethane ND ug/m3 20.2 08/22/12 00:02 107-06-28.3 1,1-Dichloroethene ND ug/m3 20.2 08/22/12 00:02 75-35-416.4 cis-1,2-Dichloroethene ND ug/m3 20.2 08/22/12 00:02 156-59-216.4 trans-1,2-Dichloroethene ND ug/m3 20.2 08/22/12 00:02 156-60-516.4 1,2-Dichloropropane ND ug/m3 20.2 08/22/12 00:02 78-87-519.0 cis-1,3-Dichloropropene ND ug/m3 20.2 08/22/12 00:02 10061-01-518.6 trans-1,3-Dichloropropene ND ug/m3 20.2 08/22/12 00:02 10061-02-618.6 Dichlorotetrafluoroethane ND ug/m3 20.2 08/22/12 00:02 76-14-228.7 Ethanol 72.1 ug/m3 20.2 08/22/12 00:02 64-17-57.7 Ethyl acetate ND ug/m3 20.2 08/22/12 00:02 141-78-614.7 Ethylbenzene ND ug/m3 20.2 08/22/12 00:02 100-41-417.8 4-Ethyltoluene 29.6 ug/m3 20.2 08/22/12 00:02 622-96-820.2 n-Heptane ND ug/m3 20.2 08/22/12 00:02 142-82-516.8 Hexachloro-1,3-butadiene ND ug/m3 20.2 08/22/12 00:02 87-68-344.4 n-Hexane ND ug/m3 20.2 08/22/12 00:02 110-54-314.5 2-Hexanone ND ug/m3 20.2 08/22/12 00:02 591-78-616.8 Methylene Chloride ND ug/m3 20.2 08/22/12 00:02 75-09-214.3 4-Methyl-2-pentanone (MIBK)ND ug/m3 20.2 08/22/12 00:02 108-10-116.8 Methyl-tert-butyl ether ND ug/m3 20.2 08/22/12 00:02 1634-04-414.7 Naphthalene 66.6 ug/m3 20.2 08/22/12 00:02 91-20-321.6 2-Propanol ND ug/m3 20.2 08/22/12 00:02 67-63-010.1 Propylene ND ug/m3 20.2 08/22/12 00:02 115-07-17.1 Styrene ND ug/m3 20.2 08/22/12 00:02 100-42-517.6 1,1,2,2-Tetrachloroethane ND ug/m3 20.2 08/22/12 00:02 79-34-514.1 Tetrachloroethene 26.8 ug/m3 20.2 08/22/12 00:02 127-18-413.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 17 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 17 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP5D:A081612 Lab ID:10202694007 Collected:08/16/12 17:15 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 20.2 08/22/12 00:02 109-99-912.1 Toluene 287 ug/m3 20.2 08/22/12 00:02 108-88-315.6 1,2,4-Trichlorobenzene ND ug/m3 20.2 08/22/12 00:02 120-82-130.5 1,1,1-Trichloroethane ND ug/m3 20.2 08/22/12 00:02 71-55-622.4 1,1,2-Trichloroethane ND ug/m3 20.2 08/22/12 00:02 79-00-511.1 Trichloroethene ND ug/m3 20.2 08/22/12 00:02 79-01-611.1 Trichlorofluoromethane ND ug/m3 20.2 08/22/12 00:02 75-69-423.0 1,1,2-Trichlorotrifluoroethane ND ug/m3 20.2 08/22/12 00:02 76-13-132.3 1,2,4-Trimethylbenzene 67.3 ug/m3 20.2 08/22/12 00:02 95-63-620.2 1,3,5-Trimethylbenzene ND ug/m3 20.2 08/22/12 00:02 108-67-820.2 Vinyl acetate ND ug/m3 20.2 08/22/12 00:02 108-05-414.5 Vinyl chloride ND ug/m3 20.2 08/22/12 00:02 75-01-45.3 m&p-Xylene 56.6 ug/m3 20.2 08/22/12 00:02 179601-23-135.6 o-Xylene 25.6 ug/m3 20.2 08/22/12 00:02 95-47-617.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 18 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 18 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP5S:A081612 Lab ID:10202694008 Collected:08/16/12 17:18 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 285 ug/m3 1.94 08/22/12 12:05 67-64-1 E0.93 Benzene 4.4 ug/m3 1.94 08/22/12 12:05 71-43-20.63 Benzyl chloride ND ug/m3 1.94 08/22/12 12:05 100-44-72.0 Bromodichloromethane ND ug/m3 1.94 08/22/12 12:05 75-27-42.6 Bromoform ND ug/m3 1.94 08/22/12 12:05 75-25-24.1 Bromomethane ND ug/m3 1.94 08/22/12 12:05 74-83-91.5 1,3-Butadiene ND ug/m3 1.94 08/22/12 12:05 106-99-00.87 2-Butanone (MEK)40.0 ug/m3 1.94 08/22/12 12:05 78-93-31.2 Carbon disulfide 17.6 ug/m3 1.94 08/22/12 12:05 75-15-01.2 Carbon tetrachloride 7.9 ug/m3 1.94 08/22/12 12:05 56-23-51.2 Chlorobenzene ND ug/m3 1.94 08/22/12 12:05 108-90-71.8 Chloroethane ND ug/m3 1.94 08/22/12 12:05 75-00-31.0 Chloroform 2.5 ug/m3 1.94 08/22/12 12:05 67-66-31.9 Chloromethane ND ug/m3 1.94 08/22/12 12:05 74-87-30.81 Cyclohexane 10.5 ug/m3 1.94 08/22/12 12:05 110-82-71.4 Dibromochloromethane ND ug/m3 1.94 08/22/12 12:05 124-48-13.4 1,2-Dibromoethane (EDB)ND ug/m3 1.94 08/22/12 12:05 106-93-43.0 1,2-Dichlorobenzene ND ug/m3 1.94 08/22/12 12:05 95-50-12.4 1,3-Dichlorobenzene ND ug/m3 1.94 08/22/12 12:05 541-73-12.4 1,4-Dichlorobenzene ND ug/m3 1.94 08/22/12 12:05 106-46-72.4 Dichlorodifluoromethane 3.6 ug/m3 1.94 08/22/12 12:05 75-71-82.0 1,1-Dichloroethane ND ug/m3 1.94 08/22/12 12:05 75-34-31.6 1,2-Dichloroethane ND ug/m3 1.94 08/22/12 12:05 107-06-20.80 1,1-Dichloroethene ND ug/m3 1.94 08/22/12 12:05 75-35-41.6 cis-1,2-Dichloroethene ND ug/m3 1.94 08/22/12 12:05 156-59-21.6 trans-1,2-Dichloroethene ND ug/m3 1.94 08/22/12 12:05 156-60-51.6 1,2-Dichloropropane ND ug/m3 1.94 08/22/12 12:05 78-87-51.8 cis-1,3-Dichloropropene ND ug/m3 1.94 08/22/12 12:05 10061-01-51.8 trans-1,3-Dichloropropene ND ug/m3 1.94 08/22/12 12:05 10061-02-61.8 Dichlorotetrafluoroethane ND ug/m3 1.94 08/22/12 12:05 76-14-22.8 Ethanol 97.1 ug/m3 1.94 08/22/12 12:05 64-17-50.74 Ethyl acetate ND ug/m3 1.94 08/22/12 12:05 141-78-61.4 Ethylbenzene 15.1 ug/m3 1.94 08/22/12 12:05 100-41-41.7 4-Ethyltoluene 10 ug/m3 1.94 08/22/12 12:05 622-96-81.9 n-Heptane 6.7 ug/m3 1.94 08/22/12 12:05 142-82-51.6 Hexachloro-1,3-butadiene ND ug/m3 1.94 08/22/12 12:05 87-68-34.3 n-Hexane 53.4 ug/m3 1.94 08/22/12 12:05 110-54-31.4 2-Hexanone ND ug/m3 1.94 08/22/12 12:05 591-78-61.6 Methylene Chloride ND ug/m3 1.94 08/22/12 12:05 75-09-21.4 4-Methyl-2-pentanone (MIBK)11.8 ug/m3 1.94 08/22/12 12:05 108-10-11.6 Methyl-tert-butyl ether ND ug/m3 1.94 08/22/12 12:05 1634-04-41.4 Naphthalene ND ug/m3 1.94 08/22/12 12:05 91-20-32.1 2-Propanol 7.8 ug/m3 1.94 08/22/12 12:05 67-63-00.97 Propylene ND ug/m3 1.94 08/22/12 12:05 115-07-10.68 Styrene ND ug/m3 1.94 08/22/12 12:05 100-42-51.7 1,1,2,2-Tetrachloroethane ND ug/m3 1.94 08/22/12 12:05 79-34-51.4 Tetrachloroethene 51.7 ug/m3 1.94 08/22/12 12:05 127-18-41.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 19 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 19 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP5S:A081612 Lab ID:10202694008 Collected:08/16/12 17:18 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 1.94 08/22/12 12:05 109-99-91.2 Toluene 117 ug/m3 1.94 08/22/12 12:05 108-88-31.5 1,2,4-Trichlorobenzene ND ug/m3 1.94 08/22/12 12:05 120-82-12.9 1,1,1-Trichloroethane 2.4 ug/m3 1.94 08/22/12 12:05 71-55-62.2 1,1,2-Trichloroethane ND ug/m3 1.94 08/22/12 12:05 79-00-51.1 Trichloroethene ND ug/m3 1.94 08/22/12 12:05 79-01-61.1 Trichlorofluoromethane 5.0 ug/m3 1.94 08/22/12 12:05 75-69-42.2 1,1,2-Trichlorotrifluoroethane ND ug/m3 1.94 08/22/12 12:05 76-13-13.1 1,2,4-Trimethylbenzene 31.6 ug/m3 1.94 08/22/12 12:05 95-63-61.9 1,3,5-Trimethylbenzene 8.7 ug/m3 1.94 08/22/12 12:05 108-67-81.9 Vinyl acetate ND ug/m3 1.94 08/22/12 12:05 108-05-41.4 Vinyl chloride ND ug/m3 1.94 08/22/12 12:05 75-01-40.50 m&p-Xylene 48.8 ug/m3 1.94 08/22/12 12:05 179601-23-13.4 o-Xylene 20.4 ug/m3 1.94 08/22/12 12:05 95-47-61.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 20 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 20 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6D:A081612A Lab ID:10202694009 Collected:08/16/12 17:02 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone 128 ug/m3 19.4 08/21/12 20:11 67-64-19.3 Benzene ND ug/m3 19.4 08/21/12 20:11 71-43-26.3 Benzyl chloride ND ug/m3 19.4 08/21/12 20:11 100-44-720.4 Bromodichloromethane ND ug/m3 19.4 08/21/12 20:11 75-27-426.4 Bromoform ND ug/m3 19.4 08/21/12 20:11 75-25-240.7 Bromomethane ND ug/m3 19.4 08/21/12 20:11 74-83-915.3 1,3-Butadiene ND ug/m3 19.4 08/21/12 20:11 106-99-08.7 2-Butanone (MEK)ND ug/m3 19.4 08/21/12 20:11 78-93-311.6 Carbon disulfide 13.5 ug/m3 19.4 08/21/12 20:11 75-15-012.2 Carbon tetrachloride ND ug/m3 19.4 08/21/12 20:11 56-23-512.4 Chlorobenzene ND ug/m3 19.4 08/21/12 20:11 108-90-718.2 Chloroethane ND ug/m3 19.4 08/21/12 20:11 75-00-310.5 Chloroform ND ug/m3 19.4 08/21/12 20:11 67-66-319.2 Chloromethane ND ug/m3 19.4 08/21/12 20:11 74-87-38.1 Cyclohexane ND ug/m3 19.4 08/21/12 20:11 110-82-713.6 Dibromochloromethane ND ug/m3 19.4 08/21/12 20:11 124-48-133.6 1,2-Dibromoethane (EDB)ND ug/m3 19.4 08/21/12 20:11 106-93-430.3 1,2-Dichlorobenzene ND ug/m3 19.4 08/21/12 20:11 95-50-123.7 1,3-Dichlorobenzene ND ug/m3 19.4 08/21/12 20:11 541-73-123.7 1,4-Dichlorobenzene ND ug/m3 19.4 08/21/12 20:11 106-46-723.7 Dichlorodifluoromethane ND ug/m3 19.4 08/21/12 20:11 75-71-819.6 1,1-Dichloroethane ND ug/m3 19.4 08/21/12 20:11 75-34-315.9 1,2-Dichloroethane ND ug/m3 19.4 08/21/12 20:11 107-06-28.0 1,1-Dichloroethene ND ug/m3 19.4 08/21/12 20:11 75-35-415.7 cis-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 20:11 156-59-215.7 trans-1,2-Dichloroethene ND ug/m3 19.4 08/21/12 20:11 156-60-515.7 1,2-Dichloropropane ND ug/m3 19.4 08/21/12 20:11 78-87-518.2 cis-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 20:11 10061-01-517.8 trans-1,3-Dichloropropene ND ug/m3 19.4 08/21/12 20:11 10061-02-617.8 Dichlorotetrafluoroethane ND ug/m3 19.4 08/21/12 20:11 76-14-227.5 Ethanol 59.5 ug/m3 19.4 08/21/12 20:11 64-17-57.4 Ethyl acetate ND ug/m3 19.4 08/21/12 20:11 141-78-614.2 Ethylbenzene ND ug/m3 19.4 08/21/12 20:11 100-41-417.1 4-Ethyltoluene ND ug/m3 19.4 08/21/12 20:11 622-96-819.4 n-Heptane ND ug/m3 19.4 08/21/12 20:11 142-82-516.1 Hexachloro-1,3-butadiene ND ug/m3 19.4 08/21/12 20:11 87-68-342.7 n-Hexane ND ug/m3 19.4 08/21/12 20:11 110-54-314.0 2-Hexanone ND ug/m3 19.4 08/21/12 20:11 591-78-616.1 Methylene Chloride ND ug/m3 19.4 08/21/12 20:11 75-09-213.8 4-Methyl-2-pentanone (MIBK)ND ug/m3 19.4 08/21/12 20:11 108-10-116.1 Methyl-tert-butyl ether ND ug/m3 19.4 08/21/12 20:11 1634-04-414.2 Naphthalene ND ug/m3 19.4 08/21/12 20:11 91-20-320.8 2-Propanol ND ug/m3 19.4 08/21/12 20:11 67-63-09.7 Propylene ND ug/m3 19.4 08/21/12 20:11 115-07-16.8 Styrene ND ug/m3 19.4 08/21/12 20:11 100-42-516.9 1,1,2,2-Tetrachloroethane ND ug/m3 19.4 08/21/12 20:11 79-34-513.5 Tetrachloroethene 74.6 ug/m3 19.4 08/21/12 20:11 127-18-413.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 21 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 21 of 36 ANALYTICAL RESULTS Pace Project No.: Project: 10202694 SBI068 Sample:ASGP6D:A081612A Lab ID:10202694009 Collected:08/16/12 17:02 Received:08/17/12 09:35 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Tetrahydrofuran ND ug/m3 19.4 08/21/12 20:11 109-99-911.6 Toluene 385 ug/m3 19.4 08/21/12 20:11 108-88-314.9 1,2,4-Trichlorobenzene ND ug/m3 19.4 08/21/12 20:11 120-82-129.3 1,1,1-Trichloroethane ND ug/m3 19.4 08/21/12 20:11 71-55-621.5 1,1,2-Trichloroethane ND ug/m3 19.4 08/21/12 20:11 79-00-510.7 Trichloroethene ND ug/m3 19.4 08/21/12 20:11 79-01-610.7 Trichlorofluoromethane ND ug/m3 19.4 08/21/12 20:11 75-69-422.1 1,1,2-Trichlorotrifluoroethane ND ug/m3 19.4 08/21/12 20:11 76-13-131.0 1,2,4-Trimethylbenzene ND ug/m3 19.4 08/21/12 20:11 95-63-619.4 1,3,5-Trimethylbenzene ND ug/m3 19.4 08/21/12 20:11 108-67-819.4 Vinyl acetate ND ug/m3 19.4 08/21/12 20:11 108-05-413.9 Vinyl chloride ND ug/m3 19.4 08/21/12 20:11 75-01-45.0 m&p-Xylene 37.0 ug/m3 19.4 08/21/12 20:11 179601-23-134.1 o-Xylene ND ug/m3 19.4 08/21/12 20:11 95-47-617.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 22 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 22 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/15578 TO-15 TO-15 TO15 MSV AIR Low Level Associated Lab Samples:10202694001, 10202694002, 10202694003, 10202694004, 10202694005, 10202694006, 10202694007, 10202694009 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1271519 Associated Lab Samples:10202694001, 10202694002, 10202694003, 10202694004, 10202694005, 10202694006, 10202694007, 10202694009 Matrix:Air Analyzed 1,1,1-Trichloroethane ug/m3 ND 1.1 08/21/12 09:06 1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 08/21/12 09:06 1,1,2-Trichloroethane ug/m3 ND 0.55 08/21/12 09:06 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 08/21/12 09:06 1,1-Dichloroethane ug/m3 ND 0.82 08/21/12 09:06 1,1-Dichloroethene ug/m3 ND 0.81 08/21/12 09:06 1,2,4-Trichlorobenzene ug/m3 ND 1.5 08/21/12 09:06 1,2,4-Trimethylbenzene ug/m3 ND 1.0 08/21/12 09:06 1,2-Dibromoethane (EDB)ug/m3 ND 1.6 08/21/12 09:06 1,2-Dichlorobenzene ug/m3 ND 1.2 08/21/12 09:06 1,2-Dichloroethane ug/m3 ND 0.41 08/21/12 09:06 1,2-Dichloropropane ug/m3 ND 0.94 08/21/12 09:06 1,3,5-Trimethylbenzene ug/m3 ND 1.0 08/21/12 09:06 1,3-Butadiene ug/m3 ND 0.45 08/21/12 09:06 1,3-Dichlorobenzene ug/m3 ND 1.2 08/21/12 09:06 1,4-Dichlorobenzene ug/m3 ND 1.2 08/21/12 09:06 2-Butanone (MEK)ug/m3 ND 0.60 08/21/12 09:06 2-Hexanone ug/m3 ND 0.83 08/21/12 09:06 2-Propanol ug/m3 ND 0.50 08/21/12 09:06 4-Ethyltoluene ug/m3 ND 1.0 08/21/12 09:06 4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 08/21/12 09:06 Acetone ug/m3 ND 0.48 08/21/12 09:06 Benzene ug/m3 ND 0.32 08/21/12 09:06 Benzyl chloride ug/m3 ND 1.0 08/21/12 09:06 Bromodichloromethane ug/m3 ND 1.4 08/21/12 09:06 Bromoform ug/m3 ND 2.1 08/21/12 09:06 Bromomethane ug/m3 ND 0.79 08/21/12 09:06 Carbon disulfide ug/m3 ND 0.63 08/21/12 09:06 Carbon tetrachloride ug/m3 ND 0.64 08/21/12 09:06 Chlorobenzene ug/m3 ND 0.94 08/21/12 09:06 Chloroethane ug/m3 ND 0.54 08/21/12 09:06 Chloroform ug/m3 ND 0.99 08/21/12 09:06 Chloromethane ug/m3 ND 0.42 08/21/12 09:06 cis-1,2-Dichloroethene ug/m3 ND 0.81 08/21/12 09:06 cis-1,3-Dichloropropene ug/m3 ND 0.92 08/21/12 09:06 Cyclohexane ug/m3 ND 0.70 08/21/12 09:06 Dibromochloromethane ug/m3 ND 1.7 08/21/12 09:06 Dichlorodifluoromethane ug/m3 ND 1.0 08/21/12 09:06 Dichlorotetrafluoroethane ug/m3 ND 1.4 08/21/12 09:06 Ethanol ug/m3 ND 0.38 08/21/12 09:06 Ethyl acetate ug/m3 ND 0.73 08/21/12 09:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 23 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 23 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1271519 Associated Lab Samples:10202694001, 10202694002, 10202694003, 10202694004, 10202694005, 10202694006, 10202694007, 10202694009 Matrix:Air Analyzed Ethylbenzene ug/m3 ND 0.88 08/21/12 09:06 Hexachloro-1,3-butadiene ug/m3 ND 2.2 08/21/12 09:06 m&p-Xylene ug/m3 ND 1.8 08/21/12 09:06 Methyl-tert-butyl ether ug/m3 ND 0.73 08/21/12 09:06 Methylene Chloride ug/m3 ND 0.71 08/21/12 09:06 n-Heptane ug/m3 ND 0.83 08/21/12 09:06 n-Hexane ug/m3 ND 0.72 08/21/12 09:06 Naphthalene ug/m3 ND 1.1 08/21/12 09:06 o-Xylene ug/m3 ND 0.88 08/21/12 09:06 Propylene ug/m3 ND 0.35 08/21/12 09:06 Styrene ug/m3 ND 0.87 08/21/12 09:06 Tetrachloroethene ug/m3 ND 0.69 08/21/12 09:06 Tetrahydrofuran ug/m3 ND 0.60 08/21/12 09:06 Toluene ug/m3 ND 0.77 08/21/12 09:06 trans-1,2-Dichloroethene ug/m3 ND 0.81 08/21/12 09:06 trans-1,3-Dichloropropene ug/m3 ND 0.92 08/21/12 09:06 Trichloroethene ug/m3 ND 0.55 08/21/12 09:06 Trichlorofluoromethane ug/m3 ND 1.1 08/21/12 09:06 Vinyl acetate ug/m3 ND 0.72 08/21/12 09:06 Vinyl chloride ug/m3 ND 0.26 08/21/12 09:06 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1271520LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/m3 50.355.5 91 72-129 1,1,2,2-Tetrachloroethane ug/m3 62.369.8 89 73-131 1,1,2-Trichloroethane ug/m3 47.855.5 86 71-128 1,1,2-Trichlorotrifluoroethane ug/m3 64.977.9 83 65-132 1,1-Dichloroethane ug/m3 36.341.2 88 67-132 1,1-Dichloroethene ug/m3 36.940.3 92 68-134 1,2,4-Trichlorobenzene ug/m3 10975.5 144 48-150 1,2,4-Trimethylbenzene ug/m3 49.850 100 72-127 1,2-Dibromoethane (EDB)ug/m3 69.378.1 89 75-130 1,2-Dichlorobenzene ug/m3 55.561.2 91 71-132 1,2-Dichloroethane ug/m3 37.941.2 92 70-131 1,2-Dichloropropane ug/m3 42.847 91 73-130 1,3,5-Trimethylbenzene ug/m3 54.150 108 70-133 1,3-Butadiene ug/m3 23.722.5 105 69-132 1,3-Dichlorobenzene ug/m3 61.761.2 101 71-128 1,4-Dichlorobenzene ug/m3 56.061.2 91 72-131 2-Butanone (MEK)ug/m3 31.030 103 69-131 2-Hexanone ug/m3 39.641.7 95 71-134 2-Propanol ug/m3 25.425 102 72-132 4-Ethyltoluene ug/m3 49.850 100 71-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 24 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 24 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1271520LABORATORY CONTROL SAMPLE: LCSSpike 4-Methyl-2-pentanone (MIBK)ug/m3 42.741.7 102 69-135 Acetone ug/m3 27.424.2 113 61-139 Benzene ug/m3 29.632.5 91 69-134 Benzyl chloride ug/m3 52.652.5 100 70-129 Bromodichloromethane ug/m3 62.268.2 91 71-130 Bromoform ug/m3 103105 98 70-130 Bromomethane ug/m3 34.639.5 88 69-125 Carbon disulfide ug/m3 28.031.7 88 66-131 Carbon tetrachloride ug/m3 54.364 85 68-128 Chlorobenzene ug/m3 37.946.8 81 75-128 Chloroethane ug/m3 23.026.8 86 66-131 Chloroform ug/m3 42.949.7 86 68-132 Chloromethane ug/m3 17.821 85 60-139 cis-1,2-Dichloroethene ug/m3 40.440.3 100 73-130 cis-1,3-Dichloropropene ug/m3 51.046.2 111 74-134 Cyclohexane ug/m3 35.935 103 67-136 Dibromochloromethane ug/m3 77.786.6 90 69-131 Dichlorodifluoromethane ug/m3 42.650.3 85 67-131 Dichlorotetrafluoroethane ug/m3 59.871.1 84 66-130 Ethanol ug/m3 16.219.2 85 69-131 Ethyl acetate ug/m3 39.736.6 108 71-131 Ethylbenzene ug/m3 45.844.2 104 69-139 Hexachloro-1,3-butadiene ug/m3 144108 132 41-150 m&p-Xylene ug/m3 86.688.3 98 66-137 Methyl-tert-butyl ether ug/m3 36.436.7 99 70-132 Methylene Chloride ug/m3 35.835.3 101 73-134 n-Heptane ug/m3 43.741.7 105 70-134 n-Hexane ug/m3 39.935.8 111 65-133 Naphthalene ug/m3 63.153.3 118 57-150 o-Xylene ug/m3 45.444.2 103 69-138 Propylene ug/m3 17.717.5 101 70-134 Styrene ug/m3 47.643.3 110 72-132 Tetrachloroethene ug/m3 57.769 84 70-130 Tetrahydrofuran ug/m3 30.730 102 74-128 Toluene ug/m3 34.138.3 89 71-132 trans-1,2-Dichloroethene ug/m3 37.140.3 92 72-128 trans-1,3-Dichloropropene ug/m3 47.246.2 102 73-130 Trichloroethene ug/m3 49.554.6 91 72-131 Trichlorofluoromethane ug/m3 48.357.1 84 66-129 Vinyl acetate ug/m3 37.735.8 105 71-131 Vinyl chloride ug/m3 22.526 86 70-131 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202722005 1272206SAMPLE DUPLICATE: 1,1,1-Trichloroethane ug/m3 ND 25ND 1,1,2,2-Tetrachloroethane ug/m3 ND 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 25 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 25 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202722005 1272206SAMPLE DUPLICATE: 1,1,2-Trichloroethane ug/m3 ND 25ND 1,1,2-Trichlorotrifluoroethane ug/m3 ND 25ND 1,1-Dichloroethane ug/m3 ND 25ND 1,1-Dichloroethene ug/m3 ND 25ND 1,2,4-Trichlorobenzene ug/m3 ND 25ND 1,2,4-Trimethylbenzene ug/m3 26.3J 25ND 1,2-Dibromoethane (EDB)ug/m3 ND 25ND 1,2-Dichlorobenzene ug/m3 ND 25ND 1,2-Dichloroethane ug/m3 ND 25ND 1,2-Dichloropropane ug/m3 ND 25ND 1,3,5-Trimethylbenzene ug/m3 ND 25ND 1,3-Butadiene ug/m3 ND 25ND 1,3-Dichlorobenzene ug/m3 ND 25ND 1,4-Dichlorobenzene ug/m3 ND 25ND 2-Butanone (MEK)ug/m3 ND 25ND 2-Hexanone ug/m3 ND 25ND 2-Propanol ug/m3 ND 25ND 4-Ethyltoluene ug/m3 ND 25ND 4-Methyl-2-pentanone (MIBK)ug/m3 ND 25ND Acetone ug/m3 ND 25ND Benzene ug/m3 97.7 5 2593.3 Benzyl chloride ug/m3 ND 25ND Bromodichloromethane ug/m3 ND 25ND Bromoform ug/m3 ND 25ND Bromomethane ug/m3 ND 25ND Carbon disulfide ug/m3 25.6 .3 2525.7 Carbon tetrachloride ug/m3 ND 25ND Chlorobenzene ug/m3 ND 25ND Chloroethane ug/m3 ND 25ND Chloroform ug/m3 ND 25ND Chloromethane ug/m3 ND 25ND cis-1,2-Dichloroethene ug/m3 32.5 15 2537.9 cis-1,3-Dichloropropene ug/m3 ND 25ND Cyclohexane ug/m3 771 5 25731 Dibromochloromethane ug/m3 ND 25ND Dichlorodifluoromethane ug/m3 1030 3 251070 Dichlorotetrafluoroethane ug/m3 2780 3 252870 Ethanol ug/m3 ND 25ND Ethyl acetate ug/m3 ND 25ND Ethylbenzene ug/m3 38.2 5 2536.3 Hexachloro-1,3-butadiene ug/m3 ND 25ND m&p-Xylene ug/m3 95.2 3 2597.8 Methyl-tert-butyl ether ug/m3 ND 25ND Methylene Chloride ug/m3 ND 25ND n-Heptane ug/m3 335 4 25322 n-Hexane ug/m3 654 4 25629 Naphthalene ug/m3 81.0 6 2576.6 o-Xylene ug/m3 53.4 1 2552.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 26 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 26 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202722005 1272206SAMPLE DUPLICATE: Propylene ug/m3 ND 25ND Styrene ug/m3 ND 25ND Tetrachloroethene ug/m3 ND 25ND Tetrahydrofuran ug/m3 ND 25ND Toluene ug/m3 55.0 5 2552.2 trans-1,2-Dichloroethene ug/m3 ND 25ND trans-1,3-Dichloropropene ug/m3 ND 25ND Trichloroethene ug/m3 ND 25ND Trichlorofluoromethane ug/m3 ND 25ND Vinyl acetate ug/m3 ND 25ND Vinyl chloride ug/m3 ND 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 27 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 27 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/15589 TO-15 TO-15 TO15 MSV AIR Low Level Associated Lab Samples:10202694008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1272412 Associated Lab Samples:10202694008 Matrix:Air Analyzed 1,1,1-Trichloroethane ug/m3 ND 1.1 08/22/12 09:05 1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 08/22/12 09:05 1,1,2-Trichloroethane ug/m3 ND 0.55 08/22/12 09:05 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 08/22/12 09:05 1,1-Dichloroethane ug/m3 ND 0.82 08/22/12 09:05 1,1-Dichloroethene ug/m3 ND 0.81 08/22/12 09:05 1,2,4-Trichlorobenzene ug/m3 ND 1.5 08/22/12 09:05 1,2,4-Trimethylbenzene ug/m3 ND 1.0 08/22/12 09:05 1,2-Dibromoethane (EDB)ug/m3 ND 1.6 08/22/12 09:05 1,2-Dichlorobenzene ug/m3 ND 1.2 08/22/12 09:05 1,2-Dichloroethane ug/m3 ND 0.41 08/22/12 09:05 1,2-Dichloropropane ug/m3 ND 0.94 08/22/12 09:05 1,3,5-Trimethylbenzene ug/m3 ND 1.0 08/22/12 09:05 1,3-Butadiene ug/m3 ND 0.45 08/22/12 09:05 1,3-Dichlorobenzene ug/m3 ND 1.2 08/22/12 09:05 1,4-Dichlorobenzene ug/m3 ND 1.2 08/22/12 09:05 2-Butanone (MEK)ug/m3 ND 0.60 08/22/12 09:05 2-Hexanone ug/m3 ND 0.83 08/22/12 09:05 2-Propanol ug/m3 ND 0.50 08/22/12 09:05 4-Ethyltoluene ug/m3 ND 1.0 08/22/12 09:05 4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 08/22/12 09:05 Acetone ug/m3 ND 0.48 08/22/12 09:05 Benzene ug/m3 ND 0.32 08/22/12 09:05 Benzyl chloride ug/m3 ND 1.0 08/22/12 09:05 Bromodichloromethane ug/m3 ND 1.4 08/22/12 09:05 Bromoform ug/m3 ND 2.1 08/22/12 09:05 Bromomethane ug/m3 ND 0.79 08/22/12 09:05 Carbon disulfide ug/m3 ND 0.63 08/22/12 09:05 Carbon tetrachloride ug/m3 ND 0.64 08/22/12 09:05 Chlorobenzene ug/m3 ND 0.94 08/22/12 09:05 Chloroethane ug/m3 ND 0.54 08/22/12 09:05 Chloroform ug/m3 ND 0.99 08/22/12 09:05 Chloromethane ug/m3 ND 0.42 08/22/12 09:05 cis-1,2-Dichloroethene ug/m3 ND 0.81 08/22/12 09:05 cis-1,3-Dichloropropene ug/m3 ND 0.92 08/22/12 09:05 Cyclohexane ug/m3 ND 0.70 08/22/12 09:05 Dibromochloromethane ug/m3 ND 1.7 08/22/12 09:05 Dichlorodifluoromethane ug/m3 ND 1.0 08/22/12 09:05 Dichlorotetrafluoroethane ug/m3 ND 1.4 08/22/12 09:05 Ethanol ug/m3 ND 0.38 08/22/12 09:05 Ethyl acetate ug/m3 ND 0.73 08/22/12 09:05 Ethylbenzene ug/m3 ND 0.88 08/22/12 09:05 Hexachloro-1,3-butadiene ug/m3 ND 2.2 08/22/12 09:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 28 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 28 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1272412 Associated Lab Samples:10202694008 Matrix:Air Analyzed m&p-Xylene ug/m3 ND 1.8 08/22/12 09:05 Methyl-tert-butyl ether ug/m3 ND 0.73 08/22/12 09:05 Methylene Chloride ug/m3 ND 0.71 08/22/12 09:05 n-Heptane ug/m3 ND 0.83 08/22/12 09:05 n-Hexane ug/m3 ND 0.72 08/22/12 09:05 Naphthalene ug/m3 ND 1.1 08/22/12 09:05 o-Xylene ug/m3 ND 0.88 08/22/12 09:05 Propylene ug/m3 ND 0.35 08/22/12 09:05 Styrene ug/m3 ND 0.87 08/22/12 09:05 Tetrachloroethene ug/m3 ND 0.69 08/22/12 09:05 Tetrahydrofuran ug/m3 ND 0.60 08/22/12 09:05 Toluene ug/m3 ND 0.77 08/22/12 09:05 trans-1,2-Dichloroethene ug/m3 ND 0.81 08/22/12 09:05 trans-1,3-Dichloropropene ug/m3 ND 0.92 08/22/12 09:05 Trichloroethene ug/m3 ND 0.55 08/22/12 09:05 Trichlorofluoromethane ug/m3 ND 1.1 08/22/12 09:05 Vinyl acetate ug/m3 ND 0.72 08/22/12 09:05 Vinyl chloride ug/m3 ND 0.26 08/22/12 09:05 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1272413LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/m3 52.555.5 95 72-129 1,1,2,2-Tetrachloroethane ug/m3 68.069.8 97 73-131 1,1,2-Trichloroethane ug/m3 51.955.5 94 71-128 1,1,2-Trichlorotrifluoroethane ug/m3 69.577.9 89 65-132 1,1-Dichloroethane ug/m3 38.741.2 94 67-132 1,1-Dichloroethene ug/m3 39.140.3 97 68-134 1,2,4-Trichlorobenzene ug/m3 117 CH,L375.5 155 48-150 1,2,4-Trimethylbenzene ug/m3 52.750 105 72-127 1,2-Dibromoethane (EDB)ug/m3 75.278.1 96 75-130 1,2-Dichlorobenzene ug/m3 59.361.2 97 71-132 1,2-Dichloroethane ug/m3 39.641.2 96 70-131 1,2-Dichloropropane ug/m3 46.147 98 73-130 1,3,5-Trimethylbenzene ug/m3 57.850 116 70-133 1,3-Butadiene ug/m3 25.322.5 112 69-132 1,3-Dichlorobenzene ug/m3 66.861.2 109 71-128 1,4-Dichlorobenzene ug/m3 60.361.2 99 72-131 2-Butanone (MEK)ug/m3 33.230 111 69-131 2-Hexanone ug/m3 42.341.7 102 71-134 2-Propanol ug/m3 23.625 94 72-132 4-Ethyltoluene ug/m3 53.150 106 71-129 4-Methyl-2-pentanone (MIBK)ug/m3 45.241.7 109 69-135 Acetone ug/m3 28.124.2 116 61-139 Benzene ug/m3 31.632.5 97 69-134 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 29 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 29 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1272413LABORATORY CONTROL SAMPLE: LCSSpike Benzyl chloride ug/m3 55.752.5 106 70-129 Bromodichloromethane ug/m3 66.168.2 97 71-130 Bromoform ug/m3 110105 105 70-130 Bromomethane ug/m3 37.039.5 94 69-125 Carbon disulfide ug/m3 29.931.7 95 66-131 Carbon tetrachloride ug/m3 57.764 90 68-128 Chlorobenzene ug/m3 41.646.8 89 75-128 Chloroethane ug/m3 25.126.8 93 66-131 Chloroform ug/m3 45.549.7 92 68-132 Chloromethane ug/m3 19.321 92 60-139 cis-1,2-Dichloroethene ug/m3 42.840.3 106 73-130 cis-1,3-Dichloropropene ug/m3 54.146.2 117 74-134 Cyclohexane ug/m3 38.935 111 67-136 Dibromochloromethane ug/m3 82.886.6 96 69-131 Dichlorodifluoromethane ug/m3 45.750.3 91 67-131 Dichlorotetrafluoroethane ug/m3 63.671.1 89 66-130 Ethanol ug/m3 16.519.2 86 69-131 Ethyl acetate ug/m3 41.636.6 114 71-131 Ethylbenzene ug/m3 49.444.2 112 69-139 Hexachloro-1,3-butadiene ug/m3 153108 141 41-150 m&p-Xylene ug/m3 91.988.3 104 66-137 Methyl-tert-butyl ether ug/m3 38.136.7 104 70-132 Methylene Chloride ug/m3 39.135.3 111 73-134 n-Heptane ug/m3 46.741.7 112 70-134 n-Hexane ug/m3 44.035.8 123 65-133 Naphthalene ug/m3 70.7 CH53.3 133 57-150 o-Xylene ug/m3 47.944.2 108 69-138 Propylene ug/m3 19.017.5 109 70-134 Styrene ug/m3 50.743.3 117 72-132 Tetrachloroethene ug/m3 62.569 91 70-130 Tetrahydrofuran ug/m3 32.130 107 74-128 Toluene ug/m3 36.738.3 96 71-132 trans-1,2-Dichloroethene ug/m3 39.540.3 98 72-128 trans-1,3-Dichloropropene ug/m3 50.046.2 108 73-130 Trichloroethene ug/m3 52.654.6 96 72-131 Trichlorofluoromethane ug/m3 50.657.1 88 66-129 Vinyl acetate ug/m3 39.635.8 111 71-131 Vinyl chloride ug/m3 24.426 94 70-131 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202561001 1273420SAMPLE DUPLICATE: 1,1,1-Trichloroethane ug/m3 ND 25ND 1,1,2,2-Tetrachloroethane ug/m3 ND 25ND 1,1,2-Trichloroethane ug/m3 ND 25ND 1,1,2-Trichlorotrifluoroethane ug/m3 ND 25ND 1,1-Dichloroethane ug/m3 ND 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 30 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 30 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202561001 1273420SAMPLE DUPLICATE: 1,1-Dichloroethene ug/m3 ND 25ND 1,2,4-Trichlorobenzene ug/m3 ND 25ND 1,2,4-Trimethylbenzene ug/m3 ND 25ND 1,2-Dibromoethane (EDB)ug/m3 ND 25ND 1,2-Dichlorobenzene ug/m3 ND 25ND 1,2-Dichloroethane ug/m3 ND 25ND 1,2-Dichloropropane ug/m3 ND 25ND 1,3,5-Trimethylbenzene ug/m3 ND 25ND 1,3-Butadiene ug/m3 ND 25ND 1,3-Dichlorobenzene ug/m3 ND 25ND 1,4-Dichlorobenzene ug/m3 ND 25ND 2-Butanone (MEK)ug/m3 242 E1125270 2-Hexanone ug/m3 ND 25ND 2-Propanol ug/m3 3.6 5 253.8 4-Ethyltoluene ug/m3 ND 25ND 4-Methyl-2-pentanone (MIBK)ug/m3 12.5 9 2513.7 Acetone ug/m3 150 E2525117 Benzene ug/m3 ND 25ND Benzyl chloride ug/m3 ND 25ND Bromodichloromethane ug/m3 ND 25ND Bromoform ug/m3 ND 25ND Bromomethane ug/m3 ND 25ND Carbon disulfide ug/m3 ND 25ND Carbon tetrachloride ug/m3 ND 25ND Chlorobenzene ug/m3 ND 25ND Chloroethane ug/m3 ND 25ND Chloroform ug/m3 ND 25ND Chloromethane ug/m3 0.72 1 250.73 cis-1,2-Dichloroethene ug/m3 ND 25ND cis-1,3-Dichloropropene ug/m3 ND 25ND Cyclohexane ug/m3 ND 25ND Dibromochloromethane ug/m3 ND 25ND Dichlorodifluoromethane ug/m3 2.5 3 252.4 Dichlorotetrafluoroethane ug/m3 ND 25ND Ethanol ug/m3 30.3 8 2532.9 Ethyl acetate ug/m3 ND 25ND Ethylbenzene ug/m3 ND 25ND Hexachloro-1,3-butadiene ug/m3 ND 25ND m&p-Xylene ug/m3 ND 25ND Methyl-tert-butyl ether ug/m3 ND 25ND Methylene Chloride ug/m3 ND 25ND n-Heptane ug/m3 ND 25ND n-Hexane ug/m3 5.8 R140253.8 Naphthalene ug/m3 ND 252.8 o-Xylene ug/m3 ND 25ND Propylene ug/m3 ND 25ND Styrene ug/m3 ND 25ND Tetrachloroethene ug/m3 ND 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 31 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 31 of 36 QUALITY CONTROL DATA Pace Project No.: Project: 10202694 SBI068 Parameter Units Dup Result Max RPD QualifiersRPDResult 10202561001 1273420SAMPLE DUPLICATE: Tetrahydrofuran ug/m3 ND 25ND Toluene ug/m3 21.2 .8 2521.4 trans-1,2-Dichloroethene ug/m3 ND 25ND trans-1,3-Dichloropropene ug/m3 ND 25ND Trichloroethene ug/m3 ND 25ND Trichlorofluoromethane ug/m3 1.3J 25ND Vinyl acetate ug/m3 ND 25ND Vinyl chloride ug/m3 ND 25ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 32 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 32 of 36 QUALIFIERS Pace Project No.: Project: 10202694 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.CH Analyte concentration exceeded the calibration range. The reported result is estimated.E Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 33 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 33 of 36 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 10202694 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 10202694001 AIR/15578ASGP8D:A081612 TO-15 10202694002 AIR/15578ASGP8S:A081612 TO-15 10202694003 AIR/15578ASGP7D:A081612 TO-15 10202694004 AIR/15578ASGP7S:A081612 TO-15 10202694005 AIR/15578ASGP6D:A081612 TO-15 10202694006 AIR/15578ASGP6S:A081612 TO-15 10202694007 AIR/15578ASGP5D:A081612 TO-15 10202694008 AIR/15589ASGP5S:A081612 TO-15 10202694009 AIR/15578ASGP6D:A081612A TO-15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 08/30/2012 04:57 PM Page 34 of 34 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607-1700 34 of 36 35 of 36 36 of 36 June 06, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5063426 5063426 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on May 24, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5063426 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5063426 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5063426001 SBI068:AMW8I:S040049 Solid 05/22/12 13:00 05/24/12 09:10 5063426002 SBI068:AMW8I:S200205 Solid 05/22/12 13:37 05/24/12 09:10 5063426003 SBI068:AMW4D:S160172 Solid 05/23/12 10:25 05/24/12 09:10 5063426004 SBI068:AMW4D:S160172A Solid 05/23/12 10:25 05/24/12 09:10 5063426005 SBI068:AMW4D:S180185 Solid 05/23/12 10:29 05/24/12 09:10 5063426006 SBI068:FB-3:W052312 Water 05/23/12 12:00 05/24/12 09:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5063426 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5063426001 SBI068:AMW8I:S040049 EPA 8260 73RSW ASTM D2974-87 1DAE 5063426002 SBI068:AMW8I:S200205 EPA 8260 73RSW ASTM D2974-87 1DAE 5063426003 SBI068:AMW4D:S160172 EPA 8260 73RSW ASTM D2974-87 1DAE 5063426004 SBI068:AMW4D:S160172A EPA 8260 73RSW ASTM D2974-87 1DAE 5063426005 SBI068:AMW4D:S180185 EPA 8260 73RSW ASTM D2974-87 1DAE 5063426006 SBI068:FB-3:W052312 EPA 8260 73RSW REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW8I:S040049 Lab ID:5063426001 Collected:05/22/12 13:00 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 15:27 67-64-188.1 Acrolein ND ug/kg 1 05/30/12 15:27 107-02-888.1 Acrylonitrile ND ug/kg 1 05/30/12 15:27 107-13-188.1 Benzene ND ug/kg 1 05/30/12 15:27 71-43-24.4 Bromobenzene ND ug/kg 1 05/30/12 15:27 108-86-14.4 Bromochloromethane ND ug/kg 1 05/30/12 15:27 74-97-54.4 Bromodichloromethane ND ug/kg 1 05/30/12 15:27 75-27-44.4 Bromoform ND ug/kg 1 05/30/12 15:27 75-25-24.4 Bromomethane ND ug/kg 1 05/30/12 15:27 74-83-94.4 2-Butanone (MEK)ND ug/kg 1 05/30/12 15:27 78-93-322.0 n-Butylbenzene ND ug/kg 1 05/30/12 15:27 104-51-84.4 sec-Butylbenzene ND ug/kg 1 05/30/12 15:27 135-98-84.4 tert-Butylbenzene ND ug/kg 1 05/30/12 15:27 98-06-64.4 Carbon disulfide ND ug/kg 1 05/30/12 15:27 75-15-08.8 Carbon tetrachloride ND ug/kg 1 05/30/12 15:27 56-23-54.4 Chlorobenzene ND ug/kg 1 05/30/12 15:27 108-90-74.4 Chloroethane ND ug/kg 1 05/30/12 15:27 75-00-34.4 Chloroform ND ug/kg 1 05/30/12 15:27 67-66-34.4 Chloromethane ND ug/kg 1 05/30/12 15:27 74-87-34.4 2-Chlorotoluene ND ug/kg 1 05/30/12 15:27 95-49-84.4 4-Chlorotoluene ND ug/kg 1 05/30/12 15:27 106-43-44.4 Dibromochloromethane ND ug/kg 1 05/30/12 15:27 124-48-14.4 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 15:27 106-93-44.4 Dibromomethane ND ug/kg 1 05/30/12 15:27 74-95-34.4 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 15:27 95-50-14.4 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 15:27 541-73-14.4 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 15:27 106-46-74.4 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 15:27 110-57-688.1 Dichlorodifluoromethane ND ug/kg 1 05/30/12 15:27 75-71-84.4 1,1-Dichloroethane ND ug/kg 1 05/30/12 15:27 75-34-34.4 1,2-Dichloroethane ND ug/kg 1 05/30/12 15:27 107-06-24.4 1,1-Dichloroethene ND ug/kg 1 05/30/12 15:27 75-35-44.4 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 15:27 156-59-24.4 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 15:27 156-60-54.4 1,2-Dichloropropane ND ug/kg 1 05/30/12 15:27 78-87-54.4 1,3-Dichloropropane ND ug/kg 1 05/30/12 15:27 142-28-94.4 2,2-Dichloropropane ND ug/kg 1 05/30/12 15:27 594-20-74.4 1,1-Dichloropropene ND ug/kg 1 05/30/12 15:27 563-58-64.4 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 15:27 10061-01-54.4 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 15:27 10061-02-64.4 Ethylbenzene ND ug/kg 1 05/30/12 15:27 100-41-44.4 Ethyl methacrylate ND ug/kg 1 05/30/12 15:27 97-63-288.1 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 15:27 87-68-34.4 n-Hexane ND ug/kg 1 05/30/12 15:27 110-54-3 N24.4 2-Hexanone ND ug/kg 1 05/30/12 15:27 591-78-688.1 Iodomethane ND ug/kg 1 05/30/12 15:27 74-88-488.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 5 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW8I:S040049 Lab ID:5063426001 Collected:05/22/12 13:00 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 15:27 98-82-84.4 p-Isopropyltoluene ND ug/kg 1 05/30/12 15:27 99-87-64.4 Methylene Chloride ND ug/kg 1 05/30/12 15:27 75-09-217.6 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 15:27 108-10-122.0 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 15:27 1634-04-44.4 Naphthalene ND ug/kg 1 05/30/12 15:27 91-20-34.4 n-Propylbenzene ND ug/kg 1 05/30/12 15:27 103-65-14.4 Styrene ND ug/kg 1 05/30/12 15:27 100-42-54.4 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 15:27 630-20-64.4 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 15:27 79-34-54.4 Tetrachloroethene ND ug/kg 1 05/30/12 15:27 127-18-44.4 Toluene ND ug/kg 1 05/30/12 15:27 108-88-34.4 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 15:27 87-61-64.4 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 15:27 120-82-14.4 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 15:27 71-55-64.4 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 15:27 79-00-54.4 Trichloroethene ND ug/kg 1 05/30/12 15:27 79-01-64.4 Trichlorofluoromethane ND ug/kg 1 05/30/12 15:27 75-69-44.4 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 15:27 96-18-44.4 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 15:27 95-63-64.4 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 15:27 108-67-84.4 Vinyl acetate ND ug/kg 1 05/30/12 15:27 108-05-488.1 Vinyl chloride ND ug/kg 1 05/30/12 15:27 75-01-44.4 Xylene (Total)ND ug/kg 1 05/30/12 15:27 1330-20-78.8 Surrogates Dibromofluoromethane (S)115 %.1 05/30/12 15:27 1868-53-771-125 Toluene-d8 (S)91 %.1 05/30/12 15:27 2037-26-576-124 4-Bromofluorobenzene (S)103 %.1 05/30/12 15:27 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.8 %1 05/30/12 18:040.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 6 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW8I:S200205 Lab ID:5063426002 Collected:05/22/12 13:37 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 16:04 67-64-189.0 Acrolein ND ug/kg 1 05/30/12 16:04 107-02-889.0 Acrylonitrile ND ug/kg 1 05/30/12 16:04 107-13-189.0 Benzene ND ug/kg 1 05/30/12 16:04 71-43-24.5 Bromobenzene ND ug/kg 1 05/30/12 16:04 108-86-14.5 Bromochloromethane ND ug/kg 1 05/30/12 16:04 74-97-54.5 Bromodichloromethane ND ug/kg 1 05/30/12 16:04 75-27-44.5 Bromoform ND ug/kg 1 05/30/12 16:04 75-25-24.5 Bromomethane ND ug/kg 1 05/30/12 16:04 74-83-94.5 2-Butanone (MEK)ND ug/kg 1 05/30/12 16:04 78-93-322.3 n-Butylbenzene ND ug/kg 1 05/30/12 16:04 104-51-84.5 sec-Butylbenzene ND ug/kg 1 05/30/12 16:04 135-98-84.5 tert-Butylbenzene ND ug/kg 1 05/30/12 16:04 98-06-64.5 Carbon disulfide ND ug/kg 1 05/30/12 16:04 75-15-08.9 Carbon tetrachloride ND ug/kg 1 05/30/12 16:04 56-23-54.5 Chlorobenzene ND ug/kg 1 05/30/12 16:04 108-90-74.5 Chloroethane ND ug/kg 1 05/30/12 16:04 75-00-34.5 Chloroform ND ug/kg 1 05/30/12 16:04 67-66-34.5 Chloromethane ND ug/kg 1 05/30/12 16:04 74-87-34.5 2-Chlorotoluene ND ug/kg 1 05/30/12 16:04 95-49-84.5 4-Chlorotoluene ND ug/kg 1 05/30/12 16:04 106-43-44.5 Dibromochloromethane ND ug/kg 1 05/30/12 16:04 124-48-14.5 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 16:04 106-93-44.5 Dibromomethane ND ug/kg 1 05/30/12 16:04 74-95-34.5 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 16:04 95-50-14.5 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 16:04 541-73-14.5 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 16:04 106-46-74.5 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 16:04 110-57-689.0 Dichlorodifluoromethane ND ug/kg 1 05/30/12 16:04 75-71-84.5 1,1-Dichloroethane ND ug/kg 1 05/30/12 16:04 75-34-34.5 1,2-Dichloroethane ND ug/kg 1 05/30/12 16:04 107-06-24.5 1,1-Dichloroethene ND ug/kg 1 05/30/12 16:04 75-35-44.5 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:04 156-59-24.5 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:04 156-60-54.5 1,2-Dichloropropane ND ug/kg 1 05/30/12 16:04 78-87-54.5 1,3-Dichloropropane ND ug/kg 1 05/30/12 16:04 142-28-94.5 2,2-Dichloropropane ND ug/kg 1 05/30/12 16:04 594-20-74.5 1,1-Dichloropropene ND ug/kg 1 05/30/12 16:04 563-58-64.5 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:04 10061-01-54.5 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:04 10061-02-64.5 Ethylbenzene ND ug/kg 1 05/30/12 16:04 100-41-44.5 Ethyl methacrylate ND ug/kg 1 05/30/12 16:04 97-63-289.0 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 16:04 87-68-34.5 n-Hexane ND ug/kg 1 05/30/12 16:04 110-54-3 N24.5 2-Hexanone ND ug/kg 1 05/30/12 16:04 591-78-689.0 Iodomethane ND ug/kg 1 05/30/12 16:04 74-88-489.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 7 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW8I:S200205 Lab ID:5063426002 Collected:05/22/12 13:37 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 16:04 98-82-84.5 p-Isopropyltoluene ND ug/kg 1 05/30/12 16:04 99-87-64.5 Methylene Chloride ND ug/kg 1 05/30/12 16:04 75-09-217.8 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 16:04 108-10-122.3 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 16:04 1634-04-44.5 Naphthalene ND ug/kg 1 05/30/12 16:04 91-20-34.5 n-Propylbenzene ND ug/kg 1 05/30/12 16:04 103-65-14.5 Styrene ND ug/kg 1 05/30/12 16:04 100-42-54.5 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:04 630-20-64.5 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:04 79-34-54.5 Tetrachloroethene ND ug/kg 1 05/30/12 16:04 127-18-44.5 Toluene ND ug/kg 1 05/30/12 16:04 108-88-34.5 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 16:04 87-61-64.5 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 16:04 120-82-14.5 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 16:04 71-55-64.5 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 16:04 79-00-54.5 Trichloroethene ND ug/kg 1 05/30/12 16:04 79-01-64.5 Trichlorofluoromethane ND ug/kg 1 05/30/12 16:04 75-69-44.5 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 16:04 96-18-44.5 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 16:04 95-63-64.5 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 16:04 108-67-84.5 Vinyl acetate ND ug/kg 1 05/30/12 16:04 108-05-489.0 Vinyl chloride ND ug/kg 1 05/30/12 16:04 75-01-44.5 Xylene (Total)ND ug/kg 1 05/30/12 16:04 1330-20-78.9 Surrogates Dibromofluoromethane (S)113 %.1 05/30/12 16:04 1868-53-771-125 Toluene-d8 (S)91 %.1 05/30/12 16:04 2037-26-576-124 4-Bromofluorobenzene (S)103 %.1 05/30/12 16:04 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.7 %1 05/30/12 18:040.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 8 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S160172 Lab ID:5063426003 Collected:05/23/12 10:25 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 16:42 67-64-192.1 Acrolein ND ug/kg 1 05/30/12 16:42 107-02-892.1 Acrylonitrile ND ug/kg 1 05/30/12 16:42 107-13-192.1 Benzene ND ug/kg 1 05/30/12 16:42 71-43-24.6 Bromobenzene ND ug/kg 1 05/30/12 16:42 108-86-14.6 Bromochloromethane ND ug/kg 1 05/30/12 16:42 74-97-54.6 Bromodichloromethane ND ug/kg 1 05/30/12 16:42 75-27-44.6 Bromoform ND ug/kg 1 05/30/12 16:42 75-25-24.6 Bromomethane ND ug/kg 1 05/30/12 16:42 74-83-94.6 2-Butanone (MEK)ND ug/kg 1 05/30/12 16:42 78-93-323.0 n-Butylbenzene ND ug/kg 1 05/30/12 16:42 104-51-84.6 sec-Butylbenzene ND ug/kg 1 05/30/12 16:42 135-98-84.6 tert-Butylbenzene ND ug/kg 1 05/30/12 16:42 98-06-64.6 Carbon disulfide ND ug/kg 1 05/30/12 16:42 75-15-09.2 Carbon tetrachloride ND ug/kg 1 05/30/12 16:42 56-23-54.6 Chlorobenzene ND ug/kg 1 05/30/12 16:42 108-90-74.6 Chloroethane ND ug/kg 1 05/30/12 16:42 75-00-34.6 Chloroform ND ug/kg 1 05/30/12 16:42 67-66-34.6 Chloromethane ND ug/kg 1 05/30/12 16:42 74-87-34.6 2-Chlorotoluene ND ug/kg 1 05/30/12 16:42 95-49-84.6 4-Chlorotoluene ND ug/kg 1 05/30/12 16:42 106-43-44.6 Dibromochloromethane ND ug/kg 1 05/30/12 16:42 124-48-14.6 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 16:42 106-93-44.6 Dibromomethane ND ug/kg 1 05/30/12 16:42 74-95-34.6 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 16:42 95-50-14.6 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 16:42 541-73-14.6 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 16:42 106-46-74.6 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 16:42 110-57-692.1 Dichlorodifluoromethane ND ug/kg 1 05/30/12 16:42 75-71-84.6 1,1-Dichloroethane ND ug/kg 1 05/30/12 16:42 75-34-34.6 1,2-Dichloroethane ND ug/kg 1 05/30/12 16:42 107-06-24.6 1,1-Dichloroethene ND ug/kg 1 05/30/12 16:42 75-35-44.6 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:42 156-59-24.6 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:42 156-60-54.6 1,2-Dichloropropane ND ug/kg 1 05/30/12 16:42 78-87-54.6 1,3-Dichloropropane ND ug/kg 1 05/30/12 16:42 142-28-94.6 2,2-Dichloropropane ND ug/kg 1 05/30/12 16:42 594-20-74.6 1,1-Dichloropropene ND ug/kg 1 05/30/12 16:42 563-58-64.6 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:42 10061-01-54.6 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:42 10061-02-64.6 Ethylbenzene ND ug/kg 1 05/30/12 16:42 100-41-44.6 Ethyl methacrylate ND ug/kg 1 05/30/12 16:42 97-63-292.1 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 16:42 87-68-34.6 n-Hexane ND ug/kg 1 05/30/12 16:42 110-54-3 N24.6 2-Hexanone ND ug/kg 1 05/30/12 16:42 591-78-692.1 Iodomethane ND ug/kg 1 05/30/12 16:42 74-88-492.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 9 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S160172 Lab ID:5063426003 Collected:05/23/12 10:25 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 16:42 98-82-84.6 p-Isopropyltoluene ND ug/kg 1 05/30/12 16:42 99-87-64.6 Methylene Chloride ND ug/kg 1 05/30/12 16:42 75-09-218.4 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 16:42 108-10-123.0 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 16:42 1634-04-44.6 Naphthalene ND ug/kg 1 05/30/12 16:42 91-20-34.6 n-Propylbenzene ND ug/kg 1 05/30/12 16:42 103-65-14.6 Styrene ND ug/kg 1 05/30/12 16:42 100-42-54.6 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:42 630-20-64.6 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:42 79-34-54.6 Tetrachloroethene ND ug/kg 1 05/30/12 16:42 127-18-44.6 Toluene ND ug/kg 1 05/30/12 16:42 108-88-34.6 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 16:42 87-61-64.6 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 16:42 120-82-14.6 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 16:42 71-55-64.6 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 16:42 79-00-54.6 Trichloroethene ND ug/kg 1 05/30/12 16:42 79-01-64.6 Trichlorofluoromethane ND ug/kg 1 05/30/12 16:42 75-69-44.6 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 16:42 96-18-44.6 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 16:42 95-63-64.6 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 16:42 108-67-84.6 Vinyl acetate ND ug/kg 1 05/30/12 16:42 108-05-492.1 Vinyl chloride ND ug/kg 1 05/30/12 16:42 75-01-44.6 Xylene (Total)ND ug/kg 1 05/30/12 16:42 1330-20-79.2 Surrogates Dibromofluoromethane (S)113 %.1 05/30/12 16:42 1868-53-771-125 Toluene-d8 (S)91 %.1 05/30/12 16:42 2037-26-576-124 4-Bromofluorobenzene (S)103 %.1 05/30/12 16:42 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.0 %1 05/30/12 18:050.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 10 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S160172A Lab ID:5063426004 Collected:05/23/12 10:25 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 17:19 67-64-188.9 Acrolein ND ug/kg 1 05/30/12 17:19 107-02-888.9 Acrylonitrile ND ug/kg 1 05/30/12 17:19 107-13-188.9 Benzene ND ug/kg 1 05/30/12 17:19 71-43-24.4 Bromobenzene ND ug/kg 1 05/30/12 17:19 108-86-14.4 Bromochloromethane ND ug/kg 1 05/30/12 17:19 74-97-54.4 Bromodichloromethane ND ug/kg 1 05/30/12 17:19 75-27-44.4 Bromoform ND ug/kg 1 05/30/12 17:19 75-25-24.4 Bromomethane ND ug/kg 1 05/30/12 17:19 74-83-94.4 2-Butanone (MEK)ND ug/kg 1 05/30/12 17:19 78-93-322.2 n-Butylbenzene ND ug/kg 1 05/30/12 17:19 104-51-84.4 sec-Butylbenzene ND ug/kg 1 05/30/12 17:19 135-98-84.4 tert-Butylbenzene ND ug/kg 1 05/30/12 17:19 98-06-64.4 Carbon disulfide ND ug/kg 1 05/30/12 17:19 75-15-08.9 Carbon tetrachloride ND ug/kg 1 05/30/12 17:19 56-23-54.4 Chlorobenzene ND ug/kg 1 05/30/12 17:19 108-90-74.4 Chloroethane ND ug/kg 1 05/30/12 17:19 75-00-34.4 Chloroform ND ug/kg 1 05/30/12 17:19 67-66-34.4 Chloromethane ND ug/kg 1 05/30/12 17:19 74-87-34.4 2-Chlorotoluene ND ug/kg 1 05/30/12 17:19 95-49-84.4 4-Chlorotoluene ND ug/kg 1 05/30/12 17:19 106-43-44.4 Dibromochloromethane ND ug/kg 1 05/30/12 17:19 124-48-14.4 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 17:19 106-93-44.4 Dibromomethane ND ug/kg 1 05/30/12 17:19 74-95-34.4 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 17:19 95-50-14.4 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 17:19 541-73-14.4 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 17:19 106-46-74.4 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 17:19 110-57-688.9 Dichlorodifluoromethane ND ug/kg 1 05/30/12 17:19 75-71-84.4 1,1-Dichloroethane ND ug/kg 1 05/30/12 17:19 75-34-34.4 1,2-Dichloroethane ND ug/kg 1 05/30/12 17:19 107-06-24.4 1,1-Dichloroethene ND ug/kg 1 05/30/12 17:19 75-35-44.4 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 17:19 156-59-24.4 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 17:19 156-60-54.4 1,2-Dichloropropane ND ug/kg 1 05/30/12 17:19 78-87-54.4 1,3-Dichloropropane ND ug/kg 1 05/30/12 17:19 142-28-94.4 2,2-Dichloropropane ND ug/kg 1 05/30/12 17:19 594-20-74.4 1,1-Dichloropropene ND ug/kg 1 05/30/12 17:19 563-58-64.4 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 17:19 10061-01-54.4 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 17:19 10061-02-64.4 Ethylbenzene ND ug/kg 1 05/30/12 17:19 100-41-44.4 Ethyl methacrylate ND ug/kg 1 05/30/12 17:19 97-63-288.9 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 17:19 87-68-34.4 n-Hexane ND ug/kg 1 05/30/12 17:19 110-54-3 N24.4 2-Hexanone ND ug/kg 1 05/30/12 17:19 591-78-688.9 Iodomethane ND ug/kg 1 05/30/12 17:19 74-88-488.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 11 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S160172A Lab ID:5063426004 Collected:05/23/12 10:25 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 17:19 98-82-84.4 p-Isopropyltoluene ND ug/kg 1 05/30/12 17:19 99-87-64.4 Methylene Chloride ND ug/kg 1 05/30/12 17:19 75-09-217.8 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 17:19 108-10-122.2 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 17:19 1634-04-44.4 Naphthalene ND ug/kg 1 05/30/12 17:19 91-20-34.4 n-Propylbenzene ND ug/kg 1 05/30/12 17:19 103-65-14.4 Styrene ND ug/kg 1 05/30/12 17:19 100-42-54.4 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 17:19 630-20-64.4 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 17:19 79-34-54.4 Tetrachloroethene ND ug/kg 1 05/30/12 17:19 127-18-44.4 Toluene ND ug/kg 1 05/30/12 17:19 108-88-34.4 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 17:19 87-61-64.4 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 17:19 120-82-14.4 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 17:19 71-55-64.4 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 17:19 79-00-54.4 Trichloroethene ND ug/kg 1 05/30/12 17:19 79-01-64.4 Trichlorofluoromethane ND ug/kg 1 05/30/12 17:19 75-69-44.4 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 17:19 96-18-44.4 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 17:19 95-63-64.4 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 17:19 108-67-84.4 Vinyl acetate ND ug/kg 1 05/30/12 17:19 108-05-488.9 Vinyl chloride ND ug/kg 1 05/30/12 17:19 75-01-44.4 Xylene (Total)ND ug/kg 1 05/30/12 17:19 1330-20-78.9 Surrogates Dibromofluoromethane (S)115 %.1 05/30/12 17:19 1868-53-771-125 Toluene-d8 (S)91 %.1 05/30/12 17:19 2037-26-576-124 4-Bromofluorobenzene (S)103 %.1 05/30/12 17:19 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.0 %1 05/30/12 18:050.