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HomeMy WebLinkAboutSB-0243 Appendix S - Lab DataApril 26, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5061800 5061800 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 6435 Castleway West Drive Suite 119 Indianapolis, IN 46250 SBI067 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kelly Jones for Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5061800 SBI067 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5061800 SBI067 Lab ID Sample ID Matrix Date Collected Date Received 5061800001 SBI067:HTB17:G350390 Water 04/19/12 12:25 04/21/12 10:00 5061800002 SBI067:HTB17:G260300 Water 04/19/12 13:00 04/21/12 10:00 5061800003 SBI067:HTB18:G450490 Water 04/19/12 14:20 04/21/12 10:00 5061800004 SBI067:HTB18:G350390 Water 04/19/12 14:50 04/21/12 10:00 5061800005 SBI067:HTB18:G350390A Water 04/19/12 14:50 04/21/12 10:00 5061800006 SBI067:HTB18:G260300 Water 04/19/12 15:30 04/21/12 10:00 5061800007 SBI067:FB1:W041912 Water 04/19/12 17:00 04/21/12 10:00 5061800008 SBI067:HTB5:G350390 Water 04/20/12 08:30 04/21/12 10:00 5061800009 SBI067:HTB5:G260300 Water 04/20/12 09:30 04/21/12 10:00 5061800010 SBI067:HTB5:G260300A Water 04/20/12 09:30 04/21/12 10:00 5061800011 SBI067:HTB14:G450490 Water 04/20/12 10:30 04/21/12 10:00 5061800012 SBI067:HTB14:G350390 Water 04/20/12 11:00 04/21/12 10:00 5061800013 SBI067:FB1:W042012 Water 04/20/12 12:00 04/21/12 10:00 5061800014 SBI067:HTB14:G260300 Water 04/20/12 11:30 04/21/12 10:00 5061800015 SBI067:TB:W041912 Water 04/19/12 08:00 04/21/12 10:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5061800 SBI067 Lab ID Sample ID Method Analytes ReportedAnalysts 5061800001 SBI067:HTB17:G350390 EPA 8082 8RAK EPA 8260 73ALA 5061800002 SBI067:HTB17:G260300 EPA 8082 8RAK EPA 8260 73ALA 5061800003 SBI067:HTB18:G450490 EPA 8082 8RAK EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800004 SBI067:HTB18:G350390 EPA 8082 8RAK EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800005 SBI067:HTB18:G350390A EPA 8270 by SIM 19CEM EPA 8270 47KES 5061800006 SBI067:HTB18:G260300 EPA 8082 8RAK EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800007 SBI067:FB1:W041912 EPA 8082 8RAK EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800008 SBI067:HTB5:G350390 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800009 SBI067:HTB5:G260300 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800010 SBI067:HTB5:G260300A EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800011 SBI067:HTB14:G450490 EPA 8260 73ALA 5061800012 SBI067:HTB14:G350390 EPA 8260 73ALA 5061800013 SBI067:FB1:W042012 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73ALA 5061800014 SBI067:HTB14:G260300 EPA 8260 73ALA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5061800 SBI067 Lab ID Sample ID Method Analytes ReportedAnalysts 5061800015 SBI067:TB:W041912 EPA 8260 73ALA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB17:G350390 Lab ID:5061800001 Collected:04/19/12 12:25 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:07 12674-11-204/24/12 15:050.52 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:07 11104-28-204/24/12 15:050.52 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:07 11141-16-504/24/12 15:050.52 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:07 53469-21-904/24/12 15:050.52 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:07 12672-29-604/24/12 15:050.52 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:07 11097-69-104/24/12 15:050.52 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:07 11096-82-504/24/12 15:050.52 Surrogates Tetrachloro-m-xylene (S)79 %.1 04/24/12 18:07 877-09-804/24/12 15:0539-110 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 08:24 67-64-1100 Acrolein ND ug/L 1 04/25/12 08:24 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 08:24 107-13-1100 Benzene ND ug/L 1 04/25/12 08:24 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 08:24 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 08:24 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 08:24 75-27-45.0 Bromoform ND ug/L 1 04/25/12 08:24 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 08:24 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 08:24 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 08:24 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 08:24 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 08:24 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 08:24 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 08:24 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 08:24 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 08:24 75-00-35.0 Chloroform ND ug/L 1 04/25/12 08:24 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 08:24 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 08:24 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 08:24 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 08:24 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 08:24 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 08:24 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 08:24 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 08:24 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 08:24 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 08:24 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 08:24 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 08:24 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 08:24 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 08:24 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 08:24 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 08:24 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 08:24 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 08:24 142-28-95.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 6 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB17:G350390 Lab ID:5061800001 Collected:04/19/12 12:25 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 2,2-Dichloropropane ND ug/L 1 04/25/12 08:24 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 08:24 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 08:24 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 08:24 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 08:24 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 08:24 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 08:24 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 08:24 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 08:24 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 08:24 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 08:24 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 08:24 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 08:24 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 08:24 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 08:24 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 08:24 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 08:24 103-65-15.0 Styrene ND ug/L 1 04/25/12 08:24 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 08:24 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 08:24 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 08:24 127-18-45.0 Toluene ND ug/L 1 04/25/12 08:24 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 08:24 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 08:24 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 08:24 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 08:24 79-00-55.0 Trichloroethene 7.3 ug/L 1 04/25/12 08:24 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 08:24 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 08:24 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 08:24 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 08:24 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 08:24 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 08:24 75-01-42.0 Xylene (Total)ND ug/L 1 04/25/12 08:24 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/25/12 08:24 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/25/12 08:24 460-00-472-125 Toluene-d8 (S)101 %.1 04/25/12 08:24 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 7 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB17:G260300 Lab ID:5061800002 Collected:04/19/12 13:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:13 12674-11-204/24/12 15:050.52 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:13 11104-28-204/24/12 15:050.52 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:13 11141-16-504/24/12 15:050.52 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:13 53469-21-904/24/12 15:050.52 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:13 12672-29-604/24/12 15:050.52 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:13 11097-69-104/24/12 15:050.52 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:13 11096-82-504/24/12 15:050.52 Surrogates Tetrachloro-m-xylene (S)80 %.1 04/24/12 18:13 877-09-804/24/12 15:0539-110 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 08:58 67-64-1100 Acrolein ND ug/L 1 04/25/12 08:58 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 08:58 107-13-1100 Benzene ND ug/L 1 04/25/12 08:58 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 08:58 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 08:58 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 08:58 75-27-45.0 Bromoform ND ug/L 1 04/25/12 08:58 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 08:58 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 08:58 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 08:58 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 08:58 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 08:58 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 08:58 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 08:58 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 08:58 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 08:58 75-00-35.0 Chloroform ND ug/L 1 04/25/12 08:58 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 08:58 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 08:58 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 08:58 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 08:58 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 08:58 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 08:58 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 08:58 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 08:58 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 08:58 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 08:58 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 08:58 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 08:58 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 08:58 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 08:58 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 08:58 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 08:58 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 08:58 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 08:58 142-28-95.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 8 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB17:G260300 Lab ID:5061800002 Collected:04/19/12 13:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 2,2-Dichloropropane ND ug/L 1 04/25/12 08:58 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 08:58 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 08:58 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 08:58 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 08:58 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 08:58 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 08:58 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 08:58 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 08:58 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 08:58 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 08:58 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 08:58 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 08:58 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 08:58 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 08:58 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 08:58 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 08:58 103-65-15.0 Styrene ND ug/L 1 04/25/12 08:58 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 08:58 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 08:58 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 08:58 127-18-45.0 Toluene ND ug/L 1 04/25/12 08:58 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 