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 12 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S180185 Lab ID:5063426005 Collected:05/23/12 10:29 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 17:57 67-64-186.0 Acrolein ND ug/kg 1 05/30/12 17:57 107-02-886.0 Acrylonitrile ND ug/kg 1 05/30/12 17:57 107-13-186.0 Benzene ND ug/kg 1 05/30/12 17:57 71-43-24.3 Bromobenzene ND ug/kg 1 05/30/12 17:57 108-86-14.3 Bromochloromethane ND ug/kg 1 05/30/12 17:57 74-97-54.3 Bromodichloromethane ND ug/kg 1 05/30/12 17:57 75-27-44.3 Bromoform ND ug/kg 1 05/30/12 17:57 75-25-24.3 Bromomethane ND ug/kg 1 05/30/12 17:57 74-83-94.3 2-Butanone (MEK)ND ug/kg 1 05/30/12 17:57 78-93-321.5 n-Butylbenzene ND ug/kg 1 05/30/12 17:57 104-51-84.3 sec-Butylbenzene ND ug/kg 1 05/30/12 17:57 135-98-84.3 tert-Butylbenzene ND ug/kg 1 05/30/12 17:57 98-06-64.3 Carbon disulfide ND ug/kg 1 05/30/12 17:57 75-15-08.6 Carbon tetrachloride ND ug/kg 1 05/30/12 17:57 56-23-54.3 Chlorobenzene ND ug/kg 1 05/30/12 17:57 108-90-74.3 Chloroethane ND ug/kg 1 05/30/12 17:57 75-00-34.3 Chloroform ND ug/kg 1 05/30/12 17:57 67-66-34.3 Chloromethane ND ug/kg 1 05/30/12 17:57 74-87-34.3 2-Chlorotoluene ND ug/kg 1 05/30/12 17:57 95-49-84.3 4-Chlorotoluene ND ug/kg 1 05/30/12 17:57 106-43-44.3 Dibromochloromethane ND ug/kg 1 05/30/12 17:57 124-48-14.3 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 17:57 106-93-44.3 Dibromomethane ND ug/kg 1 05/30/12 17:57 74-95-34.3 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 17:57 95-50-14.3 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 17:57 541-73-14.3 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 17:57 106-46-74.3 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 17:57 110-57-686.0 Dichlorodifluoromethane ND ug/kg 1 05/30/12 17:57 75-71-84.3 1,1-Dichloroethane ND ug/kg 1 05/30/12 17:57 75-34-34.3 1,2-Dichloroethane ND ug/kg 1 05/30/12 17:57 107-06-24.3 1,1-Dichloroethene ND ug/kg 1 05/30/12 17:57 75-35-44.3 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 17:57 156-59-24.3 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 17:57 156-60-54.3 1,2-Dichloropropane ND ug/kg 1 05/30/12 17:57 78-87-54.3 1,3-Dichloropropane ND ug/kg 1 05/30/12 17:57 142-28-94.3 2,2-Dichloropropane ND ug/kg 1 05/30/12 17:57 594-20-74.3 1,1-Dichloropropene ND ug/kg 1 05/30/12 17:57 563-58-64.3 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 17:57 10061-01-54.3 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 17:57 10061-02-64.3 Ethylbenzene ND ug/kg 1 05/30/12 17:57 100-41-44.3 Ethyl methacrylate ND ug/kg 1 05/30/12 17:57 97-63-286.0 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 17:57 87-68-34.3 n-Hexane ND ug/kg 1 05/30/12 17:57 110-54-3 N24.3 2-Hexanone ND ug/kg 1 05/30/12 17:57 591-78-686.0 Iodomethane ND ug/kg 1 05/30/12 17:57 74-88-486.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 13 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:AMW4D:S180185 Lab ID:5063426005 Collected:05/23/12 10:29 Received:05/24/12 09:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 17:57 98-82-84.3 p-Isopropyltoluene ND ug/kg 1 05/30/12 17:57 99-87-64.3 Methylene Chloride ND ug/kg 1 05/30/12 17:57 75-09-217.2 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 17:57 108-10-121.5 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 17:57 1634-04-44.3 Naphthalene ND ug/kg 1 05/30/12 17:57 91-20-34.3 n-Propylbenzene ND ug/kg 1 05/30/12 17:57 103-65-14.3 Styrene ND ug/kg 1 05/30/12 17:57 100-42-54.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 17:57 630-20-64.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 17:57 79-34-54.3 Tetrachloroethene ND ug/kg 1 05/30/12 17:57 127-18-44.3 Toluene ND ug/kg 1 05/30/12 17:57 108-88-34.3 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 17:57 87-61-64.3 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 17:57 120-82-14.3 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 17:57 71-55-64.3 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 17:57 79-00-54.3 Trichloroethene ND ug/kg 1 05/30/12 17:57 79-01-64.3 Trichlorofluoromethane ND ug/kg 1 05/30/12 17:57 75-69-44.3 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 17:57 96-18-44.3 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 17:57 95-63-64.3 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 17:57 108-67-84.3 Vinyl acetate ND ug/kg 1 05/30/12 17:57 108-05-486.0 Vinyl chloride ND ug/kg 1 05/30/12 17:57 75-01-44.3 Xylene (Total)ND ug/kg 1 05/30/12 17:57 1330-20-78.6 Surrogates Dibromofluoromethane (S)115 %.1 05/30/12 17:57 1868-53-771-125 Toluene-d8 (S)91 %.1 05/30/12 17:57 2037-26-576-124 4-Bromofluorobenzene (S)103 %.1 05/30/12 17:57 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 05/30/12 18:050.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 14 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:FB-3:W052312 Lab ID:5063426006 Collected:05/23/12 12:00 Received:05/24/12 09:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 05/30/12 18:16 67-64-1100 Acrolein ND ug/L 1 05/30/12 18:16 107-02-8100 Acrylonitrile ND ug/L 1 05/30/12 18:16 107-13-1100 Benzene ND ug/L 1 05/30/12 18:16 71-43-25.0 Bromobenzene ND ug/L 1 05/30/12 18:16 108-86-15.0 Bromochloromethane ND ug/L 1 05/30/12 18:16 74-97-55.0 Bromodichloromethane ND ug/L 1 05/30/12 18:16 75-27-45.0 Bromoform ND ug/L 1 05/30/12 18:16 75-25-25.0 Bromomethane ND ug/L 1 05/30/12 18:16 74-83-95.0 2-Butanone (MEK)ND ug/L 1 05/30/12 18:16 78-93-325.0 n-Butylbenzene ND ug/L 1 05/30/12 18:16 104-51-85.0 sec-Butylbenzene ND ug/L 1 05/30/12 18:16 135-98-85.0 tert-Butylbenzene ND ug/L 1 05/30/12 18:16 98-06-65.0 Carbon disulfide ND ug/L 1 05/30/12 18:16 75-15-010.0 Carbon tetrachloride ND ug/L 1 05/30/12 18:16 56-23-55.0 Chlorobenzene ND ug/L 1 05/30/12 18:16 108-90-75.0 Chloroethane ND ug/L 1 05/30/12 18:16 75-00-35.0 Chloroform 10.8 ug/L 1 05/30/12 18:16 67-66-3 1d5.0 Chloromethane ND ug/L 1 05/30/12 18:16 74-87-35.0 2-Chlorotoluene ND ug/L 1 05/30/12 18:16 95-49-85.0 4-Chlorotoluene ND ug/L 1 05/30/12 18:16 106-43-45.0 Dibromochloromethane ND ug/L 1 05/30/12 18:16 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 05/30/12 18:16 106-93-45.0 Dibromomethane ND ug/L 1 05/30/12 18:16 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 05/30/12 18:16 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 05/30/12 18:16 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 05/30/12 18:16 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 05/30/12 18:16 110-57-6100 Dichlorodifluoromethane ND ug/L 1 05/30/12 18:16 75-71-85.0 1,1-Dichloroethane ND ug/L 1 05/30/12 18:16 75-34-35.0 1,2-Dichloroethane ND ug/L 1 05/30/12 18:16 107-06-25.0 1,1-Dichloroethene ND ug/L 1 05/30/12 18:16 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 05/30/12 18:16 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 05/30/12 18:16 156-60-55.0 1,2-Dichloropropane ND ug/L 1 05/30/12 18:16 78-87-55.0 1,3-Dichloropropane ND ug/L 1 05/30/12 18:16 142-28-95.0 2,2-Dichloropropane ND ug/L 1 05/30/12 18:16 594-20-75.0 1,1-Dichloropropene ND ug/L 1 05/30/12 18:16 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 05/30/12 18:16 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 05/30/12 18:16 10061-02-65.0 Ethylbenzene ND ug/L 1 05/30/12 18:16 100-41-45.0 Ethyl methacrylate ND ug/L 1 05/30/12 18:16 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 05/30/12 18:16 87-68-35.0 n-Hexane ND ug/L 1 05/30/12 18:16 110-54-3 N25.0 2-Hexanone ND ug/L 1 05/30/12 18:16 591-78-625.0 Iodomethane ND ug/L 1 05/30/12 18:16 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 05/30/12 18:16 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 15 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063426 SBI068 Sample:SBI068:FB-3:W052312 Lab ID:5063426006 Collected:05/23/12 12:00 Received:05/24/12 09:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 05/30/12 18:16 99-87-65.0 Methylene Chloride ND ug/L 1 05/30/12 18:16 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/30/12 18:16 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 05/30/12 18:16 1634-04-44.0 Naphthalene ND ug/L 1 05/30/12 18:16 91-20-35.0 n-Propylbenzene ND ug/L 1 05/30/12 18:16 103-65-15.0 Styrene ND ug/L 1 05/30/12 18:16 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 05/30/12 18:16 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 05/30/12 18:16 79-34-55.0 Tetrachloroethene ND ug/L 1 05/30/12 18:16 127-18-45.0 Toluene ND ug/L 1 05/30/12 18:16 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 05/30/12 18:16 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 05/30/12 18:16 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 05/30/12 18:16 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 05/30/12 18:16 79-00-55.0 Trichloroethene ND ug/L 1 05/30/12 18:16 79-01-65.0 Trichlorofluoromethane ND ug/L 1 05/30/12 18:16 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 05/30/12 18:16 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 05/30/12 18:16 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 05/30/12 18:16 108-67-85.0 Vinyl acetate ND ug/L 1 05/30/12 18:16 108-05-450.0 Vinyl chloride ND ug/L 1 05/30/12 18:16 75-01-42.0 Xylene (Total)ND ug/L 1 05/30/12 18:16 1330-20-710.0 Surrogates Dibromofluoromethane (S)118 %.1 05/30/12 18:16 1868-53-783-123 4-Bromofluorobenzene (S)104 %.1 05/30/12 18:16 460-00-472-125 Toluene-d8 (S)94 %.1 05/30/12 18:16 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 16 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42590 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5063426006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:742010 Associated Lab Samples:5063426006 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/30/12 15:08 1,1,1-Trichloroethane ug/L ND 5.0 05/30/12 15:08 1,1,2,2-Tetrachloroethane ug/L ND 5.0 05/30/12 15:08 1,1,2-Trichloroethane ug/L ND 5.0 05/30/12 15:08 1,1-Dichloroethane ug/L ND 5.0 05/30/12 15:08 1,1-Dichloroethene ug/L ND 5.0 05/30/12 15:08 1,1-Dichloropropene ug/L ND 5.0 05/30/12 15:08 1,2,3-Trichlorobenzene ug/L ND 5.0 05/30/12 15:08 1,2,3-Trichloropropane ug/L ND 5.0 05/30/12 15:08 1,2,4-Trichlorobenzene ug/L ND 5.0 05/30/12 15:08 1,2,4-Trimethylbenzene ug/L ND 5.0 05/30/12 15:08 1,2-Dibromoethane (EDB)ug/L ND 5.0 05/30/12 15:08 1,2-Dichlorobenzene ug/L ND 5.0 05/30/12 15:08 1,2-Dichloroethane ug/L ND 5.0 05/30/12 15:08 1,2-Dichloropropane ug/L ND 5.0 05/30/12 15:08 1,3,5-Trimethylbenzene ug/L ND 5.0 05/30/12 15:08 1,3-Dichlorobenzene ug/L ND 5.0 05/30/12 15:08 1,3-Dichloropropane ug/L ND 5.0 05/30/12 15:08 1,4-Dichlorobenzene ug/L ND 5.0 05/30/12 15:08 2,2-Dichloropropane ug/L ND 5.0 05/30/12 15:08 2-Butanone (MEK)ug/L ND 25.0 05/30/12 15:08 2-Chlorotoluene ug/L ND 5.0 05/30/12 15:08 2-Hexanone ug/L ND 25.0 05/30/12 15:08 4-Chlorotoluene ug/L ND 5.0 05/30/12 15:08 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 05/30/12 15:08 Acetone ug/L ND 100 05/30/12 15:08 Acrolein ug/L ND 100 05/30/12 15:08 Acrylonitrile ug/L ND 100 05/30/12 15:08 Benzene ug/L ND 5.0 05/30/12 15:08 Bromobenzene ug/L ND 5.0 05/30/12 15:08 Bromochloromethane ug/L ND 5.0 05/30/12 15:08 Bromodichloromethane ug/L ND 5.0 05/30/12 15:08 Bromoform ug/L ND 5.0 05/30/12 15:08 Bromomethane ug/L ND 5.0 05/30/12 15:08 Carbon disulfide ug/L ND 10.0 05/30/12 15:08 Carbon tetrachloride ug/L ND 5.0 05/30/12 15:08 Chlorobenzene ug/L ND 5.0 05/30/12 15:08 Chloroethane ug/L ND 5.0 05/30/12 15:08 Chloroform ug/L ND 5.0 05/30/12 15:08 Chloromethane ug/L ND 5.0 05/30/12 15:08 cis-1,2-Dichloroethene ug/L ND 5.0 05/30/12 15:08 cis-1,3-Dichloropropene ug/L ND 5.0 05/30/12 15:08 Dibromochloromethane ug/L ND 5.0 05/30/12 15:08 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 17 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:742010 Associated Lab Samples:5063426006 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 05/30/12 15:08 Dichlorodifluoromethane ug/L ND 5.0 05/30/12 15:08 Ethyl methacrylate ug/L ND 100 05/30/12 15:08 Ethylbenzene ug/L ND 5.0 05/30/12 15:08 Hexachloro-1,3-butadiene ug/L ND 5.0 05/30/12 15:08 Iodomethane ug/L ND 10.0 05/30/12 15:08 Isopropylbenzene (Cumene)ug/L ND 5.0 05/30/12 15:08 Methyl-tert-butyl ether ug/L ND 4.0 05/30/12 15:08 Methylene Chloride ug/L ND 5.0 05/30/12 15:08 n-Butylbenzene ug/L ND 5.0 05/30/12 15:08 n-Hexane ug/L ND 5.0 N205/30/12 15:08 n-Propylbenzene ug/L ND 5.0 05/30/12 15:08 Naphthalene ug/L ND 5.0 05/30/12 15:08 p-Isopropyltoluene ug/L ND 5.0 05/30/12 15:08 sec-Butylbenzene ug/L ND 5.0 05/30/12 15:08 Styrene ug/L ND 5.0 05/30/12 15:08 tert-Butylbenzene ug/L ND 5.0 05/30/12 15:08 Tetrachloroethene ug/L ND 5.0 05/30/12 15:08 Toluene ug/L ND 5.0 05/30/12 15:08 trans-1,2-Dichloroethene ug/L ND 5.0 05/30/12 15:08 trans-1,3-Dichloropropene ug/L ND 5.0 05/30/12 15:08 trans-1,4-Dichloro-2-butene ug/L ND 100 05/30/12 15:08 Trichloroethene ug/L ND 5.0 05/30/12 15:08 Trichlorofluoromethane ug/L ND 5.0 05/30/12 15:08 Vinyl acetate ug/L ND 50.0 05/30/12 15:08 Vinyl chloride ug/L ND 2.0 05/30/12 15:08 Xylene (Total)ug/L ND 10.0 05/30/12 15:08 4-Bromofluorobenzene (S)%.102 72-125 05/30/12 15:08 Dibromofluoromethane (S)%.109 83-123 05/30/12 15:08 Toluene-d8 (S)%.95 81-114 05/30/12 15:08 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742011LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 52.050 104 69-122 1,1,1-Trichloroethane ug/L 50.950 102 69-126 1,1,2,2-Tetrachloroethane ug/L 48.050 96 68-134 1,1,2-Trichloroethane ug/L 54.950 110 77-129 1,1-Dichloroethane ug/L 50.950 102 70-127 1,1-Dichloroethene ug/L 54.450 109 75-145 1,1-Dichloropropene ug/L 56.850 114 75-126 1,2,3-Trichlorobenzene ug/L 49.850 100 63-130 1,2,3-Trichloropropane ug/L 99.8 L35020045-121 1,2,4-Trichlorobenzene ug/L 51.150 102 64-122 1,2,4-Trimethylbenzene ug/L 50.750 101 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 18 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742011LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 53.350 107 77-123 1,2-Dichlorobenzene ug/L 49.650 99 74-123 1,2-Dichloroethane ug/L 53.050 106 71-127 1,2-Dichloropropane ug/L 53.550 107 75-126 1,3,5-Trimethylbenzene ug/L 52.250 104 69-129 1,3-Dichlorobenzene ug/L 50.250 100 76-123 1,3-Dichloropropane ug/L 51.350 103 77-126 1,4-Dichlorobenzene ug/L 49.350 99 77-121 2,2-Dichloropropane ug/L 51.150 102 45-138 2-Butanone (MEK)ug/L 262250 105 42-177 2-Chlorotoluene ug/L 50.450 101 74-129 2-Hexanone ug/L 253250 101 57-162 4-Chlorotoluene ug/L 52.250 104 70-125 4-Methyl-2-pentanone (MIBK)ug/L 236250 94 64-135 Acetone ug/L 294250 118 10-200 Acrolein ug/L 12801000 128 10-200 Acrylonitrile ug/L 10301000 103 59-144 Benzene ug/L 53.150 106 76-123 Bromobenzene ug/L 48.550 97 67-130 Bromochloromethane ug/L 50.350 101 58-153 Bromodichloromethane ug/L 50.950 102 71-124 Bromoform ug/L 44.050 88 64-116 Bromomethane ug/L 51.250 102 23-197 Carbon disulfide ug/L 109100 109 55-146 Carbon tetrachloride ug/L 53.650 107 65-125 Chlorobenzene ug/L 50.650 101 78-120 Chloroethane ug/L 49.550 99 56-163 Chloroform ug/L 53.350 107 73-122 Chloromethane ug/L 42.150 84 46-146 cis-1,2-Dichloroethene ug/L 52.250 104 79-129 cis-1,3-Dichloropropene ug/L 53.350 107 66-123 Dibromochloromethane ug/L 50.550 101 70-123 Dibromomethane ug/L 51.050 102 73-123 Dichlorodifluoromethane ug/L 42.150 84 19-200 Ethyl methacrylate ug/L 214200 107 70-127 Ethylbenzene ug/L 51.750 103 75-120 Hexachloro-1,3-butadiene ug/L 53.350 107 64-131 Iodomethane ug/L 114100 114 16-181 Isopropylbenzene (Cumene)ug/L 50.150 100 73-123 Methyl-tert-butyl ether ug/L 102100 102 66-128 Methylene Chloride ug/L 55.350 111 61-138 n-Butylbenzene ug/L 54.150 108 69-130 n-Hexane ug/L 50.7 N25010167-142 n-Propylbenzene ug/L 51.250 102 71-132 Naphthalene ug/L 45.850 92 62-130 p-Isopropyltoluene ug/L 54.950 110 71-126 sec-Butylbenzene ug/L 50.750 101 69-130 Styrene ug/L 52.550 105 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 19 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742011LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 39.850 80 49-114 Tetrachloroethene ug/L 40.250 80 57-125 Toluene ug/L 49.150 98 72-124 trans-1,2-Dichloroethene ug/L 51.150 102 71-145 trans-1,3-Dichloropropene ug/L 50.250 100 58-118 trans-1,4-Dichloro-2-butene ug/L 215200 107 50-121 Trichloroethene ug/L 53.850 108 77-122 Trichlorofluoromethane ug/L 50.850 102 56-159 Vinyl acetate ug/L 225200 113 27-119 Vinyl chloride ug/L 42.150 84 61-146 Xylene (Total)ug/L 150150 100 72-126 4-Bromofluorobenzene (S)%.98 72-125 Dibromofluoromethane (S)%.96 83-123 Toluene-d8 (S)%.101 81-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 20 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42592 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063426001, 5063426002, 5063426003, 5063426004, 5063426005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:742016 Associated Lab Samples:5063426001, 5063426002, 5063426003, 5063426004, 5063426005 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/30/12 14:49 1,1,1-Trichloroethane ug/kg ND 5.0 05/30/12 14:49 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/30/12 14:49 1,1,2-Trichloroethane ug/kg ND 5.0 05/30/12 14:49 1,1-Dichloroethane ug/kg ND 5.0 05/30/12 14:49 1,1-Dichloroethene ug/kg ND 5.0 05/30/12 14:49 1,1-Dichloropropene ug/kg ND 5.0 05/30/12 14:49 1,2,3-Trichlorobenzene ug/kg ND 5.0 05/30/12 14:49 1,2,3-Trichloropropane ug/kg ND 5.0 05/30/12 14:49 1,2,4-Trichlorobenzene ug/kg ND 5.0 05/30/12 14:49 1,2,4-Trimethylbenzene ug/kg ND 5.0 05/30/12 14:49 1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/30/12 14:49 1,2-Dichlorobenzene ug/kg ND 5.0 05/30/12 14:49 1,2-Dichloroethane ug/kg ND 5.0 05/30/12 14:49 1,2-Dichloropropane ug/kg ND 5.0 05/30/12 14:49 1,3,5-Trimethylbenzene ug/kg ND 5.0 05/30/12 14:49 1,3-Dichlorobenzene ug/kg ND 5.0 05/30/12 14:49 1,3-Dichloropropane ug/kg ND 5.0 05/30/12 14:49 1,4-Dichlorobenzene ug/kg ND 5.0 05/30/12 14:49 2,2-Dichloropropane ug/kg ND 5.0 05/30/12 14:49 2-Butanone (MEK)ug/kg ND 25.0 05/30/12 14:49 2-Chlorotoluene ug/kg ND 5.0 05/30/12 14:49 2-Hexanone ug/kg ND 100 05/30/12 14:49 4-Chlorotoluene ug/kg ND 5.0 05/30/12 14:49 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 05/30/12 14:49 Acetone ug/kg ND 100 05/30/12 14:49 Acrolein ug/kg ND 100 05/30/12 14:49 Acrylonitrile ug/kg ND 100 05/30/12 14:49 Benzene ug/kg ND 5.0 05/30/12 14:49 Bromobenzene ug/kg ND 5.0 05/30/12 14:49 Bromochloromethane ug/kg ND 5.0 05/30/12 14:49 Bromodichloromethane ug/kg ND 5.0 05/30/12 14:49 Bromoform ug/kg ND 5.0 05/30/12 14:49 Bromomethane ug/kg ND 5.0 05/30/12 14:49 Carbon disulfide ug/kg ND 10.0 05/30/12 14:49 Carbon tetrachloride ug/kg ND 5.0 05/30/12 14:49 Chlorobenzene ug/kg ND 5.0 05/30/12 14:49 Chloroethane ug/kg ND 5.0 05/30/12 14:49 Chloroform ug/kg ND 5.0 05/30/12 14:49 Chloromethane ug/kg ND 5.0 05/30/12 14:49 cis-1,2-Dichloroethene ug/kg ND 5.0 05/30/12 14:49 cis-1,3-Dichloropropene ug/kg ND 5.0 05/30/12 14:49 Dibromochloromethane ug/kg ND 5.0 05/30/12 14:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 21 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:742016 Associated Lab Samples:5063426001, 5063426002, 5063426003, 5063426004, 5063426005 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 05/30/12 14:49 Dichlorodifluoromethane ug/kg ND 5.0 05/30/12 14:49 Ethyl methacrylate ug/kg ND 100 05/30/12 14:49 Ethylbenzene ug/kg ND 5.0 05/30/12 14:49 Hexachloro-1,3-butadiene ug/kg ND 5.0 05/30/12 14:49 Iodomethane ug/kg ND 100 05/30/12 14:49 Isopropylbenzene (Cumene)ug/kg ND 5.0 05/30/12 14:49 Methyl-tert-butyl ether ug/kg ND 5.0 05/30/12 14:49 Methylene Chloride ug/kg ND 20.0 05/30/12 14:49 n-Butylbenzene ug/kg ND 5.0 05/30/12 14:49 n-Hexane ug/kg ND 5.0 N205/30/12 14:49 n-Propylbenzene ug/kg ND 5.0 05/30/12 14:49 Naphthalene ug/kg ND 5.0 05/30/12 14:49 p-Isopropyltoluene ug/kg ND 5.0 05/30/12 14:49 sec-Butylbenzene ug/kg ND 5.0 05/30/12 14:49 Styrene ug/kg ND 5.0 05/30/12 14:49 tert-Butylbenzene ug/kg ND 5.0 05/30/12 14:49 Tetrachloroethene ug/kg ND 5.0 05/30/12 14:49 Toluene ug/kg ND 5.0 05/30/12 14:49 trans-1,2-Dichloroethene ug/kg ND 5.0 05/30/12 14:49 trans-1,3-Dichloropropene ug/kg ND 5.0 05/30/12 14:49 trans-1,4-Dichloro-2-butene ug/kg ND 100 05/30/12 14:49 Trichloroethene ug/kg ND 5.0 05/30/12 14:49 Trichlorofluoromethane ug/kg ND 5.0 05/30/12 14:49 Vinyl acetate ug/kg ND 100 05/30/12 14:49 Vinyl chloride ug/kg ND 5.0 05/30/12 14:49 Xylene (Total)ug/kg ND 10.0 05/30/12 14:49 4-Bromofluorobenzene (S)%.103 67-134 05/30/12 14:49 Dibromofluoromethane (S)%.107 71-125 05/30/12 14:49 Toluene-d8 (S)%.92 76-124 05/30/12 14:49 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742017LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 44.650 89 68-125 1,1,1-Trichloroethane ug/kg 48.850 98 63-124 1,1,2,2-Tetrachloroethane ug/kg 40.650 81 73-123 1,1,2-Trichloroethane ug/kg 49.150 98 70-124 1,1-Dichloroethane ug/kg 45.250 90 63-122 1,1-Dichloroethene ug/kg 56.150 112 71-129 1,1-Dichloropropene ug/kg 51.550 103 71-122 1,2,3-Trichlorobenzene ug/kg 46.350 93 68-123 1,2,3-Trichloropropane ug/kg 83.8 L35016847-117 1,2,4-Trichlorobenzene ug/kg 45.550 91 68-125 1,2,4-Trimethylbenzene ug/kg 36.450 73 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 22 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742017LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 47.050 94 67-121 1,2-Dichlorobenzene ug/kg 38.950 78 71-121 1,2-Dichloroethane ug/kg 46.950 94 74-120 1,2-Dichloropropane ug/kg 45.350 91 71-117 1,3,5-Trimethylbenzene ug/kg 35.950 72 64-119 1,3-Dichlorobenzene ug/kg 43.650 87 70-122 1,3-Dichloropropane ug/kg 43.750 87 68-118 1,4-Dichlorobenzene ug/kg 45.050 90 71-118 2,2-Dichloropropane ug/kg 48.050 96 62-119 2-Butanone (MEK)ug/kg 226250 90 38-154 2-Chlorotoluene ug/kg 37.050 74 71-120 2-Hexanone ug/kg 209250 84 50-134 4-Chlorotoluene ug/kg 42.650 85 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 200250 80 66-122 Acetone ug/kg 312250 125 10-200 Acrolein ug/kg 12101000 121 11-200 Acrylonitrile ug/kg 9071000 91 66-120 Benzene ug/kg 46.150 92 73-115 Bromobenzene ug/kg 42.350 85 64-130 Bromochloromethane ug/kg 46.850 94 71-127 Bromodichloromethane ug/kg 44.550 89 60-121 Bromoform ug/kg 43.450 87 44-130 Bromomethane ug/kg 86.550 173 48-175 Carbon disulfide ug/kg 109100 109 71-126 Carbon tetrachloride ug/kg 52.450 105 57-127 Chlorobenzene ug/kg 43.450 87 72-121 Chloroethane ug/kg 48.750 97 72-141 Chloroform ug/kg 48.250 96 74-114 Chloromethane ug/kg 45.950 92 51-126 cis-1,2-Dichloroethene ug/kg 47.550 95 72-115 cis-1,3-Dichloropropene ug/kg 47.650 95 64-115 Dibromochloromethane ug/kg 47.850 96 58-114 Dibromomethane ug/kg 46.550 93 73-120 Dichlorodifluoromethane ug/kg 59.750 119 32-167 Ethyl methacrylate ug/kg 165200 83 65-117 Ethylbenzene ug/kg 42.250 84 73-120 Hexachloro-1,3-butadiene ug/kg 36.250 72 65-121 Iodomethane ug/kg 111100 111 45-156 Isopropylbenzene (Cumene)ug/kg 39.250 78 74-123 Methyl-tert-butyl ether ug/kg 90.1100 90 69-123 Methylene Chloride ug/kg 70.6 L35014158-124 n-Butylbenzene ug/kg 35.550 71 71-118 n-Hexane ug/kg 44.6 N2508950-106 n-Propylbenzene ug/kg 39.350 79 70-120 Naphthalene ug/kg 47.750 95 67-124 p-Isopropyltoluene ug/kg 35.450 71 71-123 sec-Butylbenzene ug/kg 34.850 70 66-122 Styrene ug/kg 44.550 89 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 23 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 742017LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 26.6 L0505354-124 Tetrachloroethene ug/kg 38.350 77 66-126 Toluene ug/kg 42.850 86 69-115 trans-1,2-Dichloroethene ug/kg 49.650 99 69-120 trans-1,3-Dichloropropene ug/kg 50.450 101 61-116 trans-1,4-Dichloro-2-butene ug/kg 170200 85 59-130 Trichloroethene ug/kg 47.450 95 71-117 Trichlorofluoromethane ug/kg 67.250 134 67-138 Vinyl acetate ug/kg 228200 114 35-134 Vinyl chloride ug/kg 51.050 102 64-127 Xylene (Total)ug/kg 127150 85 69-117 4-Bromofluorobenzene (S)%.95 67-134 Dibromofluoromethane (S)%.103 71-125 Toluene-d8 (S)%.99 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 742018MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063426005 742019 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 42.9 99 10-111103 8 2044.8ND 42.4 46.0 1,1,1-Trichloroethane ug/kg 42.9 115 36-128119 7 2044.8ND 49.4 53.3 1,1,2,2-Tetrachloroethane ug/kg 42.9 91 10-13092 6 2044.8ND 39.0 41.4 1,1,2-Trichloroethane ug/kg 42.9 115 10-126120 9 2044.8ND 49.5 54.0 1,1-Dichloroethane ug/kg 42.9 109 39-126112 8 2044.8ND 46.6 50.3 1,1-Dichloroethene ug/kg 42.9 140 42-147145 8 2044.8ND 60.2 65.0 1,1-Dichloropropene ug/kg 42.9 120 29-129121 6 2044.8ND 51.3 54.3 1,2,3-Trichlorobenzene ug/kg 42.9 62 10-9161 2 2044.8ND 26.8 27.3 1,2,3-Trichloropropane ug/kg 42.9 183 10-99188 7 2044.8ND 78.5 84.2 1,2,4-Trichlorobenzene ug/kg 42.9 61 10-8859 .4 2044.8ND 26.4 26.3 1,2,4-Trimethylbenzene ug/kg 42.9 62 10-10961 1 2044.8ND 26.8 27.1 1,2-Dibromoethane (EDB)ug/kg 42.9 109 10-119114 8 2044.8ND 47.0 50.9 1,2-Dichlorobenzene ug/kg 42.9 66 10-10466 5 2044.8ND 28.3 29.7 1,2-Dichloroethane ug/kg 42.9 114 19-126115 5 2044.8ND 48.9 51.5 1,2-Dichloropropane ug/kg 42.9 105 24-123108 7 2044.8ND 45.1 48.2 1,3,5-Trimethylbenzene ug/kg 42.9 64 10-11862 2 2044.8ND 27.4 27.9 1,3-Dichlorobenzene ug/kg 42.9 74 10-10873 3 2044.8ND 31.7 32.7 1,3-Dichloropropane ug/kg 42.9 102 12-121107 9 2044.8ND 43.7 47.9 1,4-Dichlorobenzene ug/kg 42.9 75 10-10474 3 2044.8ND 32.0 33.0 2,2-Dichloropropane ug/kg 42.9 116 32-124120 8 2044.8ND 49.8 53.7 2-Butanone (MEK)ug/kg 215 103 10-183105 7 20224ND221236 2-Chlorotoluene ug/kg 42.9 74 10-12874 4 2044.8ND 31.7 33.1 2-Hexanone ug/kg 215 94 10-15897 7 20224ND202217 4-Chlorotoluene ug/kg 42.9 74 10-11973 3 2044.8ND 31.6 32.7 4-Methyl-2-pentanone (MIBK)ug/kg 215 93 12-13095 6 20224ND199212 Acetone ug/kg 215 149 10-200154 7 20224ND320344 Acrolein ug/kg 859 134 10-200136 6 20897ND11501220 Acrylonitrile ug/kg 859 105 19-130107 6 20897ND905959 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 24 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 742018MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063426005 742019 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 42.9 106 23-138109 7 2044.8ND 45.5 48.7 Bromobenzene ug/kg 42.9 81 10-11180 4 2044.8ND 34.6 36.0 Bromochloromethane ug/kg 42.9 109 26-126101 4 2044.8ND 46.8 45.1 Bromodichloromethane ug/kg 42.9 105 10-120106 6 2044.8ND 45.0 47.5 Bromoform ug/kg 42.9 98 10-106100 7 2044.8ND 42.0 45.0 Bromomethane ug/kg 42.9 252 10-190294 20 2044.8ND 108 132 Carbon disulfide ug/kg 85.9 129 31-128134 8 2089.7ND 111 120 Carbon tetrachloride ug/kg 42.9 124 26-126128 7 2044.8ND 53.4 57.4 Chlorobenzene ug/kg 42.9 88 10-12091 7 2044.8ND 37.8 40.6 Chloroethane ug/kg 42.9 121 18-186127 10 2044.8ND 51.8 57.1 Chloroform ug/kg 42.9 114 29-126117 7 2044.8ND 49.0 52.6 Chloromethane ug/kg 42.9 106 34-131114 11 2044.8ND 45.6 51.0 cis-1,2-Dichloroethene ug/kg 42.9 112 28-132116 8 2044.8ND 48.1 52.1 cis-1,3-Dichloropropene ug/kg 42.9 109 10-108115 9 2044.8ND 47.0 51.5 Dibromochloromethane ug/kg 42.9 111 10-108116 9 2044.8ND 47.5 51.9 Dibromomethane ug/kg 42.9 110 13-122114 8 2044.8ND 47.4 51.1 Dichlorodifluoromethane ug/kg 42.9 151 10-197158 9 2044.8ND 64.7 70.9 Ethyl methacrylate ug/kg 172 96 10-13099 7 20180ND165178 Ethylbenzene ug/kg 42.9 83 10-13585 7 2044.8ND 35.6 38.1 Hexachloro-1,3-butadiene ug/kg 42.9 43 10-10539 7 2044.8ND 18.6 17.3 Iodomethane ug/kg 85.9 136 10-163142 8 2089.7ND 117 127 Isopropylbenzene (Cumene)ug/kg 42.9 73 10-12174 5 2044.8ND 31.5 33.2 Methyl-tert-butyl ether ug/kg 85.9 109 20-140112 7 2089.7ND 93.9 101 Methylene Chloride ug/kg 42.9 129 28-131134 7 2044.8ND 56.4 60.7 n-Butylbenzene ug/kg 42.9 51 10-11047 5 2044.8ND 22.0 21.0 n-Hexane ug/kg N242.9 106 21-150110 8 2044.8ND 45.5 49.3 n-Propylbenzene ug/kg 42.9 69 10-12367 2 2044.8ND 29.6 30.2 Naphthalene ug/kg 42.9 79 10-10682 8 2044.8ND 34.0 36.9 p-Isopropyltoluene ug/kg 42.9 58 10-11755 .6 2044.8ND 24.7 24.6 sec-Butylbenzene ug/kg 42.9 60 10-12358 1 2044.8ND 25.6 25.9 Styrene ug/kg 42.9 86 10-11987 6 2044.8ND 36.9 39.2 tert-Butylbenzene ug/kg 42.9 49 10-10558 20 2044.8ND 21.2 25.9 Tetrachloroethene ug/kg 42.9 82 10-12283 5 2044.8ND 35.1 37.1 Toluene ug/kg 42.9 93 10-13196 7 2044.8ND 40.1 43.1 trans-1,2-Dichloroethene ug/kg 42.9 116 32-136120 8 2044.8ND 49.8 53.8 trans-1,3-Dichloropropene ug/kg 42.9 114 10-101119 9 2044.8ND 48.9 53.2 trans-1,4-Dichloro-2-butene ug/kg 172 94 10-10495 6 20180ND161171 Trichloroethene ug/kg 42.9 108 15-133109 5 2044.8ND 46.4 48.8 Trichlorofluoromethane ug/kg 42.9 171 37-152178 8 2044.8ND 73.3 79.7 Vinyl acetate ug/kg 172 103 10-103117 17 20180ND178210 Vinyl chloride ug/kg 42.9 124 41-147129 8 2044.8ND 53.4 57.9 Xylene (Total)ug/kg 128 82 10-13183 5 20135ND106112 4-Bromofluorobenzene (S)%.95 67-13494 20 Dibromofluoromethane (S)%.2d10471-125104 20 Toluene-d8 (S)%.100 76-124102 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 25 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063426 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/7088 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5063426001, 5063426002, 5063426003, 5063426004, 5063426005 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063310049 741894SAMPLE DUPLICATE: Percent Moisture %16.2 .7 516.3 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063426005 741895SAMPLE DUPLICATE: Percent Moisture %6.2 5 56.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 26 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5063426 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Compound commonly found in commercially distributed water. JLZ 05/31/12.1d Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits for several compounds. RSW 05/31/122d Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 The lab does not hold TNI accreditation for this parameter.N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 27 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5063426 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5063426006 MSV/42590SBI068:FB-3:W052312 EPA 8260 5063426001 MSV/42592SBI068:AMW8I:S040049 EPA 8260 5063426002 MSV/42592SBI068:AMW8I:S200205 EPA 8260 5063426003 MSV/42592SBI068:AMW4D:S160172 EPA 8260 5063426004 MSV/42592SBI068:AMW4D:S160172A EPA 8260 5063426005 MSV/42592SBI068:AMW4D:S180185 EPA 8260 5063426001 PMST/7088SBI068:AMW8I:S040049 ASTM D2974-87 5063426002 PMST/7088SBI068:AMW8I:S200205 ASTM D2974-87 5063426003 PMST/7088SBI068:AMW4D:S160172 ASTM D2974-87 5063426004 PMST/7088SBI068:AMW4D:S160172A ASTM D2974-87 5063426005 PMST/7088SBI068:AMW4D:S180185 ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/06/2012 04:42 PM Page 28 of 28 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 June 08, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5063479 5063479 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on May 25, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5063479 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5063479 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5063479001 SBI068:AMW1D:S180190 Solid 05/24/12 11:30 05/25/12 07:35 5063479002 SBI068:AMW1D:S140155 Solid 05/24/12 11:45 05/25/12 07:35 5063479003 SBI068:AMW1D:S140155A Solid 05/24/12 11:48 05/25/12 07:35 5063479004 SBI068:FB-4:W052412 Water 05/24/12 11:55 05/25/12 07:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5063479 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5063479001 SBI068:AMW1D:S180190 EPA 8260 73SLB ASTM D2974-87 1DAE 5063479002 SBI068:AMW1D:S140155 EPA 8260 73SLB ASTM D2974-87 1DAE 5063479003 SBI068:AMW1D:S140155A EPA 8260 73SLB ASTM D2974-87 1DAE 5063479004 SBI068:FB-4:W052412 EPA 8260 73SLB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S180190 Lab ID:5063479001 Collected:05/24/12 11:30 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 16:09 67-64-151.1 Acrolein ND ug/kg 1 05/30/12 16:09 107-02-851.1 Acrylonitrile ND ug/kg 1 05/30/12 16:09 107-13-151.1 Benzene ND ug/kg 1 05/30/12 16:09 71-43-22.6 Bromobenzene ND ug/kg 1 05/30/12 16:09 108-86-12.6 Bromochloromethane ND ug/kg 1 05/30/12 16:09 74-97-52.6 Bromodichloromethane ND ug/kg 1 05/30/12 16:09 75-27-42.6 Bromoform ND ug/kg 1 05/30/12 16:09 75-25-22.6 Bromomethane ND ug/kg 1 05/30/12 16:09 74-83-92.6 2-Butanone (MEK)ND ug/kg 1 05/30/12 16:09 78-93-312.8 n-Butylbenzene ND ug/kg 1 05/30/12 16:09 104-51-82.6 sec-Butylbenzene ND ug/kg 1 05/30/12 16:09 135-98-82.6 tert-Butylbenzene ND ug/kg 1 05/30/12 16:09 98-06-62.6 Carbon disulfide ND ug/kg 1 05/30/12 16:09 75-15-05.1 Carbon tetrachloride ND ug/kg 1 05/30/12 16:09 56-23-52.6 Chlorobenzene ND ug/kg 1 05/30/12 16:09 108-90-72.6 Chloroethane ND ug/kg 1 05/30/12 16:09 75-00-32.6 Chloroform ND ug/kg 1 05/30/12 16:09 67-66-32.6 Chloromethane ND ug/kg 1 05/30/12 16:09 74-87-32.6 2-Chlorotoluene ND ug/kg 1 05/30/12 16:09 95-49-82.6 4-Chlorotoluene ND ug/kg 1 05/30/12 16:09 106-43-42.6 Dibromochloromethane ND ug/kg 1 05/30/12 16:09 124-48-12.6 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 16:09 106-93-42.6 Dibromomethane ND ug/kg 1 05/30/12 16:09 74-95-32.6 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 16:09 95-50-12.6 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 16:09 541-73-12.6 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 16:09 106-46-72.6 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 16:09 110-57-651.1 Dichlorodifluoromethane ND ug/kg 1 05/30/12 16:09 75-71-82.6 1,1-Dichloroethane ND ug/kg 1 05/30/12 16:09 75-34-32.6 1,2-Dichloroethane ND ug/kg 1 05/30/12 16:09 107-06-22.6 1,1-Dichloroethene ND ug/kg 1 05/30/12 16:09 75-35-42.6 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:09 156-59-22.6 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 16:09 156-60-52.6 1,2-Dichloropropane ND ug/kg 1 05/30/12 16:09 78-87-52.6 1,3-Dichloropropane ND ug/kg 1 05/30/12 16:09 142-28-92.6 2,2-Dichloropropane ND ug/kg 1 05/30/12 16:09 594-20-72.6 1,1-Dichloropropene ND ug/kg 1 05/30/12 16:09 563-58-62.6 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:09 10061-01-52.6 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 16:09 10061-02-62.6 Ethylbenzene ND ug/kg 1 05/30/12 16:09 100-41-42.6 Ethyl methacrylate ND ug/kg 1 05/30/12 16:09 97-63-251.1 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 16:09 87-68-32.6 n-Hexane ND ug/kg 1 05/30/12 16:09 110-54-3 N22.6 2-Hexanone ND ug/kg 1 05/30/12 16:09 591-78-651.1 Iodomethane ND ug/kg 1 05/30/12 16:09 74-88-451.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 5 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S180190 Lab ID:5063479001 Collected:05/24/12 11:30 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 16:09 98-82-82.6 p-Isopropyltoluene ND ug/kg 1 05/30/12 16:09 99-87-62.6 Methylene Chloride ND ug/kg 1 05/30/12 16:09 75-09-210.2 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 16:09 108-10-112.8 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 16:09 1634-04-42.6 Naphthalene ND ug/kg 1 05/30/12 16:09 91-20-32.6 n-Propylbenzene ND ug/kg 1 05/30/12 16:09 103-65-12.6 Styrene ND ug/kg 1 05/30/12 16:09 100-42-52.6 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:09 630-20-62.6 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 16:09 79-34-52.6 Tetrachloroethene ND ug/kg 1 05/30/12 16:09 127-18-42.6 Toluene ND ug/kg 1 05/30/12 16:09 108-88-32.6 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 16:09 87-61-62.6 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 16:09 120-82-12.6 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 16:09 71-55-62.6 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 16:09 79-00-52.6 Trichloroethene ND ug/kg 1 05/30/12 16:09 79-01-62.6 Trichlorofluoromethane ND ug/kg 1 05/30/12 16:09 75-69-42.6 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 16:09 96-18-42.6 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 16:09 95-63-62.6 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 16:09 108-67-82.6 Vinyl acetate ND ug/kg 1 05/30/12 16:09 108-05-451.1 Vinyl chloride ND ug/kg 1 05/30/12 16:09 75-01-42.6 Xylene (Total)ND ug/kg 1 05/30/12 16:09 1330-20-75.1 Surrogates Dibromofluoromethane (S)105 %.1 05/30/12 16:09 1868-53-771-125 Toluene-d8 (S)98 %.1 05/30/12 16:09 2037-26-576-124 4-Bromofluorobenzene (S)101 %.1 05/30/12 16:09 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.7 %1 06/04/12 16:320.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 6 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S140155 Lab ID:5063479002 Collected:05/24/12 11:45 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 18:00 67-64-145.2 Acrolein ND ug/kg 1 05/30/12 18:00 107-02-845.2 Acrylonitrile ND ug/kg 1 05/30/12 18:00 107-13-145.2 Benzene ND ug/kg 1 05/30/12 18:00 71-43-22.3 Bromobenzene ND ug/kg 1 05/30/12 18:00 108-86-12.3 Bromochloromethane ND ug/kg 1 05/30/12 18:00 74-97-52.3 Bromodichloromethane ND ug/kg 1 05/30/12 18:00 75-27-42.3 Bromoform ND ug/kg 1 05/30/12 18:00 75-25-22.3 Bromomethane ND ug/kg 1 05/30/12 18:00 74-83-92.3 2-Butanone (MEK)ND ug/kg 1 05/30/12 18:00 78-93-311.3 n-Butylbenzene ND ug/kg 1 05/30/12 18:00 104-51-82.3 sec-Butylbenzene ND ug/kg 1 05/30/12 18:00 135-98-82.3 tert-Butylbenzene ND ug/kg 1 05/30/12 18:00 98-06-62.3 Carbon disulfide ND ug/kg 1 05/30/12 18:00 75-15-04.5 Carbon tetrachloride ND ug/kg 1 05/30/12 18:00 56-23-52.3 Chlorobenzene ND ug/kg 1 05/30/12 18:00 108-90-72.3 Chloroethane ND ug/kg 1 05/30/12 18:00 75-00-32.3 Chloroform ND ug/kg 1 05/30/12 18:00 67-66-32.3 Chloromethane ND ug/kg 1 05/30/12 18:00 74-87-32.3 2-Chlorotoluene ND ug/kg 1 05/30/12 18:00 95-49-82.3 4-Chlorotoluene ND ug/kg 1 05/30/12 18:00 106-43-42.3 Dibromochloromethane ND ug/kg 1 05/30/12 18:00 124-48-12.3 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 18:00 106-93-42.3 Dibromomethane ND ug/kg 1 05/30/12 18:00 74-95-32.3 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 18:00 95-50-12.3 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 18:00 541-73-12.3 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 18:00 106-46-72.3 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 18:00 110-57-645.2 Dichlorodifluoromethane ND ug/kg 1 05/30/12 18:00 75-71-82.3 1,1-Dichloroethane ND ug/kg 1 05/30/12 18:00 75-34-32.3 1,2-Dichloroethane ND ug/kg 1 05/30/12 18:00 107-06-22.3 1,1-Dichloroethene ND ug/kg 1 05/30/12 18:00 75-35-42.3 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 18:00 156-59-22.3 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 18:00 156-60-52.3 1,2-Dichloropropane ND ug/kg 1 05/30/12 18:00 78-87-52.3 1,3-Dichloropropane ND ug/kg 1 05/30/12 18:00 142-28-92.3 2,2-Dichloropropane ND ug/kg 1 05/30/12 18:00 594-20-72.3 1,1-Dichloropropene ND ug/kg 1 05/30/12 18:00 563-58-62.3 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 18:00 10061-01-52.3 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 18:00 10061-02-62.3 Ethylbenzene ND ug/kg 1 05/30/12 18:00 100-41-42.3 Ethyl methacrylate ND ug/kg 1 05/30/12 18:00 97-63-245.2 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 18:00 87-68-32.3 n-Hexane ND ug/kg 1 05/30/12 18:00 110-54-3 N22.3 2-Hexanone ND ug/kg 1 05/30/12 18:00 591-78-645.2 Iodomethane ND ug/kg 1 05/30/12 18:00 74-88-445.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 7 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S140155 Lab ID:5063479002 Collected:05/24/12 11:45 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 18:00 98-82-82.3 p-Isopropyltoluene ND ug/kg 1 05/30/12 18:00 99-87-62.3 Methylene Chloride ND ug/kg 1 05/30/12 18:00 75-09-29.0 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 18:00 108-10-111.3 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 18:00 1634-04-42.3 Naphthalene ND ug/kg 1 05/30/12 18:00 91-20-32.3 n-Propylbenzene ND ug/kg 1 05/30/12 18:00 103-65-12.3 Styrene ND ug/kg 1 05/30/12 18:00 100-42-52.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 18:00 630-20-62.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 18:00 79-34-52.3 Tetrachloroethene ND ug/kg 1 05/30/12 18:00 127-18-42.3 Toluene ND ug/kg 1 05/30/12 18:00 108-88-32.3 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 18:00 87-61-62.3 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 18:00 120-82-12.3 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 18:00 71-55-62.3 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 18:00 79-00-52.3 Trichloroethene ND ug/kg 1 05/30/12 18:00 79-01-62.3 Trichlorofluoromethane ND ug/kg 1 05/30/12 18:00 75-69-42.3 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 18:00 96-18-42.3 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 18:00 95-63-62.3 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 18:00 108-67-82.3 Vinyl acetate ND ug/kg 1 05/30/12 18:00 108-05-445.2 Vinyl chloride ND ug/kg 1 05/30/12 18:00 75-01-42.3 Xylene (Total)ND ug/kg 1 05/30/12 18:00 1330-20-74.5 Surrogates Dibromofluoromethane (S)106 %.1 05/30/12 18:00 1868-53-771-125 Toluene-d8 (S)102 %.1 05/30/12 18:00 2037-26-576-124 4-Bromofluorobenzene (S)100 %.1 05/30/12 18:00 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.0 %1 06/04/12 16:330.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 8 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S140155A Lab ID:5063479003 Collected:05/24/12 11:48 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 05/30/12 18:37 67-64-146.6 Acrolein ND ug/kg 1 05/30/12 18:37 107-02-846.6 Acrylonitrile ND ug/kg 1 05/30/12 18:37 107-13-146.6 Benzene ND ug/kg 1 05/30/12 18:37 71-43-22.3 Bromobenzene ND ug/kg 1 05/30/12 18:37 108-86-12.3 Bromochloromethane ND ug/kg 1 05/30/12 18:37 74-97-52.3 Bromodichloromethane ND ug/kg 1 05/30/12 18:37 75-27-42.3 Bromoform ND ug/kg 1 05/30/12 18:37 75-25-22.3 Bromomethane ND ug/kg 1 05/30/12 18:37 74-83-92.3 2-Butanone (MEK)ND ug/kg 1 05/30/12 18:37 78-93-311.6 n-Butylbenzene ND ug/kg 1 05/30/12 18:37 104-51-82.3 sec-Butylbenzene ND ug/kg 1 05/30/12 18:37 135-98-82.3 tert-Butylbenzene ND ug/kg 1 05/30/12 18:37 98-06-62.3 Carbon disulfide ND ug/kg 1 05/30/12 18:37 75-15-04.7 Carbon tetrachloride ND ug/kg 1 05/30/12 18:37 56-23-52.3 Chlorobenzene ND ug/kg 1 05/30/12 18:37 108-90-72.3 Chloroethane ND ug/kg 1 05/30/12 18:37 75-00-32.3 Chloroform ND ug/kg 1 05/30/12 18:37 67-66-32.3 Chloromethane ND ug/kg 1 05/30/12 18:37 74-87-32.3 2-Chlorotoluene ND ug/kg 1 05/30/12 18:37 95-49-82.3 4-Chlorotoluene ND ug/kg 1 05/30/12 18:37 106-43-42.3 Dibromochloromethane ND ug/kg 1 05/30/12 18:37 124-48-12.3 1,2-Dibromoethane (EDB)ND ug/kg 1 05/30/12 18:37 106-93-42.3 Dibromomethane ND ug/kg 1 05/30/12 18:37 74-95-32.3 1,2-Dichlorobenzene ND ug/kg 1 05/30/12 18:37 95-50-12.3 1,3-Dichlorobenzene ND ug/kg 1 05/30/12 18:37 541-73-12.3 1,4-Dichlorobenzene ND ug/kg 1 05/30/12 18:37 106-46-72.3 trans-1,4-Dichloro-2-butene ND ug/kg 1 05/30/12 18:37 110-57-646.6 Dichlorodifluoromethane ND ug/kg 1 05/30/12 18:37 75-71-82.3 1,1-Dichloroethane ND ug/kg 1 05/30/12 18:37 75-34-32.3 1,2-Dichloroethane ND ug/kg 1 05/30/12 18:37 107-06-22.3 1,1-Dichloroethene ND ug/kg 1 05/30/12 18:37 75-35-42.3 cis-1,2-Dichloroethene ND ug/kg 1 05/30/12 18:37 156-59-22.3 trans-1,2-Dichloroethene ND ug/kg 1 05/30/12 18:37 156-60-52.3 1,2-Dichloropropane ND ug/kg 1 05/30/12 18:37 78-87-52.3 1,3-Dichloropropane ND ug/kg 1 05/30/12 18:37 142-28-92.3 2,2-Dichloropropane ND ug/kg 1 05/30/12 18:37 594-20-72.3 1,1-Dichloropropene ND ug/kg 1 05/30/12 18:37 563-58-62.3 cis-1,3-Dichloropropene ND ug/kg 1 05/30/12 18:37 10061-01-52.3 trans-1,3-Dichloropropene ND ug/kg 1 05/30/12 18:37 10061-02-62.3 Ethylbenzene ND ug/kg 1 05/30/12 18:37 100-41-42.3 Ethyl methacrylate ND ug/kg 1 05/30/12 18:37 97-63-246.6 Hexachloro-1,3-butadiene ND ug/kg 1 05/30/12 18:37 87-68-32.3 n-Hexane ND ug/kg 1 05/30/12 18:37 110-54-3 N22.3 2-Hexanone ND ug/kg 1 05/30/12 18:37 591-78-646.6 Iodomethane ND ug/kg 1 05/30/12 18:37 74-88-446.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 9 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:AMW1D:S140155A Lab ID:5063479003 Collected:05/24/12 11:48 Received:05/25/12 07:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 05/30/12 18:37 98-82-82.3 p-Isopropyltoluene ND ug/kg 1 05/30/12 18:37 99-87-62.3 Methylene Chloride ND ug/kg 1 05/30/12 18:37 75-09-29.3 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 05/30/12 18:37 108-10-111.6 Methyl-tert-butyl ether ND ug/kg 1 05/30/12 18:37 1634-04-42.3 Naphthalene ND ug/kg 1 05/30/12 18:37 91-20-32.3 n-Propylbenzene ND ug/kg 1 05/30/12 18:37 103-65-12.3 Styrene ND ug/kg 1 05/30/12 18:37 100-42-52.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 05/30/12 18:37 630-20-62.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 05/30/12 18:37 79-34-52.3 Tetrachloroethene ND ug/kg 1 05/30/12 18:37 127-18-42.3 Toluene ND ug/kg 1 05/30/12 18:37 108-88-32.3 1,2,3-Trichlorobenzene ND ug/kg 1 05/30/12 18:37 87-61-62.3 1,2,4-Trichlorobenzene ND ug/kg 1 05/30/12 18:37 120-82-12.3 1,1,1-Trichloroethane ND ug/kg 1 05/30/12 18:37 71-55-62.3 1,1,2-Trichloroethane ND ug/kg 1 05/30/12 18:37 79-00-52.3 Trichloroethene ND ug/kg 1 05/30/12 18:37 79-01-62.3 Trichlorofluoromethane ND ug/kg 1 05/30/12 18:37 75-69-42.3 1,2,3-Trichloropropane ND ug/kg 1 05/30/12 18:37 96-18-42.3 1,2,4-Trimethylbenzene ND ug/kg 1 05/30/12 18:37 95-63-62.3 1,3,5-Trimethylbenzene ND ug/kg 1 05/30/12 18:37 108-67-82.3 Vinyl acetate ND ug/kg 1 05/30/12 18:37 108-05-446.6 Vinyl chloride ND ug/kg 1 05/30/12 18:37 75-01-42.3 Xylene (Total)ND ug/kg 1 05/30/12 18:37 1330-20-74.7 Surrogates Dibromofluoromethane (S)107 %.1 05/30/12 18:37 1868-53-771-125 Toluene-d8 (S)97 %.1 05/30/12 18:37 2037-26-576-124 4-Bromofluorobenzene (S)101 %.1 05/30/12 18:37 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.6 %1 06/04/12 16:330.