08:58 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 08:58 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 08:58 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 08:58 79-00-55.0 Trichloroethene 8.2 ug/L 1 04/25/12 08:58 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 08:58 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 08:58 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 08:58 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 08:58 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 08:58 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 08:58 75-01-42.0 Xylene (Total)ND ug/L 1 04/25/12 08:58 1330-20-710.0 Surrogates Dibromofluoromethane (S)96 %.1 04/25/12 08:58 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/25/12 08:58 460-00-472-125 Toluene-d8 (S)99 %.1 04/25/12 08:58 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 9 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G450490 Lab ID:5061800003 Collected:04/19/12 14:20 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:31 12674-11-204/24/12 15:050.51 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:31 11104-28-204/24/12 15:050.51 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:31 11141-16-504/24/12 15:050.51 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:31 53469-21-904/24/12 15:050.51 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:31 12672-29-604/24/12 15:050.51 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:31 11097-69-104/24/12 15:050.51 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:31 11096-82-504/24/12 15:050.51 Surrogates Tetrachloro-m-xylene (S)73 %.1 04/24/12 18:31 877-09-804/24/12 15:0539-110 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 19:23 83-32-904/24/12 10:001.1 Acenaphthylene ND ug/L 1 04/25/12 19:23 208-96-804/24/12 10:001.1 Anthracene ND ug/L 1 04/25/12 19:23 120-12-704/24/12 10:000.11 Benzo(a)anthracene ND ug/L 1 04/25/12 19:23 56-55-304/24/12 10:000.11 Benzo(a)pyrene ND ug/L 1 04/25/12 19:23 50-32-804/24/12 10:000.11 Benzo(b)fluoranthene ND ug/L 1 04/25/12 19:23 205-99-204/24/12 10:000.11 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 19:23 191-24-204/24/12 10:000.11 Benzo(k)fluoranthene ND ug/L 1 04/25/12 19:23 207-08-904/24/12 10:000.11 Chrysene ND ug/L 1 04/25/12 19:23 218-01-904/24/12 10:000.53 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 19:23 53-70-304/24/12 10:000.11 Fluoranthene ND ug/L 1 04/25/12 19:23 206-44-004/24/12 10:001.1 Fluorene ND ug/L 1 04/25/12 19:23 86-73-704/24/12 10:001.1 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 19:23 193-39-504/24/12 10:000.11 2-Methylnaphthalene ND ug/L 1 04/25/12 19:23 91-57-604/24/12 10:001.1 Naphthalene ND ug/L 1 04/25/12 19:23 91-20-304/24/12 10:001.1 Phenanthrene ND ug/L 1 04/25/12 19:23 85-01-804/24/12 10:001.1 Pyrene ND ug/L 1 04/25/12 19:23 129-00-004/24/12 10:001.1 Surrogates 2-Fluorobiphenyl (S)66 %.1 04/25/12 19:23 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)83 %.1 04/25/12 19:23 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 03:49 100-51-604/24/12 10:0021.1 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 03:49 101-55-304/24/12 10:0010.5 Butylbenzylphthalate ND ug/L 1 04/25/12 03:49 85-68-704/24/12 10:0010.5 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 03:49 59-50-704/24/12 10:0021.1 4-Chloroaniline ND ug/L 1 04/25/12 03:49 106-47-804/24/12 10:0021.1 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 03:49 111-91-104/24/12 10:0010.5 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 03:49 111-44-404/24/12 10:0010.5 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 03:49 108-60-104/24/12 10:005.3 2-Chloronaphthalene ND ug/L 1 04/25/12 03:49 91-58-704/24/12 10:0010.5 2-Chlorophenol ND ug/L 1 04/25/12 03:49 95-57-804/24/12 10:0010.5 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 03:49 7005-72-304/24/12 10:0010.5 Dibenzofuran ND ug/L 1 04/25/12 03:49 132-64-904/24/12 10:0010.5 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 03:49 91-94-104/24/12 10:0021.1 2,4-Dichlorophenol ND ug/L 1 04/25/12 03:49 120-83-204/24/12 10:0010.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 10 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G450490 Lab ID:5061800003 Collected:04/19/12 14:20 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate ND ug/L 1 04/25/12 03:49 84-66-204/24/12 10:0010.5 2,4-Dimethylphenol ND ug/L 1 04/25/12 03:49 105-67-904/24/12 10:0010.5 Dimethylphthalate ND ug/L 1 04/25/12 03:49 131-11-304/24/12 10:0010.5 Di-n-butylphthalate ND ug/L 1 04/25/12 03:49 84-74-204/24/12 10:0010.5 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 03:49 534-52-104/24/12 10:0052.6 2,4-Dinitrophenol ND ug/L 1 04/25/12 03:49 51-28-504/24/12 10:0052.6 2,4-Dinitrotoluene ND ug/L 1 04/25/12 03:49 121-14-204/24/12 10:0010.5 2,6-Dinitrotoluene ND ug/L 1 04/25/12 03:49 606-20-204/24/12 10:0010.5 Di-n-octylphthalate ND ug/L 1 04/25/12 03:49 117-84-004/24/12 10:0010.5 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 03:49 117-81-704/24/12 10:005.3 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 03:49 87-68-304/24/12 10:005.3 Hexachlorobenzene ND ug/L 1 04/25/12 03:49 118-74-104/24/12 10:0010.5 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 03:49 77-47-404/24/12 10:0026.3 Hexachloroethane ND ug/L 1 04/25/12 03:49 67-72-104/24/12 10:0010.5 Isophorone ND ug/L 1 04/25/12 03:49 78-59-104/24/12 10:0010.5 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 03:49 95-48-704/24/12 10:0010.5 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 03:4904/24/12 10:0021.1 2-Nitroaniline ND ug/L 1 04/25/12 03:49 88-74-404/24/12 10:0052.6 3-Nitroaniline ND ug/L 1 04/25/12 03:49 99-09-204/24/12 10:0052.6 4-Nitroaniline ND ug/L 1 04/25/12 03:49 100-01-604/24/12 10:0052.6 Nitrobenzene ND ug/L 1 04/25/12 03:49 98-95-304/24/12 10:0010.5 2-Nitrophenol ND ug/L 1 04/25/12 03:49 88-75-504/24/12 10:0010.5 4-Nitrophenol ND ug/L 1 04/25/12 03:49 100-02-704/24/12 10:0052.6 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 03:49 621-64-704/24/12 10:0010.5 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 03:49 86-30-604/24/12 10:0010.5 Pentachlorophenol ND ug/L 1 04/25/12 03:49 87-86-504/24/12 10:0052.6 Phenol ND ug/L 1 04/25/12 03:49 108-95-204/24/12 10:0010.5 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 03:49 95-95-404/24/12 10:0010.5 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 03:49 88-06-204/24/12 10:0010.5 Surrogates Nitrobenzene-d5 (S)66 %.1 04/25/12 03:49 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)20 %.1 04/25/12 03:49 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)35 %.1 04/25/12 03:49 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)85 %.1 04/25/12 03:49 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 03:23 67-64-1100 Acrolein ND ug/L 1 04/24/12 03:23 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 03:23 107-13-1100 Benzene ND ug/L 1 04/24/12 03:23 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 03:23 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 03:23 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 03:23 75-27-45.0 Bromoform ND ug/L 1 04/24/12 03:23 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 03:23 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 03:23 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 03:23 104-51-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 11 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G450490 Lab ID:5061800003 Collected:04/19/12 14:20 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 sec-Butylbenzene ND ug/L 1 04/24/12 03:23 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 03:23 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 03:23 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 03:23 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 03:23 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 03:23 75-00-35.0 Chloroform ND ug/L 1 04/24/12 03:23 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 03:23 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 03:23 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 03:23 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 03:23 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 03:23 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 03:23 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 03:23 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 03:23 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 03:23 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 03:23 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 03:23 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 03:23 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 03:23 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 03:23 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 03:23 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 03:23 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 03:23 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 03:23 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 03:23 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 03:23 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 03:23 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 03:23 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 03:23 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 03:23 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 03:23 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 03:23 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 03:23 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 03:23 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 03:23 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 03:23 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 03:23 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 03:23 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 03:23 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 03:23 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 03:23 103-65-15.0 Styrene ND ug/L 1 04/24/12 03:23 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 03:23 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 03:23 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 03:23 127-18-45.0 Toluene ND ug/L 1 04/24/12 03:23 108-88-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 12 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G450490 Lab ID:5061800003 Collected:04/19/12 14:20 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 03:23 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 03:23 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 03:23 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 03:23 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 03:23 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 03:23 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 03:23 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 03:23 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 03:23 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 03:23 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 03:23 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 03:23 1330-20-710.0 Surrogates Dibromofluoromethane (S)109 %.1 04/24/12 03:23 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/24/12 03:23 460-00-472-125 Toluene-d8 (S)90 %.1 04/24/12 03:23 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 13 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390 Lab ID:5061800004 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:37 12674-11-204/24/12 15:050.52 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:37 11104-28-204/24/12 15:050.52 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:37 11141-16-504/24/12 15:050.52 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:37 53469-21-904/24/12 15:050.52 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:37 12672-29-604/24/12 15:050.52 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:37 11097-69-104/24/12 15:050.52 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:37 11096-82-504/24/12 15:050.52 Surrogates Tetrachloro-m-xylene (S)82 %.1 04/24/12 18:37 877-09-804/24/12 15:0539-110 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 19:41 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 19:41 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 19:41 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 19:41 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 19:41 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 19:41 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 19:41 