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 10 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:FB-4:W052412 Lab ID:5063479004 Collected:05/24/12 11:55 Received:05/25/12 07:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 05/30/12 18:19 67-64-1100 Acrolein ND ug/L 1 05/30/12 18:19 107-02-8100 Acrylonitrile ND ug/L 1 05/30/12 18:19 107-13-1100 Benzene ND ug/L 1 05/30/12 18:19 71-43-25.0 Bromobenzene ND ug/L 1 05/30/12 18:19 108-86-15.0 Bromochloromethane ND ug/L 1 05/30/12 18:19 74-97-55.0 Bromodichloromethane ND ug/L 1 05/30/12 18:19 75-27-45.0 Bromoform ND ug/L 1 05/30/12 18:19 75-25-25.0 Bromomethane ND ug/L 1 05/30/12 18:19 74-83-95.0 2-Butanone (MEK)ND ug/L 1 05/30/12 18:19 78-93-325.0 n-Butylbenzene ND ug/L 1 05/30/12 18:19 104-51-85.0 sec-Butylbenzene ND ug/L 1 05/30/12 18:19 135-98-85.0 tert-Butylbenzene ND ug/L 1 05/30/12 18:19 98-06-65.0 Carbon disulfide ND ug/L 1 05/30/12 18:19 75-15-010.0 Carbon tetrachloride ND ug/L 1 05/30/12 18:19 56-23-55.0 Chlorobenzene ND ug/L 1 05/30/12 18:19 108-90-75.0 Chloroethane ND ug/L 1 05/30/12 18:19 75-00-35.0 Chloroform 9.7 ug/L 1 05/30/12 18:19 67-66-3 1d5.0 Chloromethane ND ug/L 1 05/30/12 18:19 74-87-35.0 2-Chlorotoluene ND ug/L 1 05/30/12 18:19 95-49-85.0 4-Chlorotoluene ND ug/L 1 05/30/12 18:19 106-43-45.0 Dibromochloromethane ND ug/L 1 05/30/12 18:19 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 05/30/12 18:19 106-93-45.0 Dibromomethane ND ug/L 1 05/30/12 18:19 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 05/30/12 18:19 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 05/30/12 18:19 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 05/30/12 18:19 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 05/30/12 18:19 110-57-6100 Dichlorodifluoromethane ND ug/L 1 05/30/12 18:19 75-71-85.0 1,1-Dichloroethane ND ug/L 1 05/30/12 18:19 75-34-35.0 1,2-Dichloroethane ND ug/L 1 05/30/12 18:19 107-06-25.0 1,1-Dichloroethene ND ug/L 1 05/30/12 18:19 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 05/30/12 18:19 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 05/30/12 18:19 156-60-55.0 1,2-Dichloropropane ND ug/L 1 05/30/12 18:19 78-87-55.0 1,3-Dichloropropane ND ug/L 1 05/30/12 18:19 142-28-95.0 2,2-Dichloropropane ND ug/L 1 05/30/12 18:19 594-20-75.0 1,1-Dichloropropene ND ug/L 1 05/30/12 18:19 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 05/30/12 18:19 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 05/30/12 18:19 10061-02-65.0 Ethylbenzene ND ug/L 1 05/30/12 18:19 100-41-45.0 Ethyl methacrylate ND ug/L 1 05/30/12 18:19 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 05/30/12 18:19 87-68-35.0 n-Hexane ND ug/L 1 05/30/12 18:19 110-54-3 N25.0 2-Hexanone ND ug/L 1 05/30/12 18:19 591-78-625.0 Iodomethane ND ug/L 1 05/30/12 18:19 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 05/30/12 18:19 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 11 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063479 SBI068 Sample:SBI068:FB-4:W052412 Lab ID:5063479004 Collected:05/24/12 11:55 Received:05/25/12 07:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 05/30/12 18:19 99-87-65.0 Methylene Chloride ND ug/L 1 05/30/12 18:19 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 05/30/12 18:19 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 05/30/12 18:19 1634-04-44.0 Naphthalene ND ug/L 1 05/30/12 18:19 91-20-35.0 n-Propylbenzene ND ug/L 1 05/30/12 18:19 103-65-15.0 Styrene ND ug/L 1 05/30/12 18:19 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 05/30/12 18:19 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 05/30/12 18:19 79-34-55.0 Tetrachloroethene ND ug/L 1 05/30/12 18:19 127-18-45.0 Toluene ND ug/L 1 05/30/12 18:19 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 05/30/12 18:19 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 05/30/12 18:19 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 05/30/12 18:19 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 05/30/12 18:19 79-00-55.0 Trichloroethene ND ug/L 1 05/30/12 18:19 79-01-65.0 Trichlorofluoromethane ND ug/L 1 05/30/12 18:19 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 05/30/12 18:19 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 05/30/12 18:19 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 05/30/12 18:19 108-67-85.0 Vinyl acetate ND ug/L 1 05/30/12 18:19 108-05-450.0 Vinyl chloride ND ug/L 1 05/30/12 18:19 75-01-42.0 Xylene (Total)ND ug/L 1 05/30/12 18:19 1330-20-710.0 Surrogates Dibromofluoromethane (S)121 %.1 05/30/12 18:19 1868-53-783-123 4-Bromofluorobenzene (S)105 %.1 05/30/12 18:19 460-00-472-125 Toluene-d8 (S)96 %.1 05/30/12 18:19 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 12 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42561 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5063479004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:741714 Associated Lab Samples:5063479004 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/30/12 10:52 1,1,1-Trichloroethane ug/L ND 5.0 05/30/12 10:52 1,1,2,2-Tetrachloroethane ug/L ND 5.0 05/30/12 10:52 1,1,2-Trichloroethane ug/L ND 5.0 05/30/12 10:52 1,1-Dichloroethane ug/L ND 5.0 05/30/12 10:52 1,1-Dichloroethene ug/L ND 5.0 05/30/12 10:52 1,1-Dichloropropene ug/L ND 5.0 05/30/12 10:52 1,2,3-Trichlorobenzene ug/L ND 5.0 05/30/12 10:52 1,2,3-Trichloropropane ug/L ND 5.0 05/30/12 10:52 1,2,4-Trichlorobenzene ug/L ND 5.0 05/30/12 10:52 1,2,4-Trimethylbenzene ug/L ND 5.0 05/30/12 10:52 1,2-Dibromoethane (EDB)ug/L ND 5.0 05/30/12 10:52 1,2-Dichlorobenzene ug/L ND 5.0 05/30/12 10:52 1,2-Dichloroethane ug/L ND 5.0 05/30/12 10:52 1,2-Dichloropropane ug/L ND 5.0 05/30/12 10:52 1,3,5-Trimethylbenzene ug/L ND 5.0 05/30/12 10:52 1,3-Dichlorobenzene ug/L ND 5.0 05/30/12 10:52 1,3-Dichloropropane ug/L ND 5.0 05/30/12 10:52 1,4-Dichlorobenzene ug/L ND 5.0 05/30/12 10:52 2,2-Dichloropropane ug/L ND 5.0 05/30/12 10:52 2-Butanone (MEK)ug/L ND 25.0 05/30/12 10:52 2-Chlorotoluene ug/L ND 5.0 05/30/12 10:52 2-Hexanone ug/L ND 25.0 05/30/12 10:52 4-Chlorotoluene ug/L ND 5.0 05/30/12 10:52 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 05/30/12 10:52 Acetone ug/L ND 100 05/30/12 10:52 Acrolein ug/L ND 100 05/30/12 10:52 Acrylonitrile ug/L ND 100 05/30/12 10:52 Benzene ug/L ND 5.0 05/30/12 10:52 Bromobenzene ug/L ND 5.0 05/30/12 10:52 Bromochloromethane ug/L ND 5.0 05/30/12 10:52 Bromodichloromethane ug/L ND 5.0 05/30/12 10:52 Bromoform ug/L ND 5.0 05/30/12 10:52 Bromomethane ug/L ND 5.0 05/30/12 10:52 Carbon disulfide ug/L ND 10.0 05/30/12 10:52 Carbon tetrachloride ug/L ND 5.0 05/30/12 10:52 Chlorobenzene ug/L ND 5.0 05/30/12 10:52 Chloroethane ug/L ND 5.0 05/30/12 10:52 Chloroform ug/L ND 5.0 05/30/12 10:52 Chloromethane ug/L ND 5.0 05/30/12 10:52 cis-1,2-Dichloroethene ug/L ND 5.0 05/30/12 10:52 cis-1,3-Dichloropropene ug/L ND 5.0 05/30/12 10:52 Dibromochloromethane ug/L ND 5.0 05/30/12 10:52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 13 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:741714 Associated Lab Samples:5063479004 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 05/30/12 10:52 Dichlorodifluoromethane ug/L ND 5.0 05/30/12 10:52 Ethyl methacrylate ug/L ND 100 05/30/12 10:52 Ethylbenzene ug/L ND 5.0 05/30/12 10:52 Hexachloro-1,3-butadiene ug/L ND 5.0 05/30/12 10:52 Iodomethane ug/L ND 10.0 05/30/12 10:52 Isopropylbenzene (Cumene)ug/L ND 5.0 05/30/12 10:52 Methyl-tert-butyl ether ug/L ND 4.0 05/30/12 10:52 Methylene Chloride ug/L ND 5.0 05/30/12 10:52 n-Butylbenzene ug/L ND 5.0 05/30/12 10:52 n-Hexane ug/L ND 5.0 N205/30/12 10:52 n-Propylbenzene ug/L ND 5.0 05/30/12 10:52 Naphthalene ug/L ND 5.0 05/30/12 10:52 p-Isopropyltoluene ug/L ND 5.0 05/30/12 10:52 sec-Butylbenzene ug/L ND 5.0 05/30/12 10:52 Styrene ug/L ND 5.0 05/30/12 10:52 tert-Butylbenzene ug/L ND 5.0 05/30/12 10:52 Tetrachloroethene ug/L ND 5.0 05/30/12 10:52 Toluene ug/L ND 5.0 05/30/12 10:52 trans-1,2-Dichloroethene ug/L ND 5.0 05/30/12 10:52 trans-1,3-Dichloropropene ug/L ND 5.0 05/30/12 10:52 trans-1,4-Dichloro-2-butene ug/L ND 100 05/30/12 10:52 Trichloroethene ug/L ND 5.0 05/30/12 10:52 Trichlorofluoromethane ug/L ND 5.0 05/30/12 10:52 Vinyl acetate ug/L ND 50.0 05/30/12 10:52 Vinyl chloride ug/L ND 2.0 05/30/12 10:52 Xylene (Total)ug/L ND 10.0 05/30/12 10:52 4-Bromofluorobenzene (S)%.106 72-125 05/30/12 10:52 Dibromofluoromethane (S)%.117 83-123 05/30/12 10:52 Toluene-d8 (S)%.97 81-114 05/30/12 10:52 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741715LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 49.850 100 69-122 1,1,1-Trichloroethane ug/L 48.450 97 69-126 1,1,2,2-Tetrachloroethane ug/L 43.650 87 68-134 1,1,2-Trichloroethane ug/L 49.850 100 77-129 1,1-Dichloroethane ug/L 47.050 94 70-127 1,1-Dichloroethene ug/L 45.650 91 75-145 1,1-Dichloropropene ug/L 52.350 105 75-126 1,2,3-Trichlorobenzene ug/L 50.250 100 63-130 1,2,3-Trichloropropane ug/L 74.6 L35014945-121 1,2,4-Trichlorobenzene ug/L 50.650 101 64-122 1,2,4-Trimethylbenzene ug/L 51.450 103 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 14 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741715LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 45.750 91 77-123 1,2-Dichlorobenzene ug/L 47.750 95 74-123 1,2-Dichloroethane ug/L 50.750 101 71-127 1,2-Dichloropropane ug/L 50.950 102 75-126 1,3,5-Trimethylbenzene ug/L 52.550 105 69-129 1,3-Dichlorobenzene ug/L 49.450 99 76-123 1,3-Dichloropropane ug/L 49.450 99 77-126 1,4-Dichlorobenzene ug/L 48.950 98 77-121 2,2-Dichloropropane ug/L 53.550 107 45-138 2-Butanone (MEK)ug/L 235250 94 42-177 2-Chlorotoluene ug/L 49.950 100 74-129 2-Hexanone ug/L 241250 96 57-162 4-Chlorotoluene ug/L 50.750 101 70-125 4-Methyl-2-pentanone (MIBK)ug/L 237250 95 64-135 Acetone ug/L 242250 97 10-200 Acrolein ug/L 2741000 27 10-200 Acrylonitrile ug/L 9031000 90 59-144 Benzene ug/L 47.450 95 76-123 Bromobenzene ug/L 48.750 97 67-130 Bromochloromethane ug/L 46.850 94 58-153 Bromodichloromethane ug/L 50.650 101 71-124 Bromoform ug/L 42.050 84 64-116 Bromomethane ug/L 50.950 102 23-197 Carbon disulfide ug/L 84.7100 85 55-146 Carbon tetrachloride ug/L 50.350 101 65-125 Chlorobenzene ug/L 49.050 98 78-120 Chloroethane ug/L 41.450 83 56-163 Chloroform ug/L 48.450 97 73-122 Chloromethane ug/L 43.850 88 46-146 cis-1,2-Dichloroethene ug/L 49.650 99 79-129 cis-1,3-Dichloropropene ug/L 51.250 102 66-123 Dibromochloromethane ug/L 47.650 95 70-123 Dibromomethane ug/L 49.250 98 73-123 Dichlorodifluoromethane ug/L 53.150 106 19-200 Ethyl methacrylate ug/L 191200 96 70-127 Ethylbenzene ug/L 48.950 98 75-120 Hexachloro-1,3-butadiene ug/L 51.750 103 64-131 Iodomethane ug/L 86.5100 87 16-181 Isopropylbenzene (Cumene)ug/L 50.050 100 73-123 Methyl-tert-butyl ether ug/L 107100 107 66-128 Methylene Chloride ug/L 47.150 94 61-138 n-Butylbenzene ug/L 53.550 107 69-130 n-Hexane ug/L 41.5 N2508367-142 n-Propylbenzene ug/L 52.050 104 71-132 Naphthalene ug/L 49.450 99 62-130 p-Isopropyltoluene ug/L 53.350 107 71-126 sec-Butylbenzene ug/L 50.150 100 69-130 Styrene ug/L 51.650 103 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 15 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741715LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 44.550 89 49-114 Tetrachloroethene ug/L 47.550 95 57-125 Toluene ug/L 49.850 100 72-124 trans-1,2-Dichloroethene ug/L 46.250 92 71-145 trans-1,3-Dichloropropene ug/L 50.050 100 58-118 trans-1,4-Dichloro-2-butene ug/L 175200 87 50-121 Trichloroethene ug/L 55.350 111 77-122 Trichlorofluoromethane ug/L 52.750 105 56-159 Vinyl acetate ug/L 199200 99 27-119 Vinyl chloride ug/L 46.050 92 61-146 Xylene (Total)ug/L 151150 101 72-126 4-Bromofluorobenzene (S)%.99 72-125 Dibromofluoromethane (S)%.91 83-123 Toluene-d8 (S)%.101 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 741716MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063436003 741717 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 105 30-122104 1 2050ND52.7 52.0 1,1,1-Trichloroethane ug/L 50 110 37-136110 .3 2050ND55.1 55.0 1,1,2,2-Tetrachloroethane ug/L 50 92 47-13294 3 2050ND45.9 47.1 1,1,2-Trichloroethane ug/L 50 96 53-13199 3 2050ND48.1 49.5 1,1-Dichloroethane ug/L 50 97 47-138100 3 2050ND48.7 50.2 1,1-Dichloroethene ug/L 50 101 54-152102 1 2050ND50.4 51.0 1,1-Dichloropropene ug/L 50 108 47-136109 1 2050ND53.8 54.5 1,2,3-Trichlorobenzene ug/L 50 105 15-132102 3 2050ND52.6 50.8 1,2,3-Trichloropropane ug/L M05015924-108159 .2 2050ND79.4 79.5 1,2,4-Trichlorobenzene ug/L 50 103 10-13099 5 2050ND51.7 49.3 1,2,4-Trimethylbenzene ug/L 50 101 10-141101 .2 2050ND51.0 51.0 1,2-Dibromoethane (EDB)ug/L 50 92 49-13093 1 2050ND45.9 46.4 1,2-Dichlorobenzene ug/L 50 95 20-13796 .8 2050ND47.7 48.1 1,2-Dichloroethane ug/L 50 108 42-139110 1 2050ND54.2 54.9 1,2-Dichloropropane ug/L 50 106 50-131106 .3 2050ND53.2 53.1 1,3,5-Trimethylbenzene ug/L 50 102 10-145100 2 2050ND51.1 50.2 1,3-Dichlorobenzene ug/L 50 96 13-14396 .9 2050ND48.2 47.8 1,3-Dichloropropane ug/L 50 96 53-13093 2 2050ND47.8 46.7 1,4-Dichlorobenzene ug/L 50 99 13-14095 4 2050ND49.7 47.6 2,2-Dichloropropane ug/L 50 115 13-142110 4 2050ND57.5 55.2 2-Butanone (MEK)ug/L 250 104 43-142102 2 20250ND260254 2-Chlorotoluene ug/L 50 100 15-14598 3 2050ND50.1 48.9 2-Hexanone ug/L 250 104 46-139104 .09 20250ND260260 4-Chlorotoluene ug/L 50 101 12-143100 1 2050ND50.5 50.0 4-Methyl-2-pentanone (MIBK)ug/L 250 99 43-140103 5 20250ND247258 Acetone ug/L 250 115 38-155116 1 20250ND288291 Acrolein ug/L 1000 125 11-200126 .5 201000ND12501260 Acrylonitrile ug/L 1000 103 42-150106 3 201000ND10301060 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 16 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 741716MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063436003 741717 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 103 52-13497 6 2050ND51.7 48.7 Bromobenzene ug/L 50 106 25-140102 3 2050ND52.8 51.2 Bromochloromethane ug/L 50 104 54-144104 .08 2050ND52.2 52.2 Bromodichloromethane ug/L 50 120 42-128117 2 2050ND59.8 58.3 Bromoform ug/L 50 89 34-11686 3 2050ND44.5 43.2 Bromomethane ug/L 50 110 10-200106 3 2050ND55.0 53.1 Carbon disulfide ug/L 100 91 43-14491 .3 20100ND90.9 91.2 Carbon tetrachloride ug/L 50 109 26-136109 .3 2050ND54.5 54.6 Chlorobenzene ug/L 50 98 33-13697 .8 2050ND48.9 48.5 Chloroethane ug/L 50 87 21-20091 5 2050ND43.4 45.7 Chloroform ug/L 50 101 50-134105 3 20507.6 58.1 59.9 Chloromethane ug/L 50 93 32-16094 1 2050ND46.5 47.0 cis-1,2-Dichloroethene ug/L 50 106 48-145103 3 2050ND53.0 51.5 cis-1,3-Dichloropropene ug/L 50 101 35-116100 1 2050ND50.3 49.8 Dibromochloromethane ug/L 50 98 39-12295 4 2050ND49.2 47.3 Dibromomethane ug/L 50 111 49-134110 .7 2050ND55.3 54.9 Dichlorodifluoromethane ug/L 50 114 35-200112 2 2050ND57.2 56.0 Ethyl methacrylate ug/L 200 108 54-123102 5 20200ND216204 Ethylbenzene ug/L 50 103 29-132104 .6 2050ND51.7 52.1 Hexachloro-1,3-butadiene ug/L 50 106 10-146101 5 2050ND53.0 50.5 Iodomethane ug/L 100 91 10-17198 8 20100ND90.9 98.4 Isopropylbenzene (Cumene)ug/L 50 98 11-14698 .6 2050ND49.0 49.2 Methyl-tert-butyl ether ug/L 100 113 39-137117 4 20100ND113117 Methylene Chloride ug/L 50 105 47-141105 .2 2050ND52.4 52.5 n-Butylbenzene ug/L 50 104 10-156102 2 2050ND52.0 50.8 n-Hexane ug/L N2508751-13785 3 2050ND43.7 42.4 n-Propylbenzene ug/L 50 99 10-148100 1 2050ND49.4 50.1 Naphthalene ug/L 50 104 40-124101 3 2050ND52.0 50.7 p-Isopropyltoluene ug/L 50 104 10-150102 2 2050ND52.0 50.8 sec-Butylbenzene ug/L 50 100 10-150101 1 2050ND50.1 50.7 Styrene ug/L 50 98 20-143101 3 2050ND49.0 50.3 tert-Butylbenzene ug/L 50 91 10-12390 .6 2050ND45.5 45.2 Tetrachloroethene ug/L 50 94 30-12498 5 2050ND46.8 49.0 Toluene ug/L 50 97 42-13096 1 2050ND48.8 48.2 trans-1,2-Dichloroethene ug/L 50 97 48-144101 4 2050ND48.4 50.4 trans-1,3-Dichloropropene ug/L 50 99 24-11498 .6 2050ND49.3 49.0 trans-1,4-Dichloro-2-butene ug/L 200 96 22-12095 .9 20200ND192190 Trichloroethene ug/L 50 117 44-130113 3 2050ND58.3 56.6 Trichlorofluoromethane ug/L 50 118 17-200115 3 2050ND59.2 57.6 Vinyl acetate ug/L 200 92 10-11596 4 20200ND184191 Vinyl chloride ug/L 50 101 45-159102 .3 2050ND50.7 50.8 Xylene (Total)ug/L 150 95 29-13198 3 20150ND142147 4-Bromofluorobenzene (S)%.98 72-125101 20 Dibromofluoromethane (S)%.97 83-123101 20 Toluene-d8 (S)%.99 81-114100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 17 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42554 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063479001, 5063479002, 5063479003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:741635 Associated Lab Samples:5063479001, 5063479002, 5063479003 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/30/12 10:34 1,1,1-Trichloroethane ug/kg ND 5.0 05/30/12 10:34 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/30/12 10:34 1,1,2-Trichloroethane ug/kg ND 5.0 05/30/12 10:34 1,1-Dichloroethane ug/kg ND 5.0 05/30/12 10:34 1,1-Dichloroethene ug/kg ND 5.0 05/30/12 10:34 1,1-Dichloropropene ug/kg ND 5.0 05/30/12 10:34 1,2,3-Trichlorobenzene ug/kg ND 5.0 05/30/12 10:34 1,2,3-Trichloropropane ug/kg ND 5.0 05/30/12 10:34 1,2,4-Trichlorobenzene ug/kg ND 5.0 05/30/12 10:34 1,2,4-Trimethylbenzene ug/kg ND 5.0 05/30/12 10:34 1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/30/12 10:34 1,2-Dichlorobenzene ug/kg ND 5.0 05/30/12 10:34 1,2-Dichloroethane ug/kg ND 5.0 05/30/12 10:34 1,2-Dichloropropane ug/kg ND 5.0 05/30/12 10:34 1,3,5-Trimethylbenzene ug/kg ND 5.0 05/30/12 10:34 1,3-Dichlorobenzene ug/kg ND 5.0 05/30/12 10:34 1,3-Dichloropropane ug/kg ND 5.0 05/30/12 10:34 1,4-Dichlorobenzene ug/kg ND 5.0 05/30/12 10:34 2,2-Dichloropropane ug/kg ND 5.0 05/30/12 10:34 2-Butanone (MEK)ug/kg ND 25.0 05/30/12 10:34 2-Chlorotoluene ug/kg ND 5.0 05/30/12 10:34 2-Hexanone ug/kg ND 100 05/30/12 10:34 4-Chlorotoluene ug/kg ND 5.0 05/30/12 10:34 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 05/30/12 10:34 Acetone ug/kg ND 100 05/30/12 10:34 Acrolein ug/kg ND 100 05/30/12 10:34 Acrylonitrile ug/kg ND 100 05/30/12 10:34 Benzene ug/kg ND 5.0 05/30/12 10:34 Bromobenzene ug/kg ND 5.0 05/30/12 10:34 Bromochloromethane ug/kg ND 5.0 05/30/12 10:34 Bromodichloromethane ug/kg ND 5.0 05/30/12 10:34 Bromoform ug/kg ND 5.0 05/30/12 10:34 Bromomethane ug/kg ND 5.0 05/30/12 10:34 Carbon disulfide ug/kg ND 10.0 05/30/12 10:34 Carbon tetrachloride ug/kg ND 5.0 05/30/12 10:34 Chlorobenzene ug/kg ND 5.0 05/30/12 10:34 Chloroethane ug/kg ND 5.0 05/30/12 10:34 Chloroform ug/kg ND 5.0 05/30/12 10:34 Chloromethane ug/kg ND 5.0 05/30/12 10:34 cis-1,2-Dichloroethene ug/kg ND 5.0 05/30/12 10:34 cis-1,3-Dichloropropene ug/kg ND 5.0 05/30/12 10:34 Dibromochloromethane ug/kg ND 5.0 05/30/12 10:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 18 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:741635 Associated Lab Samples:5063479001, 5063479002, 5063479003 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 05/30/12 10:34 Dichlorodifluoromethane ug/kg ND 5.0 05/30/12 10:34 Ethyl methacrylate ug/kg ND 100 05/30/12 10:34 Ethylbenzene ug/kg ND 5.0 05/30/12 10:34 Hexachloro-1,3-butadiene ug/kg ND 5.0 05/30/12 10:34 Iodomethane ug/kg ND 100 05/30/12 10:34 Isopropylbenzene (Cumene)ug/kg ND 5.0 05/30/12 10:34 Methyl-tert-butyl ether ug/kg ND 5.0 05/30/12 10:34 Methylene Chloride ug/kg ND 20.0 05/30/12 10:34 n-Butylbenzene ug/kg ND 5.0 05/30/12 10:34 n-Hexane ug/kg ND 5.0 N205/30/12 10:34 n-Propylbenzene ug/kg ND 5.0 05/30/12 10:34 Naphthalene ug/kg ND 5.0 05/30/12 10:34 p-Isopropyltoluene ug/kg ND 5.0 05/30/12 10:34 sec-Butylbenzene ug/kg ND 5.0 05/30/12 10:34 Styrene ug/kg ND 5.0 05/30/12 10:34 tert-Butylbenzene ug/kg ND 5.0 05/30/12 10:34 Tetrachloroethene ug/kg ND 5.0 05/30/12 10:34 Toluene ug/kg ND 5.0 05/30/12 10:34 trans-1,2-Dichloroethene ug/kg ND 5.0 05/30/12 10:34 trans-1,3-Dichloropropene ug/kg ND 5.0 05/30/12 10:34 trans-1,4-Dichloro-2-butene ug/kg ND 100 05/30/12 10:34 Trichloroethene ug/kg ND 5.0 05/30/12 10:34 Trichlorofluoromethane ug/kg ND 5.0 05/30/12 10:34 Vinyl acetate ug/kg ND 100 05/30/12 10:34 Vinyl chloride ug/kg ND 5.0 05/30/12 10:34 Xylene (Total)ug/kg ND 10.0 05/30/12 10:34 4-Bromofluorobenzene (S)%.98 67-134 05/30/12 10:34 Dibromofluoromethane (S)%.104 71-125 05/30/12 10:34 Toluene-d8 (S)%.101 76-124 05/30/12 10:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741636LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 58.550 117 68-125 1,1,1-Trichloroethane ug/kg 56.050 112 63-124 1,1,2,2-Tetrachloroethane ug/kg 47.650 95 73-123 1,1,2-Trichloroethane ug/kg 55.650 111 70-124 1,1-Dichloroethane ug/kg 49.650 99 63-122 1,1-Dichloroethene ug/kg 52.250 104 71-129 1,1-Dichloropropene ug/kg 56.150 112 71-122 1,2,3-Trichlorobenzene ug/kg 49.750 99 68-123 1,2,3-Trichloropropane ug/kg 83.6 L35016747-117 1,2,4-Trichlorobenzene ug/kg 51.950 104 68-125 1,2,4-Trimethylbenzene ug/kg 50.350 101 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 19 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741636LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 50.750 101 67-121 1,2-Dichlorobenzene ug/kg 49.350 99 71-121 1,2-Dichloroethane ug/kg 54.050 108 74-120 1,2-Dichloropropane ug/kg 52.450 105 71-117 1,3,5-Trimethylbenzene ug/kg 50.950 102 64-119 1,3-Dichlorobenzene ug/kg 50.150 100 70-122 1,3-Dichloropropane ug/kg 51.350 103 68-118 1,4-Dichlorobenzene ug/kg 49.150 98 71-118 2,2-Dichloropropane ug/kg 57.350 115 62-119 2-Butanone (MEK)ug/kg 273250 109 38-154 2-Chlorotoluene ug/kg 49.250 98 71-120 2-Hexanone ug/kg 268250 107 50-134 4-Chlorotoluene ug/kg 50.650 101 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 251250 100 66-122 Acetone ug/kg 297250 119 10-200 Acrolein ug/kg 5551000 56 11-200 Acrylonitrile ug/kg 9281000 93 66-120 Benzene ug/kg 48.350 97 73-115 Bromobenzene ug/kg 48.950 98 64-130 Bromochloromethane ug/kg 52.250 104 71-127 Bromodichloromethane ug/kg 52.950 106 60-121 Bromoform ug/kg 46.250 92 44-130 Bromomethane ug/kg 57.050 114 48-175 Carbon disulfide ug/kg 96.0100 96 71-126 Carbon tetrachloride ug/kg 52.050 104 57-127 Chlorobenzene ug/kg 49.750 99 72-121 Chloroethane ug/kg 48.550 97 72-141 Chloroform ug/kg 55.550 111 74-114 Chloromethane ug/kg 50.050 100 51-126 cis-1,2-Dichloroethene ug/kg 51.250 102 72-115 cis-1,3-Dichloropropene ug/kg 50.650 101 64-115 Dibromochloromethane ug/kg 49.050 98 58-114 Dibromomethane ug/kg 52.250 104 73-120 Dichlorodifluoromethane ug/kg 63.750 127 32-167 Ethyl methacrylate ug/kg 190200 95 65-117 Ethylbenzene ug/kg 51.250 102 73-120 Hexachloro-1,3-butadiene ug/kg 56.750 113 65-121 Iodomethane ug/kg 94.2J100 94 45-156 Isopropylbenzene (Cumene)ug/kg 49.150 98 74-123 Methyl-tert-butyl ether ug/kg 97.9100 98 69-123 Methylene Chloride ug/kg 51.150 102 58-124 n-Butylbenzene ug/kg 56.750 113 71-118 n-Hexane ug/kg 49.6 N2509950-106 n-Propylbenzene ug/kg 50.250 100 70-120 Naphthalene ug/kg 45.150 90 67-124 p-Isopropyltoluene ug/kg 55.850 112 71-123 sec-Butylbenzene ug/kg 51.050 102 66-122 Styrene ug/kg 51.350 103 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 20 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 741636LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 43.250 86 54-124 Tetrachloroethene ug/kg 44.150 88 66-126 Toluene ug/kg 49.550 99 69-115 trans-1,2-Dichloroethene ug/kg 49.750 99 69-120 trans-1,3-Dichloropropene ug/kg 51.650 103 61-116 trans-1,4-Dichloro-2-butene ug/kg 161200 81 59-130 Trichloroethene ug/kg 54.050 108 71-117 Trichlorofluoromethane ug/kg 57.750 115 67-138 Vinyl acetate ug/kg 197200 99 35-134 Vinyl chloride ug/kg 53.650 107 64-127 Xylene (Total)ug/kg 149150 99 69-117 4-Bromofluorobenzene (S)%.105 67-134 Dibromofluoromethane (S)%.103 71-125 Toluene-d8 (S)%.95 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 741637MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063479001 741638 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 24.1 108 10-11198 17 2022.4ND 25.9 21.9 1,1,1-Trichloroethane ug/kg 24.1 101 36-128104 5 2022.4ND 24.4 23.3 1,1,2,2-Tetrachloroethane ug/kg 24.1 83 10-13085 5 2022.4ND 20.1 19.1 1,1,2-Trichloroethane ug/kg 24.1 103 10-12696 14 2022.4ND 24.8 21.6 1,1-Dichloroethane ug/kg 24.1 90 39-12690 7 2022.4ND 21.6 20.2 1,1-Dichloroethene ug/kg 24.1 92 42-14793 6 2022.4ND 22.2 20.9 1,1-Dichloropropene ug/kg 24.1 98 29-12999 6 2022.4ND 23.7 22.2 1,2,3-Trichlorobenzene ug/kg 24.1 70 10-9165 14 2022.4ND 16.7 14.6 1,2,3-Trichloropropane ug/kg M024.1 153 10-99152 7 2022.4ND 36.8 34.2 1,2,4-Trichlorobenzene ug/kg 24.1 73 10-8865 18 2022.4ND 17.6 14.6 1,2,4-Trimethylbenzene ug/kg 24.1 86 10-10984 9 2022.4ND 20.7 18.9 1,2-Dibromoethane (EDB)ug/kg 24.1 94 10-11989 12 2022.4ND 22.7 20.1 1,2-Dichlorobenzene ug/kg 24.1 80 10-10478 10 2022.4ND 19.4 17.5 1,2-Dichloroethane ug/kg 24.1 98 19-126100 5 2022.4ND 23.6 22.4 1,2-Dichloropropane ug/kg 24.1 91 24-12393 5 2022.4ND 22.0 20.9 1,3,5-Trimethylbenzene ug/kg 24.1 87 10-11885 10 2022.4ND 21.0 19.0 1,3-Dichlorobenzene ug/kg 24.1 78 10-10880 5 2022.4ND 18.9 18.0 1,3-Dichloropropane ug/kg 24.1 96 12-12189 14 2022.4ND 23.0 19.9 1,4-Dichlorobenzene ug/kg 24.1 79 10-10478 7 2022.4ND 18.9 17.6 2,2-Dichloropropane ug/kg 24.1 99 32-124101 5 2022.4ND 23.7 22.6 2-Butanone (MEK)ug/kg 120 126 10-183122 10 20112ND151136 2-Chlorotoluene ug/kg 24.1 84 10-12883 8 2022.4ND 20.1 18.6 2-Hexanone ug/kg 120 138 10-158123 19 20112ND166138 4-Chlorotoluene ug/kg 24.1 82 10-11983 5 2022.4ND 19.6 18.7 4-Methyl-2-pentanone (MIBK)ug/kg 120 101 12-13099 8 20112ND121111 Acetone ug/kg R112017510-200147 25 20112ND211165 Acrolein ug/kg 481 44 10-20040 16 20449ND211179 Acrylonitrile ug/kg 481 86 19-13082 12 20449ND416368 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 21 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 741637MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063479001 741638 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 24.1 85 23-13884 8 2022.4ND 20.4 18.8 Bromobenzene ug/kg 24.1 85 10-11179 15 2022.4ND 20.6 17.7 Bromochloromethane ug/kg 24.1 92 26-12691 8 2022.4ND 22.1 20.4 Bromodichloromethane ug/kg 24.1 100 10-12097 10 2022.4ND 24.2 21.8 Bromoform ug/kg 24.1 85 10-10682 11 2022.4ND 20.5 18.5 Bromomethane ug/kg 24.1 96 10-190104 .2 2022.4ND 23.2 23.3 Carbon disulfide ug/kg 48.1 85 31-12884 9 2044.9ND 41.1 37.8 Carbon tetrachloride ug/kg 24.1 96 26-12696 6 2022.4ND 23.0 21.6 Chlorobenzene ug/kg 24.1 86 10-12085 8 2022.4ND 20.7 19.0 Chloroethane ug/kg 24.1 85 18-18685 7 2022.4ND 20.5 19.2 Chloroform ug/kg 24.1 98 29-12699 6 2022.4ND 23.5 22.2 Chloromethane ug/kg 24.1 89 34-13189 6 2022.4ND 21.3 20.1 cis-1,2-Dichloroethene ug/kg 24.1 88 28-13289 6 2022.4ND 21.1 19.9 cis-1,3-Dichloropropene ug/kg 24.1 93 10-10888 12 2022.4ND 22.3 19.8 Dibromochloromethane ug/kg 24.1 95 10-10885 18 2022.4ND 22.8 19.0 Dibromomethane ug/kg 24.1 95 13-12295 6 2022.4ND 22.8 21.4 Dichlorodifluoromethane ug/kg 24.1 113 10-197110 9 2022.4ND 27.2 24.7 Ethyl methacrylate ug/kg 96.3 98 10-13087 19 2089.8ND 94.8 78.4 Ethylbenzene ug/kg 24.1 89 10-13584 13 2022.4ND 21.4 18.8 Hexachloro-1,3-butadiene ug/kg 24.1 75 10-10572 12 2022.4ND 18.1 16.1 Iodomethane ug/kg 48.1 80 10-16384 2044.9ND 38.3J 37.7J Isopropylbenzene (Cumene)ug/kg 24.1 88 10-12184 11 2022.4ND 21.2 18.9 Methyl-tert-butyl ether ug/kg 48.1 94 20-14090 11 2044.9ND 45.0 40.3 Methylene Chloride ug/kg 24.1 93 28-131114 13 2022.4ND 22.4 25.6 n-Butylbenzene ug/kg 24.1 86 10-11082 11 2022.4ND 20.7 18.5 n-Hexane ug/kg N224.1 75 21-15076 5 2022.4ND 18.1 17.1 n-Propylbenzene ug/kg 24.1 84 10-12384 7 2022.4ND 20.2 18.9 Naphthalene ug/kg 24.1 75 10-10673 10 2022.4ND 18.0 16.3 p-Isopropyltoluene ug/kg 24.1 88 10-11794 .4 2022.4ND 21.2 21.1 sec-Butylbenzene ug/kg 24.1 84 10-12382 9 2022.4ND 20.2 18.5 Styrene ug/kg 24.1 91 10-11987 12 2022.4ND 22.0 19.5 tert-Butylbenzene ug/kg 24.1 73 10-10571 10 2022.4ND 17.6 16.0 Tetrachloroethene ug/kg 24.1 85 10-12283 10 2022.4ND 20.5 18.5 Toluene ug/kg 24.1 89 10-13187 9 2022.4ND 21.5 19.6 trans-1,2-Dichloroethene ug/kg 24.1 88 32-13688 7 2022.4ND 21.1 19.8 trans-1,3-Dichloropropene ug/kg 24.1 97 10-10189 16 2022.4ND 23.4 20.0 trans-1,4-Dichloro-2-butene ug/kg 96.3 77 10-10471 15 2089.8ND 74.1 63.8 Trichloroethene ug/kg 24.1 100 15-13399 8 2022.4ND 24.0 22.1 Trichlorofluoromethane ug/kg 24.1 102 37-152106 3 2022.4ND 24.6 23.8 Vinyl acetate ug/kg 96.3 69 10-10368 9 2089.8ND 66.8 60.9 Vinyl chloride ug/kg 24.1 97 41-14797 7 2022.4ND 23.3 21.7 Xylene (Total)ug/kg 72.2 90 10-13183 15 2067.3ND 65.0 56.1 4-Bromofluorobenzene (S)%.103 67-134100 20 Dibromofluoromethane (S)%.103 71-125103 20 Toluene-d8 (S)%.101 76-12494 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 22 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 741639MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063501002 741640 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 47.2 79 10-11192 16 2047.7ND 37.4 43.8 1,1,1-Trichloroethane ug/kg 47.2 92 36-12894 3 2047.7ND 43.4 44.9 1,1,2,2-Tetrachloroethane ug/kg 47.2 65 10-13072 11 2047.7ND 30.9 34.4 1,1,2-Trichloroethane ug/kg 47.2 81 10-12686 7 2047.7ND 38.3 41.2 1,1-Dichloroethane ug/kg 47.2 79 39-12679 1 2047.7ND 37.4 37.8 1,1-Dichloroethene ug/kg 47.2 88 42-14785 3 2047.7ND 41.8 40.6 1,1-Dichloropropene ug/kg 47.2 90 29-12992 3 2047.7ND 42.6 44.0 1,2,3-Trichlorobenzene ug/kg 47.2 30 10-9131 5 2047.7ND 14.2 14.8 1,2,3-Trichloropropane ug/kg M047.2 106 10-99126 18 2047.7ND 50.0 60.0 1,2,4-Trichlorobenzene ug/kg 47.2 31 10-8833 7 2047.7ND 14.7 15.8 1,2,4-Trimethylbenzene ug/kg 47.2 57 10-10959 4 2047.7ND 26.8 28.0 1,2-Dibromoethane (EDB)ug/kg 47.2 73 10-11980 10 2047.7ND 34.5 38.1 1,2-Dichlorobenzene ug/kg 47.2 46 10-10453 15 2047.7ND 21.9 25.4 1,2-Dichloroethane ug/kg 47.2 89 19-12690 2 2047.7ND 42.0 43.0 1,2-Dichloropropane ug/kg 47.2 79 24-12383 6 2047.7ND 37.5 39.8 1,3,5-Trimethylbenzene ug/kg 47.2 59 10-11863 8 2047.7ND 27.7 30.0 1,3-Dichlorobenzene ug/kg 47.2 49 10-10854 10 2047.7ND 23.2 25.6 1,3-Dichloropropane ug/kg 47.2 71 12-12179 11 2047.7ND 33.7 37.6 1,4-Dichlorobenzene ug/kg 47.2 48 10-10453 11 2047.7ND 22.5 25.1 2,2-Dichloropropane ug/kg 47.2 92 32-12488 3 2047.7ND 43.6 42.2 2-Butanone (MEK)ug/kg 237 79 10-18376 2 20239ND186182 2-Chlorotoluene ug/kg 47.2 57 10-12861 7 2047.7ND 27.1 29.1 2-Hexanone ug/kg 237 78 10-15885 9 20239ND184202 4-Chlorotoluene ug/kg 47.2 55 10-11962 14 2047.7ND 25.9 29.8 4-Methyl-2-pentanone (MIBK)ug/kg 237 81 12-13083 4 20239ND190198 Acetone ug/kg R123712510-20099 22 20239ND295237 Acrolein ug/kg 945 34 10-20033 2 20955ND318312 Acrylonitrile ug/kg 945 72 19-13068 5 20955ND681645 Benzene ug/kg 47.2 78 23-13878 2 2047.7ND 36.7 37.3 Bromobenzene ug/kg 47.2 59 10-11165 10 2047.7ND 28.0 30.9 Bromochloromethane ug/kg 47.2 83 26-12683 2 2047.7ND 39.0 39.7 Bromodichloromethane ug/kg 47.2 89 10-12094 6 2047.7ND 42.1 44.7 Bromoform ug/kg 47.2 62 10-10674 19 2047.7ND 29.4 35.5 Bromomethane ug/kg 47.2 92 10-19095 5 2047.7ND 43.4 45.4 Carbon disulfide ug/kg 94.5 78 31-12879 2 2095.5ND 74.1 75.3 Carbon tetrachloride ug/kg 47.2 89 26-12693 5 2047.7ND 42.0 44.3 Chlorobenzene ug/kg 47.2 64 10-12069 9 2047.7ND 30.0 33.0 Chloroethane ug/kg 47.2 80 18-18677 4 2047.7ND 38.0 36.7 Chloroform ug/kg 47.2 88 29-12690 3 2047.7ND 41.7 43.0 Chloromethane ug/kg 47.2 88 34-13186 1 2047.7ND 41.4 40.9 cis-1,2-Dichloroethene ug/kg 47.2 76 28-13275 1 2047.7ND 36.1 35.6 cis-1,3-Dichloropropene ug/kg 47.2 71 10-10883 16 2047.7ND 33.7 39.6 Dibromochloromethane ug/kg 47.2 72 10-10882 14 2047.7ND 34.0 39.2 Dibromomethane ug/kg 47.2 84 13-12287 4 2047.7ND 39.8 41.5 Dichlorodifluoromethane ug/kg 47.2 113 10-197108 4 2047.7ND 53.6 51.7 Ethyl methacrylate ug/kg 189 21 10-13041 20191NDND77.5J Ethylbenzene ug/kg 47.2 66 10-13571 8 2047.7ND 31.1 33.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 23 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 741639MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063501002 741640 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Hexachloro-1,3-butadiene ug/kg 47.2 44 10-10545 3 2047.7ND 20.8 21.3 Iodomethane ug/kg 94.5 74 10-16379 2095.5ND 69.9J 75.5J Isopropylbenzene (Cumene)ug/kg 47.2 62 10-12165 6 2047.7ND 29.3 31.1 Methyl-tert-butyl ether ug/kg 94.5 84 20-14080 3 2095.5ND 79.0 76.8 Methylene Chloride ug/kg 47.2 88 28-13191 4 2047.7ND 41.8 43.4 n-Butylbenzene ug/kg 47.2 53 10-11054 3 2047.7ND 24.8 25.7 n-Hexane ug/kg N247.2 62 21-15058 4 2047.7ND 29.1 27.9 n-Propylbenzene ug/kg 47.2 59 10-12363 8 2047.7ND 28.0 30.3 Naphthalene ug/kg 47.2 34 10-10637 10 2047.7ND 16.1 17.9 p-Isopropyltoluene ug/kg 47.2 59 10-11762 6 2047.7ND 27.8 29.5 sec-Butylbenzene ug/kg 47.2 57 10-12358 3 2047.7ND 27.0 27.8 Styrene ug/kg 47.2 61 10-11970 15 2047.7ND 28.7 33.4 tert-Butylbenzene ug/kg 47.2 51 10-10553 5 2047.7ND 24.1 25.4 Tetrachloroethene ug/kg 47.2 63 10-12265 4 2047.7ND 30.0 31.1 Toluene ug/kg 47.2 71 10-13176 8 2047.7ND 33.5 36.3 trans-1,2-Dichloroethene ug/kg 47.2 78 32-13678 .4 2047.7ND 36.9 37.1 trans-1,3-Dichloropropene ug/kg 47.2 72 10-10180 12 2047.7ND 34.0 38.2 trans-1,4-Dichloro-2-butene ug/kg 189 53 10-10463 17 20191ND101120 Trichloroethene ug/kg 47.2 84 15-13387 5 2047.7ND 39.6 41.6 Trichlorofluoromethane ug/kg 47.2 103 37-152103 1 2047.7ND 48.5 49.2 Vinyl acetate ug/kg M0189210-1036 20191NDNDND Vinyl chloride ug/kg 47.2 92 41-14790 1 2047.7ND 43.6 43.1 Xylene (Total)ug/kg 142 65 10-13171 10 20143ND91.9 101 4-Bromofluorobenzene (S)%.103 67-134105 20 Dibromofluoromethane (S)%.108 71-125103 20 Toluene-d8 (S)%.99 76-12497 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 24 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063479 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/7101 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5063479001, 5063479002, 5063479003 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063479001 743944SAMPLE DUPLICATE: Percent Moisture %11.0 3 510.7 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063698004 743945SAMPLE DUPLICATE: Percent Moisture %15.1 R110516.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 25 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5063479 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS The presence of this compound indicates the possible use of commercially purchased deionized water. slb0531121d Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 26 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5063479 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5063479004 MSV/42561SBI068:FB-4:W052412 EPA 8260 5063479001 MSV/42554SBI068:AMW1D:S180190 EPA 8260 5063479002 MSV/42554SBI068:AMW1D:S140155 EPA 8260 5063479003 MSV/42554SBI068:AMW1D:S140155A EPA 8260 5063479001 PMST/7101SBI068:AMW1D:S180190 ASTM D2974-87 5063479002 PMST/7101SBI068:AMW1D:S140155 ASTM D2974-87 5063479003 PMST/7101SBI068:AMW1D:S140155A ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:42 AM Page 27 of 27 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 June 08, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5063623 5063623 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on May 30, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5063623 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5063623 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5063623001 SBI068:AMW3D:S160176 Solid 05/29/12 12:00 05/30/12 12:19 5063623002 SBI068:AMW3D:S040054 Solid 05/29/12 12:15 05/30/12 12:19 5063623003 SBI068:AMW3D:S040054A Solid 05/29/12 12:18 05/30/12 12:19 5063623004 SBI068:FB5:W052912 Water 05/29/12 12:25 05/30/12 12:19 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5063623 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5063623001 SBI068:AMW3D:S160176 EPA 8260 73GRM ASTM D2974-87 1DAE 5063623002 SBI068:AMW3D:S040054 EPA 8260 73GRM ASTM D2974-87 1DAE 5063623003 SBI068:AMW3D:S040054A EPA 8260 73GRM ASTM D2974-87 1DAE 5063623004 SBI068:FB5:W052912 EPA 8260 73GRM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S160176 Lab ID:5063623001 Collected:05/29/12 12:00 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/01/12 18:40 67-64-159.6 Acrolein ND ug/kg 1 06/01/12 18:40 107-02-859.6 Acrylonitrile ND ug/kg 1 06/01/12 18:40 107-13-159.6 Benzene ND ug/kg 1 06/01/12 18:40 71-43-23.0 Bromobenzene ND ug/kg 1 06/01/12 18:40 108-86-13.0 Bromochloromethane ND ug/kg 1 06/01/12 18:40 74-97-53.0 Bromodichloromethane ND ug/kg 1 06/01/12 18:40 75-27-43.0 Bromoform ND ug/kg 1 06/01/12 18:40 75-25-23.0 Bromomethane ND ug/kg 1 06/01/12 18:40 74-83-93.0 2-Butanone (MEK)ND ug/kg 1 06/01/12 18:40 78-93-314.9 n-Butylbenzene ND ug/kg 1 06/01/12 18:40 104-51-83.0 sec-Butylbenzene ND ug/kg 1 06/01/12 18:40 135-98-83.0 tert-Butylbenzene ND ug/kg 1 06/01/12 18:40 98-06-63.0 Carbon disulfide ND ug/kg 1 06/01/12 18:40 75-15-06.0 Carbon tetrachloride ND ug/kg 1 06/01/12 18:40 56-23-53.0 Chlorobenzene ND ug/kg 1 06/01/12 18:40 108-90-73.0 Chloroethane ND ug/kg 1 06/01/12 18:40 75-00-33.0 Chloroform ND ug/kg 1 06/01/12 18:40 67-66-33.0 Chloromethane ND ug/kg 1 06/01/12 18:40 74-87-33.0 2-Chlorotoluene ND ug/kg 1 06/01/12 18:40 95-49-83.0 4-Chlorotoluene ND ug/kg 1 06/01/12 18:40 106-43-43.0 Dibromochloromethane ND ug/kg 1 06/01/12 18:40 124-48-13.0 1,2-Dibromoethane (EDB)ND ug/kg 1 06/01/12 18:40 106-93-43.0 Dibromomethane ND ug/kg 1 06/01/12 18:40 74-95-33.0 1,2-Dichlorobenzene ND ug/kg 1 06/01/12 18:40 95-50-13.0 1,3-Dichlorobenzene ND ug/kg 1 06/01/12 18:40 541-73-13.0 1,4-Dichlorobenzene ND ug/kg 1 06/01/12 18:40 106-46-73.0 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/01/12 18:40 110-57-659.6 Dichlorodifluoromethane ND ug/kg 1 06/01/12 18:40 75-71-83.0 1,1-Dichloroethane ND ug/kg 1 06/01/12 18:40 75-34-33.0 1,2-Dichloroethane ND ug/kg 1 06/01/12 18:40 107-06-23.0 1,1-Dichloroethene ND ug/kg 1 06/01/12 18:40 75-35-43.0 cis-1,2-Dichloroethene ND ug/kg 1 06/01/12 18:40 156-59-23.0 trans-1,2-Dichloroethene ND ug/kg 1 06/01/12 18:40 156-60-53.0 1,2-Dichloropropane ND ug/kg 1 06/01/12 18:40 78-87-53.0 1,3-Dichloropropane ND ug/kg 1 06/01/12 18:40 142-28-93.0 2,2-Dichloropropane ND ug/kg 1 06/01/12 18:40 594-20-73.0 1,1-Dichloropropene ND ug/kg 1 06/01/12 18:40 563-58-63.0 cis-1,3-Dichloropropene ND ug/kg 1 06/01/12 18:40 10061-01-53.0 trans-1,3-Dichloropropene ND ug/kg 1 06/01/12 18:40 10061-02-63.0 Ethylbenzene ND ug/kg 1 06/01/12 18:40 100-41-43.0 Ethyl methacrylate ND ug/kg 1 06/01/12 18:40 97-63-259.6 Hexachloro-1,3-butadiene ND ug/kg 1 06/01/12 18:40 87-68-33.0 n-Hexane ND ug/kg 1 06/01/12 18:40 110-54-3 N23.0 2-Hexanone ND ug/kg 1 06/01/12 18:40 591-78-659.6 Iodomethane ND ug/kg 1 06/01/12 18:40 74-88-459.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 5 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S160176 Lab ID:5063623001 Collected:05/29/12 12:00 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/01/12 18:40 98-82-83.0 p-Isopropyltoluene ND ug/kg 1 06/01/12 18:40 99-87-63.0 Methylene Chloride ND ug/kg 1 06/01/12 18:40 75-09-211.9 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/01/12 18:40 108-10-114.9 Methyl-tert-butyl ether ND ug/kg 1 06/01/12 18:40 1634-04-43.0 Naphthalene ND ug/kg 1 06/01/12 18:40 91-20-33.0 n-Propylbenzene ND ug/kg 1 06/01/12 18:40 103-65-13.0 Styrene ND ug/kg 1 06/01/12 18:40 100-42-53.0 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/01/12 18:40 630-20-63.0 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/01/12 18:40 79-34-53.0 Tetrachloroethene ND ug/kg 1 06/01/12 18:40 127-18-43.0 Toluene ND ug/kg 1 06/01/12 18:40 108-88-33.0 1,2,3-Trichlorobenzene ND ug/kg 1 06/01/12 18:40 87-61-63.0 1,2,4-Trichlorobenzene ND ug/kg 1 06/01/12 18:40 120-82-13.0 1,1,1-Trichloroethane ND ug/kg 1 06/01/12 18:40 71-55-63.0 1,1,2-Trichloroethane ND ug/kg 1 06/01/12 18:40 79-00-53.0 Trichloroethene ND ug/kg 1 06/01/12 18:40 79-01-63.0 Trichlorofluoromethane ND ug/kg 1 06/01/12 18:40 75-69-43.0 1,2,3-Trichloropropane ND ug/kg 1 06/01/12 18:40 96-18-43.0 1,2,4-Trimethylbenzene ND ug/kg 1 06/01/12 18:40 95-63-63.0 1,3,5-Trimethylbenzene ND ug/kg 1 06/01/12 18:40 108-67-83.0 Vinyl acetate ND ug/kg 1 06/01/12 18:40 108-05-459.6 Vinyl chloride ND ug/kg 1 06/01/12 18:40 75-01-43.0 Xylene (Total)ND ug/kg 1 06/01/12 18:40 1330-20-76.0 Surrogates Dibromofluoromethane (S)92 %.1 06/01/12 18:40 1868-53-771-125 Toluene-d8 (S)100 %.1 06/01/12 18:40 2037-26-576-124 4-Bromofluorobenzene (S)91 %.1 06/01/12 18:40 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 11.4 %1 06/05/12 18:170.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 6 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S040054 Lab ID:5063623002 Collected:05/29/12 12:15 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/01/12 20:16 67-64-156.7 Acrolein ND ug/kg 1 06/01/12 20:16 107-02-856.7 Acrylonitrile ND ug/kg 1 06/01/12 20:16 107-13-156.7 Benzene ND ug/kg 1 06/01/12 20:16 71-43-22.8 Bromobenzene ND ug/kg 1 06/01/12 20:16 108-86-12.8 Bromochloromethane ND ug/kg 1 06/01/12 20:16 74-97-52.8 Bromodichloromethane ND ug/kg 1 06/01/12 20:16 75-27-42.8 Bromoform ND ug/kg 1 06/01/12 20:16 75-25-22.8 Bromomethane ND ug/kg 1 06/01/12 20:16 74-83-92.8 2-Butanone (MEK)ND ug/kg 1 06/01/12 20:16 78-93-314.2 n-Butylbenzene ND ug/kg 1 06/01/12 20:16 104-51-82.8 sec-Butylbenzene ND ug/kg 1 06/01/12 20:16 135-98-82.8 tert-Butylbenzene ND ug/kg 1 06/01/12 20:16 98-06-62.8 Carbon disulfide ND ug/kg 1 06/01/12 20:16 75-15-05.7 Carbon tetrachloride ND ug/kg 1 06/01/12 20:16 56-23-52.8 Chlorobenzene ND ug/kg 1 06/01/12 20:16 108-90-72.8 Chloroethane ND ug/kg 1 06/01/12 20:16 75-00-32.8 Chloroform ND ug/kg 1 06/01/12 20:16 67-66-32.8 Chloromethane ND ug/kg 1 06/01/12 20:16 74-87-32.8 2-Chlorotoluene ND ug/kg 1 06/01/12 20:16 95-49-82.8 4-Chlorotoluene ND ug/kg 1 06/01/12 20:16 106-43-42.8 Dibromochloromethane ND ug/kg 1 06/01/12 20:16 124-48-12.8 1,2-Dibromoethane (EDB)ND ug/kg 1 06/01/12 20:16 106-93-42.8 Dibromomethane ND ug/kg 1 06/01/12 20:16 74-95-32.8 1,2-Dichlorobenzene ND ug/kg 1 06/01/12 20:16 95-50-12.8 1,3-Dichlorobenzene ND ug/kg 1 06/01/12 20:16 541-73-12.8 1,4-Dichlorobenzene ND ug/kg 1 06/01/12 20:16 106-46-72.8 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/01/12 20:16 110-57-656.7 Dichlorodifluoromethane ND ug/kg 1 06/01/12 20:16 75-71-82.8 1,1-Dichloroethane ND ug/kg 1 06/01/12 20:16 75-34-32.8 1,2-Dichloroethane ND ug/kg 1 06/01/12 20:16 107-06-22.8 1,1-Dichloroethene ND ug/kg 1 06/01/12 20:16 75-35-42.8 cis-1,2-Dichloroethene ND ug/kg 1 06/01/12 20:16 156-59-22.8 trans-1,2-Dichloroethene ND ug/kg 1 06/01/12 20:16 156-60-52.8 1,2-Dichloropropane ND ug/kg 1 06/01/12 20:16 78-87-52.8 1,3-Dichloropropane ND ug/kg 1 06/01/12 20:16 142-28-92.8 2,2-Dichloropropane ND ug/kg 1 06/01/12 20:16 594-20-72.8 1,1-Dichloropropene ND ug/kg 1 06/01/12 20:16 563-58-62.8 cis-1,3-Dichloropropene ND ug/kg 1 06/01/12 20:16 10061-01-52.8 trans-1,3-Dichloropropene ND ug/kg 1 06/01/12 20:16 10061-02-62.8 Ethylbenzene ND ug/kg 1 06/01/12 20:16 100-41-42.8 Ethyl methacrylate ND ug/kg 1 06/01/12 20:16 97-63-256.7 Hexachloro-1,3-butadiene ND ug/kg 1 06/01/12 20:16 87-68-32.8 n-Hexane ND ug/kg 1 06/01/12 20:16 110-54-3 N22.8 2-Hexanone ND ug/kg 1 06/01/12 20:16 591-78-656.7 Iodomethane ND ug/kg 1 06/01/12 20:16 74-88-456.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 7 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S040054 Lab ID:5063623002 Collected:05/29/12 12:15 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/01/12 20:16 98-82-82.8 p-Isopropyltoluene ND ug/kg 1 06/01/12 20:16 99-87-62.8 Methylene Chloride ND ug/kg 1 06/01/12 20:16 75-09-211.3 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/01/12 20:16 108-10-114.2 Methyl-tert-butyl ether ND ug/kg 1 06/01/12 20:16 1634-04-42.8 Naphthalene ND ug/kg 1 06/01/12 20:16 91-20-32.8 n-Propylbenzene ND ug/kg 1 06/01/12 20:16 103-65-12.8 Styrene ND ug/kg 1 06/01/12 20:16 100-42-52.8 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/01/12 20:16 630-20-62.8 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/01/12 20:16 79-34-52.8 Tetrachloroethene ND ug/kg 1 06/01/12 20:16 127-18-42.8 Toluene ND ug/kg 1 06/01/12 20:16 108-88-32.8 1,2,3-Trichlorobenzene ND ug/kg 1 06/01/12 20:16 87-61-62.8 1,2,4-Trichlorobenzene ND ug/kg 1 06/01/12 20:16 120-82-12.8 1,1,1-Trichloroethane ND ug/kg 1 06/01/12 20:16 71-55-62.8 1,1,2-Trichloroethane ND ug/kg 1 06/01/12 20:16 79-00-52.8 Trichloroethene ND ug/kg 1 06/01/12 20:16 79-01-62.8 Trichlorofluoromethane ND ug/kg 1 06/01/12 20:16 75-69-42.8 1,2,3-Trichloropropane ND ug/kg 1 06/01/12 20:16 96-18-42.8 1,2,4-Trimethylbenzene ND ug/kg 1 06/01/12 20:16 95-63-62.8 1,3,5-Trimethylbenzene ND ug/kg 1 06/01/12 20:16 108-67-82.8 Vinyl acetate ND ug/kg 1 06/01/12 20:16 108-05-456.7 Vinyl chloride ND ug/kg 1 06/01/12 20:16 75-01-42.8 Xylene (Total)ND ug/kg 1 06/01/12 20:16 1330-20-75.7 Surrogates Dibromofluoromethane (S)96 %.1 06/01/12 20:16 1868-53-771-125 Toluene-d8 (S)98 %.1 06/01/12 20:16 2037-26-576-124 4-Bromofluorobenzene (S)93 %.1 06/01/12 20:16 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.9 %1 06/05/12 18:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 8 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S040054A Lab ID:5063623003 Collected:05/29/12 12:18 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/01/12 20:48 67-64-141.2 Acrolein ND ug/kg 1 06/01/12 20:48 107-02-841.2 Acrylonitrile ND ug/kg 1 06/01/12 20:48 107-13-141.2 Benzene ND ug/kg 1 06/01/12 20:48 71-43-22.1 Bromobenzene ND ug/kg 1 06/01/12 20:48 108-86-12.1 Bromochloromethane ND ug/kg 1 06/01/12 20:48 74-97-52.1 Bromodichloromethane ND ug/kg 1 06/01/12 20:48 75-27-42.1 Bromoform ND ug/kg 1 06/01/12 20:48 75-25-22.1 Bromomethane ND ug/kg 1 06/01/12 20:48 74-83-92.1 2-Butanone (MEK)ND ug/kg 1 06/01/12 20:48 78-93-310.3 n-Butylbenzene ND ug/kg 1 06/01/12 20:48 104-51-82.1 sec-Butylbenzene ND ug/kg 1 06/01/12 20:48 135-98-82.1 tert-Butylbenzene ND ug/kg 1 06/01/12 20:48 98-06-62.1 Carbon disulfide ND ug/kg 1 06/01/12 20:48 75-15-04.1 Carbon tetrachloride ND ug/kg 1 06/01/12 20:48 56-23-52.1 Chlorobenzene ND ug/kg 1 06/01/12 20:48 108-90-72.1 Chloroethane ND ug/kg 1 06/01/12 20:48 75-00-32.1 Chloroform ND ug/kg 1 06/01/12 20:48 67-66-32.1 Chloromethane ND ug/kg 1 06/01/12 20:48 74-87-32.1 2-Chlorotoluene ND ug/kg 1 06/01/12 20:48 95-49-82.1 4-Chlorotoluene ND ug/kg 1 06/01/12 20:48 106-43-42.1 Dibromochloromethane ND ug/kg 1 06/01/12 20:48 124-48-12.1 1,2-Dibromoethane (EDB)ND ug/kg 1 06/01/12 20:48 106-93-42.1 Dibromomethane ND ug/kg 1 06/01/12 20:48 74-95-32.1 1,2-Dichlorobenzene ND ug/kg 1 06/01/12 20:48 95-50-12.1 1,3-Dichlorobenzene ND ug/kg 1 06/01/12 20:48 541-73-12.1 1,4-Dichlorobenzene ND ug/kg 1 06/01/12 20:48 106-46-72.1 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/01/12 20:48 110-57-641.2 Dichlorodifluoromethane ND ug/kg 1 06/01/12 20:48 75-71-82.1 1,1-Dichloroethane ND ug/kg 1 06/01/12 20:48 75-34-32.1 1,2-Dichloroethane ND ug/kg 1 06/01/12 20:48 107-06-22.1 1,1-Dichloroethene ND ug/kg 1 06/01/12 20:48 75-35-42.1 cis-1,2-Dichloroethene ND ug/kg 1 06/01/12 20:48 156-59-22.1 trans-1,2-Dichloroethene ND ug/kg 1 06/01/12 20:48 156-60-52.1 1,2-Dichloropropane ND ug/kg 1 06/01/12 20:48 78-87-52.1 1,3-Dichloropropane ND ug/kg 1 06/01/12 20:48 142-28-92.1 2,2-Dichloropropane ND ug/kg 1 06/01/12 20:48 594-20-72.1 1,1-Dichloropropene ND ug/kg 1 06/01/12 20:48 563-58-62.1 cis-1,3-Dichloropropene ND ug/kg 1 06/01/12 20:48 10061-01-52.1 trans-1,3-Dichloropropene ND ug/kg 1 06/01/12 20:48 10061-02-62.1 Ethylbenzene ND ug/kg 1 06/01/12 20:48 100-41-42.1 Ethyl methacrylate ND ug/kg 1 06/01/12 20:48 97-63-241.2 Hexachloro-1,3-butadiene ND ug/kg 1 06/01/12 20:48 87-68-32.1 n-Hexane ND ug/kg 1 06/01/12 20:48 110-54-3 N22.1 2-Hexanone ND ug/kg 1 06/01/12 20:48 591-78-641.2 Iodomethane ND ug/kg 1 06/01/12 20:48 74-88-441.