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene 0.10 ug/L 1 04/25/12 19:41 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 19:41 218-01-904/24/12 10:000.52 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 19:41 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 19:41 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 19:41 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 19:41 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 19:41 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 19:41 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 19:41 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 19:41 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)59 %.1 04/25/12 19:41 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)90 %.1 04/25/12 19:41 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 04:10 100-51-604/24/12 10:0020.6 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 04:10 101-55-304/24/12 10:0010.3 Butylbenzylphthalate ND ug/L 1 04/25/12 04:10 85-68-704/24/12 10:0010.3 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 04:10 59-50-704/24/12 10:0020.6 4-Chloroaniline ND ug/L 1 04/25/12 04:10 106-47-804/24/12 10:0020.6 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 04:10 111-91-104/24/12 10:0010.3 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 04:10 111-44-404/24/12 10:0010.3 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 04:10 108-60-104/24/12 10:005.2 2-Chloronaphthalene ND ug/L 1 04/25/12 04:10 91-58-704/24/12 10:0010.3 2-Chlorophenol ND ug/L 1 04/25/12 04:10 95-57-804/24/12 10:0010.3 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 04:10 7005-72-304/24/12 10:0010.3 Dibenzofuran ND ug/L 1 04/25/12 04:10 132-64-904/24/12 10:0010.3 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 04:10 91-94-104/24/12 10:0020.6 2,4-Dichlorophenol ND ug/L 1 04/25/12 04:10 120-83-204/24/12 10:0010.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 14 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390 Lab ID:5061800004 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate ND ug/L 1 04/25/12 04:10 84-66-204/24/12 10:0010.3 2,4-Dimethylphenol ND ug/L 1 04/25/12 04:10 105-67-904/24/12 10:0010.3 Dimethylphthalate ND ug/L 1 04/25/12 04:10 131-11-304/24/12 10:0010.3 Di-n-butylphthalate ND ug/L 1 04/25/12 04:10 84-74-204/24/12 10:0010.3 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 04:10 534-52-104/24/12 10:0051.5 2,4-Dinitrophenol ND ug/L 1 04/25/12 04:10 51-28-504/24/12 10:0051.5 2,4-Dinitrotoluene ND ug/L 1 04/25/12 04:10 121-14-204/24/12 10:0010.3 2,6-Dinitrotoluene ND ug/L 1 04/25/12 04:10 606-20-204/24/12 10:0010.3 Di-n-octylphthalate ND ug/L 1 04/25/12 04:10 117-84-004/24/12 10:0010.3 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 04:10 117-81-704/24/12 10:005.2 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 04:10 87-68-304/24/12 10:005.2 Hexachlorobenzene ND ug/L 1 04/25/12 04:10 118-74-104/24/12 10:0010.3 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 04:10 77-47-404/24/12 10:0025.8 Hexachloroethane ND ug/L 1 04/25/12 04:10 67-72-104/24/12 10:0010.3 Isophorone ND ug/L 1 04/25/12 04:10 78-59-104/24/12 10:0010.3 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 04:10 95-48-704/24/12 10:0010.3 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 04:1004/24/12 10:0020.6 2-Nitroaniline ND ug/L 1 04/25/12 04:10 88-74-404/24/12 10:0051.5 3-Nitroaniline ND ug/L 1 04/25/12 04:10 99-09-204/24/12 10:0051.5 4-Nitroaniline ND ug/L 1 04/25/12 04:10 100-01-604/24/12 10:0051.5 Nitrobenzene ND ug/L 1 04/25/12 04:10 98-95-304/24/12 10:0010.3 2-Nitrophenol ND ug/L 1 04/25/12 04:10 88-75-504/24/12 10:0010.3 4-Nitrophenol ND ug/L 1 04/25/12 04:10 100-02-704/24/12 10:0051.5 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 04:10 621-64-704/24/12 10:0010.3 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 04:10 86-30-604/24/12 10:0010.3 Pentachlorophenol ND ug/L 1 04/25/12 04:10 87-86-504/24/12 10:0051.5 Phenol ND ug/L 1 04/25/12 04:10 108-95-204/24/12 10:0010.3 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 04:10 95-95-404/24/12 10:0010.3 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 04:10 88-06-204/24/12 10:0010.3 Surrogates Nitrobenzene-d5 (S)63 %.1 04/25/12 04:10 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)16 %.1 04/25/12 04:10 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)28 %.1 04/25/12 04:10 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)88 %.1 04/25/12 04:10 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 03:57 67-64-1100 Acrolein ND ug/L 1 04/24/12 03:57 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 03:57 107-13-1100 Benzene ND ug/L 1 04/24/12 03:57 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 03:57 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 03:57 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 03:57 75-27-45.0 Bromoform ND ug/L 1 04/24/12 03:57 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 03:57 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 03:57 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 03:57 104-51-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 15 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390 Lab ID:5061800004 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 sec-Butylbenzene ND ug/L 1 04/24/12 03:57 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 03:57 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 03:57 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 03:57 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 03:57 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 03:57 75-00-35.0 Chloroform ND ug/L 1 04/24/12 03:57 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 03:57 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 03:57 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 03:57 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 03:57 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 03:57 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 03:57 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 03:57 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 03:57 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 03:57 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 03:57 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 03:57 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 03:57 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 03:57 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 03:57 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 03:57 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 03:57 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 03:57 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 03:57 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 03:57 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 03:57 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 03:57 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 03:57 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 03:57 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 03:57 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 03:57 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 03:57 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 03:57 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 03:57 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 03:57 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 03:57 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 03:57 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 03:57 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 03:57 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 03:57 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 03:57 103-65-15.0 Styrene ND ug/L 1 04/24/12 03:57 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 03:57 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 03:57 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 03:57 127-18-45.0 Toluene ND ug/L 1 04/24/12 03:57 108-88-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 16 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390 Lab ID:5061800004 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 03:57 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 03:57 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 03:57 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 03:57 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 03:57 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 03:57 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 03:57 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 03:57 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 03:57 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 03:57 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 03:57 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 03:57 1330-20-710.0 Surrogates Dibromofluoromethane (S)105 %.1 04/24/12 03:57 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/24/12 03:57 460-00-472-125 Toluene-d8 (S)92 %.1 04/24/12 03:57 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 17 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390A Lab ID:5061800005 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 19:59 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 19:59 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 19:59 120-12-704/24/12 10:000.10 Benzo(a)anthracene 0.12 ug/L 1 04/25/12 19:59 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 19:59 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene 0.11 ug/L 1 04/25/12 19:59 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene 0.13 ug/L 1 04/25/12 19:59 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene 0.15 ug/L 1 04/25/12 19:59 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 19:59 218-01-904/24/12 10:000.51 Dibenz(a,h)anthracene 0.13 ug/L 1 04/25/12 19:59 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 19:59 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 19:59 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene 0.13 ug/L 1 04/25/12 19:59 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 19:59 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 19:59 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 19:59 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 19:59 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)59 %.1 04/25/12 19:59 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)91 %.1 04/25/12 19:59 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 04:30 100-51-604/24/12 10:0020.4 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 04:30 101-55-304/24/12 10:0010.2 Butylbenzylphthalate ND ug/L 1 04/25/12 04:30 85-68-704/24/12 10:0010.2 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 04:30 59-50-704/24/12 10:0020.4 4-Chloroaniline ND ug/L 1 04/25/12 04:30 106-47-804/24/12 10:0020.4 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 04:30 111-91-104/24/12 10:0010.2 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 04:30 111-44-404/24/12 10:0010.2 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 04:30 108-60-104/24/12 10:005.1 2-Chloronaphthalene ND ug/L 1 04/25/12 04:30 91-58-704/24/12 10:0010.2 2-Chlorophenol ND ug/L 1 04/25/12 04:30 95-57-804/24/12 10:0010.2 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 04:30 7005-72-304/24/12 10:0010.2 Dibenzofuran ND ug/L 1 04/25/12 04:30 132-64-904/24/12 10:0010.2 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 04:30 91-94-104/24/12 10:0020.4 2,4-Dichlorophenol ND ug/L 1 04/25/12 04:30 120-83-204/24/12 10:0010.2 Diethylphthalate ND ug/L 1 04/25/12 04:30 84-66-204/24/12 10:0010.2 2,4-Dimethylphenol ND ug/L 1 04/25/12 04:30 105-67-904/24/12 10:0010.2 Dimethylphthalate ND ug/L 1 04/25/12 04:30 131-11-304/24/12 10:0010.2 Di-n-butylphthalate ND ug/L 1 04/25/12 04:30 84-74-204/24/12 10:0010.2 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 04:30 534-52-104/24/12 10:0051.0 2,4-Dinitrophenol ND ug/L 1 04/25/12 04:30 51-28-504/24/12 10:0051.0 2,4-Dinitrotoluene ND ug/L 1 04/25/12 04:30 121-14-204/24/12 10:0010.2 2,6-Dinitrotoluene ND ug/L 1 04/25/12 04:30 606-20-204/24/12 10:0010.2 Di-n-octylphthalate ND ug/L 1 04/25/12 04:30 117-84-004/24/12 10:0010.2 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 04:30 117-81-704/24/12 10:005.1 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 04:30 87-68-304/24/12 10:005.