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 9 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:AMW3D:S040054A Lab ID:5063623003 Collected:05/29/12 12:18 Received:05/30/12 12:19 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/01/12 20:48 98-82-82.1 p-Isopropyltoluene ND ug/kg 1 06/01/12 20:48 99-87-62.1 Methylene Chloride ND ug/kg 1 06/01/12 20:48 75-09-28.2 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/01/12 20:48 108-10-110.3 Methyl-tert-butyl ether ND ug/kg 1 06/01/12 20:48 1634-04-42.1 Naphthalene ND ug/kg 1 06/01/12 20:48 91-20-32.1 n-Propylbenzene ND ug/kg 1 06/01/12 20:48 103-65-12.1 Styrene ND ug/kg 1 06/01/12 20:48 100-42-52.1 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/01/12 20:48 630-20-62.1 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/01/12 20:48 79-34-52.1 Tetrachloroethene ND ug/kg 1 06/01/12 20:48 127-18-42.1 Toluene ND ug/kg 1 06/01/12 20:48 108-88-32.1 1,2,3-Trichlorobenzene ND ug/kg 1 06/01/12 20:48 87-61-62.1 1,2,4-Trichlorobenzene ND ug/kg 1 06/01/12 20:48 120-82-12.1 1,1,1-Trichloroethane ND ug/kg 1 06/01/12 20:48 71-55-62.1 1,1,2-Trichloroethane ND ug/kg 1 06/01/12 20:48 79-00-52.1 Trichloroethene ND ug/kg 1 06/01/12 20:48 79-01-62.1 Trichlorofluoromethane ND ug/kg 1 06/01/12 20:48 75-69-42.1 1,2,3-Trichloropropane ND ug/kg 1 06/01/12 20:48 96-18-42.1 1,2,4-Trimethylbenzene ND ug/kg 1 06/01/12 20:48 95-63-62.1 1,3,5-Trimethylbenzene ND ug/kg 1 06/01/12 20:48 108-67-82.1 Vinyl acetate ND ug/kg 1 06/01/12 20:48 108-05-441.2 Vinyl chloride ND ug/kg 1 06/01/12 20:48 75-01-42.1 Xylene (Total)ND ug/kg 1 06/01/12 20:48 1330-20-74.1 Surrogates Dibromofluoromethane (S)94 %.1 06/01/12 20:48 1868-53-771-125 Toluene-d8 (S)98 %.1 06/01/12 20:48 2037-26-576-124 4-Bromofluorobenzene (S)94 %.1 06/01/12 20:48 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.8 %1 06/05/12 18:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 10 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:FB5:W052912 Lab ID:5063623004 Collected:05/29/12 12:25 Received:05/30/12 12:19 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/01/12 17:35 67-64-1100 Acrolein ND ug/L 1 06/01/12 17:35 107-02-8100 Acrylonitrile ND ug/L 1 06/01/12 17:35 107-13-1100 Benzene ND ug/L 1 06/01/12 17:35 71-43-25.0 Bromobenzene ND ug/L 1 06/01/12 17:35 108-86-15.0 Bromochloromethane ND ug/L 1 06/01/12 17:35 74-97-55.0 Bromodichloromethane ND ug/L 1 06/01/12 17:35 75-27-45.0 Bromoform ND ug/L 1 06/01/12 17:35 75-25-25.0 Bromomethane ND ug/L 1 06/01/12 17:35 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/01/12 17:35 78-93-325.0 n-Butylbenzene ND ug/L 1 06/01/12 17:35 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/01/12 17:35 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/01/12 17:35 98-06-65.0 Carbon disulfide ND ug/L 1 06/01/12 17:35 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/01/12 17:35 56-23-55.0 Chlorobenzene ND ug/L 1 06/01/12 17:35 108-90-75.0 Chloroethane ND ug/L 1 06/01/12 17:35 75-00-35.0 Chloroform ND ug/L 1 06/01/12 17:35 67-66-35.0 Chloromethane ND ug/L 1 06/01/12 17:35 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/01/12 17:35 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/01/12 17:35 106-43-45.0 Dibromochloromethane ND ug/L 1 06/01/12 17:35 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/01/12 17:35 106-93-45.0 Dibromomethane ND ug/L 1 06/01/12 17:35 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/01/12 17:35 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/01/12 17:35 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/01/12 17:35 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/01/12 17:35 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/01/12 17:35 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/01/12 17:35 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/01/12 17:35 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/01/12 17:35 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/01/12 17:35 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/01/12 17:35 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/01/12 17:35 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/01/12 17:35 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/01/12 17:35 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/01/12 17:35 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/01/12 17:35 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/01/12 17:35 10061-02-65.0 Ethylbenzene ND ug/L 1 06/01/12 17:35 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/01/12 17:35 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/01/12 17:35 87-68-35.0 n-Hexane ND ug/L 1 06/01/12 17:35 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/01/12 17:35 591-78-625.0 Iodomethane ND ug/L 1 06/01/12 17:35 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/01/12 17:35 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 11 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063623 SBI068 Sample:SBI068:FB5:W052912 Lab ID:5063623004 Collected:05/29/12 12:25 Received:05/30/12 12:19 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/01/12 17:35 99-87-65.0 Methylene Chloride ND ug/L 1 06/01/12 17:35 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/01/12 17:35 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/01/12 17:35 1634-04-44.0 Naphthalene ND ug/L 1 06/01/12 17:35 91-20-35.0 n-Propylbenzene ND ug/L 1 06/01/12 17:35 103-65-15.0 Styrene ND ug/L 1 06/01/12 17:35 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/01/12 17:35 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/01/12 17:35 79-34-55.0 Tetrachloroethene ND ug/L 1 06/01/12 17:35 127-18-45.0 Toluene ND ug/L 1 06/01/12 17:35 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/01/12 17:35 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/01/12 17:35 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/01/12 17:35 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/01/12 17:35 79-00-55.0 Trichloroethene ND ug/L 1 06/01/12 17:35 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/01/12 17:35 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/01/12 17:35 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/01/12 17:35 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/01/12 17:35 108-67-85.0 Vinyl acetate ND ug/L 1 06/01/12 17:35 108-05-450.0 Vinyl chloride ND ug/L 1 06/01/12 17:35 75-01-42.0 Xylene (Total)ND ug/L 1 06/01/12 17:35 1330-20-710.0 Surrogates Dibromofluoromethane (S)94 %.1 06/01/12 17:35 1868-53-783-123 4-Bromofluorobenzene (S)93 %.1 06/01/12 17:35 460-00-472-125 Toluene-d8 (S)98 %.1 06/01/12 17:35 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 12 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42701 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5063623004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:743893 Associated Lab Samples:5063623004 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/01/12 13:53 1,1,1-Trichloroethane ug/L ND 5.0 06/01/12 13:53 1,1,2,2-Tetrachloroethane ug/L ND 5.0 06/01/12 13:53 1,1,2-Trichloroethane ug/L ND 5.0 06/01/12 13:53 1,1-Dichloroethane ug/L ND 5.0 06/01/12 13:53 1,1-Dichloroethene ug/L ND 5.0 06/01/12 13:53 1,1-Dichloropropene ug/L ND 5.0 06/01/12 13:53 1,2,3-Trichlorobenzene ug/L ND 5.0 06/01/12 13:53 1,2,3-Trichloropropane ug/L ND 5.0 06/01/12 13:53 1,2,4-Trichlorobenzene ug/L ND 5.0 06/01/12 13:53 1,2,4-Trimethylbenzene ug/L ND 5.0 06/01/12 13:53 1,2-Dibromoethane (EDB)ug/L ND 5.0 06/01/12 13:53 1,2-Dichlorobenzene ug/L ND 5.0 06/01/12 13:53 1,2-Dichloroethane ug/L ND 5.0 06/01/12 13:53 1,2-Dichloropropane ug/L ND 5.0 06/01/12 13:53 1,3,5-Trimethylbenzene ug/L ND 5.0 06/01/12 13:53 1,3-Dichlorobenzene ug/L ND 5.0 06/01/12 13:53 1,3-Dichloropropane ug/L ND 5.0 06/01/12 13:53 1,4-Dichlorobenzene ug/L ND 5.0 06/01/12 13:53 2,2-Dichloropropane ug/L ND 5.0 06/01/12 13:53 2-Butanone (MEK)ug/L ND 25.0 06/01/12 13:53 2-Chlorotoluene ug/L ND 5.0 06/01/12 13:53 2-Hexanone ug/L ND 25.0 06/01/12 13:53 4-Chlorotoluene ug/L ND 5.0 06/01/12 13:53 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 06/01/12 13:53 Acetone ug/L ND 100 06/01/12 13:53 Acrolein ug/L ND 100 06/01/12 13:53 Acrylonitrile ug/L ND 100 06/01/12 13:53 Benzene ug/L ND 5.0 06/01/12 13:53 Bromobenzene ug/L ND 5.0 06/01/12 13:53 Bromochloromethane ug/L ND 5.0 06/01/12 13:53 Bromodichloromethane ug/L ND 5.0 06/01/12 13:53 Bromoform ug/L ND 5.0 06/01/12 13:53 Bromomethane ug/L ND 5.0 06/01/12 13:53 Carbon disulfide ug/L ND 10.0 06/01/12 13:53 Carbon tetrachloride ug/L ND 5.0 06/01/12 13:53 Chlorobenzene ug/L ND 5.0 06/01/12 13:53 Chloroethane ug/L ND 5.0 06/01/12 13:53 Chloroform ug/L ND 5.0 06/01/12 13:53 Chloromethane ug/L ND 5.0 06/01/12 13:53 cis-1,2-Dichloroethene ug/L ND 5.0 06/01/12 13:53 cis-1,3-Dichloropropene ug/L ND 5.0 06/01/12 13:53 Dibromochloromethane ug/L ND 5.0 06/01/12 13:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 13 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:743893 Associated Lab Samples:5063623004 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 06/01/12 13:53 Dichlorodifluoromethane ug/L ND 5.0 06/01/12 13:53 Ethyl methacrylate ug/L ND 100 06/01/12 13:53 Ethylbenzene ug/L ND 5.0 06/01/12 13:53 Hexachloro-1,3-butadiene ug/L ND 5.0 06/01/12 13:53 Iodomethane ug/L ND 10.0 06/01/12 13:53 Isopropylbenzene (Cumene)ug/L ND 5.0 06/01/12 13:53 Methyl-tert-butyl ether ug/L ND 4.0 06/01/12 13:53 Methylene Chloride ug/L ND 5.0 06/01/12 13:53 n-Butylbenzene ug/L ND 5.0 06/01/12 13:53 n-Hexane ug/L ND 5.0 N206/01/12 13:53 n-Propylbenzene ug/L ND 5.0 06/01/12 13:53 Naphthalene ug/L ND 5.0 06/01/12 13:53 p-Isopropyltoluene ug/L ND 5.0 06/01/12 13:53 sec-Butylbenzene ug/L ND 5.0 06/01/12 13:53 Styrene ug/L ND 5.0 06/01/12 13:53 tert-Butylbenzene ug/L ND 5.0 06/01/12 13:53 Tetrachloroethene ug/L ND 5.0 06/01/12 13:53 Toluene ug/L ND 5.0 06/01/12 13:53 trans-1,2-Dichloroethene ug/L ND 5.0 06/01/12 13:53 trans-1,3-Dichloropropene ug/L ND 5.0 06/01/12 13:53 trans-1,4-Dichloro-2-butene ug/L ND 100 06/01/12 13:53 Trichloroethene ug/L ND 5.0 06/01/12 13:53 Trichlorofluoromethane ug/L ND 5.0 06/01/12 13:53 Vinyl acetate ug/L ND 50.0 06/01/12 13:53 Vinyl chloride ug/L ND 2.0 06/01/12 13:53 Xylene (Total)ug/L ND 10.0 06/01/12 13:53 4-Bromofluorobenzene (S)%.94 72-125 06/01/12 13:53 Dibromofluoromethane (S)%.92 83-123 06/01/12 13:53 Toluene-d8 (S)%.98 81-114 06/01/12 13:53 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743894LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 36.250 72 69-122 1,1,1-Trichloroethane ug/L 40.750 81 69-126 1,1,2,2-Tetrachloroethane ug/L 49.350 99 68-134 1,1,2-Trichloroethane ug/L 52.450 105 77-129 1,1-Dichloroethane ug/L 44.450 89 70-127 1,1-Dichloroethene ug/L 42.850 86 75-145 1,1-Dichloropropene ug/L 48.550 97 75-126 1,2,3-Trichlorobenzene ug/L 52.150 104 63-130 1,2,3-Trichloropropane ug/L 67.5 L35013545-121 1,2,4-Trichlorobenzene ug/L 48.250 96 64-122 1,2,4-Trimethylbenzene ug/L 47.750 95 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 14 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743894LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 47.450 95 77-123 1,2-Dichlorobenzene ug/L 46.650 93 74-123 1,2-Dichloroethane ug/L 49.250 98 71-127 1,2-Dichloropropane ug/L 47.850 96 75-126 1,3,5-Trimethylbenzene ug/L 46.950 94 69-129 1,3-Dichlorobenzene ug/L 46.850 94 76-123 1,3-Dichloropropane ug/L 48.250 96 77-126 1,4-Dichlorobenzene ug/L 46.050 92 77-121 2,2-Dichloropropane ug/L 38.950 78 45-138 2-Butanone (MEK)ug/L 248250 99 42-177 2-Chlorotoluene ug/L 46.450 93 74-129 2-Hexanone ug/L 245250 98 57-162 4-Chlorotoluene ug/L 46.050 92 70-125 4-Methyl-2-pentanone (MIBK)ug/L 237250 95 64-135 Acetone ug/L 296250 118 10-200 Acrolein ug/L 6201000 62 10-200 Acrylonitrile ug/L 9431000 94 59-144 Benzene ug/L 46.450 93 76-123 Bromobenzene ug/L 47.250 94 67-130 Bromochloromethane ug/L 47.650 95 58-153 Bromodichloromethane ug/L 41.950 84 71-124 Bromoform ug/L 33.750 67 64-116 Bromomethane ug/L 59.050 118 23-197 Carbon disulfide ug/L 74.7100 75 55-146 Carbon tetrachloride ug/L 34.650 69 65-125 Chlorobenzene ug/L 46.150 92 78-120 Chloroethane ug/L 40.150 80 56-163 Chloroform ug/L 48.950 98 73-122 Chloromethane ug/L 35.550 71 46-146 cis-1,2-Dichloroethene ug/L 46.750 93 79-129 cis-1,3-Dichloropropene ug/L 40.950 82 66-123 Dibromochloromethane ug/L 37.150 74 70-123 Dibromomethane ug/L 47.150 94 73-123 Dichlorodifluoromethane ug/L 42.250 84 19-200 Ethyl methacrylate ug/L 184200 92 70-127 Ethylbenzene ug/L 46.850 94 75-120 Hexachloro-1,3-butadiene ug/L 48.350 97 64-131 Iodomethane ug/L 93.3100 93 16-181 Isopropylbenzene (Cumene)ug/L 44.850 90 73-123 Methyl-tert-butyl ether ug/L 88.5100 88 66-128 Methylene Chloride ug/L 41.150 82 61-138 n-Butylbenzene ug/L 49.150 98 69-130 n-Hexane ug/L 40.7 N2508167-142 n-Propylbenzene ug/L 46.450 93 71-132 Naphthalene ug/L 54.050 108 62-130 p-Isopropyltoluene ug/L 49.450 99 71-126 sec-Butylbenzene ug/L 47.150 94 69-130 Styrene ug/L 46.750 93 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 15 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743894LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 43.550 87 49-114 Tetrachloroethene ug/L 41.150 82 57-125 Toluene ug/L 44.850 90 72-124 trans-1,2-Dichloroethene ug/L 45.950 92 71-145 trans-1,3-Dichloropropene ug/L 39.550 79 58-118 trans-1,4-Dichloro-2-butene ug/L 155200 78 50-121 Trichloroethene ug/L 48.950 98 77-122 Trichlorofluoromethane ug/L 47.150 94 56-159 Vinyl acetate ug/L 145200 72 27-119 Vinyl chloride ug/L 40.350 81 61-146 Xylene (Total)ug/L 137150 91 72-126 4-Bromofluorobenzene (S)%.98 72-125 Dibromofluoromethane (S)%.97 83-123 Toluene-d8 (S)%.97 81-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 16 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42702 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063623001, 5063623002, 5063623003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:743896 Associated Lab Samples:5063623001, 5063623002, 5063623003 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/01/12 14:25 1,1,1-Trichloroethane ug/kg ND 5.0 06/01/12 14:25 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/01/12 14:25 1,1,2-Trichloroethane ug/kg ND 5.0 06/01/12 14:25 1,1-Dichloroethane ug/kg ND 5.0 06/01/12 14:25 1,1-Dichloroethene ug/kg ND 5.0 06/01/12 14:25 1,1-Dichloropropene ug/kg ND 5.0 06/01/12 14:25 1,2,3-Trichlorobenzene ug/kg ND 5.0 06/01/12 14:25 1,2,3-Trichloropropane ug/kg ND 5.0 06/01/12 14:25 1,2,4-Trichlorobenzene ug/kg ND 5.0 06/01/12 14:25 1,2,4-Trimethylbenzene ug/kg ND 5.0 06/01/12 14:25 1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/01/12 14:25 1,2-Dichlorobenzene ug/kg ND 5.0 06/01/12 14:25 1,2-Dichloroethane ug/kg ND 5.0 06/01/12 14:25 1,2-Dichloropropane ug/kg ND 5.0 06/01/12 14:25 1,3,5-Trimethylbenzene ug/kg ND 5.0 06/01/12 14:25 1,3-Dichlorobenzene ug/kg ND 5.0 06/01/12 14:25 1,3-Dichloropropane ug/kg ND 5.0 06/01/12 14:25 1,4-Dichlorobenzene ug/kg ND 5.0 06/01/12 14:25 2,2-Dichloropropane ug/kg ND 5.0 06/01/12 14:25 2-Butanone (MEK)ug/kg ND 25.0 06/01/12 14:25 2-Chlorotoluene ug/kg ND 5.0 06/01/12 14:25 2-Hexanone ug/kg ND 100 06/01/12 14:25 4-Chlorotoluene ug/kg ND 5.0 06/01/12 14:25 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 06/01/12 14:25 Acetone ug/kg ND 100 06/01/12 14:25 Acrolein ug/kg ND 100 06/01/12 14:25 Acrylonitrile ug/kg ND 100 06/01/12 14:25 Benzene ug/kg ND 5.0 06/01/12 14:25 Bromobenzene ug/kg ND 5.0 06/01/12 14:25 Bromochloromethane ug/kg ND 5.0 06/01/12 14:25 Bromodichloromethane ug/kg ND 5.0 06/01/12 14:25 Bromoform ug/kg ND 5.0 06/01/12 14:25 Bromomethane ug/kg ND 5.0 06/01/12 14:25 Carbon disulfide ug/kg ND 10.0 06/01/12 14:25 Carbon tetrachloride ug/kg ND 5.0 06/01/12 14:25 Chlorobenzene ug/kg ND 5.0 06/01/12 14:25 Chloroethane ug/kg ND 5.0 06/01/12 14:25 Chloroform ug/kg ND 5.0 06/01/12 14:25 Chloromethane ug/kg ND 5.0 06/01/12 14:25 cis-1,2-Dichloroethene ug/kg ND 5.0 06/01/12 14:25 cis-1,3-Dichloropropene ug/kg ND 5.0 06/01/12 14:25 Dibromochloromethane ug/kg ND 5.0 06/01/12 14:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 17 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:743896 Associated Lab Samples:5063623001, 5063623002, 5063623003 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 06/01/12 14:25 Dichlorodifluoromethane ug/kg ND 5.0 06/01/12 14:25 Ethyl methacrylate ug/kg ND 100 06/01/12 14:25 Ethylbenzene ug/kg ND 5.0 06/01/12 14:25 Hexachloro-1,3-butadiene ug/kg ND 5.0 06/01/12 14:25 Iodomethane ug/kg ND 100 06/01/12 14:25 Isopropylbenzene (Cumene)ug/kg ND 5.0 06/01/12 14:25 Methyl-tert-butyl ether ug/kg ND 5.0 06/01/12 14:25 Methylene Chloride ug/kg ND 20.0 06/01/12 14:25 n-Butylbenzene ug/kg ND 5.0 06/01/12 14:25 n-Hexane ug/kg ND 5.0 N206/01/12 14:25 n-Propylbenzene ug/kg ND 5.0 06/01/12 14:25 Naphthalene ug/kg ND 5.0 06/01/12 14:25 p-Isopropyltoluene ug/kg ND 5.0 06/01/12 14:25 sec-Butylbenzene ug/kg ND 5.0 06/01/12 14:25 Styrene ug/kg ND 5.0 06/01/12 14:25 tert-Butylbenzene ug/kg ND 5.0 06/01/12 14:25 Tetrachloroethene ug/kg ND 5.0 06/01/12 14:25 Toluene ug/kg ND 5.0 06/01/12 14:25 trans-1,2-Dichloroethene ug/kg ND 5.0 06/01/12 14:25 trans-1,3-Dichloropropene ug/kg ND 5.0 06/01/12 14:25 trans-1,4-Dichloro-2-butene ug/kg ND 100 06/01/12 14:25 Trichloroethene ug/kg ND 5.0 06/01/12 14:25 Trichlorofluoromethane ug/kg ND 5.0 06/01/12 14:25 Vinyl acetate ug/kg ND 100 06/01/12 14:25 Vinyl chloride ug/kg ND 5.0 06/01/12 14:25 Xylene (Total)ug/kg ND 10.0 06/01/12 14:25 4-Bromofluorobenzene (S)%.94 67-134 06/01/12 14:25 Dibromofluoromethane (S)%.92 71-125 06/01/12 14:25 Toluene-d8 (S)%.98 76-124 06/01/12 14:25 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743897LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 39.350 79 68-125 1,1,1-Trichloroethane ug/kg 42.750 85 63-124 1,1,2,2-Tetrachloroethane ug/kg 47.850 96 73-123 1,1,2-Trichloroethane ug/kg 51.250 102 70-124 1,1-Dichloroethane ug/kg 44.550 89 63-122 1,1-Dichloroethene ug/kg 42.650 85 71-129 1,1-Dichloropropene ug/kg 48.050 96 71-122 1,2,3-Trichlorobenzene ug/kg 50.050 100 68-123 1,2,3-Trichloropropane ug/kg 69.5 L35013947-117 1,2,4-Trichlorobenzene ug/kg 45.650 91 68-125 1,2,4-Trimethylbenzene ug/kg 46.550 93 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 18 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743897LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 46.450 93 67-121 1,2-Dichlorobenzene ug/kg 45.750 91 71-121 1,2-Dichloroethane ug/kg 47.950 96 74-120 1,2-Dichloropropane ug/kg 47.450 95 71-117 1,3,5-Trimethylbenzene ug/kg 46.550 93 64-119 1,3-Dichlorobenzene ug/kg 45.950 92 70-122 1,3-Dichloropropane ug/kg 47.550 95 68-118 1,4-Dichlorobenzene ug/kg 44.950 90 71-118 2,2-Dichloropropane ug/kg 40.750 81 62-119 2-Butanone (MEK)ug/kg 224250 90 38-154 2-Chlorotoluene ug/kg 46.050 92 71-120 2-Hexanone ug/kg 229250 92 50-134 4-Chlorotoluene ug/kg 45.350 91 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 226250 91 66-122 Acetone ug/kg 217250 87 10-200 Acrolein ug/kg 5711000 57 11-200 Acrylonitrile ug/kg 8931000 89 66-120 Benzene ug/kg 46.650 93 73-115 Bromobenzene ug/kg 46.350 93 64-130 Bromochloromethane ug/kg 46.450 93 71-127 Bromodichloromethane ug/kg 43.950 88 60-121 Bromoform ug/kg 37.150 74 44-130 Bromomethane ug/kg 63.950 128 48-175 Carbon disulfide ug/kg 74.1100 74 71-126 Carbon tetrachloride ug/kg 38.350 77 57-127 Chlorobenzene ug/kg 45.450 91 72-121 Chloroethane ug/kg 38.750 77 72-141 Chloroform ug/kg 48.950 98 74-114 Chloromethane ug/kg 35.150 70 51-126 cis-1,2-Dichloroethene ug/kg 47.450 95 72-115 cis-1,3-Dichloropropene ug/kg 42.250 84 64-115 Dibromochloromethane ug/kg 40.250 80 58-114 Dibromomethane ug/kg 45.950 92 73-120 Dichlorodifluoromethane ug/kg 40.650 81 32-167 Ethyl methacrylate ug/kg 185200 92 65-117 Ethylbenzene ug/kg 45.650 91 73-120 Hexachloro-1,3-butadiene ug/kg 46.450 93 65-121 Iodomethane ug/kg 94.6J100 95 45-156 Isopropylbenzene (Cumene)ug/kg 44.150 88 74-123 Methyl-tert-butyl ether ug/kg 88.4100 88 69-123 Methylene Chloride ug/kg 40.150 80 58-124 n-Butylbenzene ug/kg 47.750 95 71-118 n-Hexane ug/kg 40.0 N2508050-106 n-Propylbenzene ug/kg 46.050 92 70-120 Naphthalene ug/kg 52.350 105 67-124 p-Isopropyltoluene ug/kg 48.150 96 71-123 sec-Butylbenzene ug/kg 46.750 93 66-122 Styrene ug/kg 46.350 93 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 19 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 743897LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 42.950 86 54-124 Tetrachloroethene ug/kg 41.050 82 66-126 Toluene ug/kg 44.450 89 69-115 trans-1,2-Dichloroethene ug/kg 45.450 91 69-120 trans-1,3-Dichloropropene ug/kg 41.650 83 61-116 trans-1,4-Dichloro-2-butene ug/kg 152200 76 59-130 Trichloroethene ug/kg 49.750 99 71-117 Trichlorofluoromethane ug/kg 46.650 93 67-138 Vinyl acetate ug/kg 151200 76 35-134 Vinyl chloride ug/kg 38.850 78 64-127 Xylene (Total)ug/kg 135150 90 69-117 4-Bromofluorobenzene (S)%.97 67-134 Dibromofluoromethane (S)%.97 71-125 Toluene-d8 (S)%.97 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 743898MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063623001 743899 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 23.6 67 10-11173 22 2027.4ND 15.9 19.9 1,1,1-Trichloroethane ug/kg 23.6 75 36-12881 22 2027.4ND 17.8 22.2 1,1,2,2-Tetrachloroethane ug/kg 23.6 88 10-13090 16 2027.4ND 20.9 24.5 1,1,2-Trichloroethane ug/kg 23.6 100 10-12699 14 2027.4ND 23.7 27.2 1,1-Dichloroethane ug/kg 23.6 88 39-12688 15 2027.4ND 20.8 24.1 1,1-Dichloroethene ug/kg 23.6 83 42-14784 17 2027.4ND 19.5 23.1 1,1-Dichloropropene ug/kg 23.6 91 29-12991 14 2027.4ND 21.6 24.8 1,2,3-Trichlorobenzene ug/kg 23.6 71 10-9164 4 2027.4ND 16.8 17.5 1,2,3-Trichloropropane ug/kg M023.6 116 10-99125 22 2027.4ND 27.4 34.3 1,2,4-Trichlorobenzene ug/kg 23.6 70 10-8864 6 2027.4ND 16.5 17.4 1,2,4-Trimethylbenzene ug/kg 23.6 86 10-10984 12 2027.4ND 20.4 23.0 1,2-Dibromoethane (EDB)ug/kg 23.6 90 10-11988 13 2027.4ND 21.3 24.2 1,2-Dichlorobenzene ug/kg 23.6 81 10-10475 8 2027.4ND 19.1 20.7 1,2-Dichloroethane ug/kg 23.6 97 19-12696 13 2027.4ND 23.0 26.2 1,2-Dichloropropane ug/kg 23.6 95 24-12394 14 2027.4ND 22.3 25.6 1,3,5-Trimethylbenzene ug/kg 23.6 85 10-11883 12 2027.4ND 20.2 22.7 1,3-Dichlorobenzene ug/kg 23.6 80 10-10875 8 2027.4ND 19.0 20.6 1,3-Dichloropropane ug/kg 23.6 94 12-12193 13 2027.4ND 22.2 25.4 1,4-Dichlorobenzene ug/kg 23.6 79 10-10475 9 2027.4ND 18.7 20.4 2,2-Dichloropropane ug/kg 23.6 69 32-12477 26 2027.4ND 16.4 21.2 2-Butanone (MEK)ug/kg 118 99 10-18397 13 20136ND117133 2-Chlorotoluene ug/kg 23.6 83 10-12881 11 2027.4ND 19.7 22.1 2-Hexanone ug/kg 118 95 10-15896 16 20136ND112132 4-Chlorotoluene ug/kg 23.6 83 10-11979 10 2027.4ND 19.5 21.6 4-Methyl-2-pentanone (MIBK)ug/kg 118 90 12-13088 13 20136ND106120 Acetone ug/kg 118 157 10-200144 6 20136ND185196 Acrolein ug/kg 473 52 10-20049 9 20547ND246267 Acrylonitrile ug/kg 473 89 19-13089 15 20547ND421488 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 20 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 743898MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063623001 743899 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 23.6 91 23-13890 14 2027.4ND 21.4 24.7 Bromobenzene ug/kg 23.6 86 10-11182 11 2027.4ND 20.2 22.6 Bromochloromethane ug/kg 23.6 93 26-12693 15 2027.4ND 21.9 25.4 Bromodichloromethane ug/kg 23.6 79 10-12083 20 2027.4ND 18.6 22.8 Bromoform ug/kg 23.6 60 10-10666 23 2027.4ND 14.2 17.9 Bromomethane ug/kg 23.6 121 10-190120 15 2027.4ND 28.5 33.0 Carbon disulfide ug/kg 47.3 73 31-12873 15 2054.7ND 34.3 40.0 Carbon tetrachloride ug/kg 23.6 61 26-12670 28 2027.4ND 14.4 19.1 Chlorobenzene ug/kg 23.6 87 10-12084 12 2027.4ND 20.4 23.0 Chloroethane ug/kg 23.6 79 18-18679 15 2027.4ND 18.6 21.7 Chloroform ug/kg 23.6 96 29-12696 15 2027.4ND 22.6 26.4 Chloromethane ug/kg 23.6 72 34-13172 15 2027.4ND 17.0 19.7 cis-1,2-Dichloroethene ug/kg 23.6 93 28-13293 14 2027.4ND 22.0 25.3 cis-1,3-Dichloropropene ug/kg 23.6 77 10-10881 20 2027.4ND 18.2 22.2 Dibromochloromethane ug/kg 23.6 67 10-10873 23 2027.4ND 15.8 20.0 Dibromomethane ug/kg 23.6 91 13-12291 14 2027.4ND 21.6 24.9 Dichlorodifluoromethane ug/kg 23.6 88 10-19790 17 2027.4ND 20.8 24.6 Ethyl methacrylate ug/kg 94.5 84 10-13088 18 20110ND79.8 96.0 Ethylbenzene ug/kg 23.6 87 10-13586 14 2027.4ND 20.6 23.6 Hexachloro-1,3-butadiene ug/kg 23.6 67 10-10562 6 2027.4ND 15.8 16.8 Iodomethane ug/kg 47.3 90 10-16395 2054.7ND 42.5J 51.9J Isopropylbenzene (Cumene)ug/kg 23.6 82 10-12181 13 2027.4ND 19.5 22.1 Methyl-tert-butyl ether ug/kg 47.3 85 20-14087 18 2054.7ND 40.2 47.9 Methylene Chloride ug/kg 23.6 79 28-13181 17 2027.4ND 18.6 22.1 n-Butylbenzene ug/kg 23.6 82 10-11079 10 2027.4ND 19.5 21.6 n-Hexane ug/kg N223.6 74 21-15072 12 2027.4ND 17.4 19.6 n-Propylbenzene ug/kg 23.6 85 10-12383 13 2027.4ND 20.0 22.7 Naphthalene ug/kg 23.6 83 10-10678 9 2027.4ND 19.5 21.4 p-Isopropyltoluene ug/kg 23.6 87 10-11784 12 2027.4ND 20.5 23.1 sec-Butylbenzene ug/kg 23.6 84 10-12381 11 2027.4ND 19.8 22.2 Styrene ug/kg 23.6 87 10-11983 11 2027.4ND 20.5 22.8 tert-Butylbenzene ug/kg 23.6 80 10-10578 13 2027.4ND 18.8 21.4 Tetrachloroethene ug/kg 23.6 75 10-12284 23 2027.4ND 19.9 25.1 Toluene ug/kg 23.6 86 10-13185 13 2027.4ND 20.4 23.3 trans-1,2-Dichloroethene ug/kg 23.6 88 32-13689 15 2027.4ND 20.9 24.4 trans-1,3-Dichloropropene ug/kg 23.6 72 10-10177 21 2027.4ND 17.0 21.0 trans-1,4-Dichloro-2-butene ug/kg 94.5 68 10-10470 18 20110ND64.2 76.9 Trichloroethene ug/kg 23.6 94 15-13394 14 2027.4ND 22.3 25.7 Trichlorofluoromethane ug/kg 23.6 91 37-15293 17 2027.4ND 21.5 25.5 Vinyl acetate ug/kg 94.5 60 10-10366 24 20110ND57.0 72.5 Vinyl chloride ug/kg 23.6 80 41-14781 16 2027.4ND 18.9 22.2 Xylene (Total)ug/kg 70.8 85 10-13184 13 2082.1ND 60.3 68.6 4-Bromofluorobenzene (S)%.97 67-13497 20 Dibromofluoromethane (S)%.1d9671-12597 20 Toluene-d8 (S)%.98 76-12498 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 21 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063623 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/7106 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5063623001, 5063623002, 5063623003 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063619001 744507SAMPLE DUPLICATE: Percent Moisture %24.9 .2 524.9 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063623001 744508SAMPLE DUPLICATE: Percent Moisture %10.5 R18511.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 22 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5063623 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Several compounds are outside of acceptance limits for RPD value. Refer to the LCS for system control. grm 6-4-121d Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 23 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5063623 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5063623004 MSV/42701SBI068:FB5:W052912 EPA 8260 5063623001 MSV/42702SBI068:AMW3D:S160176 EPA 8260 5063623002 MSV/42702SBI068:AMW3D:S040054 EPA 8260 5063623003 MSV/42702SBI068:AMW3D:S040054A EPA 8260 5063623001 PMST/7106SBI068:AMW3D:S160176 ASTM D2974-87 5063623002 PMST/7106SBI068:AMW3D:S040054 ASTM D2974-87 5063623003 PMST/7106SBI068:AMW3D:S040054A ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/08/2012 08:44 AM Page 24 of 24 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 June 09, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5063723 5063723 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on May 31, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5063723 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5063723 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5063723001 SBI068:AMW2D:S180187 Solid 05/30/12 13:40 05/31/12 17:10 5063723002 SBI068:AMW2D:S120131 Solid 05/30/12 13:50 05/31/12 17:10 5063723003 SBI068:AMW2D:S120131A Solid 05/30/12 13:52 05/31/12 17:10 5063723004 SBI068:AMW5D:S220225 Solid 05/31/12 12:35 05/31/12 17:10 5063723005 SBI068:AMW5D:S160172 Solid 05/31/12 12:45 05/31/12 17:10 5063723006 SBI068:AMW5D:S160172A Solid 05/31/12 12:48 05/31/12 17:10 5063723007 SBI068:FB6:W053012 Water 05/30/12 14:00 05/31/12 17:10 5063723008 SBI068:FB7:W053112 Water 05/31/12 12:50 05/31/12 17:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5063723 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5063723001 SBI068:AMW2D:S180187 EPA 8260 73ALA ASTM D2974-87 1DAE 5063723002 SBI068:AMW2D:S120131 EPA 8260 73ALA ASTM D2974-87 1DAE 5063723003 SBI068:AMW2D:S120131A EPA 8260 73ALA ASTM D2974-87 1DAE 5063723004 SBI068:AMW5D:S220225 EPA 8260 73ALA ASTM D2974-87 1DAE 5063723005 SBI068:AMW5D:S160172 EPA 8260 73ALA ASTM D2974-87 1DAE 5063723006 SBI068:AMW5D:S160172A EPA 8260 73ALA ASTM D2974-87 1DAE 5063723007 SBI068:FB6:W053012 EPA 8260 73ALA 5063723008 SBI068:FB7:W053112 EPA 8260 73ALA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S180187 Lab ID:5063723001 Collected:05/30/12 13:40 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/04/12 23:43 67-64-143.5 Acrolein ND ug/kg 1 06/04/12 23:43 107-02-843.5 Acrylonitrile ND ug/kg 1 06/04/12 23:43 107-13-143.5 Benzene ND ug/kg 1 06/04/12 23:43 71-43-22.2 Bromobenzene ND ug/kg 1 06/04/12 23:43 108-86-12.2 Bromochloromethane ND ug/kg 1 06/04/12 23:43 74-97-52.2 Bromodichloromethane ND ug/kg 1 06/04/12 23:43 75-27-42.2 Bromoform ND ug/kg 1 06/04/12 23:43 75-25-22.2 Bromomethane ND ug/kg 1 06/04/12 23:43 74-83-92.2 2-Butanone (MEK)ND ug/kg 1 06/04/12 23:43 78-93-310.9 n-Butylbenzene ND ug/kg 1 06/04/12 23:43 104-51-82.2 sec-Butylbenzene ND ug/kg 1 06/04/12 23:43 135-98-82.2 tert-Butylbenzene ND ug/kg 1 06/04/12 23:43 98-06-62.2 Carbon disulfide ND ug/kg 1 06/04/12 23:43 75-15-04.3 Carbon tetrachloride ND ug/kg 1 06/04/12 23:43 56-23-52.2 Chlorobenzene ND ug/kg 1 06/04/12 23:43 108-90-72.2 Chloroethane ND ug/kg 1 06/04/12 23:43 75-00-32.2 Chloroform ND ug/kg 1 06/04/12 23:43 67-66-32.2 Chloromethane ND ug/kg 1 06/04/12 23:43 74-87-32.2 2-Chlorotoluene ND ug/kg 1 06/04/12 23:43 95-49-82.2 4-Chlorotoluene ND ug/kg 1 06/04/12 23:43 106-43-42.2 Dibromochloromethane ND ug/kg 1 06/04/12 23:43 124-48-12.2 1,2-Dibromoethane (EDB)ND ug/kg 1 06/04/12 23:43 106-93-42.2 Dibromomethane ND ug/kg 1 06/04/12 23:43 74-95-32.2 1,2-Dichlorobenzene ND ug/kg 1 06/04/12 23:43 95-50-12.2 1,3-Dichlorobenzene ND ug/kg 1 06/04/12 23:43 541-73-12.2 1,4-Dichlorobenzene ND ug/kg 1 06/04/12 23:43 106-46-72.2 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/04/12 23:43 110-57-643.5 Dichlorodifluoromethane ND ug/kg 1 06/04/12 23:43 75-71-82.2 1,1-Dichloroethane ND ug/kg 1 06/04/12 23:43 75-34-32.2 1,2-Dichloroethane ND ug/kg 1 06/04/12 23:43 107-06-22.2 1,1-Dichloroethene ND ug/kg 1 06/04/12 23:43 75-35-42.2 cis-1,2-Dichloroethene ND ug/kg 1 06/04/12 23:43 156-59-22.2 trans-1,2-Dichloroethene ND ug/kg 1 06/04/12 23:43 156-60-52.2 1,2-Dichloropropane ND ug/kg 1 06/04/12 23:43 78-87-52.2 1,3-Dichloropropane ND ug/kg 1 06/04/12 23:43 142-28-92.2 2,2-Dichloropropane ND ug/kg 1 06/04/12 23:43 594-20-72.2 1,1-Dichloropropene ND ug/kg 1 06/04/12 23:43 563-58-62.2 cis-1,3-Dichloropropene ND ug/kg 1 06/04/12 23:43 10061-01-52.2 trans-1,3-Dichloropropene ND ug/kg 1 06/04/12 23:43 10061-02-62.2 Ethylbenzene ND ug/kg 1 06/04/12 23:43 100-41-42.2 Ethyl methacrylate ND ug/kg 1 06/04/12 23:43 97-63-243.5 Hexachloro-1,3-butadiene ND ug/kg 1 06/04/12 23:43 87-68-32.2 n-Hexane ND ug/kg 1 06/04/12 23:43 110-54-3 N22.2 2-Hexanone ND ug/kg 1 06/04/12 23:43 591-78-643.5 Iodomethane ND ug/kg 1 06/04/12 23:43 74-88-443.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 5 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S180187 Lab ID:5063723001 Collected:05/30/12 13:40 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/04/12 23:43 98-82-82.2 p-Isopropyltoluene ND ug/kg 1 06/04/12 23:43 99-87-62.2 Methylene Chloride ND ug/kg 1 06/04/12 23:43 75-09-28.7 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/04/12 23:43 108-10-110.9 Methyl-tert-butyl ether ND ug/kg 1 06/04/12 23:43 1634-04-42.2 Naphthalene ND ug/kg 1 06/04/12 23:43 91-20-32.2 n-Propylbenzene ND ug/kg 1 06/04/12 23:43 103-65-12.2 Styrene ND ug/kg 1 06/04/12 23:43 100-42-52.2 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/04/12 23:43 630-20-62.2 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/04/12 23:43 79-34-52.2 Tetrachloroethene ND ug/kg 1 06/04/12 23:43 127-18-42.2 Toluene ND ug/kg 1 06/04/12 23:43 108-88-32.2 1,2,3-Trichlorobenzene ND ug/kg 1 06/04/12 23:43 87-61-62.2 1,2,4-Trichlorobenzene ND ug/kg 1 06/04/12 23:43 120-82-12.2 1,1,1-Trichloroethane ND ug/kg 1 06/04/12 23:43 71-55-62.2 1,1,2-Trichloroethane ND ug/kg 1 06/04/12 23:43 79-00-52.2 Trichloroethene ND ug/kg 1 06/04/12 23:43 79-01-62.2 Trichlorofluoromethane ND ug/kg 1 06/04/12 23:43 75-69-42.2 1,2,3-Trichloropropane ND ug/kg 1 06/04/12 23:43 96-18-42.2 1,2,4-Trimethylbenzene ND ug/kg 1 06/04/12 23:43 95-63-62.2 1,3,5-Trimethylbenzene ND ug/kg 1 06/04/12 23:43 108-67-82.2 Vinyl acetate ND ug/kg 1 06/04/12 23:43 108-05-443.5 Vinyl chloride ND ug/kg 1 06/04/12 23:43 75-01-42.2 Xylene (Total)ND ug/kg 1 06/04/12 23:43 1330-20-74.3 Surrogates Dibromofluoromethane (S)102 %.1 06/04/12 23:43 1868-53-771-125 Toluene-d8 (S)103 %.1 06/04/12 23:43 2037-26-576-124 4-Bromofluorobenzene (S)100 %.1 06/04/12 23:43 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 13.1 %1 06/07/12 17:150.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 6 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S120131 Lab ID:5063723002 Collected:05/30/12 13:50 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/05/12 01:25 67-64-167.0 Acrolein ND ug/kg 1 06/05/12 01:25 107-02-867.0 Acrylonitrile ND ug/kg 1 06/05/12 01:25 107-13-167.0 Benzene ND ug/kg 1 06/05/12 01:25 71-43-23.4 Bromobenzene ND ug/kg 1 06/05/12 01:25 108-86-13.4 Bromochloromethane ND ug/kg 1 06/05/12 01:25 74-97-53.4 Bromodichloromethane ND ug/kg 1 06/05/12 01:25 75-27-43.4 Bromoform ND ug/kg 1 06/05/12 01:25 75-25-23.4 Bromomethane ND ug/kg 1 06/05/12 01:25 74-83-93.4 2-Butanone (MEK)ND ug/kg 1 06/05/12 01:25 78-93-316.8 n-Butylbenzene ND ug/kg 1 06/05/12 01:25 104-51-83.4 sec-Butylbenzene ND ug/kg 1 06/05/12 01:25 135-98-83.4 tert-Butylbenzene ND ug/kg 1 06/05/12 01:25 98-06-63.4 Carbon disulfide ND ug/kg 1 06/05/12 01:25 75-15-06.7 Carbon tetrachloride ND ug/kg 1 06/05/12 01:25 56-23-53.4 Chlorobenzene ND ug/kg 1 06/05/12 01:25 108-90-73.4 Chloroethane ND ug/kg 1 06/05/12 01:25 75-00-33.4 Chloroform ND ug/kg 1 06/05/12 01:25 67-66-33.4 Chloromethane ND ug/kg 1 06/05/12 01:25 74-87-33.4 2-Chlorotoluene ND ug/kg 1 06/05/12 01:25 95-49-83.4 4-Chlorotoluene ND ug/kg 1 06/05/12 01:25 106-43-43.4 Dibromochloromethane ND ug/kg 1 06/05/12 01:25 124-48-13.4 1,2-Dibromoethane (EDB)ND ug/kg 1 06/05/12 01:25 106-93-43.4 Dibromomethane ND ug/kg 1 06/05/12 01:25 74-95-33.4 1,2-Dichlorobenzene ND ug/kg 1 06/05/12 01:25 95-50-13.4 1,3-Dichlorobenzene ND ug/kg 1 06/05/12 01:25 541-73-13.4 1,4-Dichlorobenzene ND ug/kg 1 06/05/12 01:25 106-46-73.4 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/05/12 01:25 110-57-667.0 Dichlorodifluoromethane ND ug/kg 1 06/05/12 01:25 75-71-83.4 1,1-Dichloroethane ND ug/kg 1 06/05/12 01:25 75-34-33.4 1,2-Dichloroethane ND ug/kg 1 06/05/12 01:25 107-06-23.4 1,1-Dichloroethene ND ug/kg 1 06/05/12 01:25 75-35-43.4 cis-1,2-Dichloroethene ND ug/kg 1 06/05/12 01:25 156-59-23.4 trans-1,2-Dichloroethene ND ug/kg 1 06/05/12 01:25 156-60-53.4 1,2-Dichloropropane ND ug/kg 1 06/05/12 01:25 78-87-53.4 1,3-Dichloropropane ND ug/kg 1 06/05/12 01:25 142-28-93.4 2,2-Dichloropropane ND ug/kg 1 06/05/12 01:25 594-20-73.4 1,1-Dichloropropene ND ug/kg 1 06/05/12 01:25 563-58-63.4 cis-1,3-Dichloropropene ND ug/kg 1 06/05/12 01:25 10061-01-53.4 trans-1,3-Dichloropropene ND ug/kg 1 06/05/12 01:25 10061-02-63.4 Ethylbenzene ND ug/kg 1 06/05/12 01:25 100-41-43.4 Ethyl methacrylate ND ug/kg 1 06/05/12 01:25 97-63-267.0 Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 01:25 87-68-33.4 n-Hexane ND ug/kg 1 06/05/12 01:25 110-54-3 N23.4 2-Hexanone ND ug/kg 1 06/05/12 01:25 591-78-667.0 Iodomethane ND ug/kg 1 06/05/12 01:25 74-88-467.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 7 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S120131 Lab ID:5063723002 Collected:05/30/12 13:50 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/05/12 01:25 98-82-83.4 p-Isopropyltoluene ND ug/kg 1 06/05/12 01:25 99-87-63.4 Methylene Chloride ND ug/kg 1 06/05/12 01:25 75-09-213.4 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/05/12 01:25 108-10-116.8 Methyl-tert-butyl ether ND ug/kg 1 06/05/12 01:25 1634-04-43.4 Naphthalene ND ug/kg 1 06/05/12 01:25 91-20-33.4 n-Propylbenzene ND ug/kg 1 06/05/12 01:25 103-65-13.4 Styrene ND ug/kg 1 06/05/12 01:25 100-42-53.4 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/05/12 01:25 630-20-63.4 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/05/12 01:25 79-34-53.4 Tetrachloroethene ND ug/kg 1 06/05/12 01:25 127-18-43.4 Toluene ND ug/kg 1 06/05/12 01:25 108-88-33.4 1,2,3-Trichlorobenzene ND ug/kg 1 06/05/12 01:25 87-61-63.4 1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 01:25 120-82-13.4 1,1,1-Trichloroethane ND ug/kg 1 06/05/12 01:25 71-55-63.4 1,1,2-Trichloroethane ND ug/kg 1 06/05/12 01:25 79-00-53.4 Trichloroethene ND ug/kg 1 06/05/12 01:25 79-01-63.4 Trichlorofluoromethane ND ug/kg 1 06/05/12 01:25 75-69-43.4 1,2,3-Trichloropropane ND ug/kg 1 06/05/12 01:25 96-18-43.4 1,2,4-Trimethylbenzene ND ug/kg 1 06/05/12 01:25 95-63-63.4 1,3,5-Trimethylbenzene ND ug/kg 1 06/05/12 01:25 108-67-83.4 Vinyl acetate ND ug/kg 1 06/05/12 01:25 108-05-467.0 Vinyl chloride ND ug/kg 1 06/05/12 01:25 75-01-43.4 Xylene (Total)ND ug/kg 1 06/05/12 01:25 1330-20-76.7 Surrogates Dibromofluoromethane (S)104 %.1 06/05/12 01:25 1868-53-771-125 Toluene-d8 (S)101 %.1 06/05/12 01:25 2037-26-576-124 4-Bromofluorobenzene (S)101 %.1 06/05/12 01:25 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.9 %1 06/07/12 17:150.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 8 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S120131A Lab ID:5063723003 Collected:05/30/12 13:52 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/05/12 01:59 67-64-143.0 Acrolein ND ug/kg 1 06/05/12 01:59 107-02-843.0 Acrylonitrile ND ug/kg 1 06/05/12 01:59 107-13-143.0 Benzene ND ug/kg 1 06/05/12 01:59 71-43-22.1 Bromobenzene ND ug/kg 1 06/05/12 01:59 108-86-12.1 Bromochloromethane ND ug/kg 1 06/05/12 01:59 74-97-52.1 Bromodichloromethane ND ug/kg 1 06/05/12 01:59 75-27-42.1 Bromoform ND ug/kg 1 06/05/12 01:59 75-25-22.1 Bromomethane ND ug/kg 1 06/05/12 01:59 74-83-92.1 2-Butanone (MEK)ND ug/kg 1 06/05/12 01:59 78-93-310.7 n-Butylbenzene ND ug/kg 1 06/05/12 01:59 104-51-82.1 sec-Butylbenzene ND ug/kg 1 06/05/12 01:59 135-98-82.1 tert-Butylbenzene ND ug/kg 1 06/05/12 01:59 98-06-62.1 Carbon disulfide ND ug/kg 1 06/05/12 01:59 75-15-04.3 Carbon tetrachloride ND ug/kg 1 06/05/12 01:59 56-23-52.1 Chlorobenzene ND ug/kg 1 06/05/12 01:59 108-90-72.1 Chloroethane ND ug/kg 1 06/05/12 01:59 75-00-32.1 Chloroform ND ug/kg 1 06/05/12 01:59 67-66-32.1 Chloromethane ND ug/kg 1 06/05/12 01:59 74-87-32.1 2-Chlorotoluene ND ug/kg 1 06/05/12 01:59 95-49-82.1 4-Chlorotoluene ND ug/kg 1 06/05/12 01:59 106-43-42.1 Dibromochloromethane ND ug/kg 1 06/05/12 01:59 124-48-12.1 1,2-Dibromoethane (EDB)ND ug/kg 1 06/05/12 01:59 106-93-42.1 Dibromomethane ND ug/kg 1 06/05/12 01:59 74-95-32.1 1,2-Dichlorobenzene ND ug/kg 1 06/05/12 01:59 95-50-12.1 1,3-Dichlorobenzene ND ug/kg 1 06/05/12 01:59 541-73-12.1 1,4-Dichlorobenzene ND ug/kg 1 06/05/12 01:59 106-46-72.1 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/05/12 01:59 110-57-643.0 Dichlorodifluoromethane ND ug/kg 1 06/05/12 01:59 75-71-82.1 1,1-Dichloroethane ND ug/kg 1 06/05/12 01:59 75-34-32.1 1,2-Dichloroethane ND ug/kg 1 06/05/12 01:59 107-06-22.1 1,1-Dichloroethene ND ug/kg 1 06/05/12 01:59 75-35-42.1 cis-1,2-Dichloroethene ND ug/kg 1 06/05/12 01:59 156-59-22.1 trans-1,2-Dichloroethene ND ug/kg 1 06/05/12 01:59 156-60-52.1 1,2-Dichloropropane ND ug/kg 1 06/05/12 01:59 78-87-52.1 1,3-Dichloropropane ND ug/kg 1 06/05/12 01:59 142-28-92.1 2,2-Dichloropropane ND ug/kg 1 06/05/12 01:59 594-20-72.1 1,1-Dichloropropene ND ug/kg 1 06/05/12 01:59 563-58-62.1 cis-1,3-Dichloropropene ND ug/kg 1 06/05/12 01:59 10061-01-52.1 trans-1,3-Dichloropropene ND ug/kg 1 06/05/12 01:59 10061-02-62.1 Ethylbenzene ND ug/kg 1 06/05/12 01:59 100-41-42.1 Ethyl methacrylate ND ug/kg 1 06/05/12 01:59 97-63-243.0 Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 01:59 87-68-32.1 n-Hexane ND ug/kg 1 06/05/12 01:59 110-54-3 N22.1 2-Hexanone ND ug/kg 1 06/05/12 01:59 591-78-643.0 Iodomethane ND ug/kg 1 06/05/12 01:59 74-88-443.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 9 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW2D:S120131A Lab ID:5063723003 Collected:05/30/12 13:52 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/05/12 01:59 98-82-82.1 p-Isopropyltoluene ND ug/kg 1 06/05/12 01:59 99-87-62.1 Methylene Chloride ND ug/kg 1 06/05/12 01:59 75-09-28.6 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/05/12 01:59 108-10-110.7 Methyl-tert-butyl ether ND ug/kg 1 06/05/12 01:59 1634-04-42.1 Naphthalene ND ug/kg 1 06/05/12 01:59 91-20-32.1 n-Propylbenzene ND ug/kg 1 06/05/12 01:59 103-65-12.1 Styrene ND ug/kg 1 06/05/12 01:59 100-42-52.1 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/05/12 01:59 630-20-62.1 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/05/12 01:59 79-34-52.1 Tetrachloroethene ND ug/kg 1 06/05/12 01:59 127-18-42.1 Toluene ND ug/kg 1 06/05/12 01:59 108-88-32.1 1,2,3-Trichlorobenzene ND ug/kg 1 06/05/12 01:59 87-61-62.1 1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 01:59 120-82-12.1 1,1,1-Trichloroethane ND ug/kg 1 06/05/12 01:59 71-55-62.1 1,1,2-Trichloroethane ND ug/kg 1 06/05/12 01:59 79-00-52.1 Trichloroethene ND ug/kg 1 06/05/12 01:59 79-01-62.1 Trichlorofluoromethane ND ug/kg 1 06/05/12 01:59 75-69-42.1 1,2,3-Trichloropropane ND ug/kg 1 06/05/12 01:59 96-18-42.1 1,2,4-Trimethylbenzene ND ug/kg 1 06/05/12 01:59 95-63-62.1 1,3,5-Trimethylbenzene ND ug/kg 1 06/05/12 01:59 108-67-82.1 Vinyl acetate ND ug/kg 1 06/05/12 01:59 108-05-443.0 Vinyl chloride ND ug/kg 1 06/05/12 01:59 75-01-42.1 Xylene (Total)ND ug/kg 1 06/05/12 01:59 1330-20-74.3 Surrogates Dibromofluoromethane (S)106 %.1 06/05/12 01:59 1868-53-771-125 Toluene-d8 (S)102 %.1 06/05/12 01:59 2037-26-576-124 4-Bromofluorobenzene (S)102 %.1 06/05/12 01:59 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.2 %1 06/07/12 17:150.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 10 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S220225 Lab ID:5063723004 Collected:05/31/12 12:35 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/05/12 02:32 67-64-194.7 Acrolein ND ug/kg 1 06/05/12 02:32 107-02-894.7 Acrylonitrile ND ug/kg 1 06/05/12 02:32 107-13-194.7 Benzene ND ug/kg 1 06/05/12 02:32 71-43-24.7 Bromobenzene ND ug/kg 1 06/05/12 02:32 108-86-14.7 Bromochloromethane ND ug/kg 1 06/05/12 02:32 74-97-54.7 Bromodichloromethane ND ug/kg 1 06/05/12 02:32 75-27-44.7 Bromoform ND ug/kg 1 06/05/12 02:32 75-25-24.7 Bromomethane ND ug/kg 1 06/05/12 02:32 74-83-94.7 2-Butanone (MEK)ND ug/kg 1 06/05/12 02:32 78-93-323.7 n-Butylbenzene ND ug/kg 1 06/05/12 02:32 104-51-84.7 sec-Butylbenzene ND ug/kg 1 06/05/12 02:32 135-98-84.7 tert-Butylbenzene ND ug/kg 1 06/05/12 02:32 98-06-64.7 Carbon disulfide ND ug/kg 1 06/05/12 02:32 75-15-09.5 Carbon tetrachloride ND ug/kg 1 06/05/12 02:32 56-23-54.7 Chlorobenzene ND ug/kg 1 06/05/12 02:32 108-90-74.7 Chloroethane ND ug/kg 1 06/05/12 02:32 75-00-34.7 Chloroform ND ug/kg 1 06/05/12 02:32 67-66-34.7 Chloromethane ND ug/kg 1 06/05/12 02:32 74-87-34.7 2-Chlorotoluene ND ug/kg 1 06/05/12 02:32 95-49-84.7 4-Chlorotoluene ND ug/kg 1 06/05/12 02:32 106-43-44.7 Dibromochloromethane ND ug/kg 1 06/05/12 02:32 124-48-14.7 1,2-Dibromoethane (EDB)ND ug/kg 1 06/05/12 02:32 106-93-44.7 Dibromomethane ND ug/kg 1 06/05/12 02:32 74-95-34.7 1,2-Dichlorobenzene ND ug/kg 1 06/05/12 02:32 95-50-14.7 1,3-Dichlorobenzene ND ug/kg 1 06/05/12 02:32 541-73-14.7 1,4-Dichlorobenzene ND ug/kg 1 06/05/12 02:32 106-46-74.7 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/05/12 02:32 110-57-694.7 Dichlorodifluoromethane ND ug/kg 1 06/05/12 02:32 75-71-84.7 1,1-Dichloroethane ND ug/kg 1 06/05/12 02:32 75-34-34.7 1,2-Dichloroethane ND ug/kg 1 06/05/12 02:32 107-06-24.7 1,1-Dichloroethene ND ug/kg 1 06/05/12 02:32 75-35-44.7 cis-1,2-Dichloroethene ND ug/kg 1 06/05/12 02:32 156-59-24.7 trans-1,2-Dichloroethene ND ug/kg 1 06/05/12 02:32 156-60-54.7 1,2-Dichloropropane ND ug/kg 1 06/05/12 02:32 78-87-54.7 1,3-Dichloropropane ND ug/kg 1 06/05/12 02:32 142-28-94.7 2,2-Dichloropropane ND ug/kg 1 06/05/12 02:32 594-20-74.7 1,1-Dichloropropene ND ug/kg 1 06/05/12 02:32 563-58-64.7 cis-1,3-Dichloropropene ND ug/kg 1 06/05/12 02:32 10061-01-54.7 trans-1,3-Dichloropropene ND ug/kg 1 06/05/12 02:32 10061-02-64.7 Ethylbenzene ND ug/kg 1 06/05/12 02:32 100-41-44.7 Ethyl methacrylate ND ug/kg 1 06/05/12 02:32 97-63-294.7 Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 02:32 87-68-34.7 n-Hexane ND ug/kg 1 06/05/12 02:32 110-54-3 N24.7 2-Hexanone ND ug/kg 1 06/05/12 02:32 591-78-694.7 Iodomethane ND ug/kg 1 06/05/12 02:32 74-88-494.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 11 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S220225 Lab ID:5063723004 Collected:05/31/12 12:35 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/05/12 02:32 98-82-84.7 p-Isopropyltoluene ND ug/kg 1 06/05/12 02:32 99-87-64.7 Methylene Chloride ND ug/kg 1 06/05/12 02:32 75-09-218.9 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/05/12 02:32 108-10-123.7 Methyl-tert-butyl ether ND ug/kg 1 06/05/12 02:32 1634-04-44.7 Naphthalene ND ug/kg 1 06/05/12 02:32 91-20-34.7 n-Propylbenzene ND ug/kg 1 06/05/12 02:32 103-65-14.7 Styrene ND ug/kg 1 06/05/12 02:32 100-42-54.7 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/05/12 02:32 630-20-64.7 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/05/12 02:32 79-34-54.7 Tetrachloroethene ND ug/kg 1 06/05/12 02:32 127-18-44.7 Toluene ND ug/kg 1 06/05/12 02:32 108-88-34.7 1,2,3-Trichlorobenzene ND ug/kg 1 06/05/12 02:32 87-61-64.7 1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 02:32 120-82-14.7 1,1,1-Trichloroethane ND ug/kg 1 06/05/12 02:32 71-55-64.7 1,1,2-Trichloroethane ND ug/kg 1 06/05/12 02:32 79-00-54.7 Trichloroethene ND ug/kg 1 06/05/12 02:32 79-01-64.7 Trichlorofluoromethane ND ug/kg 1 06/05/12 02:32 75-69-44.7 1,2,3-Trichloropropane ND ug/kg 1 06/05/12 02:32 96-18-44.7 1,2,4-Trimethylbenzene ND ug/kg 1 06/05/12 02:32 95-63-64.7 1,3,5-Trimethylbenzene ND ug/kg 1 06/05/12 02:32 108-67-84.7 Vinyl acetate ND ug/kg 1 06/05/12 02:32 108-05-494.7 Vinyl chloride ND ug/kg 1 06/05/12 02:32 75-01-44.7 Xylene (Total)ND ug/kg 1 06/05/12 02:32 1330-20-79.5 Surrogates Dibromofluoromethane (S)104 %.1 06/05/12 02:32 1868-53-771-125 Toluene-d8 (S)102 %.1 06/05/12 02:32 2037-26-576-124 4-Bromofluorobenzene (S)102 %.1 06/05/12 02:32 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 %1 06/07/12 17:150.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 12 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S160172 Lab ID:5063723005 Collected:05/31/12 12:45 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/05/12 04:14 67-64-1139 Acrolein ND ug/kg 1 06/05/12 04:14 107-02-8139 Acrylonitrile ND ug/kg 1 06/05/12 04:14 107-13-1139 Benzene ND ug/kg 1 06/05/12 04:14 71-43-27.0 Bromobenzene ND ug/kg 1 06/05/12 04:14 108-86-17.0 Bromochloromethane ND ug/kg 1 06/05/12 04:14 74-97-57.0 Bromodichloromethane ND ug/kg 1 06/05/12 04:14 75-27-47.0 Bromoform ND ug/kg 1 06/05/12 04:14 75-25-27.0 Bromomethane ND ug/kg 1 06/05/12 04:14 74-83-97.0 2-Butanone (MEK)ND ug/kg 1 06/05/12 04:14 78-93-334.9 n-Butylbenzene ND ug/kg 1 06/05/12 04:14 104-51-87.0 sec-Butylbenzene ND ug/kg 1 06/05/12 04:14 135-98-87.0 tert-Butylbenzene ND ug/kg 1 06/05/12 04:14 98-06-67.0 Carbon disulfide ND ug/kg 1 06/05/12 04:14 75-15-013.9 Carbon tetrachloride ND ug/kg 1 06/05/12 04:14 56-23-57.0 Chlorobenzene ND ug/kg 1 06/05/12 04:14 108-90-77.0 Chloroethane ND ug/kg 1 06/05/12 04:14 75-00-37.0 Chloroform ND ug/kg 1 06/05/12 04:14 67-66-37.0 Chloromethane ND ug/kg 1 06/05/12 04:14 74-87-37.0 2-Chlorotoluene ND ug/kg 1 06/05/12 04:14 95-49-87.0 4-Chlorotoluene ND ug/kg 1 06/05/12 04:14 106-43-47.0 Dibromochloromethane ND ug/kg 1 06/05/12 04:14 124-48-17.0 1,2-Dibromoethane (EDB)ND ug/kg 1 06/05/12 04:14 106-93-47.0 Dibromomethane ND ug/kg 1 06/05/12 04:14 74-95-37.0 1,2-Dichlorobenzene ND ug/kg 1 06/05/12 04:14 95-50-17.0 1,3-Dichlorobenzene ND ug/kg 1 06/05/12 04:14 541-73-17.0 1,4-Dichlorobenzene ND ug/kg 1 06/05/12 04:14 106-46-77.0 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/05/12 04:14 110-57-6139 Dichlorodifluoromethane ND ug/kg 1 06/05/12 04:14 75-71-87.0 1,1-Dichloroethane ND ug/kg 1 06/05/12 04:14 75-34-37.0 1,2-Dichloroethane ND ug/kg 1 06/05/12 04:14 107-06-27.0 1,1-Dichloroethene ND ug/kg 1 06/05/12 04:14 75-35-47.0 cis-1,2-Dichloroethene ND ug/kg 1 06/05/12 04:14 156-59-27.0 trans-1,2-Dichloroethene ND ug/kg 1 06/05/12 04:14 156-60-57.0 1,2-Dichloropropane ND ug/kg 1 06/05/12 04:14 78-87-57.0 1,3-Dichloropropane ND ug/kg 1 06/05/12 04:14 142-28-97.0 2,2-Dichloropropane ND ug/kg 1 06/05/12 04:14 594-20-77.0 1,1-Dichloropropene ND ug/kg 1 06/05/12 04:14 563-58-67.0 cis-1,3-Dichloropropene ND ug/kg 1 06/05/12 04:14 10061-01-57.0 trans-1,3-Dichloropropene ND ug/kg 1 06/05/12 04:14 10061-02-67.0 Ethylbenzene ND ug/kg 1 06/05/12 04:14 100-41-47.0 Ethyl methacrylate ND ug/kg 1 06/05/12 04:14 97-63-2139 Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 04:14 87-68-37.0 n-Hexane ND ug/kg 1 06/05/12 04:14 110-54-3 N27.0 2-Hexanone ND ug/kg 1 06/05/12 04:14 591-78-6139 Iodomethane ND ug/kg 1 06/05/12 04:14 74-88-4139 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 13 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S160172 Lab ID:5063723005 Collected:05/31/12 12:45 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/05/12 04:14 98-82-87.0 p-Isopropyltoluene ND ug/kg 1 06/05/12 04:14 99-87-67.0 Methylene Chloride ND ug/kg 1 06/05/12 04:14 75-09-227.9 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/05/12 04:14 108-10-134.9 Methyl-tert-butyl ether ND ug/kg 1 06/05/12 04:14 1634-04-47.0 Naphthalene ND ug/kg 1 06/05/12 04:14 91-20-37.0 n-Propylbenzene ND ug/kg 1 06/05/12 04:14 103-65-17.0 Styrene ND ug/kg 1 06/05/12 04:14 100-42-57.0 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/05/12 04:14 630-20-67.0 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/05/12 04:14 79-34-57.0 Tetrachloroethene ND ug/kg 1 06/05/12 04:14 127-18-47.0 Toluene ND ug/kg 1 06/05/12 04:14 108-88-37.0 1,2,3-Trichlorobenzene ND ug/kg 1 06/05/12 04:14 87-61-67.0 1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 04:14 120-82-17.0 1,1,1-Trichloroethane ND ug/kg 1 06/05/12 04:14 71-55-67.0 1,1,2-Trichloroethane ND ug/kg 1 06/05/12 04:14 79-00-57.0 Trichloroethene ND ug/kg 1 06/05/12 04:14 79-01-67.0 Trichlorofluoromethane ND ug/kg 1 06/05/12 04:14 75-69-47.0 1,2,3-Trichloropropane ND ug/kg 1 06/05/12 04:14 96-18-47.0 1,2,4-Trimethylbenzene ND ug/kg 1 06/05/12 04:14 95-63-67.0 1,3,5-Trimethylbenzene ND ug/kg 1 06/05/12 04:14 108-67-87.0 Vinyl acetate ND ug/kg 1 06/05/12 04:14 108-05-4139 Vinyl chloride ND ug/kg 1 06/05/12 04:14 75-01-47.0 Xylene (Total)ND ug/kg 1 06/05/12 04:14 1330-20-713.9 Surrogates Dibromofluoromethane (S)107 %.1 06/05/12 04:14 1868-53-771-125 Toluene-d8 (S)100 %.1 06/05/12 04:14 2037-26-576-124 4-Bromofluorobenzene (S)102 %.1 06/05/12 04:14 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.9 %1 06/07/12 17:150.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 14 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S160172A Lab ID:5063723006 Collected:05/31/12 12:48 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 06/05/12 04:48 67-64-174.1 Acrolein ND ug/kg 1 06/05/12 04:48 107-02-874.1 Acrylonitrile ND ug/kg 1 06/05/12 04:48 107-13-174.1 Benzene ND ug/kg 1 06/05/12 04:48 71-43-23.7 Bromobenzene ND ug/kg 1 06/05/12 04:48 108-86-13.7 Bromochloromethane ND ug/kg 1 06/05/12 04:48 74-97-53.7 Bromodichloromethane ND ug/kg 1 06/05/12 04:48 75-27-43.7 Bromoform ND ug/kg 1 06/05/12 04:48 75-25-23.7 Bromomethane ND ug/kg 1 06/05/12 04:48 74-83-93.7 2-Butanone (MEK)ND ug/kg 1 06/05/12 04:48 78-93-318.5 n-Butylbenzene ND ug/kg 1 06/05/12 04:48 104-51-83.7 sec-Butylbenzene ND ug/kg 1 06/05/12 04:48 135-98-83.7 tert-Butylbenzene ND ug/kg 1 06/05/12 04:48 98-06-63.7 Carbon disulfide ND ug/kg 1 06/05/12 04:48 75-15-07.4 Carbon tetrachloride ND ug/kg 1 06/05/12 04:48 56-23-53.7 Chlorobenzene ND ug/kg 1 06/05/12 04:48 108-90-73.7 Chloroethane ND ug/kg 1 06/05/12 04:48 75-00-33.7 Chloroform ND ug/kg 1 06/05/12 04:48 67-66-33.7 Chloromethane ND ug/kg 1 06/05/12 04:48 74-87-33.7 2-Chlorotoluene ND ug/kg 1 06/05/12 04:48 95-49-83.7 4-Chlorotoluene ND ug/kg 1 06/05/12 04:48 106-43-43.7 Dibromochloromethane ND ug/kg 1 06/05/12 04:48 124-48-13.7 1,2-Dibromoethane (EDB)ND ug/kg 1 06/05/12 04:48 106-93-43.7 Dibromomethane ND ug/kg 1 06/05/12 04:48 74-95-33.7 1,2-Dichlorobenzene ND ug/kg 1 06/05/12 04:48 95-50-13.7 1,3-Dichlorobenzene ND ug/kg 1 06/05/12 04:48 541-73-13.7 1,4-Dichlorobenzene ND ug/kg 1 06/05/12 04:48 106-46-73.7 trans-1,4-Dichloro-2-butene ND ug/kg 1 06/05/12 04:48 110-57-674.1 Dichlorodifluoromethane ND ug/kg 1 06/05/12 04:48 75-71-83.7 1,1-Dichloroethane ND ug/kg 1 06/05/12 04:48 75-34-33.7 1,2-Dichloroethane ND ug/kg 1 06/05/12 04:48 107-06-23.7 1,1-Dichloroethene ND ug/kg 1 06/05/12 04:48 75-35-43.7 cis-1,2-Dichloroethene ND ug/kg 1 06/05/12 04:48 156-59-23.7 trans-1,2-Dichloroethene ND ug/kg 1 06/05/12 04:48 156-60-53.7 1,2-Dichloropropane ND ug/kg 1 06/05/12 04:48 78-87-53.7 1,3-Dichloropropane ND ug/kg 1 06/05/12 04:48 142-28-93.7 2,2-Dichloropropane ND ug/kg 1 06/05/12 04:48 594-20-73.7 1,1-Dichloropropene ND ug/kg 1 06/05/12 04:48 563-58-63.7 cis-1,3-Dichloropropene ND ug/kg 1 06/05/12 04:48 10061-01-53.7 trans-1,3-Dichloropropene ND ug/kg 1 06/05/12 04:48 10061-02-63.7 Ethylbenzene ND ug/kg 1 06/05/12 04:48 100-41-43.7 Ethyl methacrylate ND ug/kg 1 06/05/12 04:48 97-63-274.1 Hexachloro-1,3-butadiene ND ug/kg 1 06/05/12 04:48 87-68-33.7 n-Hexane ND ug/kg 1 06/05/12 04:48 110-54-3 N23.7 2-Hexanone ND ug/kg 1 06/05/12 04:48 591-78-674.1 Iodomethane ND ug/kg 1 06/05/12 04:48 74-88-474.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 15 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:AMW5D:S160172A Lab ID:5063723006 Collected:05/31/12 12:48 Received:05/31/12 17:10 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/kg 1 06/05/12 04:48 98-82-83.7 p-Isopropyltoluene ND ug/kg 1 06/05/12 04:48 99-87-63.7 Methylene Chloride ND ug/kg 1 06/05/12 04:48 75-09-214.8 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 06/05/12 04:48 108-10-118.5 Methyl-tert-butyl ether ND ug/kg 1 06/05/12 04:48 1634-04-43.7 Naphthalene ND ug/kg 1 06/05/12 04:48 91-20-33.7 n-Propylbenzene ND ug/kg 1 06/05/12 04:48 103-65-13.7 Styrene ND ug/kg 1 06/05/12 04:48 100-42-53.7 1,1,1,2-Tetrachloroethane ND ug/kg 1 06/05/12 04:48 630-20-63.7 1,1,2,2-Tetrachloroethane ND ug/kg 1 06/05/12 04:48 79-34-53.7 Tetrachloroethene ND ug/kg 1 06/05/12 04:48 127-18-43.7 Toluene ND ug/kg 1 06/05/12 04:48 108-88-33.7 1,2,3-Trichlorobenzene ND ug/kg 1 06/05/12 04:48 87-61-63.7 1,2,4-Trichlorobenzene ND ug/kg 1 06/05/12 04:48 120-82-13.7 1,1,1-Trichloroethane ND ug/kg 1 06/05/12 04:48 71-55-63.7 1,1,2-Trichloroethane ND ug/kg 1 06/05/12 04:48 79-00-53.7 Trichloroethene ND ug/kg 1 06/05/12 04:48 79-01-63.7 Trichlorofluoromethane ND ug/kg 1 06/05/12 04:48 75-69-43.7 1,2,3-Trichloropropane ND ug/kg 1 06/05/12 04:48 96-18-43.7 1,2,4-Trimethylbenzene ND ug/kg 1 06/05/12 04:48 95-63-63.7 1,3,5-Trimethylbenzene ND ug/kg 1 06/05/12 04:48 108-67-83.7 Vinyl acetate ND ug/kg 1 06/05/12 04:48 108-05-474.1 Vinyl chloride ND ug/kg 1 06/05/12 04:48 75-01-43.7 Xylene (Total)ND ug/kg 1 06/05/12 04:48 1330-20-77.4 Surrogates Dibromofluoromethane (S)102 %.1 06/05/12 04:48 1868-53-771-125 Toluene-d8 (S)100 %.1 06/05/12 04:48 2037-26-576-124 4-Bromofluorobenzene (S)102 %.1 06/05/12 04:48 460-00-467-134 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.9 %1 06/07/12 17:160.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 16 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:FB6:W053012 Lab ID:5063723007 Collected:05/30/12 14:00 Received:05/31/12 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/05/12 05:22 67-64-1100 Acrolein ND ug/L 1 06/05/12 05:22 107-02-8100 Acrylonitrile ND ug/L 1 06/05/12 05:22 107-13-1100 Benzene ND ug/L 1 06/05/12 05:22 71-43-25.0 Bromobenzene ND ug/L 1 06/05/12 05:22 108-86-15.0 Bromochloromethane ND ug/L 1 06/05/12 05:22 74-97-55.0 Bromodichloromethane ND ug/L 1 06/05/12 05:22 75-27-45.0 Bromoform ND ug/L 1 06/05/12 05:22 75-25-25.0 Bromomethane ND ug/L 1 06/05/12 05:22 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/05/12 05:22 78-93-325.0 n-Butylbenzene ND ug/L 1 06/05/12 05:22 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/05/12 05:22 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/05/12 05:22 98-06-65.0 Carbon disulfide ND ug/L 1 06/05/12 05:22 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/05/12 05:22 56-23-55.0 Chlorobenzene ND ug/L 1 06/05/12 05:22 108-90-75.0 Chloroethane ND ug/L 1 06/05/12 05:22 75-00-35.0 Chloroform ND ug/L 1 06/05/12 05:22 67-66-35.0 Chloromethane ND ug/L 1 06/05/12 05:22 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/05/12 05:22 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/05/12 05:22 106-43-45.0 Dibromochloromethane ND ug/L 1 06/05/12 05:22 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/05/12 05:22 106-93-45.0 Dibromomethane ND ug/L 1 06/05/12 05:22 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/05/12 05:22 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/05/12 05:22 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/05/12 05:22 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/05/12 05:22 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/05/12 05:22 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/05/12 05:22 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/05/12 05:22 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/05/12 05:22 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/05/12 05:22 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/05/12 05:22 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/05/12 05:22 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/05/12 05:22 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/05/12 05:22 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/05/12 05:22 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/05/12 05:22 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/05/12 05:22 10061-02-65.0 Ethylbenzene ND ug/L 1 06/05/12 05:22 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/05/12 05:22 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/05/12 05:22 87-68-35.0 n-Hexane ND ug/L 1 06/05/12 05:22 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/05/12 05:22 591-78-625.0 Iodomethane ND ug/L 1 06/05/12 05:22 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/05/12 05:22 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 17 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:FB6:W053012 Lab ID:5063723007 Collected:05/30/12 14:00 Received:05/31/12 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/05/12 05:22 99-87-65.0 Methylene Chloride ND ug/L 1 06/05/12 05:22 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/05/12 05:22 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/05/12 05:22 1634-04-44.0 Naphthalene ND ug/L 1 06/05/12 05:22 91-20-35.0 n-Propylbenzene ND ug/L 1 06/05/12 05:22 103-65-15.0 Styrene ND ug/L 1 06/05/12 05:22 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/05/12 05:22 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/05/12 05:22 79-34-55.0 Tetrachloroethene ND ug/L 1 06/05/12 05:22 127-18-45.0 Toluene ND ug/L 1 06/05/12 05:22 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/05/12 05:22 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/05/12 05:22 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/05/12 05:22 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/05/12 05:22 79-00-55.0 Trichloroethene ND ug/L 1 06/05/12 05:22 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/05/12 05:22 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/05/12 05:22 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/05/12 05:22 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/05/12 05:22 108-67-85.0 Vinyl acetate ND ug/L 1 06/05/12 05:22 108-05-450.0 Vinyl chloride ND ug/L 1 06/05/12 05:22 75-01-42.0 Xylene (Total)ND ug/L 1 06/05/12 05:22 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/05/12 05:22 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 06/05/12 05:22 460-00-472-125 Toluene-d8 (S)101 %.1 06/05/12 05:22 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 18 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:FB7:W053112 Lab ID:5063723008 Collected:05/31/12 12:50 Received:05/31/12 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/05/12 05:55 67-64-1100 Acrolein ND ug/L 1 06/05/12 05:55 107-02-8100 Acrylonitrile ND ug/L 1 06/05/12 05:55 107-13-1100 Benzene ND ug/L 1 06/05/12 05:55 71-43-25.0 Bromobenzene ND ug/L 1 06/05/12 05:55 108-86-15.0 Bromochloromethane ND ug/L 1 06/05/12 05:55 74-97-55.0 Bromodichloromethane ND ug/L 1 06/05/12 05:55 75-27-45.0 Bromoform ND ug/L 1 06/05/12 05:55 75-25-25.0 Bromomethane ND ug/L 1 06/05/12 05:55 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/05/12 05:55 78-93-325.0 n-Butylbenzene ND ug/L 1 06/05/12 05:55 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/05/12 05:55 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/05/12 05:55 98-06-65.0 Carbon disulfide ND ug/L 1 06/05/12 05:55 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/05/12 05:55 56-23-55.0 Chlorobenzene ND ug/L 1 06/05/12 05:55 108-90-75.0 Chloroethane ND ug/L 1 06/05/12 05:55 75-00-35.0 Chloroform 11.6 ug/L 1 06/05/12 05:55 67-66-3 2d5.0 Chloromethane ND ug/L 1 06/05/12 05:55 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/05/12 05:55 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/05/12 05:55 106-43-45.0 Dibromochloromethane ND ug/L 1 06/05/12 05:55 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/05/12 05:55 106-93-45.0 Dibromomethane ND ug/L 1 06/05/12 05:55 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/05/12 05:55 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/05/12 05:55 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/05/12 05:55 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/05/12 05:55 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/05/12 05:55 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/05/12 05:55 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/05/12 05:55 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/05/12 05:55 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/05/12 05:55 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/05/12 05:55 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/05/12 05:55 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/05/12 05:55 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/05/12 05:55 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/05/12 05:55 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/05/12 05:55 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/05/12 05:55 10061-02-65.0 Ethylbenzene ND ug/L 1 06/05/12 05:55 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/05/12 05:55 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/05/12 05:55 87-68-35.0 n-Hexane ND ug/L 1 06/05/12 05:55 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/05/12 05:55 591-78-625.0 Iodomethane ND ug/L 1 06/05/12 05:55 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/05/12 05:55 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 19 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5063723 SBI068 Sample:SBI068:FB7:W053112 Lab ID:5063723008 Collected:05/31/12 12:50 Received:05/31/12 17:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/05/12 05:55 99-87-65.0 Methylene Chloride ND ug/L 1 06/05/12 05:55 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/05/12 05:55 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/05/12 05:55 1634-04-44.0 Naphthalene ND ug/L 1 06/05/12 05:55 91-20-35.0 n-Propylbenzene ND ug/L 1 06/05/12 05:55 103-65-15.0 Styrene ND ug/L 1 06/05/12 05:55 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/05/12 05:55 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/05/12 05:55 79-34-55.0 Tetrachloroethene ND ug/L 1 06/05/12 05:55 127-18-45.0 Toluene ND ug/L 1 06/05/12 05:55 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/05/12 05:55 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/05/12 05:55 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/05/12 05:55 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/05/12 05:55 79-00-55.0 Trichloroethene ND ug/L 1 06/05/12 05:55 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/05/12 05:55 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/05/12 05:55 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/05/12 05:55 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/05/12 05:55 108-67-85.0 Vinyl acetate ND ug/L 1 06/05/12 05:55 108-05-450.0 Vinyl chloride ND ug/L 1 06/05/12 05:55 75-01-42.0 Xylene (Total)ND ug/L 1 06/05/12 05:55 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 06/05/12 05:55 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/05/12 05:55 460-00-472-125 Toluene-d8 (S)101 %.1 06/05/12 05:55 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 20 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42723 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5063723007, 5063723008 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:744135 Associated Lab Samples:5063723007, 5063723008 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/12 22:01 1,1,1-Trichloroethane ug/L ND 5.0 06/04/12 22:01 1,1,2,2-Tetrachloroethane ug/L ND 5.0 06/04/12 22:01 1,1,2-Trichloroethane ug/L ND 5.0 06/04/12 22:01 1,1-Dichloroethane ug/L ND 5.0 06/04/12 22:01 1,1-Dichloroethene ug/L ND 5.0 06/04/12 22:01 1,1-Dichloropropene ug/L ND 5.0 06/04/12 22:01 1,2,3-Trichlorobenzene ug/L ND 5.0 06/04/12 22:01 1,2,3-Trichloropropane ug/L ND 5.0 06/04/12 22:01 1,2,4-Trichlorobenzene ug/L ND 5.0 06/04/12 22:01 1,2,4-Trimethylbenzene ug/L ND 5.0 06/04/12 22:01 1,2-Dibromoethane (EDB)ug/L ND 5.0 06/04/12 22:01 1,2-Dichlorobenzene ug/L ND 5.0 06/04/12 22:01 1,2-Dichloroethane ug/L ND 5.0 06/04/12 22:01 1,2-Dichloropropane ug/L ND 5.0 06/04/12 22:01 1,3,5-Trimethylbenzene ug/L ND 5.0 06/04/12 22:01 1,3-Dichlorobenzene ug/L ND 5.0 06/04/12 22:01 1,3-Dichloropropane ug/L ND 5.0 06/04/12 22:01 1,4-Dichlorobenzene ug/L ND 5.0 06/04/12 22:01 2,2-Dichloropropane ug/L ND 5.0 06/04/12 22:01 2-Butanone (MEK)ug/L ND 25.0 06/04/12 22:01 2-Chlorotoluene ug/L ND 5.0 06/04/12 22:01 2-Hexanone ug/L ND 25.0 06/04/12 22:01 4-Chlorotoluene ug/L ND 5.0 06/04/12 22:01 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 06/04/12 22:01 Acetone ug/L ND 100 06/04/12 22:01 Acrolein ug/L ND 100 06/04/12 22:01 Acrylonitrile ug/L ND 100 06/04/12 22:01 Benzene ug/L ND 5.0 06/04/12 22:01 Bromobenzene ug/L ND 5.0 06/04/12 22:01 Bromochloromethane ug/L ND 5.0 06/04/12 22:01 Bromodichloromethane ug/L ND 5.0 06/04/12 22:01 Bromoform ug/L ND 5.0 06/04/12 22:01 Bromomethane ug/L ND 5.0 06/04/12 22:01 Carbon disulfide ug/L ND 10.0 06/04/12 22:01 Carbon tetrachloride ug/L ND 5.0 06/04/12 22:01 Chlorobenzene ug/L ND 5.0 06/04/12 22:01 Chloroethane ug/L ND 5.0 06/04/12 22:01 Chloroform ug/L ND 5.0 06/04/12 22:01 Chloromethane ug/L ND 5.0 06/04/12 22:01 cis-1,2-Dichloroethene ug/L ND 5.0 06/04/12 22:01 cis-1,3-Dichloropropene ug/L ND 5.0 06/04/12 22:01 Dibromochloromethane ug/L ND 5.0 06/04/12 22:01 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 21 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:744135 Associated Lab Samples:5063723007, 5063723008 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 06/04/12 22:01 Dichlorodifluoromethane ug/L ND 5.0 06/04/12 22:01 Ethyl methacrylate ug/L ND 100 06/04/12 22:01 Ethylbenzene ug/L ND 5.0 06/04/12 22:01 Hexachloro-1,3-butadiene ug/L ND 5.0 06/04/12 22:01 Iodomethane ug/L ND 10.0 06/04/12 22:01 Isopropylbenzene (Cumene)ug/L ND 5.0 06/04/12 22:01 Methyl-tert-butyl ether ug/L ND 4.0 06/04/12 22:01 Methylene Chloride ug/L ND 5.0 06/04/12 22:01 n-Butylbenzene ug/L ND 5.0 06/04/12 22:01 n-Hexane ug/L ND 5.0 N206/04/12 22:01 n-Propylbenzene ug/L ND 5.0 06/04/12 22:01 Naphthalene ug/L ND 5.0 06/04/12 22:01 p-Isopropyltoluene ug/L ND 5.0 06/04/12 22:01 sec-Butylbenzene ug/L ND 5.0 06/04/12 22:01 Styrene ug/L ND 5.0 06/04/12 22:01 tert-Butylbenzene ug/L ND 5.0 06/04/12 22:01 Tetrachloroethene ug/L ND 5.0 06/04/12 22:01 Toluene ug/L ND 5.0 06/04/12 22:01 trans-1,2-Dichloroethene ug/L ND 5.0 06/04/12 22:01 trans-1,3-Dichloropropene ug/L ND 5.0 06/04/12 22:01 trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/12 22:01 Trichloroethene ug/L ND 5.0 06/04/12 22:01 Trichlorofluoromethane ug/L ND 5.0 06/04/12 22:01 Vinyl acetate ug/L ND 50.0 06/04/12 22:01 Vinyl chloride ug/L ND 2.0 06/04/12 22:01 Xylene (Total)ug/L ND 10.0 06/04/12 22:01 4-Bromofluorobenzene (S)%.105 72-125 06/04/12 22:01 Dibromofluoromethane (S)%.103 83-123 06/04/12 22:01 Toluene-d8 (S)%.102 81-114 06/04/12 22:01 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744136LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 46.950 94 69-122 1,1,1-Trichloroethane ug/L 48.650 97 69-126 1,1,2,2-Tetrachloroethane ug/L 46.650 93 68-134 1,1,2-Trichloroethane ug/L 46.850 94 77-129 1,1-Dichloroethane ug/L 52.950 106 70-127 1,1-Dichloroethene ug/L 58.550 117 75-145 1,1-Dichloropropene ug/L 52.350 105 75-126 1,2,3-Trichlorobenzene ug/L 45.150 90 63-130 1,2,3-Trichloropropane ug/L 80.9 L35016245-121 1,2,4-Trichlorobenzene ug/L 44.150 88 64-122 1,2,4-Trimethylbenzene ug/L 53.450 107 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 22 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744136LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 45.450 91 77-123 1,2-Dichlorobenzene ug/L 52.050 104 74-123 1,2-Dichloroethane ug/L 48.750 97 71-127 1,2-Dichloropropane ug/L 46.850 94 75-126 1,3,5-Trimethylbenzene ug/L 44.050 88 69-129 1,3-Dichlorobenzene ug/L 42.450 85 76-123 1,3-Dichloropropane ug/L 50.150 100 77-126 1,4-Dichlorobenzene ug/L 44.450 89 77-121 2,2-Dichloropropane ug/L 45.050 90 45-138 2-Butanone (MEK)ug/L 269250 108 42-177 2-Chlorotoluene ug/L 43.350 87 74-129 2-Hexanone ug/L 276250 110 57-162 4-Chlorotoluene ug/L 52.450 105 70-125 4-Methyl-2-pentanone (MIBK)ug/L 254250 102 64-135 Acetone ug/L 270250 108 10-200 Acrolein ug/L 13701000 137 10-200 Acrylonitrile ug/L 11301000 113 59-144 Benzene ug/L 54.550 109 76-123 Bromobenzene ug/L 48.250 96 67-130 Bromochloromethane ug/L 41.850 84 58-153 Bromodichloromethane ug/L 47.450 95 71-124 Bromoform ug/L 42.050 84 64-116 Bromomethane ug/L 57.150 114 23-197 Carbon disulfide ug/L 107100 107 55-146 Carbon tetrachloride ug/L 51.050 102 65-125 Chlorobenzene ug/L 45.750 91 78-120 Chloroethane ug/L 55.850 112 56-163 Chloroform ug/L 49.250 98 73-122 Chloromethane ug/L 51.950 104 46-146 cis-1,2-Dichloroethene ug/L 53.550 107 79-129 cis-1,3-Dichloropropene ug/L 49.750 99 66-123 Dibromochloromethane ug/L 46.850 94 70-123 Dibromomethane ug/L 47.250 94 73-123 Dichlorodifluoromethane ug/L 47.850 96 19-200 Ethyl methacrylate ug/L 198200 99 70-127 Ethylbenzene ug/L 46.350 93 75-120 Hexachloro-1,3-butadiene ug/L 47.350 95 64-131 Iodomethane ug/L 85.8100 86 16-181 Isopropylbenzene (Cumene)ug/L 50.550 101 73-123 Methyl-tert-butyl ether ug/L 110100 110 66-128 Methylene Chloride ug/L 48.250 96 61-138 n-Butylbenzene ug/L 45.550 91 69-130 n-Hexane ug/L 48.0 N2509667-142 n-Propylbenzene ug/L 42.850 86 71-132 Naphthalene ug/L 47.550 95 62-130 p-Isopropyltoluene ug/L 45.450 91 71-126 sec-Butylbenzene ug/L 45.750 91 69-130 Styrene ug/L 50.550 101 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 23 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744136LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 37.850 76 49-114 Tetrachloroethene ug/L 46.550 93 57-125 Toluene ug/L 50.950 102 72-124 trans-1,2-Dichloroethene ug/L 54.450 109 71-145 trans-1,3-Dichloropropene ug/L 51.750 103 58-118 trans-1,4-Dichloro-2-butene ug/L 167200 84 50-121 Trichloroethene ug/L 48.350 97 77-122 Trichlorofluoromethane ug/L 62.850 126 56-159 Vinyl acetate ug/L 255 L320012727-119 Vinyl chloride ug/L 54.350 109 61-146 Xylene (Total)ug/L 148150 99 72-126 4-Bromofluorobenzene (S)%.99 72-125 Dibromofluoromethane (S)%.101 83-123 Toluene-d8 (S)%.97 81-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 24 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42722 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5063723001, 5063723002, 5063723003, 5063723004, 5063723005, 5063723006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:744129 Associated Lab Samples:5063723001, 5063723002, 5063723003, 5063723004, 5063723005, 5063723006 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/04/12 23:09 1,1,1-Trichloroethane ug/kg ND 5.0 06/04/12 23:09 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/04/12 23:09 1,1,2-Trichloroethane ug/kg ND 5.0 06/04/12 23:09 1,1-Dichloroethane ug/kg ND 5.0 06/04/12 23:09 1,1-Dichloroethene ug/kg ND 5.0 06/04/12 23:09 1,1-Dichloropropene ug/kg ND 5.0 06/04/12 23:09 1,2,3-Trichlorobenzene ug/kg ND 5.0 06/04/12 23:09 1,2,3-Trichloropropane ug/kg ND 5.0 06/04/12 23:09 1,2,4-Trichlorobenzene ug/kg ND 5.0 06/04/12 23:09 1,2,4-Trimethylbenzene ug/kg ND 5.0 06/04/12 23:09 1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/04/12 23:09 1,2-Dichlorobenzene ug/kg ND 5.0 06/04/12 23:09 1,2-Dichloroethane ug/kg ND 5.0 06/04/12 23:09 1,2-Dichloropropane ug/kg ND 5.0 06/04/12 23:09 1,3,5-Trimethylbenzene ug/kg ND 5.0 06/04/12 23:09 1,3-Dichlorobenzene ug/kg ND 5.0 06/04/12 23:09 1,3-Dichloropropane ug/kg ND 5.0 06/04/12 23:09 1,4-Dichlorobenzene ug/kg ND 5.0 06/04/12 23:09 2,2-Dichloropropane ug/kg ND 5.0 06/04/12 23:09 2-Butanone (MEK)ug/kg ND 25.0 06/04/12 23:09 2-Chlorotoluene ug/kg ND 5.0 06/04/12 23:09 2-Hexanone ug/kg ND 100 06/04/12 23:09 4-Chlorotoluene ug/kg ND 5.0 06/04/12 23:09 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 06/04/12 23:09 Acetone ug/kg ND 100 06/04/12 23:09 Acrolein ug/kg ND 100 06/04/12 23:09 Acrylonitrile ug/kg ND 100 06/04/12 23:09 Benzene ug/kg ND 5.0 06/04/12 23:09 Bromobenzene ug/kg ND 5.0 06/04/12 23:09 Bromochloromethane ug/kg ND 5.0 06/04/12 23:09 Bromodichloromethane ug/kg ND 5.0 06/04/12 23:09 Bromoform ug/kg ND 5.0 06/04/12 23:09 Bromomethane ug/kg ND 5.0 06/04/12 23:09 Carbon disulfide ug/kg ND 10.0 06/04/12 23:09 Carbon tetrachloride ug/kg ND 5.0 06/04/12 23:09 Chlorobenzene ug/kg ND 5.0 06/04/12 23:09 Chloroethane ug/kg ND 5.0 06/04/12 23:09 Chloroform ug/kg ND 5.0 06/04/12 23:09 Chloromethane ug/kg ND 5.0 06/04/12 23:09 cis-1,2-Dichloroethene ug/kg ND 5.0 06/04/12 23:09 cis-1,3-Dichloropropene ug/kg ND 5.0 06/04/12 23:09 Dibromochloromethane ug/kg ND 5.0 06/04/12 23:09 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 25 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:744129 Associated Lab Samples:5063723001, 5063723002, 5063723003, 5063723004, 5063723005, 5063723006 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 06/04/12 23:09 Dichlorodifluoromethane ug/kg ND 5.0 06/04/12 23:09 Ethyl methacrylate ug/kg ND 100 06/04/12 23:09 Ethylbenzene ug/kg ND 5.0 06/04/12 23:09 Hexachloro-1,3-butadiene ug/kg ND 5.0 06/04/12 23:09 Iodomethane ug/kg ND 100 06/04/12 23:09 Isopropylbenzene (Cumene)ug/kg ND 5.0 06/04/12 23:09 Methyl-tert-butyl ether ug/kg ND 5.0 06/04/12 23:09 Methylene Chloride ug/kg ND 20.0 06/04/12 23:09 n-Butylbenzene ug/kg ND 5.0 06/04/12 23:09 n-Hexane ug/kg ND 5.0 N206/04/12 23:09 n-Propylbenzene ug/kg ND 5.0 06/04/12 23:09 Naphthalene ug/kg ND 5.0 06/04/12 23:09 p-Isopropyltoluene ug/kg ND 5.0 06/04/12 23:09 sec-Butylbenzene ug/kg ND 5.0 06/04/12 23:09 Styrene ug/kg ND 5.0 06/04/12 23:09 tert-Butylbenzene ug/kg ND 5.0 06/04/12 23:09 Tetrachloroethene ug/kg ND 5.0 06/04/12 23:09 Toluene ug/kg ND 5.0 06/04/12 23:09 trans-1,2-Dichloroethene ug/kg ND 5.0 06/04/12 23:09 trans-1,3-Dichloropropene ug/kg ND 5.0 06/04/12 23:09 trans-1,4-Dichloro-2-butene ug/kg ND 100 06/04/12 23:09 Trichloroethene ug/kg ND 5.0 06/04/12 23:09 Trichlorofluoromethane ug/kg ND 5.0 06/04/12 23:09 Vinyl acetate ug/kg ND 100 06/04/12 23:09 Vinyl chloride ug/kg ND 5.0 06/04/12 23:09 Xylene (Total)ug/kg ND 10.0 06/04/12 23:09 4-Bromofluorobenzene (S)%.102 67-134 06/04/12 23:09 Dibromofluoromethane (S)%.106 71-125 06/04/12 23:09 Toluene-d8 (S)%.101 76-124 06/04/12 23:09 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744130LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 43.850 88 68-125 1,1,1-Trichloroethane ug/kg 44.850 90 63-124 1,1,2,2-Tetrachloroethane ug/kg 42.050 84 73-123 1,1,2-Trichloroethane ug/kg 43.950 88 70-124 1,1-Dichloroethane ug/kg 49.650 99 63-122 1,1-Dichloroethene ug/kg 53.250 106 71-129 1,1-Dichloropropene ug/kg 48.350 97 71-122 1,2,3-Trichlorobenzene ug/kg 42.650 85 68-123 1,2,3-Trichloropropane ug/kg 74.5 L35014947-117 1,2,4-Trichlorobenzene ug/kg 43.550 87 68-125 1,2,4-Trimethylbenzene ug/kg 50.650 101 69-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 26 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744130LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 41.250 82 67-121 1,2-Dichlorobenzene ug/kg 49.950 100 71-121 1,2-Dichloroethane ug/kg 45.750 91 74-120 1,2-Dichloropropane ug/kg 46.250 92 71-117 1,3,5-Trimethylbenzene ug/kg 41.350 83 64-119 1,3-Dichlorobenzene ug/kg 40.850 82 70-122 1,3-Dichloropropane ug/kg 46.750 93 68-118 1,4-Dichlorobenzene ug/kg 42.050 84 71-118 2,2-Dichloropropane ug/kg 43.150 86 62-119 2-Butanone (MEK)ug/kg 245250 98 38-154 2-Chlorotoluene ug/kg 40.550 81 71-120 2-Hexanone ug/kg 239250 95 50-134 4-Chlorotoluene ug/kg 49.550 99 72-123 4-Methyl-2-pentanone (MIBK)ug/kg 227250 91 66-122 Acetone ug/kg 242250 97 10-200 Acrolein ug/kg 12201000 122 11-200 Acrylonitrile ug/kg 10101000 101 66-120 Benzene ug/kg 52.250 104 73-115 Bromobenzene ug/kg 46.650 93 64-130 Bromochloromethane ug/kg 41.250 82 71-127 Bromodichloromethane ug/kg 43.850 88 60-121 Bromoform ug/kg 37.150 74 44-130 Bromomethane ug/kg 55.550 111 48-175 Carbon disulfide ug/kg 98.7100 99 71-126 Carbon tetrachloride ug/kg 46.050 92 57-127 Chlorobenzene ug/kg 43.250 86 72-121 Chloroethane ug/kg 51.750 103 72-141 Chloroform ug/kg 46.950 94 74-114 Chloromethane ug/kg 49.050 98 51-126 cis-1,2-Dichloroethene ug/kg 52.250 104 72-115 cis-1,3-Dichloropropene ug/kg 46.950 94 64-115 Dibromochloromethane ug/kg 43.550 87 58-114 Dibromomethane ug/kg 44.750 89 73-120 Dichlorodifluoromethane ug/kg 42.650 85 32-167 Ethyl methacrylate ug/kg 181200 91 65-117 Ethylbenzene ug/kg 42.750 85 73-120 Hexachloro-1,3-butadiene ug/kg 42.650 85 65-121 Iodomethane ug/kg 81.4J100 81 45-156 Isopropylbenzene (Cumene)ug/kg 46.750 93 74-123 Methyl-tert-butyl ether ug/kg 105100 105 69-123 Methylene Chloride ug/kg 46.450 93 58-124 n-Butylbenzene ug/kg 42.650 85 71-118 n-Hexane ug/kg 43.8 N2508850-106 n-Propylbenzene ug/kg 40.450 81 70-120 Naphthalene ug/kg 42.950 86 67-124 p-Isopropyltoluene ug/kg 42.450 85 71-123 sec-Butylbenzene ug/kg 42.150 84 66-122 Styrene ug/kg 48.250 96 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 27 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 744130LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 35.450 71 54-124 Tetrachloroethene ug/kg 42.550 85 66-126 Toluene ug/kg 47.950 96 69-115 trans-1,2-Dichloroethene ug/kg 52.250 104 69-120 trans-1,3-Dichloropropene ug/kg 49.050 98 61-116 trans-1,4-Dichloro-2-butene ug/kg 158200 79 59-130 Trichloroethene ug/kg 45.250 90 71-117 Trichlorofluoromethane ug/kg 58.250 116 67-138 Vinyl acetate ug/kg 232200 116 35-134 Vinyl chloride ug/kg 51.050 102 64-127 Xylene (Total)ug/kg 139150 92 69-117 4-Bromofluorobenzene (S)%.98 67-134 Dibromofluoromethane (S)%.100 71-125 Toluene-d8 (S)%.98 76-124 Parameter Units MS Result % Rec Limits Qual% RecConc. 744131MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063723001 744132 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 25.4 94 10-11184 22 2023ND23.9 19.2 1,1,1-Trichloroethane ug/kg 25.4 97 36-12885 23 2023ND24.6 19.6 1,1,2,2-Tetrachloroethane ug/kg 25.4 86 10-13077 21 2023ND22.0 17.7 1,1,2-Trichloroethane ug/kg 25.4 90 10-12681 20 2023ND22.9 18.7 1,1-Dichloroethane ug/kg 25.4 106 39-12695 21 2023ND27.0 21.8 1,1-Dichloroethene ug/kg 25.4 109 42-14799 20 2023ND27.7 22.7 1,1-Dichloropropene ug/kg 25.4 99 29-12990 19 2023ND25.1 20.7 1,2,3-Trichlorobenzene ug/kg 25.4 85 10-9172 26 2023ND21.5 16.6 1,2,3-Trichloropropane ug/kg M025.4 147 10-99136 18 2023ND37.4 31.2 1,2,4-Trichlorobenzene ug/kg 25.4 86 10-8871 29 2023ND21.8 16.3 1,2,4-Trimethylbenzene ug/kg 25.4 108 10-10994 24 2023ND27.5 21.5 1,2-Dibromoethane (EDB)ug/kg 25.4 86 10-11978 21 2023ND22.0 17.9 1,2-Dichlorobenzene ug/kg M025.4 105 10-10490 25 2023ND26.6 20.6 1,2-Dichloroethane ug/kg 25.4 93 19-12684 19 2023ND23.6 19.4 1,2-Dichloropropane ug/kg 25.4 97 24-12385 23 2023ND24.5 19.5 1,3,5-Trimethylbenzene ug/kg 25.4 89 10-11877 24 2023ND22.6 17.8 1,3-Dichlorobenzene ug/kg 25.4 86 10-10873 26 2023ND21.8 16.8 1,3-Dichloropropane ug/kg 25.4 100 12-12189 21 2023ND25.4 20.5 1,4-Dichlorobenzene ug/kg 25.4 89 10-10475 26 2023ND22.6 17.3 2,2-Dichloropropane ug/kg 25.4 88 32-12480 19 2023ND22.3 18.3 2-Butanone (MEK)ug/kg 127 129 10-183118 18 20115ND164136 2-Chlorotoluene ug/kg 25.4 87 10-12875 25 2023ND22.1 17.3 2-Hexanone ug/kg 127 112 10-158107 15 20115ND143123 4-Chlorotoluene ug/kg 25.4 108 10-11990 28 2023ND27.3 20.7 4-Methyl-2-pentanone (MIBK)ug/kg 127 92 12-13085 18 20115ND11797.8 Acetone ug/kg M012720510-200186 19 20115ND260214 Acrolein ug/kg 509 120 10-200113 16 20460ND612521 Acrylonitrile ug/kg 509 98 19-13085 24 20460ND498392 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 28 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 744131MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063723001 744132 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 25.4 110 23-13898 21 2023ND27.9 22.5 Bromobenzene ug/kg 25.4 98 10-111105 3 2023ND24.9 24.1 Bromochloromethane ug/kg 25.4 86 26-12675 24 2023ND21.9 17.2 Bromodichloromethane ug/kg 25.4 92 10-12083 20 2023ND23.3 19.1 Bromoform ug/kg 25.4 76 10-10667 23 2023ND19.3 15.4 Bromomethane ug/kg 25.4 113 10-190110 13 2023ND28.7 25.2 Carbon disulfide ug/kg 50.9 103 31-12890 24 2046ND52.3 41.2 Carbon tetrachloride ug/kg 25.4 95 26-12686 20 2023ND24.3 19.8 Chlorobenzene ug/kg 25.4 92 10-12080 24 2023ND23.4 18.5 Chloroethane ug/kg 25.4 101 18-18695 16 2023ND25.6 21.8 Chloroform ug/kg 25.4 99 29-12689 21 2023ND25.2 20.5 Chloromethane ug/kg 25.4 102 34-13194 18 2023ND26.0 21.6 cis-1,2-Dichloroethene ug/kg 25.4 109 28-13294 25 2023ND27.8 21.6 cis-1,3-Dichloropropene ug/kg 25.4 99 10-10888 21 2023ND25.2 20.3 Dibromochloromethane ug/kg 25.4 90 10-10881 21 2023ND22.9 18.6 Dibromomethane ug/kg 25.4 89 13-12282 18 2023ND22.7 18.9 Dichlorodifluoromethane ug/kg 25.4 91 10-19782 20 2023ND23.2 19.0 Ethyl methacrylate ug/kg 102 94 10-13086 19 2091.9ND 95.5 79.2 Ethylbenzene ug/kg 25.4 91 10-13580 22 2023ND23.2 18.5 Hexachloro-1,3-butadiene ug/kg 25.4 91 10-10581 22 2023ND23.1 18.6 Iodomethane ug/kg 50.9 87 10-16388 2046ND44.2J 40.3J Isopropylbenzene (Cumene)ug/kg 25.4 100 10-12189 22 2023ND25.5 20.4 Methyl-tert-butyl ether ug/kg 50.9 108 20-140100 18 2046ND55.0 46.0 Methylene Chloride ug/kg 25.4 75 28-13174 12 2023ND19.1 16.9 n-Butylbenzene ug/kg 25.4 89 10-11076 25 2023ND22.6 17.5 n-Hexane ug/kg N225.4 104 21-15088 26 2023ND26.4 20.3 n-Propylbenzene ug/kg 25.4 86 10-12375 23 2023ND21.8 17.2 Naphthalene ug/kg 25.4 83 10-10676 19 2023ND21.6 17.9 p-Isopropyltoluene ug/kg 25.4 89 10-11778 23 2023ND22.6 17.9 sec-Butylbenzene ug/kg 25.4 90 10-12379 23 2023ND22.9 18.2 Styrene ug/kg 25.4 102 10-11990 23 2023ND26.0 20.6 tert-Butylbenzene ug/kg 25.4 75 10-10566 24 2023ND19.1 15.1 Tetrachloroethene ug/kg 25.4 96 10-12283 25 2023ND24.5 19.1 Toluene ug/kg 25.4 104 10-13191 23 2023ND26.4 20.8 trans-1,2-Dichloroethene ug/kg 25.4 109 32-13687 32 2023ND27.7 20.1 trans-1,3-Dichloropropene ug/kg 25.4 100 10-10190 21 2023ND25.4 20.6 trans-1,4-Dichloro-2-butene ug/kg 102 76 10-10472 15 2091.9ND 77.4 66.4 Trichloroethene ug/kg 25.4 95 15-13387 20 2023ND24.2 19.9 Trichlorofluoromethane ug/kg 25.4 121 37-152108 21 2023ND30.8 25.0 Vinyl acetate ug/kg 102 96 10-10388 19 2091.9ND 97.9 81.2 Vinyl chloride ug/kg 25.4 106 41-14796 20 2023ND26.9 22.0 Xylene (Total)ug/kg 76.3 99 10-13187 23 2069ND75.4 59.8 4-Bromofluorobenzene (S)%.98 67-13498 20 Dibromofluoromethane (S)%.1d9871-125100 20 Toluene-d8 (S)%.99 76-12498 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 29 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 744133MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063723004 744134 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 46 75 10-11184 6 2043.6ND 34.5 36.6 1,1,1-Trichloroethane ug/kg 46 77 36-12888 8 2043.6ND 35.6 38.5 1,1,2,2-Tetrachloroethane ug/kg 46 69 10-13075 3 2043.6ND 31.9 32.8 1,1,2-Trichloroethane ug/kg 46 74 10-12682 6 2043.6ND 33.9 35.9 1,1-Dichloroethane ug/kg 46 89 39-12695 1 2043.6ND 40.9 41.4 1,1-Dichloroethene ug/kg 46 91 42-147102 6 2043.6ND 42.0 44.7 1,1-Dichloropropene ug/kg 46 82 29-12992 5 2043.6ND 37.9 40.0 1,2,3-Trichlorobenzene ug/kg 46 62 10-9168 4 2043.6ND 28.4 29.7 1,2,3-Trichloropropane ug/kg M04611710-99128 4 2043.6ND 53.8 56.0 1,2,4-Trichlorobenzene ug/kg 46 63 10-8871 7 2043.6ND 28.8 30.8 1,2,4-Trimethylbenzene ug/kg 46 85 10-10996 7 2043.6ND 39.2 42.0 1,2-Dibromoethane (EDB)ug/kg 46 69 10-11977 6 2043.6ND 31.5 33.5 1,2-Dichlorobenzene ug/kg 46 79 10-10488 5 2043.6ND 36.4 38.4 1,2-Dichloroethane ug/kg 46 76 19-12685 6 2043.6ND 35.1 37.1 1,2-Dichloropropane ug/kg 46 79 24-12388 5 2043.6ND 36.6 38.4 1,3,5-Trimethylbenzene ug/kg 46 72 10-11880 5 2043.6ND 33.1 34.8 1,3-Dichlorobenzene ug/kg 46 66 10-10874 5 2043.6ND 30.6 32.3 1,3-Dichloropropane ug/kg 46 78 12-12186 4 2043.6ND 36.0 37.6 1,4-Dichlorobenzene ug/kg 46 69 10-10476 4 2043.6ND 31.9 33.2 2,2-Dichloropropane ug/kg 46 73 32-12482 6 2043.6ND 33.5 35.6 2-Butanone (MEK)ug/kg 230 100 10-183107 2 20218ND230233 2-Chlorotoluene ug/kg 46 70 10-12877 4 2043.6ND 32.3 33.8 2-Hexanone ug/kg 230 89 10-158100 6 20218ND206218 4-Chlorotoluene ug/kg 46 83 10-11994 8 2043.6ND 38.1 41.1 4-Methyl-2-pentanone (MIBK)ug/kg 230 75 12-13081 2 20218ND173177 Acetone ug/kg 230 156 10-200180 9 20218ND358392 Acrolein ug/kg 920 92 10-200109 12 20873ND846954 Acrylonitrile ug/kg 920 72 19-13089 15 20873ND664774 Benzene ug/kg 46 88 23-138100 8 2043.6ND 40.4 43.7 Bromobenzene ug/kg 46 93 10-11187 12 2043.6ND 42.8 37.9 Bromochloromethane ug/kg 46 68 26-12676 6 2043.6ND 31.1 33.1 Bromodichloromethane ug/kg 46 74 10-12082 6 2043.6ND 33.9 35.9 Bromoform ug/kg 46 59 10-10666 6 2043.6ND 27.1 28.7 Bromomethane ug/kg 46 87 10-190104 12 2043.6ND 40.0 45.2 Carbon disulfide ug/kg 92 79 31-12893 11 2087.3ND 72.7 80.8 Carbon tetrachloride ug/kg 46 79 26-12686 3 2043.6ND 36.4 37.7 Chlorobenzene ug/kg 46 74 10-12083 6 2043.6ND 34.1 36.3 Chloroethane ug/kg 46 84 18-18699 12 2043.6ND 38.5 43.3 Chloroform ug/kg 46 80 29-12691 8 2043.6ND 37.0 39.9 Chloromethane ug/kg 46 76 34-13188 10 2043.6ND 34.9 38.6 cis-1,2-Dichloroethene ug/kg 46 88 28-132101 8 2043.6ND 40.6 43.9 cis-1,3-Dichloropropene ug/kg 46 81 10-10888 2 2043.6ND 37.5 38.2 Dibromochloromethane ug/kg 46 70 10-10877 4 2043.6ND 32.0 33.4 Dibromomethane ug/kg 46 72 13-12281 5 2043.6ND 33.3 35.2 Dichlorodifluoromethane ug/kg 46 61 10-19769 7 2043.6ND 28.2 30.1 Ethyl methacrylate ug/kg 184 75 10-13078 1 20175ND137135 Ethylbenzene ug/kg 46 74 10-13583 6 2043.6ND 34.0 36.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 30 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 744133MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5063723004 744134 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Hexachloro-1,3-butadiene ug/kg 46 72 10-10581 7 2043.6ND 33.1 35.5 Iodomethane ug/kg 92 71 10-16382 2087.3ND 65.7J 71.3J Isopropylbenzene (Cumene)ug/kg 46 81 10-12191 7 2043.6ND 37.1 39.9 Methyl-tert-butyl ether ug/kg 92 86 20-14099 8 2087.3ND 79.6 86.4 Methylene Chloride ug/kg 46 60 28-13173 13 2043.6ND 27.8 31.8 n-Butylbenzene ug/kg 46 71 10-11080 7 2043.6ND 32.5 34.9 n-Hexane ug/kg N2466821-15079 9 2043.6ND 31.4 34.4 n-Propylbenzene ug/kg 46 70 10-12378 5 2043.6ND 32.2 33.9 Naphthalene ug/kg 46 65 10-10670 2 2043.6ND 29.8 30.5 p-Isopropyltoluene ug/kg 46 72 10-11781 6 2043.6ND 33.0 35.1 sec-Butylbenzene ug/kg 46 74 10-12382 5 2043.6ND 33.9 35.7 Styrene ug/kg 46 82 10-11992 6 2043.6ND 37.7 40.0 tert-Butylbenzene ug/kg 46 62 10-10568 4 2043.6ND 28.7 29.8 Tetrachloroethene ug/kg 46 75 10-12287 9 2043.6ND 34.5 37.8 Toluene ug/kg 46 84 10-13193 5 2043.6ND 38.6 40.5 trans-1,2-Dichloroethene ug/kg 46 86 32-13698 8 2043.6ND 39.4 42.6 trans-1,3-Dichloropropene ug/kg 46 79 10-10189 6 2043.6ND 36.5 38.8 trans-1,4-Dichloro-2-butene ug/kg 184 60 10-10464 .7 20175ND111112 Trichloroethene ug/kg 46 79 15-13389 7 2043.6ND 36.3 38.8 Trichlorofluoromethane ug/kg 46 96 37-152110 8 2043.6ND 44.2 47.9 Vinyl acetate ug/kg 184 59 10-10349 20175ND10985.9J Vinyl chloride ug/kg 46 81 41-14789 4 2043.6ND 37.5 38.9 Xylene (Total)ug/kg 138 80 10-13190 7 20131ND110118 4-Bromofluorobenzene (S)%.96 67-13498 20 Dibromofluoromethane (S)%.99 71-125103 20 Toluene-d8 (S)%.99 76-124100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 31 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5063723 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/7120 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5063723001, 5063723002, 5063723003, 5063723004, 5063723005, 5063723006 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063723001 746432SAMPLE DUPLICATE: Percent Moisture %13.0 1 513.1 Parameter Units Dup Result Max RPD QualifiersRPDResult 5063723004 746433SAMPLE DUPLICATE: Percent Moisture %8.2 R11659.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 32 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5063723 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Several compounds are outside of acceptance limits for percent recovery and/or RPD value. aa 6/5/121d The presence of this compound indicates the possibe use of commercially purched deionized water. aa 6/5/122d Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 33 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5063723 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5063723007 MSV/42723SBI068:FB6:W053012 EPA 8260 5063723008 MSV/42723SBI068:FB7:W053112 EPA 8260 5063723001 MSV/42722SBI068:AMW2D:S180187 EPA 8260 5063723002 MSV/42722SBI068:AMW2D:S120131 EPA 8260 5063723003 MSV/42722SBI068:AMW2D:S120131A EPA 8260 5063723004 MSV/42722SBI068:AMW5D:S220225 EPA 8260 5063723005 MSV/42722SBI068:AMW5D:S160172 EPA 8260 5063723006 MSV/42722SBI068:AMW5D:S160172A EPA 8260 5063723001 PMST/7120SBI068:AMW2D:S180187 ASTM D2974-87 5063723002 PMST/7120SBI068:AMW2D:S120131 ASTM D2974-87 5063723003 PMST/7120SBI068:AMW2D:S120131A ASTM D2974-87 5063723004 PMST/7120SBI068:AMW5D:S220225 ASTM D2974-87 5063723005 PMST/7120SBI068:AMW5D:S160172 ASTM D2974-87 5063723006 PMST/7120SBI068:AMW5D:S160172A ASTM D2974-87 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/09/2012 10:13 AM Page 34 of 34 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 June 22, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5064189 5064189 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 8470 Allison Pointe Blvd. Suite 120 Indianapolis, IN 46250 SBI068 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on June 08, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5064189 SBI068 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5064189 SBI068 Lab ID Sample ID Matrix Date Collected Date Received 5064189001 SBI068:AMW6I:G060512 Water 06/05/12 10:18 06/08/12 11:47 5064189002 SBI068:AMW6S:G060512 Water 06/05/12 11:05 06/08/12 11:47 5064189003 SBI068:AMW7I:G060512 Water 06/05/12 12:15 06/08/12 11:47 5064189004 SBI068:AMW7S:G060512 Water 06/05/12 13:08 06/08/12 11:47 5064189005 SBI068:AMW8I:G060512 Water 06/05/12 13:58 06/08/12 11:47 5064189006 SBI068:AMW8S:G060512 Water 06/05/12 14:55 06/08/12 11:47 5064189007 SBI068:AMW5S:G060612 Water 06/06/12 11:13 06/08/12 11:47 5064189008 SBI068:AMW5I:G060512 Water 06/05/12 16:43 06/08/12 11:47 5064189009 SBI068:AMW5D:G060512 Water 06/05/12 16:10 06/08/12 11:47 5064189010 SBI068:AMW6I:G060512A Water 06/05/12 10:20 06/08/12 11:47 5064189011 SBI068:EB1:W060512 Water 06/05/12 14:50 06/08/12 11:47 5064189012 SBI068:EB2:W060612 Water 06/06/12 18:00 06/08/12 11:47 5064189013 SBI068:AMW4D:G060612 Water 06/06/12 12:03 06/08/12 11:47 5064189014 SBI068:AMW4I:G060612 Water 06/06/12 12:30 06/08/12 11:47 5064189015 SBI068:AMW4S:G060612 Water 06/06/12 13:10 06/08/12 11:47 5064189016 SBI068:AMW1D:G060612 Water 06/06/12 14:01 06/08/12 11:47 5064189017 SBI068:AMW1I:G060612 Water 06/06/12 14:43 06/08/12 11:47 5064189018 SBI068:AMW1S:G060612 Water 06/06/12 15:28 06/08/12 11:47 5064189019 SBI068:AMW3D:G060612 Water 06/06/12 15:54 06/08/12 11:47 5064189020 SBI068:AMW3I:G060612 Water 06/06/12 16:47 06/08/12 11:47 5064189021 SBI068:AMW3S:G060612 Water 06/06/12 17:53 06/08/12 11:47 5064189022 SBI068:AMW2D:G060712 Water 06/07/12 09:18 06/08/12 11:47 5064189023 SBI068:AMW2I:G060712 Water 06/07/12 10:12 06/08/12 11:47 5064189024 SBI068:AMW2S:G060712 Water 06/07/12 10:32 06/08/12 11:47 5064189025 SBI068:EB3:W060712 Water 06/07/12 10:50 06/08/12 11:47 5064189026 SBI068:AMW1I:G060612A Water 06/06/12 14:45 06/08/12 11:47 5064189027 SBI068:AMW2I:G060712A Water 06/07/12 10:12 06/08/12 11:47 5064189028 SBI068:LTB:W060512 Water 06/05/12 08:00 06/08/12 11:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5064189 SBI068 Lab ID Sample ID Method Analytes ReportedAnalysts 5064189001 SBI068:AMW6I:G060512 EPA 8260 73JLZ 5064189002 SBI068:AMW6S:G060512 EPA 8260 73JLZ 5064189003 SBI068:AMW7I:G060512 EPA 8260 73JLZ 5064189004 SBI068:AMW7S:G060512 EPA 8260 73ALA 5064189005 SBI068:AMW8I:G060512 EPA 8260 73JLZ 5064189006 SBI068:AMW8S:G060512 EPA 8260 73JLZ 5064189007 SBI068:AMW5S:G060612 EPA 8260 73JLZ 5064189008 SBI068:AMW5I:G060512 EPA 8260 73ALA 5064189009 SBI068:AMW5D:G060512 EPA 8260 73ALA 5064189010 SBI068:AMW6I:G060512A EPA 8260 73ALA 5064189011 SBI068:EB1:W060512 EPA 8260 73ALA 5064189012 SBI068:EB2:W060612 EPA 8260 73ALA 5064189013 SBI068:AMW4D:G060612 EPA 8260 73ALA 5064189014 SBI068:AMW4I:G060612 EPA 8260 73ALA 5064189015 SBI068:AMW4S:G060612 EPA 8260 73ALA 5064189016 SBI068:AMW1D:G060612 EPA 8260 73ALA 5064189017 SBI068:AMW1I:G060612 EPA 8260 73ALA 5064189018 SBI068:AMW1S:G060612 EPA 8260 73ALA 5064189019 SBI068:AMW3D:G060612 EPA 8260 73ALA 5064189020 SBI068:AMW3I:G060612 EPA 8260 73ALA 5064189021 SBI068:AMW3S:G060612 EPA 8260 73ALA 5064189022 SBI068:AMW2D:G060712 EPA 8260 73ALA 5064189023 SBI068:AMW2I:G060712 EPA 8260 73ALA 5064189024 SBI068:AMW2S:G060712 EPA 8260 73ALA 5064189025 SBI068:EB3:W060712 EPA 8260 73ALA 5064189026 SBI068:AMW1I:G060612A EPA 8260 73ALA 5064189027 SBI068:AMW2I:G060712A EPA 8260 73ALA 5064189028 SBI068:LTB:W060512 EPA 8260 73ALA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6I:G060512 Lab ID:5064189001 Collected:06/05/12 10:18 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 12:42 67-64-1100 Acrolein ND ug/L 1 06/12/12 12:42 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 12:42 107-13-1100 Benzene ND ug/L 1 06/12/12 12:42 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 12:42 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 12:42 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 12:42 75-27-45.0 Bromoform ND ug/L 1 06/12/12 12:42 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 12:42 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 12:42 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 12:42 104-51-85.0 sec-Butylbenzene 7.9 ug/L 1 06/12/12 12:42 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 12:42 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 12:42 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 12:42 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 12:42 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 12:42 75-00-35.0 Chloroform ND ug/L 1 06/12/12 12:42 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 12:42 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 12:42 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 12:42 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 12:42 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 12:42 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 12:42 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 12:42 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 12:42 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 12:42 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 12:42 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 12:42 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 12:42 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 12:42 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 12:42 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 12:42 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 12:42 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 12:42 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 12:42 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 12:42 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 12:42 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 12:42 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 12:42 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 12:42 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 12:42 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 12:42 87-68-35.0 n-Hexane 19.1 ug/L 1 06/12/12 12:42 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 12:42 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 12:42 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 12:42 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 5 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6I:G060512 Lab ID:5064189001 Collected:06/05/12 10:18 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 12:42 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 12:42 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 12:42 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 12:42 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 12:42 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 12:42 103-65-15.0 Styrene ND ug/L 1 06/12/12 12:42 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 12:42 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 12:42 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 12:42 127-18-45.0 Toluene ND ug/L 1 06/12/12 12:42 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 12:42 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 12:42 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 12:42 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 12:42 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 12:42 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 12:42 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 12:42 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 12:42 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 12:42 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 12:42 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 12:42 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 12:42 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/12/12 12:42 1868-53-783-123 4-Bromofluorobenzene (S)103 %.1 06/12/12 12:42 460-00-472-125 Toluene-d8 (S)102 %.1 06/12/12 12:42 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 6 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6S:G060512 Lab ID:5064189002 Collected:06/05/12 11:05 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 13:14 67-64-1100 Acrolein ND ug/L 1 06/12/12 13:14 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 13:14 107-13-1100 Benzene ND ug/L 1 06/12/12 13:14 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 13:14 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 13:14 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 13:14 75-27-45.0 Bromoform ND ug/L 1 06/12/12 13:14 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 13:14 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 13:14 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 13:14 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 13:14 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 13:14 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 13:14 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 13:14 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 13:14 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 13:14 75-00-35.0 Chloroform ND ug/L 1 06/12/12 13:14 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 13:14 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 13:14 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 13:14 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 13:14 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 13:14 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 13:14 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 13:14 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 13:14 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 13:14 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 13:14 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 13:14 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 13:14 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 13:14 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 13:14 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 13:14 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 13:14 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 13:14 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 13:14 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 13:14 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 13:14 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 13:14 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 13:14 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 13:14 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 13:14 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 13:14 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 13:14 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 13:14 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 13:14 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 13:14 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 7 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6S:G060512 Lab ID:5064189002 Collected:06/05/12 11:05 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 13:14 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 13:14 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 13:14 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 13:14 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 13:14 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 13:14 103-65-15.0 Styrene ND ug/L 1 06/12/12 13:14 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 13:14 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 13:14 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 13:14 127-18-45.0 Toluene ND ug/L 1 06/12/12 13:14 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 13:14 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 13:14 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 13:14 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 13:14 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 13:14 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 13:14 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 13:14 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 13:14 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 13:14 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 13:14 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 13:14 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 13:14 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 13:14 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/12/12 13:14 460-00-472-125 Toluene-d8 (S)100 %.1 06/12/12 13:14 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 8 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW7I:G060512 Lab ID:5064189003 Collected:06/05/12 12:15 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 13:46 67-64-1100 Acrolein ND ug/L 1 06/12/12 13:46 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 13:46 107-13-1100 Benzene ND ug/L 1 06/12/12 13:46 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 13:46 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 13:46 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 13:46 75-27-45.0 Bromoform ND ug/L 1 06/12/12 13:46 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 13:46 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 13:46 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 13:46 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 13:46 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 13:46 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 13:46 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 13:46 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 13:46 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 13:46 75-00-35.0 Chloroform ND ug/L 1 06/12/12 13:46 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 13:46 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 13:46 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 13:46 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 13:46 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 13:46 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 13:46 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 13:46 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 13:46 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 