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 18 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G350390A Lab ID:5061800005 Collected:04/19/12 14:50 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/25/12 04:30 118-74-104/24/12 10:0010.2 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 04:30 77-47-404/24/12 10:0025.5 Hexachloroethane ND ug/L 1 04/25/12 04:30 67-72-104/24/12 10:0010.2 Isophorone ND ug/L 1 04/25/12 04:30 78-59-104/24/12 10:0010.2 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 04:30 95-48-704/24/12 10:0010.2 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 04:3004/24/12 10:0020.4 2-Nitroaniline ND ug/L 1 04/25/12 04:30 88-74-404/24/12 10:0051.0 3-Nitroaniline ND ug/L 1 04/25/12 04:30 99-09-204/24/12 10:0051.0 4-Nitroaniline ND ug/L 1 04/25/12 04:30 100-01-604/24/12 10:0051.0 Nitrobenzene ND ug/L 1 04/25/12 04:30 98-95-304/24/12 10:0010.2 2-Nitrophenol ND ug/L 1 04/25/12 04:30 88-75-504/24/12 10:0010.2 4-Nitrophenol ND ug/L 1 04/25/12 04:30 100-02-704/24/12 10:0051.0 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 04:30 621-64-704/24/12 10:0010.2 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 04:30 86-30-604/24/12 10:0010.2 Pentachlorophenol ND ug/L 1 04/25/12 04:30 87-86-504/24/12 10:0051.0 Phenol ND ug/L 1 04/25/12 04:30 108-95-204/24/12 10:0010.2 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 04:30 95-95-404/24/12 10:0010.2 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 04:30 88-06-204/24/12 10:0010.2 Surrogates Nitrobenzene-d5 (S)62 %.1 04/25/12 04:30 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)17 %.1 04/25/12 04:30 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)29 %.1 04/25/12 04:30 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)84 %.1 04/25/12 04:30 118-79-604/24/12 10:0032-124 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 19 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G260300 Lab ID:5061800006 Collected:04/19/12 15:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:43 12674-11-204/24/12 15:050.51 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:43 11104-28-204/24/12 15:050.51 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:43 11141-16-504/24/12 15:050.51 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:43 53469-21-904/24/12 15:050.51 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:43 12672-29-604/24/12 15:050.51 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:43 11097-69-104/24/12 15:050.51 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:43 11096-82-504/24/12 15:050.51 Surrogates Tetrachloro-m-xylene (S)78 %.1 04/24/12 18:43 877-09-804/24/12 15:0539-110 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 20:17 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 20:17 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 20:17 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 20:17 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 20:17 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 20:17 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 20:17 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene ND ug/L 1 04/25/12 20:17 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 20:17 218-01-904/24/12 10:000.52 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 20:17 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 20:17 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 20:17 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 20:17 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 20:17 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 20:17 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 20:17 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 20:17 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)56 %.1 04/25/12 20:17 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)86 %.1 04/25/12 20:17 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 04:51 100-51-604/24/12 10:0020.8 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 04:51 101-55-304/24/12 10:0010.4 Butylbenzylphthalate ND ug/L 1 04/25/12 04:51 85-68-704/24/12 10:0010.4 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 04:51 59-50-704/24/12 10:0020.8 4-Chloroaniline ND ug/L 1 04/25/12 04:51 106-47-804/24/12 10:0020.8 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 04:51 111-91-104/24/12 10:0010.4 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 04:51 111-44-404/24/12 10:0010.4 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 04:51 108-60-104/24/12 10:005.2 2-Chloronaphthalene ND ug/L 1 04/25/12 04:51 91-58-704/24/12 10:0010.4 2-Chlorophenol ND ug/L 1 04/25/12 04:51 95-57-804/24/12 10:0010.4 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 04:51 7005-72-304/24/12 10:0010.4 Dibenzofuran ND ug/L 1 04/25/12 04:51 132-64-904/24/12 10:0010.4 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 04:51 91-94-104/24/12 10:0020.8 2,4-Dichlorophenol ND ug/L 1 04/25/12 04:51 120-83-204/24/12 10:0010.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 20 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G260300 Lab ID:5061800006 Collected:04/19/12 15:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate ND ug/L 1 04/25/12 04:51 84-66-204/24/12 10:0010.4 2,4-Dimethylphenol ND ug/L 1 04/25/12 04:51 105-67-904/24/12 10:0010.4 Dimethylphthalate ND ug/L 1 04/25/12 04:51 131-11-304/24/12 10:0010.4 Di-n-butylphthalate ND ug/L 1 04/25/12 04:51 84-74-204/24/12 10:0010.4 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 04:51 534-52-104/24/12 10:0052.1 2,4-Dinitrophenol ND ug/L 1 04/25/12 04:51 51-28-504/24/12 10:0052.1 2,4-Dinitrotoluene ND ug/L 1 04/25/12 04:51 121-14-204/24/12 10:0010.4 2,6-Dinitrotoluene ND ug/L 1 04/25/12 04:51 606-20-204/24/12 10:0010.4 Di-n-octylphthalate ND ug/L 1 04/25/12 04:51 117-84-004/24/12 10:0010.4 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 04:51 117-81-704/24/12 10:005.2 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 04:51 87-68-304/24/12 10:005.2 Hexachlorobenzene ND ug/L 1 04/25/12 04:51 118-74-104/24/12 10:0010.4 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 04:51 77-47-404/24/12 10:0026.0 Hexachloroethane ND ug/L 1 04/25/12 04:51 67-72-104/24/12 10:0010.4 Isophorone ND ug/L 1 04/25/12 04:51 78-59-104/24/12 10:0010.4 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 04:51 95-48-704/24/12 10:0010.4 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 04:5104/24/12 10:0020.8 2-Nitroaniline ND ug/L 1 04/25/12 04:51 88-74-404/24/12 10:0052.1 3-Nitroaniline ND ug/L 1 