13:46 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 13:46 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 13:46 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 13:46 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 13:46 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 13:46 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 13:46 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 13:46 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 13:46 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 13:46 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 13:46 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 13:46 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 13:46 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 13:46 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 13:46 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 13:46 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 13:46 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 13:46 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 13:46 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 13:46 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 13:46 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 9 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW7I:G060512 Lab ID:5064189003 Collected:06/05/12 12:15 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 13:46 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 13:46 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 13:46 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 13:46 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 13:46 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 13:46 103-65-15.0 Styrene ND ug/L 1 06/12/12 13:46 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 13:46 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 13:46 79-34-55.0 Tetrachloroethene 92.5 ug/L 1 06/12/12 13:46 127-18-45.0 Toluene ND ug/L 1 06/12/12 13:46 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 13:46 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 13:46 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 13:46 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 13:46 79-00-55.0 Trichloroethene 11.1 ug/L 1 06/12/12 13:46 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 13:46 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 13:46 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 13:46 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 13:46 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 13:46 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 13:46 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 13:46 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 06/12/12 13:46 1868-53-783-123 4-Bromofluorobenzene (S)103 %.1 06/12/12 13:46 460-00-472-125 Toluene-d8 (S)102 %.1 06/12/12 13:46 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 10 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW7S:G060512 Lab ID:5064189004 Collected:06/05/12 13:08 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 19:37 67-64-1100 Acrolein ND ug/L 1 06/12/12 19:37 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 19:37 107-13-1100 Benzene ND ug/L 1 06/12/12 19:37 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 19:37 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 19:37 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 19:37 75-27-45.0 Bromoform ND ug/L 1 06/12/12 19:37 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 19:37 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 19:37 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 19:37 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 19:37 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 19:37 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 19:37 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 19:37 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 19:37 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 19:37 75-00-35.0 Chloroform ND ug/L 1 06/12/12 19:37 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 19:37 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 19:37 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 19:37 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 19:37 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 19:37 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 19:37 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 19:37 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 19:37 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 19:37 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 19:37 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 19:37 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 19:37 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 19:37 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 19:37 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 19:37 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 19:37 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 19:37 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 19:37 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 19:37 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 19:37 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 19:37 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 19:37 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 19:37 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 19:37 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 19:37 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 19:37 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 19:37 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 19:37 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 19:37 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 11 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW7S:G060512 Lab ID:5064189004 Collected:06/05/12 13:08 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 19:37 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 19:37 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 19:37 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 19:37 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 19:37 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 19:37 103-65-15.0 Styrene ND ug/L 1 06/12/12 19:37 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 19:37 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 19:37 79-34-55.0 Tetrachloroethene 71.5 ug/L 1 06/12/12 19:37 127-18-45.0 Toluene ND ug/L 1 06/12/12 19:37 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 19:37 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 19:37 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 19:37 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 19:37 79-00-55.0 Trichloroethene 6.2 ug/L 1 06/12/12 19:37 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 19:37 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 19:37 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 19:37 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 19:37 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 19:37 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 19:37 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 19:37 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/12/12 19:37 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/12/12 19:37 460-00-472-125 Toluene-d8 (S)100 %.1 06/12/12 19:37 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 12 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW8I:G060512 Lab ID:5064189005 Collected:06/05/12 13:58 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 14:18 67-64-1100 Acrolein ND ug/L 1 06/12/12 14:18 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 14:18 107-13-1100 Benzene ND ug/L 1 06/12/12 14:18 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 14:18 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 14:18 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 14:18 75-27-45.0 Bromoform ND ug/L 1 06/12/12 14:18 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 14:18 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 14:18 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 14:18 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 14:18 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 14:18 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 14:18 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 14:18 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 14:18 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 14:18 75-00-35.0 Chloroform ND ug/L 1 06/12/12 14:18 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 14:18 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 14:18 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 14:18 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 14:18 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 14:18 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 14:18 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 14:18 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 14:18 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 14:18 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 14:18 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 14:18 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 14:18 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 14:18 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 14:18 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 14:18 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 14:18 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 14:18 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 14:18 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 14:18 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 14:18 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 14:18 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 14:18 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 14:18 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 14:18 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 14:18 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 14:18 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 14:18 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 14:18 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 14:18 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 13 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW8I:G060512 Lab ID:5064189005 Collected:06/05/12 13:58 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 14:18 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 14:18 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 14:18 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 14:18 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 14:18 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 14:18 103-65-15.0 Styrene ND ug/L 1 06/12/12 14:18 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 14:18 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 14:18 79-34-55.0 Tetrachloroethene 8.8 ug/L 1 06/12/12 14:18 127-18-45.0 Toluene ND ug/L 1 06/12/12 14:18 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 14:18 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 14:18 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 14:18 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 14:18 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 14:18 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 14:18 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 14:18 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 14:18 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 14:18 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 14:18 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 14:18 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 14:18 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 14:18 1868-53-783-123 4-Bromofluorobenzene (S)103 %.1 06/12/12 14:18 460-00-472-125 Toluene-d8 (S)102 %.1 06/12/12 14:18 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 14 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW8S:G060512 Lab ID:5064189006 Collected:06/05/12 14:55 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 14:50 67-64-1100 Acrolein ND ug/L 1 06/12/12 14:50 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 14:50 107-13-1100 Benzene ND ug/L 1 06/12/12 14:50 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 14:50 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 14:50 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 14:50 75-27-45.0 Bromoform ND ug/L 1 06/12/12 14:50 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 14:50 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 14:50 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 14:50 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 14:50 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 14:50 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 14:50 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 14:50 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 14:50 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 14:50 75-00-35.0 Chloroform ND ug/L 1 06/12/12 14:50 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 14:50 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 14:50 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 14:50 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 14:50 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 14:50 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 14:50 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 14:50 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 14:50 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 14:50 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 14:50 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 14:50 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 14:50 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 14:50 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 14:50 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 14:50 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 14:50 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 14:50 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 14:50 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 14:50 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 14:50 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 14:50 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 14:50 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 14:50 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 14:50 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 14:50 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 14:50 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 14:50 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 14:50 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 14:50 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 15 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW8S:G060512 Lab ID:5064189006 Collected:06/05/12 14:55 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 14:50 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 14:50 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 14:50 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 14:50 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 14:50 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 14:50 103-65-15.0 Styrene ND ug/L 1 06/12/12 14:50 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 14:50 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 14:50 79-34-55.0 Tetrachloroethene 7.6 ug/L 1 06/12/12 14:50 127-18-45.0 Toluene ND ug/L 1 06/12/12 14:50 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 14:50 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 14:50 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 14:50 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 14:50 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 14:50 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 14:50 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 14:50 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 14:50 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 14:50 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 14:50 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 14:50 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 14:50 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 06/12/12 14:50 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/12/12 14:50 460-00-472-125 Toluene-d8 (S)99 %.1 06/12/12 14:50 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 16 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5S:G060612 Lab ID:5064189007 Collected:06/06/12 11:13 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 15:22 67-64-1100 Acrolein ND ug/L 1 06/12/12 15:22 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 15:22 107-13-1100 Benzene ND ug/L 1 06/12/12 15:22 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 15:22 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 15:22 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 15:22 75-27-45.0 Bromoform ND ug/L 1 06/12/12 15:22 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 15:22 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 15:22 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 15:22 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 15:22 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 15:22 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 15:22 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 15:22 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 15:22 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 15:22 75-00-35.0 Chloroform ND ug/L 1 06/12/12 15:22 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 15:22 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 15:22 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 15:22 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 15:22 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 15:22 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 15:22 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 15:22 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 15:22 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 15:22 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 15:22 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 15:22 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 15:22 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 15:22 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 15:22 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 15:22 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 15:22 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 15:22 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 15:22 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 15:22 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 15:22 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 15:22 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 15:22 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 15:22 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 15:22 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 15:22 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 15:22 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 15:22 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 15:22 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 15:22 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 17 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5S:G060612 Lab ID:5064189007 Collected:06/06/12 11:13 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 15:22 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 15:22 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 15:22 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 15:22 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 15:22 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 15:22 103-65-15.0 Styrene ND ug/L 1 06/12/12 15:22 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 15:22 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 15:22 79-34-55.0 Tetrachloroethene 15.3 ug/L 1 06/12/12 15:22 127-18-45.0 Toluene ND ug/L 1 06/12/12 15:22 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 15:22 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 15:22 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 15:22 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 15:22 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 15:22 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 15:22 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 15:22 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 15:22 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 15:22 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 15:22 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 15:22 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 15:22 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 15:22 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 06/12/12 15:22 460-00-472-125 Toluene-d8 (S)101 %.1 06/12/12 15:22 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 18 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5I:G060512 Lab ID:5064189008 Collected:06/05/12 16:43 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 15:54 67-64-1100 Acrolein ND ug/L 1 06/12/12 15:54 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 15:54 107-13-1100 Benzene ND ug/L 1 06/12/12 15:54 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 15:54 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 15:54 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 15:54 75-27-45.0 Bromoform ND ug/L 1 06/12/12 15:54 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 15:54 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 15:54 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 15:54 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 15:54 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 15:54 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 15:54 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 15:54 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 15:54 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 15:54 75-00-35.0 Chloroform ND ug/L 1 06/12/12 15:54 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 15:54 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 15:54 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 15:54 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 15:54 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 15:54 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 15:54 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 15:54 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 15:54 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 15:54 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 15:54 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 15:54 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 15:54 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 15:54 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 15:54 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 15:54 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 15:54 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 15:54 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 15:54 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 15:54 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 15:54 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 15:54 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 15:54 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 15:54 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 15:54 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 15:54 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 15:54 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 15:54 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 15:54 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 15:54 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 19 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5I:G060512 Lab ID:5064189008 Collected:06/05/12 16:43 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 15:54 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 15:54 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 15:54 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 15:54 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 15:54 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 15:54 103-65-15.0 Styrene ND ug/L 1 06/12/12 15:54 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 15:54 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 15:54 79-34-55.0 Tetrachloroethene 123 ug/L 1 06/12/12 15:54 127-18-45.0 Toluene ND ug/L 1 06/12/12 15:54 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 15:54 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 15:54 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 15:54 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 15:54 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 15:54 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 15:54 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 15:54 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 15:54 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 15:54 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 15:54 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 15:54 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 15:54 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/12/12 15:54 1868-53-783-123 4-Bromofluorobenzene (S)97 %.1 06/12/12 15:54 460-00-472-125 Toluene-d8 (S)96 %.1 06/12/12 15:54 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 20 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5D:G060512 Lab ID:5064189009 Collected:06/05/12 16:10 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 16:26 67-64-1100 Acrolein ND ug/L 1 06/12/12 16:26 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 16:26 107-13-1100 Benzene ND ug/L 1 06/12/12 16:26 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 16:26 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 16:26 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 16:26 75-27-45.0 Bromoform ND ug/L 1 06/12/12 16:26 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 16:26 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 16:26 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 16:26 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 16:26 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 16:26 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 16:26 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 16:26 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 16:26 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 16:26 75-00-35.0 Chloroform ND ug/L 1 06/12/12 16:26 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 16:26 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 16:26 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 16:26 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 16:26 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 16:26 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 16:26 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 16:26 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 16:26 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 16:26 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 16:26 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 16:26 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 16:26 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 16:26 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 16:26 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 16:26 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 16:26 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 16:26 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 16:26 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 16:26 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 16:26 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 16:26 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 16:26 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 16:26 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 16:26 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 16:26 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 16:26 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 16:26 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 16:26 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 16:26 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 21 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW5D:G060512 Lab ID:5064189009 Collected:06/05/12 16:10 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 16:26 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 16:26 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 16:26 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 16:26 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 16:26 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 16:26 103-65-15.0 Styrene ND ug/L 1 06/12/12 16:26 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 16:26 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 16:26 79-34-55.0 Tetrachloroethene 73.9 ug/L 1 06/12/12 16:26 127-18-45.0 Toluene ND ug/L 1 06/12/12 16:26 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 16:26 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 16:26 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 16:26 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 16:26 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 16:26 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 16:26 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 16:26 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 16:26 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 16:26 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 16:26 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 16:26 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 16:26 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/12/12 16:26 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/12/12 16:26 460-00-472-125 Toluene-d8 (S)100 %.1 06/12/12 16:26 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 22 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6I:G060512A Lab ID:5064189010 Collected:06/05/12 10:20 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 16:58 67-64-1100 Acrolein ND ug/L 1 06/12/12 16:58 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 16:58 107-13-1100 Benzene ND ug/L 1 06/12/12 16:58 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 16:58 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 16:58 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 16:58 75-27-45.0 Bromoform ND ug/L 1 06/12/12 16:58 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 16:58 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 16:58 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 16:58 104-51-85.0 sec-Butylbenzene 7.4 ug/L 1 06/12/12 16:58 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 16:58 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 16:58 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 16:58 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 16:58 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 16:58 75-00-35.0 Chloroform ND ug/L 1 06/12/12 16:58 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 16:58 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 16:58 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 16:58 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 16:58 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 16:58 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 16:58 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 16:58 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 16:58 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 16:58 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 16:58 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 16:58 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 16:58 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 16:58 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 16:58 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 16:58 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 16:58 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 16:58 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 16:58 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 16:58 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 16:58 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 16:58 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 16:58 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 16:58 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 16:58 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 16:58 87-68-35.0 n-Hexane 17.7 ug/L 1 06/12/12 16:58 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 16:58 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 16:58 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 16:58 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 23 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW6I:G060512A Lab ID:5064189010 Collected:06/05/12 10:20 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 16:58 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 16:58 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 16:58 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 16:58 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 16:58 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 16:58 103-65-15.0 Styrene ND ug/L 1 06/12/12 16:58 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 16:58 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 16:58 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 16:58 127-18-45.0 Toluene ND ug/L 1 06/12/12 16:58 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 16:58 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 16:58 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 16:58 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 16:58 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 16:58 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 16:58 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 16:58 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 16:58 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 16:58 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 16:58 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 16:58 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 16:58 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/12/12 16:58 1868-53-783-123 4-Bromofluorobenzene (S)104 %.1 06/12/12 16:58 460-00-472-125 Toluene-d8 (S)103 %.1 06/12/12 16:58 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 24 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB1:W060512 Lab ID:5064189011 Collected:06/05/12 14:50 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 17:30 67-64-1100 Acrolein ND ug/L 1 06/12/12 17:30 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 17:30 107-13-1100 Benzene ND ug/L 1 06/12/12 17:30 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 17:30 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 17:30 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 17:30 75-27-45.0 Bromoform ND ug/L 1 06/12/12 17:30 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 17:30 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 17:30 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 17:30 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 17:30 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 17:30 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 17:30 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 17:30 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 17:30 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 17:30 75-00-35.0 Chloroform ND ug/L 1 06/12/12 17:30 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 17:30 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 17:30 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 17:30 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 17:30 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 17:30 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 17:30 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 17:30 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 17:30 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 17:30 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 17:30 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 17:30 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 17:30 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 17:30 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 17:30 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 17:30 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 17:30 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 17:30 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 17:30 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 17:30 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 17:30 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 17:30 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 17:30 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 17:30 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 17:30 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 17:30 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 17:30 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 17:30 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 17:30 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 17:30 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 25 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB1:W060512 Lab ID:5064189011 Collected:06/05/12 14:50 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 17:30 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 17:30 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 17:30 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 17:30 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 17:30 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 17:30 103-65-15.0 Styrene ND ug/L 1 06/12/12 17:30 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 17:30 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 17:30 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 17:30 127-18-45.0 Toluene ND ug/L 1 06/12/12 17:30 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 17:30 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 17:30 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 17:30 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 17:30 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 17:30 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 17:30 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 17:30 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 17:30 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 17:30 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 17:30 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 17:30 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 17:30 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 17:30 1868-53-783-123 4-Bromofluorobenzene (S)96 %.1 06/12/12 17:30 460-00-472-125 Toluene-d8 (S)99 %.1 06/12/12 17:30 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 26 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB2:W060612 Lab ID:5064189012 Collected:06/06/12 18:00 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 18:02 67-64-1100 Acrolein ND ug/L 1 06/12/12 18:02 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 18:02 107-13-1100 Benzene ND ug/L 1 06/12/12 18:02 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 18:02 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 18:02 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 18:02 75-27-45.0 Bromoform ND ug/L 1 06/12/12 18:02 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 18:02 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 18:02 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 18:02 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 18:02 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 18:02 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 18:02 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 18:02 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 18:02 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 18:02 75-00-35.0 Chloroform ND ug/L 1 06/12/12 18:02 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 18:02 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 18:02 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 18:02 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 18:02 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 18:02 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 18:02 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 18:02 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 18:02 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 18:02 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 18:02 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 18:02 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 18:02 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 18:02 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 18:02 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 18:02 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 18:02 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 18:02 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 18:02 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 18:02 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 18:02 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 18:02 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 18:02 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 18:02 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 18:02 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 18:02 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 18:02 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 18:02 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 18:02 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 18:02 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 27 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB2:W060612 Lab ID:5064189012 Collected:06/06/12 18:00 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 18:02 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 18:02 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 18:02 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 18:02 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 18:02 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 18:02 103-65-15.0 Styrene ND ug/L 1 06/12/12 18:02 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 18:02 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 18:02 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 18:02 127-18-45.0 Toluene ND ug/L 1 06/12/12 18:02 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 18:02 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 18:02 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 18:02 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 18:02 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 18:02 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 18:02 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 18:02 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 18:02 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 18:02 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 18:02 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 18:02 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 18:02 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 06/12/12 18:02 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/12/12 18:02 460-00-472-125 Toluene-d8 (S)102 %.1 06/12/12 18:02 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 28 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4D:G060612 Lab ID:5064189013 Collected:06/06/12 12:03 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 18:34 67-64-1100 Acrolein ND ug/L 1 06/12/12 18:34 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 18:34 107-13-1100 Benzene ND ug/L 1 06/12/12 18:34 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 18:34 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 18:34 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 18:34 75-27-45.0 Bromoform ND ug/L 1 06/12/12 18:34 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 18:34 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 18:34 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 18:34 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 18:34 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 18:34 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 18:34 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 18:34 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 18:34 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 18:34 75-00-35.0 Chloroform ND ug/L 1 06/12/12 18:34 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 18:34 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 18:34 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 18:34 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 18:34 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 18:34 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 18:34 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 18:34 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 18:34 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 18:34 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 18:34 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 18:34 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 18:34 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 18:34 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 18:34 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 18:34 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 18:34 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 18:34 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 18:34 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 18:34 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 18:34 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 18:34 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 18:34 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 18:34 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 18:34 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 18:34 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 18:34 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 18:34 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 18:34 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 18:34 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 29 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4D:G060612 Lab ID:5064189013 Collected:06/06/12 12:03 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 18:34 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 18:34 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 18:34 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 18:34 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 18:34 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 18:34 103-65-15.0 Styrene ND ug/L 1 06/12/12 18:34 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 18:34 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 18:34 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 18:34 127-18-45.0 Toluene ND ug/L 1 06/12/12 18:34 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 18:34 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 18:34 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 18:34 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 18:34 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 18:34 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 18:34 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 18:34 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 18:34 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 18:34 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 18:34 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 18:34 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 18:34 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 18:34 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/12/12 18:34 460-00-472-125 Toluene-d8 (S)101 %.1 06/12/12 18:34 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 30 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4I:G060612 Lab ID:5064189014 Collected:06/06/12 12:30 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 19:05 67-64-1100 Acrolein ND ug/L 1 06/12/12 19:05 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 19:05 107-13-1100 Benzene ND ug/L 1 06/12/12 19:05 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 19:05 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 19:05 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 19:05 75-27-45.0 Bromoform ND ug/L 1 06/12/12 19:05 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 19:05 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 19:05 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 19:05 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 19:05 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 19:05 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 19:05 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 19:05 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 19:05 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 19:05 75-00-35.0 Chloroform ND ug/L 1 06/12/12 19:05 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 19:05 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 19:05 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 19:05 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 19:05 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 19:05 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 19:05 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 19:05 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 19:05 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 19:05 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 19:05 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 19:05 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 19:05 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 19:05 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 19:05 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 19:05 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 19:05 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 19:05 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 19:05 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 19:05 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 19:05 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 19:05 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 19:05 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 19:05 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 19:05 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 19:05 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 19:05 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 19:05 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 19:05 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 19:05 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 31 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4I:G060612 Lab ID:5064189014 Collected:06/06/12 12:30 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 19:05 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 19:05 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 19:05 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 19:05 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 19:05 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 19:05 103-65-15.0 Styrene ND ug/L 1 06/12/12 19:05 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 19:05 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 19:05 79-34-55.0 Tetrachloroethene ND ug/L 1 06/12/12 19:05 127-18-45.0 Toluene ND ug/L 1 06/12/12 19:05 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 19:05 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 19:05 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 19:05 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 19:05 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 19:05 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 19:05 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 19:05 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 19:05 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 19:05 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 19:05 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 19:05 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 19:05 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 06/12/12 19:05 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/12/12 19:05 460-00-472-125 Toluene-d8 (S)100 %.1 06/12/12 19:05 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 32 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4S:G060612 Lab ID:5064189015 Collected:06/06/12 13:10 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 00:57 67-64-1100 Acrolein ND ug/L 1 06/13/12 00:57 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 00:57 107-13-1100 Benzene ND ug/L 1 06/13/12 00:57 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 00:57 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 00:57 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 00:57 75-27-45.0 Bromoform ND ug/L 1 06/13/12 00:57 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 00:57 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 00:57 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 00:57 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 00:57 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 00:57 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 00:57 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 00:57 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 00:57 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 00:57 75-00-35.0 Chloroform ND ug/L 1 06/13/12 00:57 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 00:57 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 00:57 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 00:57 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 00:57 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 00:57 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 00:57 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 00:57 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 00:57 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 00:57 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 00:57 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 00:57 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 00:57 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 00:57 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 00:57 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 00:57 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 00:57 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 00:57 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 00:57 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 00:57 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 00:57 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 00:57 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 00:57 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 00:57 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 00:57 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 00:57 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 00:57 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 00:57 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 00:57 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 00:57 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 33 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW4S:G060612 Lab ID:5064189015 Collected:06/06/12 13:10 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 00:57 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 00:57 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 00:57 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 00:57 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 00:57 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 00:57 103-65-15.0 Styrene ND ug/L 1 06/13/12 00:57 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 00:57 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 00:57 79-34-55.0 Tetrachloroethene ND ug/L 1 06/13/12 00:57 127-18-45.0 Toluene ND ug/L 1 06/13/12 00:57 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 00:57 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 00:57 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 00:57 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 00:57 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 00:57 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 00:57 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 00:57 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 00:57 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 00:57 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 00:57 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 00:57 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 00:57 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 00:57 1868-53-783-123 4-Bromofluorobenzene (S)97 %.1 06/13/12 00:57 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 00:57 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 34 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1D:G060612 Lab ID:5064189016 Collected:06/06/12 14:01 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/12/12 20:09 67-64-1100 Acrolein ND ug/L 1 06/12/12 20:09 107-02-8100 Acrylonitrile ND ug/L 1 06/12/12 20:09 107-13-1100 Benzene ND ug/L 1 06/12/12 20:09 71-43-25.0 Bromobenzene ND ug/L 1 06/12/12 20:09 108-86-15.0 Bromochloromethane ND ug/L 1 06/12/12 20:09 74-97-55.0 Bromodichloromethane ND ug/L 1 06/12/12 20:09 75-27-45.0 Bromoform ND ug/L 1 06/12/12 20:09 75-25-25.0 Bromomethane ND ug/L 1 06/12/12 20:09 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/12/12 20:09 78-93-325.0 n-Butylbenzene ND ug/L 1 06/12/12 20:09 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/12/12 20:09 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/12/12 20:09 98-06-65.0 Carbon disulfide ND ug/L 1 06/12/12 20:09 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/12/12 20:09 56-23-55.0 Chlorobenzene ND ug/L 1 06/12/12 20:09 108-90-75.0 Chloroethane ND ug/L 1 06/12/12 20:09 75-00-35.0 Chloroform ND ug/L 1 06/12/12 20:09 67-66-35.0 Chloromethane ND ug/L 1 06/12/12 20:09 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/12/12 20:09 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/12/12 20:09 106-43-45.0 Dibromochloromethane ND ug/L 1 06/12/12 20:09 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/12/12 20:09 106-93-45.0 Dibromomethane ND ug/L 1 06/12/12 20:09 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/12/12 20:09 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/12/12 20:09 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/12/12 20:09 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/12/12 20:09 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/12/12 20:09 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/12/12 20:09 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/12/12 20:09 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/12/12 20:09 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/12/12 20:09 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/12/12 20:09 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/12/12 20:09 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/12/12 20:09 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/12/12 20:09 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/12/12 20:09 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/12/12 20:09 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/12/12 20:09 10061-02-65.0 Ethylbenzene ND ug/L 1 06/12/12 20:09 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/12/12 20:09 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/12/12 20:09 87-68-35.0 n-Hexane ND ug/L 1 06/12/12 20:09 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/12/12 20:09 591-78-625.0 Iodomethane ND ug/L 1 06/12/12 20:09 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/12/12 20:09 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 35 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1D:G060612 Lab ID:5064189016 Collected:06/06/12 14:01 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/12/12 20:09 99-87-65.0 Methylene Chloride ND ug/L 1 06/12/12 20:09 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/12/12 20:09 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/12/12 20:09 1634-04-44.0 Naphthalene ND ug/L 1 06/12/12 20:09 91-20-35.0 n-Propylbenzene ND ug/L 1 06/12/12 20:09 103-65-15.0 Styrene ND ug/L 1 06/12/12 20:09 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/12/12 20:09 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/12/12 20:09 79-34-55.0 Tetrachloroethene 179 ug/L 1 06/12/12 20:09 127-18-45.0 Toluene ND ug/L 1 06/12/12 20:09 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/12/12 20:09 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/12/12 20:09 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/12/12 20:09 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/12/12 20:09 79-00-55.0 Trichloroethene ND ug/L 1 06/12/12 20:09 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/12/12 20:09 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/12/12 20:09 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/12/12 20:09 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/12/12 20:09 108-67-85.0 Vinyl acetate ND ug/L 1 06/12/12 20:09 108-05-450.0 Vinyl chloride ND ug/L 1 06/12/12 20:09 75-01-42.0 Xylene (Total)ND ug/L 1 06/12/12 20:09 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/12/12 20:09 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/12/12 20:09 460-00-472-125 Toluene-d8 (S)102 %.1 06/12/12 20:09 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 36 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1I:G060612 Lab ID:5064189017 Collected:06/06/12 14:43 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 01:29 67-64-1100 Acrolein ND ug/L 1 06/13/12 01:29 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 01:29 107-13-1100 Benzene ND ug/L 1 06/13/12 01:29 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 01:29 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 01:29 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 01:29 75-27-45.0 Bromoform ND ug/L 1 06/13/12 01:29 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 01:29 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 01:29 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 01:29 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 01:29 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 01:29 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 01:29 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 01:29 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 01:29 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 01:29 75-00-35.0 Chloroform ND ug/L 1 06/13/12 01:29 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 01:29 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 01:29 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 01:29 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 01:29 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 01:29 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 01:29 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 01:29 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 01:29 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 01:29 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 01:29 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 01:29 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 01:29 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 01:29 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 01:29 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 01:29 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 01:29 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 01:29 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 01:29 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 01:29 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 01:29 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 01:29 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 01:29 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 01:29 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 01:29 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 01:29 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 01:29 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 01:29 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 01:29 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 01:29 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 37 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1I:G060612 Lab ID:5064189017 Collected:06/06/12 14:43 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 01:29 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 01:29 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 01:29 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 01:29 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 01:29 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 01:29 103-65-15.0 Styrene ND ug/L 1 06/13/12 01:29 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 01:29 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 01:29 79-34-55.0 Tetrachloroethene 1540 ug/L 10 06/14/12 18:06 127-18-450.0 Toluene ND ug/L 1 06/13/12 01:29 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 01:29 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 01:29 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 01:29 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 01:29 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 01:29 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 01:29 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 01:29 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 01:29 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 01:29 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 01:29 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 01:29 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 01:29 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 01:29 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/13/12 01:29 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 01:29 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 38 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1S:G060612 Lab ID:5064189018 Collected:06/06/12 15:28 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 02:01 67-64-1100 Acrolein ND ug/L 1 06/13/12 02:01 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 02:01 107-13-1100 Benzene ND ug/L 1 06/13/12 02:01 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 02:01 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 02:01 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 02:01 75-27-45.0 Bromoform ND ug/L 1 06/13/12 02:01 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 02:01 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 02:01 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 02:01 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 02:01 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 02:01 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 02:01 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 02:01 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 02:01 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 02:01 75-00-35.0 Chloroform ND ug/L 1 06/13/12 02:01 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 02:01 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 02:01 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 02:01 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 02:01 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 02:01 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 02:01 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 02:01 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 02:01 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 02:01 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 02:01 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 02:01 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 02:01 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 02:01 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 02:01 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 02:01 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 02:01 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 02:01 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 02:01 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 02:01 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 02:01 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 02:01 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 02:01 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 02:01 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 02:01 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 02:01 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 02:01 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 02:01 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 02:01 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 02:01 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 39 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1S:G060612 Lab ID:5064189018 Collected:06/06/12 15:28 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 02:01 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 02:01 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 02:01 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 02:01 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 02:01 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 02:01 103-65-15.0 Styrene ND ug/L 1 06/13/12 02:01 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 02:01 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 02:01 79-34-55.0 Tetrachloroethene 1080 ug/L 10 06/14/12 18:38 127-18-450.0 Toluene ND ug/L 1 06/13/12 02:01 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 02:01 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 02:01 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 02:01 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 02:01 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 02:01 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 02:01 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 02:01 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 02:01 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 02:01 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 02:01 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 02:01 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 02:01 1330-20-710.0 Surrogates Dibromofluoromethane (S)99 %.1 06/13/12 02:01 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/13/12 02:01 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 02:01 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 40 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3D:G060612 Lab ID:5064189019 Collected:06/06/12 15:54 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 02:33 67-64-1100 Acrolein ND ug/L 1 06/13/12 02:33 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 02:33 107-13-1100 Benzene ND ug/L 1 06/13/12 02:33 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 02:33 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 02:33 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 02:33 75-27-45.0 Bromoform ND ug/L 1 06/13/12 02:33 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 02:33 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 02:33 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 02:33 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 02:33 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 02:33 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 02:33 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 02:33 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 02:33 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 02:33 75-00-35.0 Chloroform ND ug/L 1 06/13/12 02:33 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 02:33 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 02:33 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 02:33 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 02:33 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 02:33 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 02:33 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 02:33 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 02:33 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 02:33 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 02:33 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 02:33 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 02:33 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 02:33 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 02:33 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 02:33 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 02:33 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 02:33 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 02:33 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 02:33 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 02:33 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 02:33 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 02:33 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 02:33 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 02:33 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 02:33 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 02:33 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 02:33 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 02:33 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 02:33 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 41 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3D:G060612 Lab ID:5064189019 Collected:06/06/12 15:54 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 02:33 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 02:33 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 02:33 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 02:33 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 02:33 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 02:33 103-65-15.0 Styrene ND ug/L 1 06/13/12 02:33 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 02:33 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 02:33 79-34-55.0 Tetrachloroethene 31.3 ug/L 1 06/13/12 02:33 127-18-45.0 Toluene ND ug/L 1 06/13/12 02:33 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 02:33 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 02:33 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 02:33 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 02:33 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 02:33 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 02:33 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 02:33 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 02:33 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 02:33 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 02:33 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 02:33 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 02:33 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 02:33 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/13/12 02:33 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 02:33 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 42 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3I:G060612 Lab ID:5064189020 Collected:06/06/12 16:47 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 03:05 67-64-1100 Acrolein ND ug/L 1 06/13/12 03:05 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 03:05 107-13-1100 Benzene ND ug/L 1 06/13/12 03:05 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 03:05 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 03:05 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 03:05 75-27-45.0 Bromoform ND ug/L 1 06/13/12 03:05 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 03:05 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 03:05 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 03:05 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 03:05 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 03:05 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 03:05 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 03:05 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 03:05 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 03:05 75-00-35.0 Chloroform ND ug/L 1 06/13/12 03:05 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 03:05 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 03:05 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 03:05 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 03:05 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 03:05 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 03:05 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 03:05 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 03:05 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 03:05 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 03:05 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 03:05 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 03:05 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 03:05 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 03:05 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 03:05 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 03:05 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 03:05 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 03:05 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 03:05 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 03:05 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 03:05 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 03:05 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 03:05 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 03:05 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 03:05 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 03:05 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 03:05 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 03:05 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 03:05 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 43 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3I:G060612 Lab ID:5064189020 Collected:06/06/12 16:47 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 03:05 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 03:05 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 03:05 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 03:05 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 03:05 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 03:05 103-65-15.0 Styrene ND ug/L 1 06/13/12 03:05 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 03:05 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 03:05 79-34-55.0 Tetrachloroethene 43.0 ug/L 1 06/13/12 03:05 127-18-45.0 Toluene ND ug/L 1 06/13/12 03:05 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 03:05 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 03:05 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 03:05 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 03:05 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 03:05 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 03:05 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 03:05 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 03:05 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 03:05 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 03:05 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 03:05 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 03:05 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/13/12 03:05 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/13/12 03:05 460-00-472-125 Toluene-d8 (S)101 %.1 06/13/12 03:05 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 44 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3S:G060612 Lab ID:5064189021 Collected:06/06/12 17:53 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 03:37 67-64-1100 Acrolein ND ug/L 1 06/13/12 03:37 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 03:37 107-13-1100 Benzene ND ug/L 1 06/13/12 03:37 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 03:37 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 03:37 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 03:37 75-27-45.0 Bromoform ND ug/L 1 06/13/12 03:37 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 03:37 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 03:37 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 03:37 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 03:37 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 03:37 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 03:37 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 03:37 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 03:37 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 03:37 75-00-35.0 Chloroform ND ug/L 1 06/13/12 03:37 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 03:37 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 03:37 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 03:37 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 03:37 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 03:37 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 03:37 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 03:37 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 03:37 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 03:37 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 03:37 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 03:37 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 03:37 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 03:37 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 03:37 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 03:37 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 03:37 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 03:37 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 03:37 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 03:37 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 03:37 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 03:37 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 03:37 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 03:37 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 03:37 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 03:37 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 03:37 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 03:37 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 03:37 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 03:37 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 45 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW3S:G060612 Lab ID:5064189021 Collected:06/06/12 17:53 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 03:37 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 03:37 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 03:37 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 03:37 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 03:37 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 03:37 103-65-15.0 Styrene ND ug/L 1 06/13/12 03:37 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 03:37 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 03:37 79-34-55.0 Tetrachloroethene ND ug/L 1 06/13/12 03:37 127-18-45.0 Toluene ND ug/L 1 06/13/12 03:37 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 03:37 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 03:37 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 03:37 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 03:37 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 03:37 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 03:37 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 03:37 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 03:37 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 03:37 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 03:37 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 03:37 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 03:37 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/13/12 03:37 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/13/12 03:37 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 03:37 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 46 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2D:G060712 Lab ID:5064189022 Collected:06/07/12 09:18 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 07:21 67-64-1100 Acrolein ND ug/L 1 06/13/12 07:21 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 07:21 107-13-1100 Benzene ND ug/L 1 06/13/12 07:21 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 07:21 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 07:21 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 07:21 75-27-45.0 Bromoform ND ug/L 1 06/13/12 07:21 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 07:21 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 07:21 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 07:21 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 07:21 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 07:21 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 07:21 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 07:21 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 07:21 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 07:21 75-00-35.0 Chloroform ND ug/L 1 06/13/12 07:21 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 07:21 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 07:21 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 07:21 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 07:21 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 07:21 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 07:21 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 07:21 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 07:21 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 07:21 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 07:21 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 07:21 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 07:21 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 07:21 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 07:21 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 07:21 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 07:21 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 07:21 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 07:21 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 07:21 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 07:21 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 07:21 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 07:21 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 07:21 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 07:21 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 07:21 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 07:21 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 07:21 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 07:21 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 07:21 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 47 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2D:G060712 Lab ID:5064189022 Collected:06/07/12 09:18 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 07:21 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 07:21 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 07:21 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 07:21 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 07:21 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 07:21 103-65-15.0 Styrene ND ug/L 1 06/13/12 07:21 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 07:21 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 07:21 79-34-55.0 Tetrachloroethene 851 ug/L 10 06/14/12 19:10 127-18-450.0 Toluene ND ug/L 1 06/13/12 07:21 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 07:21 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 07:21 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 07:21 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 07:21 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 07:21 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 07:21 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 07:21 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 07:21 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 07:21 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 07:21 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 07:21 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 07:21 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 07:21 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/13/12 07:21 460-00-472-125 Toluene-d8 (S)101 %.1 06/13/12 07:21 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 48 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2I:G060712 Lab ID:5064189023 Collected:06/07/12 10:12 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 04:09 67-64-1100 Acrolein ND ug/L 1 06/13/12 04:09 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 04:09 107-13-1100 Benzene ND ug/L 1 06/13/12 04:09 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 04:09 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 04:09 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 04:09 75-27-45.0 Bromoform ND ug/L 1 06/13/12 04:09 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 04:09 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 04:09 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 04:09 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 04:09 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 04:09 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 04:09 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 04:09 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 04:09 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 04:09 75-00-35.0 Chloroform ND ug/L 1 06/13/12 04:09 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 04:09 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 04:09 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 04:09 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 04:09 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 04:09 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 04:09 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 04:09 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 04:09 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 04:09 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 04:09 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 04:09 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 04:09 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 04:09 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 04:09 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 04:09 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 04:09 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 04:09 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 04:09 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 04:09 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 04:09 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 04:09 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 04:09 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 04:09 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 04:09 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 04:09 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 04:09 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 04:09 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 04:09 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 04:09 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 49 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2I:G060712 Lab ID:5064189023 Collected:06/07/12 10:12 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 04:09 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 04:09 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 04:09 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 04:09 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 04:09 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 04:09 103-65-15.0 Styrene ND ug/L 1 06/13/12 04:09 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 04:09 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 04:09 79-34-55.0 Tetrachloroethene 596 ug/L 10 06/14/12 19:42 127-18-450.0 Toluene ND ug/L 1 06/13/12 04:09 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 04:09 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 04:09 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 04:09 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 04:09 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 04:09 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 04:09 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 04:09 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 04:09 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 04:09 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 04:09 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 04:09 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 04:09 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 04:09 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/13/12 04:09 460-00-472-125 Toluene-d8 (S)101 %.1 06/13/12 04:09 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 50 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2S:G060712 Lab ID:5064189024 Collected:06/07/12 10:32 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 04:41 67-64-1100 Acrolein ND ug/L 1 06/13/12 04:41 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 04:41 107-13-1100 Benzene ND ug/L 1 06/13/12 04:41 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 04:41 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 04:41 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 04:41 75-27-45.0 Bromoform ND ug/L 1 06/13/12 04:41 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 04:41 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 04:41 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 04:41 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 04:41 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 04:41 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 04:41 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 04:41 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 04:41 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 04:41 75-00-35.0 Chloroform ND ug/L 1 06/13/12 04:41 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 04:41 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 04:41 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 04:41 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 04:41 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 04:41 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 04:41 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 04:41 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 04:41 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 04:41 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 04:41 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 04:41 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 04:41 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 04:41 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 04:41 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 04:41 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 04:41 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 04:41 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 04:41 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 04:41 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 04:41 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 04:41 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 04:41 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 04:41 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 04:41 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 04:41 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 04:41 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 04:41 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 04:41 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 04:41 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 51 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2S:G060712 Lab ID:5064189024 Collected:06/07/12 10:32 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 04:41 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 04:41 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 04:41 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 04:41 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 04:41 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 04:41 103-65-15.0 Styrene ND ug/L 1 06/13/12 04:41 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 04:41 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 04:41 79-34-55.0 Tetrachloroethene 499 ug/L 10 06/14/12 20:14 127-18-450.0 Toluene ND ug/L 1 06/13/12 04:41 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 04:41 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 04:41 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 04:41 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 04:41 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 04:41 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 04:41 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 04:41 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 04:41 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 04:41 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 04:41 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 04:41 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 04:41 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/13/12 04:41 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 06/13/12 04:41 460-00-472-125 Toluene-d8 (S)98 %.1 06/13/12 04:41 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 52 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB3:W060712 Lab ID:5064189025 Collected:06/07/12 10:50 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 05:13 67-64-1100 Acrolein ND ug/L 1 06/13/12 05:13 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 05:13 107-13-1100 Benzene ND ug/L 1 06/13/12 05:13 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 05:13 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 05:13 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 05:13 75-27-45.0 Bromoform ND ug/L 1 06/13/12 05:13 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 05:13 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 05:13 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 05:13 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 05:13 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 05:13 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 05:13 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 05:13 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 05:13 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 05:13 75-00-35.0 Chloroform ND ug/L 1 06/13/12 05:13 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 05:13 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 05:13 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 05:13 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 05:13 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 05:13 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 05:13 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 05:13 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 05:13 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 05:13 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 05:13 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 05:13 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 05:13 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 05:13 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 05:13 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 05:13 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 05:13 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 05:13 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 05:13 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 05:13 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 05:13 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 05:13 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 05:13 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 05:13 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 05:13 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 05:13 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 05:13 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 05:13 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 05:13 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 05:13 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 53 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:EB3:W060712 Lab ID:5064189025 Collected:06/07/12 10:50 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 05:13 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 05:13 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 05:13 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 05:13 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 05:13 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 05:13 103-65-15.0 Styrene ND ug/L 1 06/13/12 05:13 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 05:13 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 05:13 79-34-55.0 Tetrachloroethene ND ug/L 1 06/13/12 05:13 127-18-45.0 Toluene ND ug/L 1 06/13/12 05:13 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 05:13 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 05:13 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 05:13 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 05:13 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 05:13 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 05:13 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 05:13 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 05:13 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 05:13 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 05:13 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 05:13 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 05:13 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 06/13/12 05:13 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 06/13/12 05:13 460-00-472-125 Toluene-d8 (S)101 %.1 06/13/12 05:13 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 54 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1I:G060612A Lab ID:5064189026 Collected:06/06/12 14:45 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 05:45 67-64-1100 Acrolein ND ug/L 1 06/13/12 05:45 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 05:45 107-13-1100 Benzene ND ug/L 1 06/13/12 05:45 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 05:45 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 05:45 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 05:45 75-27-45.0 Bromoform ND ug/L 1 06/13/12 05:45 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 05:45 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 05:45 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 05:45 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 05:45 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 05:45 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 05:45 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 05:45 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 05:45 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 05:45 75-00-35.0 Chloroform ND ug/L 1 06/13/12 05:45 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 05:45 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 05:45 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 05:45 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 05:45 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 05:45 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 05:45 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 05:45 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 05:45 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 05:45 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 05:45 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 05:45 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 05:45 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 05:45 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 05:45 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 05:45 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 05:45 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 05:45 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 05:45 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 05:45 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 05:45 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 05:45 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 05:45 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 05:45 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 05:45 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 05:45 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 05:45 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 05:45 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 05:45 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 05:45 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 55 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW1I:G060612A Lab ID:5064189026 Collected:06/06/12 14:45 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 05:45 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 05:45 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 05:45 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 05:45 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 05:45 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 05:45 103-65-15.0 Styrene ND ug/L 1 06/13/12 05:45 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 05:45 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 05:45 79-34-55.0 Tetrachloroethene 1540 ug/L 10 06/14/12 20:46 127-18-450.0 Toluene ND ug/L 1 06/13/12 05:45 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 05:45 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 05:45 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 05:45 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 05:45 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 05:45 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 05:45 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 05:45 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 05:45 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 05:45 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 05:45 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 05:45 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 05:45 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/13/12 05:45 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 06/13/12 05:45 460-00-472-125 Toluene-d8 (S)101 %.1 06/13/12 05:45 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 56 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2I:G060712A Lab ID:5064189027 Collected:06/07/12 10:12 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 06:17 67-64-1100 Acrolein ND ug/L 1 06/13/12 06:17 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 06:17 107-13-1100 Benzene ND ug/L 1 06/13/12 06:17 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 06:17 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 06:17 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 06:17 75-27-45.0 Bromoform ND ug/L 1 06/13/12 06:17 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 06:17 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 06:17 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 06:17 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 06:17 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 06:17 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 06:17 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 06:17 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 06:17 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 06:17 75-00-35.0 Chloroform ND ug/L 1 06/13/12 06:17 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 06:17 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 06:17 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 06:17 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 06:17 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 06:17 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 06:17 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 06:17 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 06:17 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 06:17 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 06:17 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 06:17 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 06:17 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 06:17 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 06:17 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 06:17 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 06:17 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 06:17 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 06:17 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 06:17 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 06:17 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 06:17 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 06:17 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 06:17 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 06:17 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 06:17 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 06:17 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 06:17 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 06:17 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 06:17 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 57 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:AMW2I:G060712A Lab ID:5064189027 Collected:06/07/12 10:12 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 06:17 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 06:17 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 06:17 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 06:17 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 06:17 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 06:17 103-65-15.0 Styrene ND ug/L 1 06/13/12 06:17 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 06:17 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 06:17 79-34-55.0 Tetrachloroethene 581 ug/L 10 06/14/12 21:18 127-18-450.0 Toluene ND ug/L 1 06/13/12 06:17 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 06:17 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 06:17 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 06:17 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 06:17 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 06:17 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 06:17 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 06:17 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 06:17 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 06:17 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 06:17 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 06:17 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 06:17 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 06/13/12 06:17 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 06/13/12 06:17 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 06:17 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 58 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:LTB:W060512 Lab ID:5064189028 Collected:06/05/12 08:00 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 06/13/12 06:49 67-64-1100 Acrolein ND ug/L 1 06/13/12 06:49 107-02-8100 Acrylonitrile ND ug/L 1 06/13/12 06:49 107-13-1100 Benzene ND ug/L 1 06/13/12 06:49 71-43-25.0 Bromobenzene ND ug/L 1 06/13/12 06:49 108-86-15.0 Bromochloromethane ND ug/L 1 06/13/12 06:49 74-97-55.0 Bromodichloromethane ND ug/L 1 06/13/12 06:49 75-27-45.0 Bromoform ND ug/L 1 06/13/12 06:49 75-25-25.0 Bromomethane ND ug/L 1 06/13/12 06:49 74-83-95.0 2-Butanone (MEK)ND ug/L 1 06/13/12 06:49 78-93-325.0 n-Butylbenzene ND ug/L 1 06/13/12 06:49 104-51-85.0 sec-Butylbenzene ND ug/L 1 06/13/12 06:49 135-98-85.0 tert-Butylbenzene ND ug/L 1 06/13/12 06:49 98-06-65.0 Carbon disulfide ND ug/L 1 06/13/12 06:49 75-15-010.0 Carbon tetrachloride ND ug/L 1 06/13/12 06:49 56-23-55.0 Chlorobenzene ND ug/L 1 06/13/12 06:49 108-90-75.0 Chloroethane ND ug/L 1 06/13/12 06:49 75-00-35.0 Chloroform ND ug/L 1 06/13/12 06:49 67-66-35.0 Chloromethane ND ug/L 1 06/13/12 06:49 74-87-35.0 2-Chlorotoluene ND ug/L 1 06/13/12 06:49 95-49-85.0 4-Chlorotoluene ND ug/L 1 06/13/12 06:49 106-43-45.0 Dibromochloromethane ND ug/L 1 06/13/12 06:49 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 06/13/12 06:49 106-93-45.0 Dibromomethane ND ug/L 1 06/13/12 06:49 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 06/13/12 06:49 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 06/13/12 06:49 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 06/13/12 06:49 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 06/13/12 06:49 110-57-6100 Dichlorodifluoromethane ND ug/L 1 06/13/12 06:49 75-71-85.0 1,1-Dichloroethane ND ug/L 1 06/13/12 06:49 75-34-35.0 1,2-Dichloroethane ND ug/L 1 06/13/12 06:49 107-06-25.0 1,1-Dichloroethene ND ug/L 1 06/13/12 06:49 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 06/13/12 06:49 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 06/13/12 06:49 156-60-55.0 1,2-Dichloropropane ND ug/L 1 06/13/12 06:49 78-87-55.0 1,3-Dichloropropane ND ug/L 1 06/13/12 06:49 142-28-95.0 2,2-Dichloropropane ND ug/L 1 06/13/12 06:49 594-20-75.0 1,1-Dichloropropene ND ug/L 1 06/13/12 06:49 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 06/13/12 06:49 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 06/13/12 06:49 10061-02-65.0 Ethylbenzene ND ug/L 1 06/13/12 06:49 100-41-45.0 Ethyl methacrylate ND ug/L 1 06/13/12 06:49 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 06/13/12 06:49 87-68-35.0 n-Hexane ND ug/L 1 06/13/12 06:49 110-54-3 N25.0 2-Hexanone ND ug/L 1 06/13/12 06:49 591-78-625.0 Iodomethane ND ug/L 1 06/13/12 06:49 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 06/13/12 06:49 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 59 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5064189 SBI068 Sample:SBI068:LTB:W060512 Lab ID:5064189028 Collected:06/05/12 08:00 Received:06/08/12 11:47 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 06/13/12 06:49 99-87-65.0 Methylene Chloride ND ug/L 1 06/13/12 06:49 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 06/13/12 06:49 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 06/13/12 06:49 1634-04-44.0 Naphthalene ND ug/L 1 06/13/12 06:49 91-20-35.0 n-Propylbenzene ND ug/L 1 06/13/12 06:49 103-65-15.0 Styrene ND ug/L 1 06/13/12 06:49 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 06/13/12 06:49 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 06/13/12 06:49 79-34-55.0 Tetrachloroethene ND ug/L 1 06/13/12 06:49 127-18-45.0 Toluene ND ug/L 1 06/13/12 06:49 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 06/13/12 06:49 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 06/13/12 06:49 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 06/13/12 06:49 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 06/13/12 06:49 79-00-55.0 Trichloroethene ND ug/L 1 06/13/12 06:49 79-01-65.0 Trichlorofluoromethane ND ug/L 1 06/13/12 06:49 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 06/13/12 06:49 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 06/13/12 06:49 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 06/13/12 06:49 108-67-85.0 Vinyl acetate ND ug/L 1 06/13/12 06:49 108-05-450.0 Vinyl chloride ND ug/L 1 06/13/12 06:49 75-01-42.0 Xylene (Total)ND ug/L 1 06/13/12 06:49 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 06/13/12 06:49 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 06/13/12 06:49 460-00-472-125 Toluene-d8 (S)100 %.1 06/13/12 06:49 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 60 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42945 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5064189001, 5064189002, 5064189003, 5064189004, 5064189005, 5064189006, 5064189007, 5064189008, 5064189009, 5064189010, 5064189011, 5064189012, 5064189013, 5064189014, 5064189016 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:748908 Associated Lab Samples:5064189001, 5064189002, 5064189003, 5064189004, 5064189005, 5064189006, 5064189007, 5064189008, 5064189009, 5064189010, 5064189011, 5064189012, 5064189013, 5064189014, 5064189016 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/12/12 12:10 1,1,1-Trichloroethane ug/L ND 5.0 06/12/12 12:10 1,1,2,2-Tetrachloroethane ug/L ND 5.0 06/12/12 12:10 1,1,2-Trichloroethane ug/L ND 5.0 06/12/12 12:10 1,1-Dichloroethane ug/L ND 5.0 06/12/12 12:10 1,1-Dichloroethene ug/L ND 5.0 06/12/12 12:10 1,1-Dichloropropene ug/L ND 5.0 06/12/12 12:10 1,2,3-Trichlorobenzene ug/L ND 5.0 06/12/12 12:10 1,2,3-Trichloropropane ug/L ND 5.0 06/12/12 12:10 1,2,4-Trichlorobenzene ug/L ND 5.0 06/12/12 12:10 1,2,4-Trimethylbenzene ug/L ND 5.0 06/12/12 12:10 1,2-Dibromoethane (EDB)ug/L ND 5.0 06/12/12 12:10 1,2-Dichlorobenzene ug/L ND 5.0 06/12/12 12:10 1,2-Dichloroethane ug/L ND 5.0 06/12/12 12:10 1,2-Dichloropropane ug/L ND 5.0 06/12/12 12:10 1,3,5-Trimethylbenzene ug/L ND 5.0 06/12/12 12:10 1,3-Dichlorobenzene ug/L ND 5.0 06/12/12 12:10 1,3-Dichloropropane ug/L ND 5.0 06/12/12 12:10 1,4-Dichlorobenzene ug/L ND 5.0 06/12/12 12:10 2,2-Dichloropropane ug/L ND 5.0 06/12/12 12:10 2-Butanone (MEK)ug/L ND 25.0 06/12/12 12:10 2-Chlorotoluene ug/L ND 5.0 06/12/12 12:10 2-Hexanone ug/L ND 25.0 06/12/12 12:10 4-Chlorotoluene ug/L ND 5.0 06/12/12 12:10 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 06/12/12 12:10 Acetone ug/L ND 100 06/12/12 12:10 Acrolein ug/L ND 100 06/12/12 12:10 Acrylonitrile ug/L ND 100 06/12/12 12:10 Benzene ug/L ND 5.0 06/12/12 12:10 Bromobenzene ug/L ND 5.0 06/12/12 12:10 Bromochloromethane ug/L ND 5.0 06/12/12 12:10 Bromodichloromethane ug/L ND 5.0 06/12/12 12:10 Bromoform ug/L ND 5.0 06/12/12 12:10 Bromomethane ug/L ND 5.0 06/12/12 12:10 Carbon disulfide ug/L ND 10.0 06/12/12 12:10 Carbon tetrachloride ug/L ND 5.0 06/12/12 12:10 Chlorobenzene ug/L ND 5.0 06/12/12 12:10 Chloroethane ug/L ND 5.0 06/12/12 12:10 Chloroform ug/L ND 5.0 06/12/12 12:10 Chloromethane ug/L ND 5.0 06/12/12 12:10 cis-1,2-Dichloroethene ug/L ND 5.0 06/12/12 12:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 61 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:748908 Associated Lab Samples:5064189001, 5064189002, 5064189003, 5064189004, 5064189005, 5064189006, 5064189007, 5064189008, 5064189009, 5064189010, 5064189011, 5064189012, 5064189013, 5064189014, 5064189016 Matrix:Water Analyzed cis-1,3-Dichloropropene ug/L ND 5.0 06/12/12 12:10 Dibromochloromethane ug/L ND 5.0 06/12/12 12:10 Dibromomethane ug/L ND 5.0 06/12/12 12:10 Dichlorodifluoromethane ug/L ND 5.0 06/12/12 12:10 Ethyl methacrylate ug/L ND 100 06/12/12 12:10 Ethylbenzene ug/L ND 5.0 06/12/12 12:10 Hexachloro-1,3-butadiene ug/L ND 5.0 06/12/12 12:10 Iodomethane ug/L ND 10.0 06/12/12 12:10 Isopropylbenzene (Cumene)ug/L ND 5.0 06/12/12 12:10 Methyl-tert-butyl ether ug/L ND 4.0 06/12/12 12:10 Methylene Chloride ug/L ND 5.0 06/12/12 12:10 n-Butylbenzene ug/L ND 5.0 06/12/12 12:10 n-Hexane ug/L ND 5.0 N206/12/12 12:10 n-Propylbenzene ug/L ND 5.0 06/12/12 12:10 Naphthalene ug/L ND 5.0 06/12/12 12:10 p-Isopropyltoluene ug/L ND 5.0 06/12/12 12:10 sec-Butylbenzene ug/L ND 5.0 06/12/12 12:10 Styrene ug/L ND 5.0 06/12/12 12:10 tert-Butylbenzene ug/L ND 5.0 06/12/12 12:10 Tetrachloroethene ug/L ND 5.0 06/12/12 12:10 Toluene ug/L ND 5.0 06/12/12 12:10 trans-1,2-Dichloroethene ug/L ND 5.0 06/12/12 12:10 trans-1,3-Dichloropropene ug/L ND 5.0 06/12/12 12:10 trans-1,4-Dichloro-2-butene ug/L ND 100 06/12/12 12:10 Trichloroethene ug/L ND 5.0 06/12/12 12:10 Trichlorofluoromethane ug/L ND 5.0 06/12/12 12:10 Vinyl acetate ug/L ND 50.0 06/12/12 12:10 Vinyl chloride ug/L ND 2.0 06/12/12 12:10 Xylene (Total)ug/L ND 10.0 06/12/12 12:10 4-Bromofluorobenzene (S)%.99 72-125 06/12/12 12:10 Dibromofluoromethane (S)%.102 83-123 06/12/12 12:10 Toluene-d8 (S)%.101 81-114 06/12/12 12:10 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748909LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 49.850 100 69-122 1,1,1-Trichloroethane ug/L 57.250 114 69-126 1,1,2,2-Tetrachloroethane ug/L 51.350 103 68-134 1,1,2-Trichloroethane ug/L 51.750 103 77-129 1,1-Dichloroethane ug/L 48.150 96 70-127 1,1-Dichloroethene ug/L 47.250 94 75-145 1,1-Dichloropropene ug/L 54.050 108 75-126 1,2,3-Trichlorobenzene ug/L 41.150 82 63-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 62 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748909LABORATORY CONTROL SAMPLE: LCSSpike 1,2,3-Trichloropropane ug/L 83.5 L35016745-121 1,2,4-Trichlorobenzene ug/L 41.850 84 64-122 1,2,4-Trimethylbenzene ug/L 52.150 104 68-129 1,2-Dibromoethane (EDB)ug/L 55.250 110 77-123 1,2-Dichlorobenzene ug/L 50.950 102 74-123 1,2-Dichloroethane ug/L 55.350 111 71-127 1,2-Dichloropropane ug/L 50.050 100 75-126 1,3,5-Trimethylbenzene ug/L 52.050 104 69-129 1,3-Dichlorobenzene ug/L 49.750 99 76-123 1,3-Dichloropropane ug/L 49.650 99 77-126 1,4-Dichlorobenzene ug/L 49.750 99 77-121 2,2-Dichloropropane ug/L 46.750 93 45-138 2-Butanone (MEK)ug/L 253250 101 42-177 2-Chlorotoluene ug/L 48.550 97 74-129 2-Hexanone ug/L 270250 108 57-162 4-Chlorotoluene ug/L 51.750 103 70-125 4-Methyl-2-pentanone (MIBK)ug/L 263250 105 64-135 Acetone ug/L 257250 103 10-200 Acrolein ug/L 12901000 129 10-200 Acrylonitrile ug/L 9141000 91 59-144 Benzene ug/L 46.150 92 76-123 Bromobenzene ug/L 49.050 98 67-130 Bromochloromethane ug/L 45.150 90 58-153 Bromodichloromethane ug/L 51.850 104 71-124 Bromoform ug/L 46.550 93 64-116 Bromomethane ug/L 62.050 124 23-197 Carbon disulfide ug/L 93.5100 93 55-146 Carbon tetrachloride ug/L 50.050 100 65-125 Chlorobenzene ug/L 49.050 98 78-120 Chloroethane ug/L 56.850 114 56-163 Chloroform ug/L 55.950 112 73-122 Chloromethane ug/L 41.850 84 46-146 cis-1,2-Dichloroethene ug/L 49.050 98 79-129 cis-1,3-Dichloropropene ug/L 48.250 96 66-123 Dibromochloromethane ug/L 49.550 99 70-123 Dibromomethane ug/L 52.950 106 73-123 Dichlorodifluoromethane ug/L 55.950 112 19-200 Ethyl methacrylate ug/L 190200 95 70-127 Ethylbenzene ug/L 49.550 99 75-120 Hexachloro-1,3-butadiene ug/L 46.250 92 64-131 Iodomethane ug/L 113100 113 16-181 Isopropylbenzene (Cumene)ug/L 48.950 98 73-123 Methyl-tert-butyl ether ug/L 103100 103 66-128 Methylene Chloride ug/L 43.650 87 61-138 n-Butylbenzene ug/L 49.150 98 69-130 n-Hexane ug/L 42.2 N2508467-142 n-Propylbenzene ug/L 48.850 98 71-132 Naphthalene ug/L 41.450 83 62-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 63 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748909LABORATORY CONTROL SAMPLE: LCSSpike p-Isopropyltoluene ug/L 54.150 108 71-126 sec-Butylbenzene ug/L 50.850 102 69-130 Styrene ug/L 53.750 107 75-125 tert-Butylbenzene ug/L 42.150 84 49-114 Tetrachloroethene ug/L 48.050 96 57-125 Toluene ug/L 46.450 93 72-124 trans-1,2-Dichloroethene ug/L 48.550 97 71-145 trans-1,3-Dichloropropene ug/L 49.250 98 58-118 trans-1,4-Dichloro-2-butene ug/L 186200 93 50-121 Trichloroethene ug/L 50.650 101 77-122 Trichlorofluoromethane ug/L 55.350 111 56-159 Vinyl acetate ug/L 218200 109 27-119 Vinyl chloride ug/L 43.350 87 61-146 Xylene (Total)ug/L 149150 99 72-126 4-Bromofluorobenzene (S)%.100 72-125 Dibromofluoromethane (S)%.106 83-123 Toluene-d8 (S)%.101 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 748910MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189004 748911 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 61 30-12291 39 2050ND30.7 45.4 1,1,1-Trichloroethane ug/L 50 72 37-136102 34 2050ND35.9 50.8 1,1,2,2-Tetrachloroethane ug/L 50 59 47-13284 35 2050ND29.3 42.0 1,1,2-Trichloroethane ug/L 50 63 53-13190 35 2050ND31.6 44.8 1,1-Dichloroethane ug/L 50 63 47-13888 33 2050ND31.5 44.1 1,1-Dichloroethene ug/L 50 65 54-15290 32 2050ND32.3 44.8 1,1-Dichloropropene ug/L 50 69 47-13698 35 2050ND34.5 49.0 1,2,3-Trichlorobenzene ug/L 50 48 15-13267 32 2050ND24.1 33.3 1,2,3-Trichloropropane ug/L 50 88 24-108128 37 2050ND44.0 63.9 1,2,4-Trichlorobenzene ug/L 50 49 10-13069 35 2050ND24.4 34.6 1,2,4-Trimethylbenzene ug/L 50 65 10-14192 34 2050ND32.7 46.0 1,2-Dibromoethane (EDB)ug/L 50 68 49-13098 36 2050ND33.9 48.9 1,2-Dichlorobenzene ug/L 50 60 20-13787 37 2050ND30.2 43.7 1,2-Dichloroethane ug/L 50 68 42-13996 35 2050ND33.9 48.0 1,2-Dichloropropane ug/L 50 63 50-13191 37 2050ND31.4 45.4 1,3,5-Trimethylbenzene ug/L 50 65 10-14593 35 2050ND32.6 46.4 1,3-Dichlorobenzene ug/L 50 61 13-14390 38 2050ND30.7 44.9 1,3-Dichloropropane ug/L 50 62 53-13088 35 2050ND31.0 44.0 1,4-Dichlorobenzene ug/L 50 59 13-14087 39 2050ND29.4 43.4 2,2-Dichloropropane ug/L 50 50 13-14271 34 2050ND25.2 35.4 2-Butanone (MEK)ug/L 250 58 43-14280 32 20250ND145201 2-Chlorotoluene ug/L 50 62 15-14586 33 2050ND30.9 43.2 2-Hexanone ug/L 250 63 46-13986 32 20250ND156216 4-Chlorotoluene ug/L 50 64 12-14392 36 2050ND32.1 46.1 4-Methyl-2-pentanone (MIBK)ug/L 250 59 43-14085 35 20250ND149212 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 64 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 748910MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189004 748911 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Acetone ug/L 250 58 38-15580 33 20250ND144200 Acrolein ug/L 1000 77 11-200107 32 201000ND7731070 Acrylonitrile ug/L 1000 56 42-15076 30 201000ND556756 Benzene ug/L 50 59 52-13485 36 2050ND29.6 42.4 Bromobenzene ug/L 50 61 25-14088 36 2050ND30.6 44.0 Bromochloromethane ug/L 50 61 54-14483 31 2050ND30.6 41.7 Bromodichloromethane ug/L 50 64 42-12891 35 2050ND31.8 45.4 Bromoform ug/L 50 53 34-11677 36 2050ND26.6 38.4 Bromomethane ug/L 50 86 10-200123 35 2050ND43.0 61.5 Carbon disulfide ug/L 100 63 43-14488 33 20100ND63.3 88.3 Carbon tetrachloride ug/L 50 63 26-13690 36 2050ND31.3 45.1 Chlorobenzene ug/L 50 64 33-13688 32 2050ND31.9 44.0 Chloroethane ug/L 50 75 21-200109 37 2050ND37.6 54.4 Chloroform ug/L 50 71 50-134100 34 2050ND35.3 49.8 Chloromethane ug/L 50 61 32-16087 35 2050ND30.4 43.4 cis-1,2-Dichloroethene ug/L 50 64 48-14590 32 2050ND33.7 46.5 cis-1,3-Dichloropropene ug/L 50 60 35-11685 35 2050ND29.8 42.6 Dibromochloromethane ug/L 50 60 39-12286 36 2050ND30.1 43.2 Dibromomethane ug/L 50 65 49-13492 35 2050ND32.4 46.2 Dichlorodifluoromethane ug/L 50 78 35-200107 31 2050ND39.1 53.6 Ethyl methacrylate ug/L 200 57 54-12380 34 20200ND114160 Ethylbenzene ug/L 50 65 29-13291 34 2050ND32.4 45.6 Hexachloro-1,3-butadiene ug/L 50 64 10-14684 27 2050ND32.1 42.1 Iodomethane ug/L 100 79 10-171115 37 20100ND79.3 115 Isopropylbenzene (Cumene)ug/L 50 64 11-14691 35 2050ND31.9 45.4 Methyl-tert-butyl ether ug/L 100 60 39-13787 36 20100ND60.4 86.6 Methylene Chloride ug/L 50 55 47-14177 34 2050ND27.4 38.6 n-Butylbenzene ug/L 50 61 10-15685 32 2050ND30.7 42.5 n-Hexane ug/L N2505751-13776 27 2050ND28.7 37.8 n-Propylbenzene ug/L 50 63 10-14890 36 2050ND31.4 45.1 Naphthalene ug/L 50 45 40-12464 34 2050ND22.6 31.8 p-Isopropyltoluene ug/L 50 68 10-15099 37 2050ND33.8 49.3 sec-Butylbenzene ug/L 50 65 10-15094 36 2050ND32.5 47.0 Styrene ug/L 50 68 20-14397 35 2050ND34.2 48.5 tert-Butylbenzene ug/L 50 53 10-12377 36 2050ND26.6 38.5 Tetrachloroethene ug/L 50 67 30-12490 10 205071.5 105 117 Toluene ug/L 50 60 42-13089 38 2050ND30.2 44.5 trans-1,2-Dichloroethene ug/L 50 67 48-14494 34 2050ND33.4 47.0 trans-1,3-Dichloropropene ug/L 50 59 24-11484 35 2050ND29.6 42.1 trans-1,4-Dichloro-2-butene ug/L 200 50 22-12072 35 20200ND101144 Trichloroethene ug/L 50 67 44-13092 28 20506.2 39.5 52.2 Trichlorofluoromethane ug/L 50 76 17-200104 31 2050ND38.7 52.9 Vinyl acetate ug/L 200 55 10-11575 30 20200ND111150 Vinyl chloride ug/L 50 60 45-15988 38 2050ND29.9 44.2 Xylene (Total)ug/L 150 63 29-13192 37 20150ND95.2 138 4-Bromofluorobenzene (S)%.100 72-125103 20 Dibromofluoromethane (S)%.1d10483-123105 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 65 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 748910MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189004 748911 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Toluene-d8 (S)%.99 81-114103 20 Parameter Units MS Result % Rec Limits Qual% RecConc. 748912MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189016 748913 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 95 30-12281 15 2050ND47.4 40.7 1,1,1-Trichloroethane ug/L 50 105 37-13690 15 2050ND52.5 45.1 1,1,2,2-Tetrachloroethane ug/L 50 91 47-13275 18 2050ND45.4 37.7 1,1,2-Trichloroethane ug/L 50 99 53-13185 15 2050ND49.3 42.4 1,1-Dichloroethane ug/L 50 90 47-13877 16 2050ND44.9 38.4 1,1-Dichloroethene ug/L 50 93 54-15280 15 2050ND46.5 40.2 1,1-Dichloropropene ug/L 50 103 47-13689 14 2050ND51.7 44.7 1,2,3-Trichlorobenzene ug/L 50 66 15-13262 7 2050ND33.2 31.0 1,2,3-Trichloropropane ug/L M05013524-108117 15 2050ND67.7 58.3 1,2,4-Trichlorobenzene ug/L 50 71 10-13063 11 2050ND35.3 31.7 1,2,4-Trimethylbenzene ug/L 50 96 10-14182 16 2050ND47.9 40.8 1,2-Dibromoethane (EDB)ug/L 50 103 49-13087 17 2050ND51.6 43.6 1,2-Dichlorobenzene ug/L 50 92 20-13779 14 2050ND45.8 39.7 1,2-Dichloroethane ug/L 50 106 42-13987 19 2050ND53.0 43.7 1,2-Dichloropropane ug/L 50 94 50-13182 14 2050ND46.9 40.9 1,3,5-Trimethylbenzene ug/L 50 95 10-14581 15 2050ND47.4 40.7 1,3-Dichlorobenzene ug/L 50 91 13-14380 13 2050ND45.6 40.0 1,3-Dichloropropane ug/L 50 96 53-13081 16 2050ND47.8 40.5 1,4-Dichlorobenzene ug/L 50 88 13-14077 14 2050ND44.1 38.3 2,2-Dichloropropane ug/L 50 70 13-14263 10 2050ND35.0 31.6 2-Butanone (MEK)ug/L 250 87 43-14276 14 20250ND218189 2-Chlorotoluene ug/L 50 91 15-14577 17 2050ND45.6 38.5 2-Hexanone ug/L 250 91 46-13981 12 20250ND228204 4-Chlorotoluene ug/L 50 93 12-14383 12 2050ND46.5 41.4 4-Methyl-2-pentanone (MIBK)ug/L 250 91 43-14079 15 20250ND228196 Acetone ug/L 250 85 38-15572 16 20250ND211181 Acrolein ug/L 1000 111 11-20098 13 201000ND1110980 Acrylonitrile ug/L 1000 80 42-15072 11 201000ND804719 Benzene ug/L 50 90 52-13477 16 2050ND45.1 38.3 Bromobenzene ug/L 50 97 25-14079 20 2050ND48.4 39.7 Bromochloromethane ug/L 50 89 54-14480 11 2050ND44.7 40.0 Bromodichloromethane ug/L 50 94 42-12882 14 2050ND47.2 41.1 Bromoform ug/L 50 80 34-11670 13 2050ND40.0 35.0 Bromomethane ug/L 50 122 10-200110 10 2050ND60.9 54.9 Carbon disulfide ug/L 100 93 43-14481 14 20100ND93.2 80.7 Carbon tetrachloride ug/L 50 89 26-13679 11 2050ND44.3 39.5 Chlorobenzene ug/L 50 93 33-13680 14 2050ND46.5 40.2 Chloroethane ug/L 50 115 21-200101 14 2050ND57.7 50.3 Chloroform ug/L 50 104 50-13491 13 2050ND52.2 45.7 Chloromethane ug/L 50 87 32-16075 15 2050ND43.5 37.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 66 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 748912MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189016 748913 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. cis-1,2-Dichloroethene ug/L 50 96 48-14580 18 2050ND47.9 40.1 cis-1,3-Dichloropropene ug/L 50 89 35-11675 17 2050ND44.4 37.5 Dibromochloromethane ug/L 50 91 39-12277 17 2050ND45.4 38.4 Dibromomethane ug/L 50 99 49-13486 14 2050ND49.3 42.9 Dichlorodifluoromethane ug/L R15011535-20094 21 2050ND57.7 46.9 Ethyl methacrylate ug/L 200 87 54-12373 18 20200ND173145 Ethylbenzene ug/L 50 99 29-13283 18 2050ND49.3 41.3 Hexachloro-1,3-butadiene ug/L 50 84 10-14679 7 2050ND42.0 39.4 Iodomethane ug/L 100 113 10-171102 10 20100ND113102 Isopropylbenzene (Cumene)ug/L 50 93 11-14681 14 2050ND46.5 40.3 Methyl-tert-butyl ether ug/L 100 91 39-13780 13 20100ND91.3 80.1 Methylene Chloride ug/L 50 82 47-14170 15 2050ND41.1 35.2 n-Butylbenzene ug/L 50 87 10-15677 12 2050ND43.3 38.3 n-Hexane ug/L N2507251-13769 5 2050ND36.2 34.3 n-Propylbenzene ug/L 50 91 10-14879 14 2050ND45.6 39.6 Naphthalene ug/L 50 62 40-12459 4 2050ND31.0 29.6 p-Isopropyltoluene ug/L 50 100 10-15089 13 2050ND50.2 44.3 sec-Butylbenzene ug/L 50 95 10-15083 14 2050ND47.3 41.3 Styrene ug/L 50 102 20-14388 14 2050ND50.9 44.0 tert-Butylbenzene ug/L 50 80 10-12368 15 2050ND39.8 34.2 Tetrachloroethene ug/L M05017530-124117 12 2050179266237 Toluene ug/L 50 93 42-13079 16 2050ND46.7 39.7 trans-1,2-Dichloroethene ug/L 50 96 48-14484 14 2050ND48.1 41.9 trans-1,3-Dichloropropene ug/L 50 86 24-11475 14 2050ND43.2 37.4 trans-1,4-Dichloro-2-butene ug/L 200 77 22-12069 11 20200ND155138 Trichloroethene ug/L 50 96 44-13082 16 2050ND48.2 41.0 Trichlorofluoromethane ug/L 50 110 17-20095 14 2050ND55.1 47.7 Vinyl acetate ug/L 200 77 10-11569 11 20200ND155138 Vinyl chloride ug/L 50 90 45-15979 13 2050ND45.1 39.6 Xylene (Total)ug/L 150 95 29-13182 14 20150ND142123 4-Bromofluorobenzene (S)%.101 72-125104 20 Dibromofluoromethane (S)%.104 83-123104 20 Toluene-d8 (S)%.103 81-114101 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 67 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/42946 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5064189015, 5064189017, 5064189018, 5064189019, 5064189020, 5064189021, 5064189022, 5064189023, 5064189024, 5064189025, 5064189026, 5064189027, 5064189028 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:748915 Associated Lab Samples:5064189015, 5064189017, 5064189018, 5064189019, 5064189020, 5064189021, 5064189022, 5064189023, 5064189024, 5064189025, 5064189026, 5064189027, 5064189028 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/13/12 00:25 1,1,1-Trichloroethane ug/L ND 5.0 06/13/12 00:25 1,1,2,2-Tetrachloroethane ug/L ND 5.0 06/13/12 00:25 1,1,2-Trichloroethane ug/L ND 5.0 06/13/12 00:25 1,1-Dichloroethane ug/L ND 5.0 06/13/12 00:25 1,1-Dichloroethene ug/L ND 5.0 06/13/12 00:25 1,1-Dichloropropene ug/L ND 5.0 06/13/12 00:25 1,2,3-Trichlorobenzene ug/L ND 5.0 06/13/12 00:25 1,2,3-Trichloropropane ug/L ND 5.0 06/13/12 00:25 1,2,4-Trichlorobenzene ug/L ND 5.0 06/13/12 00:25 1,2,4-Trimethylbenzene ug/L ND 5.0 06/13/12 00:25 1,2-Dibromoethane (EDB)ug/L ND 5.0 06/13/12 00:25 1,2-Dichlorobenzene ug/L ND 5.0 06/13/12 00:25 1,2-Dichloroethane ug/L ND 5.0 06/13/12 00:25 1,2-Dichloropropane ug/L ND 5.0 06/13/12 00:25 1,3,5-Trimethylbenzene ug/L ND 5.0 06/13/12 00:25 1,3-Dichlorobenzene ug/L ND 5.0 06/13/12 00:25 1,3-Dichloropropane ug/L ND 5.0 06/13/12 00:25 1,4-Dichlorobenzene ug/L ND 5.0 06/13/12 00:25 2,2-Dichloropropane ug/L ND 5.0 06/13/12 00:25 2-Butanone (MEK)ug/L ND 25.0 06/13/12 00:25 2-Chlorotoluene ug/L ND 5.0 06/13/12 00:25 2-Hexanone ug/L ND 25.0 06/13/12 00:25 4-Chlorotoluene ug/L ND 5.0 06/13/12 00:25 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 06/13/12 00:25 Acetone ug/L ND 100 06/13/12 00:25 Acrolein ug/L ND 100 06/13/12 00:25 Acrylonitrile ug/L ND 100 06/13/12 00:25 Benzene ug/L ND 5.0 06/13/12 00:25 Bromobenzene ug/L ND 5.0 06/13/12 00:25 Bromochloromethane ug/L ND 5.0 06/13/12 00:25 Bromodichloromethane ug/L ND 5.0 06/13/12 00:25 Bromoform ug/L ND 5.0 06/13/12 00:25 Bromomethane ug/L ND 5.0 06/13/12 00:25 Carbon disulfide ug/L ND 10.0 06/13/12 00:25 Carbon tetrachloride ug/L ND 5.0 06/13/12 00:25 Chlorobenzene ug/L ND 5.0 06/13/12 00:25 Chloroethane ug/L ND 5.0 06/13/12 00:25 Chloroform ug/L ND 5.0 06/13/12 00:25 Chloromethane ug/L ND 5.0 06/13/12 00:25 cis-1,2-Dichloroethene ug/L ND 5.0 06/13/12 00:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 68 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:748915 Associated Lab Samples:5064189015, 5064189017, 5064189018, 5064189019, 5064189020, 5064189021, 5064189022, 5064189023, 5064189024, 5064189025, 5064189026, 5064189027, 5064189028 Matrix:Water Analyzed cis-1,3-Dichloropropene ug/L ND 5.0 06/13/12 00:25 Dibromochloromethane ug/L ND 5.0 06/13/12 00:25 Dibromomethane ug/L ND 5.0 06/13/12 00:25 Dichlorodifluoromethane ug/L ND 5.0 06/13/12 00:25 Ethyl methacrylate ug/L ND 100 06/13/12 00:25 Ethylbenzene ug/L ND 5.0 06/13/12 00:25 Hexachloro-1,3-butadiene ug/L ND 5.0 06/13/12 00:25 Iodomethane ug/L ND 10.0 06/13/12 00:25 Isopropylbenzene (Cumene)ug/L ND 5.0 06/13/12 00:25 Methyl-tert-butyl ether ug/L ND 4.0 06/13/12 00:25 Methylene Chloride ug/L ND 5.0 06/13/12 00:25 n-Butylbenzene ug/L ND 5.0 06/13/12 00:25 n-Hexane ug/L ND 5.0 N206/13/12 00:25 n-Propylbenzene ug/L ND 5.0 06/13/12 00:25 Naphthalene ug/L ND 5.0 06/13/12 00:25 p-Isopropyltoluene ug/L ND 5.0 06/13/12 00:25 sec-Butylbenzene ug/L ND 5.0 06/13/12 00:25 Styrene ug/L ND 5.0 06/13/12 00:25 tert-Butylbenzene ug/L ND 5.0 06/13/12 00:25 Tetrachloroethene ug/L ND 5.0 06/13/12 00:25 Toluene ug/L ND 5.0 06/13/12 00:25 trans-1,2-Dichloroethene ug/L ND 5.0 06/13/12 00:25 trans-1,3-Dichloropropene ug/L ND 5.0 06/13/12 00:25 trans-1,4-Dichloro-2-butene ug/L ND 100 06/13/12 00:25 Trichloroethene ug/L ND 5.0 06/13/12 00:25 Trichlorofluoromethane ug/L ND 5.0 06/13/12 00:25 Vinyl acetate ug/L ND 50.0 06/13/12 00:25 Vinyl chloride ug/L ND 2.0 06/13/12 00:25 Xylene (Total)ug/L ND 10.0 06/13/12 00:25 4-Bromofluorobenzene (S)%.99 72-125 06/13/12 00:25 Dibromofluoromethane (S)%.103 83-123 06/13/12 00:25 Toluene-d8 (S)%.102 81-114 06/13/12 00:25 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748916LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 50.350 101 69-122 1,1,1-Trichloroethane ug/L 54.550 109 69-126 1,1,2,2-Tetrachloroethane ug/L 46.950 94 68-134 1,1,2-Trichloroethane ug/L 51.250 102 77-129 1,1-Dichloroethane ug/L 47.150 94 70-127 1,1-Dichloroethene ug/L 43.850 88 75-145 1,1-Dichloropropene ug/L 52.150 104 75-126 1,2,3-Trichlorobenzene ug/L 38.050 76 63-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 69 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748916LABORATORY CONTROL SAMPLE: LCSSpike 1,2,3-Trichloropropane ug/L 71.7 L35014345-121 1,2,4-Trichlorobenzene ug/L 37.650 75 64-122 1,2,4-Trimethylbenzene ug/L 49.050 98 68-129 1,2-Dibromoethane (EDB)ug/L 53.850 108 77-123 1,2-Dichlorobenzene ug/L 48.750 97 74-123 1,2-Dichloroethane ug/L 52.450 105 71-127 1,2-Dichloropropane ug/L 49.150 98 75-126 1,3,5-Trimethylbenzene ug/L 48.450 97 69-129 1,3-Dichlorobenzene ug/L 47.450 95 76-123 1,3-Dichloropropane ug/L 49.350 99 77-126 1,4-Dichlorobenzene ug/L 46.050 92 77-121 2,2-Dichloropropane ug/L 36.250 72 45-138 2-Butanone (MEK)ug/L 229250 91 42-177 2-Chlorotoluene ug/L 46.050 92 74-129 2-Hexanone ug/L 250250 100 57-162 4-Chlorotoluene ug/L 47.550 95 70-125 4-Methyl-2-pentanone (MIBK)ug/L 247250 99 64-135 Acetone ug/L 234250 94 10-200 Acrolein ug/L 12201000 122 10-200 Acrylonitrile ug/L 8571000 86 59-144 Benzene ug/L 45.150 90 76-123 Bromobenzene ug/L 50.750 101 67-130 Bromochloromethane ug/L 45.250 90 58-153 Bromodichloromethane ug/L 49.250 98 71-124 Bromoform ug/L 42.450 85 64-116 Bromomethane ug/L 67.050 134 23-197 Carbon disulfide ug/L 90.2100 90 55-146 Carbon tetrachloride ug/L 48.250 96 65-125 Chlorobenzene ug/L 48.050 96 78-120 Chloroethane ug/L 57.150 114 56-163 Chloroform ug/L 54.050 108 73-122 Chloromethane ug/L 44.550 89 46-146 cis-1,2-Dichloroethene ug/L 48.150 96 79-129 cis-1,3-Dichloropropene ug/L 45.850 92 66-123 Dibromochloromethane ug/L 48.450 97 70-123 Dibromomethane ug/L 50.850 102 73-123 Dichlorodifluoromethane ug/L 52.250 104 19-200 Ethyl methacrylate ug/L 181200 91 70-127 Ethylbenzene ug/L 50.850 102 75-120 Hexachloro-1,3-butadiene ug/L 42.950 86 64-131 Iodomethane ug/L 118100 118 16-181 Isopropylbenzene (Cumene)ug/L 48.550 97 73-123 Methyl-tert-butyl ether ug/L 97.1100 97 66-128 Methylene Chloride ug/L 42.850 86 61-138 n-Butylbenzene ug/L 45.650 91 69-130 n-Hexane ug/L 35.2 N2507067-142 n-Propylbenzene ug/L 46.150 92 71-132 Naphthalene ug/L 35.950 72 62-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 70 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 748916LABORATORY CONTROL SAMPLE: LCSSpike p-Isopropyltoluene ug/L 51.750 103 71-126 sec-Butylbenzene ug/L 48.050 96 69-130 Styrene ug/L 53.750 107 75-125 tert-Butylbenzene ug/L 40.050 80 49-114 Tetrachloroethene ug/L 47.150 94 57-125 Toluene ug/L 47.850 96 72-124 trans-1,2-Dichloroethene ug/L 47.350 95 71-145 trans-1,3-Dichloropropene ug/L 47.450 95 58-118 trans-1,4-Dichloro-2-butene ug/L 166200 83 50-121 Trichloroethene ug/L 48.050 96 77-122 Trichlorofluoromethane ug/L 53.550 107 56-159 Vinyl acetate ug/L 207200 103 27-119 Vinyl chloride ug/L 43.750 87 61-146 Xylene (Total)ug/L 149150 99 72-126 4-Bromofluorobenzene (S)%.103 72-125 Dibromofluoromethane (S)%.104 83-123 Toluene-d8 (S)%.103 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 748917MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189022 748918 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 85 30-12291 7 2050ND42.4 45.7 1,1,1-Trichloroethane ug/L 50 94 37-136102 9 2050ND46.9 51.2 1,1,2,2-Tetrachloroethane ug/L 50 80 47-13285 6 2050ND40.0 42.4 1,1,2-Trichloroethane ug/L 50 88 53-13196 9 2050ND43.8 47.9 1,1-Dichloroethane ug/L 50 82 47-13888 7 2050ND41.1 44.1 1,1-Dichloroethene ug/L 50 85 54-15289 5 2050ND42.3 44.4 1,1-Dichloropropene ug/L 50 92 47-13699 7 2050ND46.2 49.4 1,2,3-Trichlorobenzene ug/L 50 62 15-13267 8 2050ND31.1 33.7 1,2,3-Trichloropropane ug/L M05011724-108127 8 2050ND58.7 63.4 1,2,4-Trichlorobenzene ug/L 50 63 10-13066 6 2050ND31.3 33.1 1,2,4-Trimethylbenzene ug/L 50 84 10-14191 8 2050ND42.1 45.7 1,2-Dibromoethane (EDB)ug/L 50 91 49-13096 5 2050ND45.6 48.1 1,2-Dichlorobenzene ug/L 50 82 20-13787 6 2050ND40.8 43.3 1,2-Dichloroethane ug/L 50 90 42-13997 7 2050ND45.2 48.5 1,2-Dichloropropane ug/L 50 84 50-13191 8 2050ND41.9 45.3 1,3,5-Trimethylbenzene ug/L 50 84 10-14591 9 2050ND41.9 45.7 1,3-Dichlorobenzene ug/L 50 78 13-14387 11 2050ND39.2 43.6 1,3-Dichloropropane ug/L 50 83 53-13090 8 2050ND41.5 45.1 1,4-Dichlorobenzene ug/L 50 79 13-14086 8 2050ND39.5 43.0 2,2-Dichloropropane ug/L 50 54 13-14262 15 2050ND26.8 31.0 2-Butanone (MEK)ug/L 250 81 43-14283 3 20250ND202208 2-Chlorotoluene ug/L 50 79 15-14585 8 2050ND39.4 42.7 2-Hexanone ug/L 250 87 46-13988 2 20250ND216220 4-Chlorotoluene ug/L 50 83 12-14390 8 2050ND41.4 44.8 4-Methyl-2-pentanone (MIBK)ug/L 250 85 43-14088 4 20250ND211219 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 71 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 748917MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189022 748918 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Acetone ug/L 250 83 38-15584 .9 20250ND208209 Acrolein ug/L 1000 96 11-20099 2 201000ND965989 Acrylonitrile ug/L 1000 76 42-15079 4 201000ND764795 Benzene ug/L 50 80 52-13486 6 2050ND40.2 42.8 Bromobenzene ug/L 50 82 25-14091 10 2050ND41.1 45.3 Bromochloromethane ug/L 50 80 54-14486 7 2050ND40.1 43.0 Bromodichloromethane ug/L 50 85 42-12889 5 2050ND42.5 44.5 Bromoform ug/L 50 74 34-11677 4 2050ND37.0 38.6 Bromomethane ug/L 50 98 10-200110 11 2050ND49.0 54.8 Carbon disulfide ug/L 100 82 43-14486 5 20100ND82.0 86.2 Carbon tetrachloride ug/L 50 80 26-13690 11 2050ND40.2 44.9 Chlorobenzene ug/L 50 84 33-13688 5 2050ND41.8 43.9 Chloroethane ug/L 50 101 21-200111 9 2050ND50.6 55.5 Chloroform ug/L 50 96 50-134102 6 2050ND47.8 51.0 Chloromethane ug/L 50 76 32-16081 6 2050ND38.1 40.6 cis-1,2-Dichloroethene ug/L 50 84 48-14591 8 2050ND42.0 45.4 cis-1,3-Dichloropropene ug/L 50 73 35-11682 12 2050ND36.6 41.1 Dibromochloromethane ug/L 50 83 39-12290 8 2050ND41.5 45.2 Dibromomethane ug/L 50 91 49-13493 2 2050ND45.4 46.5 Dichlorodifluoromethane ug/L 50 93 35-20094 .7 2050ND46.5 46.9 Ethyl methacrylate ug/L 200 78 54-12380 3 20200ND156161 Ethylbenzene ug/L 50 86 29-13291 6 2050ND42.8 45.3 Hexachloro-1,3-butadiene ug/L 50 71 10-14679 10 2050ND35.6 39.4 Iodomethane ug/L 100 100 10-171112 11 20100ND99.7 112 Isopropylbenzene (Cumene)ug/L 50 84 11-14691 8 2050ND42.0 45.5 Methyl-tert-butyl ether ug/L 100 82 39-13788 6 20100ND82.1 87.6 Methylene Chloride ug/L 50 73 47-14178 7 2050ND36.5 39.1 n-Butylbenzene ug/L 50 75 10-15682 9 2050ND37.3 40.8 n-Hexane ug/L N2506051-13768 12 2050ND30.0 34.0 n-Propylbenzene ug/L 50 80 10-14887 8 2050ND40.1 43.5 Naphthalene ug/L 50 60 40-12464 6 2050ND30.1 32.0 p-Isopropyltoluene ug/L 50 86 10-15094 9 2050ND43.2 47.2 sec-Butylbenzene ug/L 50 84 10-15089 6 2050ND41.8 44.5 Styrene ug/L 50 92 20-14398 7 2050ND45.9 49.0 tert-Butylbenzene ug/L 50 72 10-12376 6 2050ND35.8 38.0 Tetrachloroethene ug/L M050-2 30-1244 .4 2050851850853 Toluene ug/L 50 82 42-13088 7 2050ND41.0 44.2 trans-1,2-Dichloroethene ug/L 50 85 48-14491 7 2050ND42.4 45.3 trans-1,3-Dichloropropene ug/L 50 76 24-11482 8 2050ND37.8 40.8 trans-1,4-Dichloro-2-butene ug/L 200 66 22-12074 11 20200ND133148 Trichloroethene ug/L 50 87 44-13091 4 2050ND44.2 46.0 Trichlorofluoromethane ug/L 50 99 17-200103 5 2050ND49.3 51.7 Vinyl acetate ug/L 200 61 10-11560 2 20200ND121119 Vinyl chloride ug/L 50 78 45-15982 5 2050ND39.2 41.2 Xylene (Total)ug/L 150 83 29-13191 9 20150ND125137 4-Bromofluorobenzene (S)%.100 72-125103 20 Dibromofluoromethane (S)%.106 83-123104 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 72 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5064189 SBI068 Parameter Units MS Result % Rec Limits Qual% RecConc. 748917MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5064189022 748918 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Toluene-d8 (S)%.101 81-114103 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 73 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5064189 SBI068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Several compounds are outside of acceptance limits for percent recovery and/or RPD value. aa 6/14/121d Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 74 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5064189 SBI068 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5064189001 MSV/42945SBI068:AMW6I:G060512 EPA 8260 5064189002 MSV/42945SBI068:AMW6S:G060512 EPA 8260 5064189003 MSV/42945SBI068:AMW7I:G060512 EPA 8260 5064189004 MSV/42945SBI068:AMW7S:G060512 EPA 8260 5064189005 MSV/42945SBI068:AMW8I:G060512 EPA 8260 5064189006 MSV/42945SBI068:AMW8S:G060512 EPA 8260 5064189007 MSV/42945SBI068:AMW5S:G060612 EPA 8260 5064189008 MSV/42945SBI068:AMW5I:G060512 EPA 8260 5064189009 MSV/42945SBI068:AMW5D:G060512 EPA 8260 5064189010 MSV/42945SBI068:AMW6I:G060512A EPA 8260 5064189011 MSV/42945SBI068:EB1:W060512 EPA 8260 5064189012 MSV/42945SBI068:EB2:W060612 EPA 8260 5064189013 MSV/42945SBI068:AMW4D:G060612 EPA 8260 5064189014 MSV/42945SBI068:AMW4I:G060612 EPA 8260 5064189015 MSV/42946SBI068:AMW4S:G060612 EPA 8260 5064189016 MSV/42945SBI068:AMW1D:G060612 EPA 8260 5064189017 MSV/42946SBI068:AMW1I:G060612 EPA 8260 5064189018 MSV/42946SBI068:AMW1S:G060612 EPA 8260 5064189019 MSV/42946SBI068:AMW3D:G060612 EPA 8260 5064189020 MSV/42946SBI068:AMW3I:G060612 EPA 8260 5064189021 MSV/42946SBI068:AMW3S:G060612 EPA 8260 5064189022 MSV/42946SBI068:AMW2D:G060712 EPA 8260 5064189023 MSV/42946SBI068:AMW2I:G060712 EPA 8260 5064189024 MSV/42946SBI068:AMW2S:G060712 EPA 8260 5064189025 MSV/42946SBI068:EB3:W060712 EPA 8260 5064189026 MSV/42946SBI068:AMW1I:G060612A EPA 8260 5064189027 MSV/42946SBI068:AMW2I:G060712A EPA 8260 5064189028 MSV/42946SBI068:LTB:W060512 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 06/22/2012 10:33 AM Page 75 of 75 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421