04/25/12 04:51 99-09-204/24/12 10:0052.1 4-Nitroaniline ND ug/L 1 04/25/12 04:51 100-01-604/24/12 10:0052.1 Nitrobenzene ND ug/L 1 04/25/12 04:51 98-95-304/24/12 10:0010.4 2-Nitrophenol ND ug/L 1 04/25/12 04:51 88-75-504/24/12 10:0010.4 4-Nitrophenol ND ug/L 1 04/25/12 04:51 100-02-704/24/12 10:0052.1 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 04:51 621-64-704/24/12 10:0010.4 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 04:51 86-30-604/24/12 10:0010.4 Pentachlorophenol ND ug/L 1 04/25/12 04:51 87-86-504/24/12 10:0052.1 Phenol ND ug/L 1 04/25/12 04:51 108-95-204/24/12 10:0010.4 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 04:51 95-95-404/24/12 10:0010.4 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 04:51 88-06-204/24/12 10:0010.4 Surrogates Nitrobenzene-d5 (S)55 %.1 04/25/12 04:51 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)16 %.1 04/25/12 04:51 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)27 %.1 04/25/12 04:51 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)71 %.1 04/25/12 04:51 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 04:31 67-64-1100 Acrolein ND ug/L 1 04/24/12 04:31 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 04:31 107-13-1100 Benzene ND ug/L 1 04/24/12 04:31 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 04:31 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 04:31 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 04:31 75-27-45.0 Bromoform ND ug/L 1 04/24/12 04:31 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 04:31 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 04:31 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 04:31 104-51-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 21 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G260300 Lab ID:5061800006 Collected:04/19/12 15:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 sec-Butylbenzene ND ug/L 1 04/24/12 04:31 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 04:31 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 04:31 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 04:31 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 04:31 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 04:31 75-00-35.0 Chloroform ND ug/L 1 04/24/12 04:31 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 04:31 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 04:31 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 04:31 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 04:31 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 04:31 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 04:31 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 04:31 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 04:31 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 04:31 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 04:31 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 04:31 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 04:31 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 04:31 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 04:31 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 04:31 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 04:31 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 04:31 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 04:31 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 04:31 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 04:31 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 04:31 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 04:31 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 04:31 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 04:31 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 04:31 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 04:31 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 04:31 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 04:31 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 04:31 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 04:31 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 04:31 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 04:31 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 04:31 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 04:31 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 04:31 103-65-15.0 Styrene ND ug/L 1 04/24/12 04:31 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 04:31 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 04:31 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 04:31 127-18-45.0 Toluene ND ug/L 1 04/24/12 04:31 108-88-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 22 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB18:G260300 Lab ID:5061800006 Collected:04/19/12 15:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 04:31 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 04:31 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 04:31 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 04:31 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 04:31 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 04:31 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 04:31 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 04:31 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 04:31 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 04:31 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 04:31 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 04:31 1330-20-710.0 Surrogates Dibromofluoromethane (S)112 %.1 04/24/12 04:31 1868-53-783-123 4-Bromofluorobenzene (S)107 %.1 04/24/12 04:31 460-00-472-125 Toluene-d8 (S)91 %.1 04/24/12 04:31 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 23 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W041912 Lab ID:5061800007 Collected:04/19/12 17:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016)ND ug/L 1 04/24/12 18:49 12674-11-204/24/12 15:050.52 PCB-1221 (Aroclor 1221)ND ug/L 1 04/24/12 18:49 11104-28-204/24/12 15:050.52 PCB-1232 (Aroclor 1232)ND ug/L 1 04/24/12 18:49 11141-16-504/24/12 15:050.52 PCB-1242 (Aroclor 1242)ND ug/L 1 04/24/12 18:49 53469-21-904/24/12 15:050.52 PCB-1248 (Aroclor 1248)ND ug/L 1 04/24/12 18:49 12672-29-604/24/12 15:050.52 PCB-1254 (Aroclor 1254)ND ug/L 1 04/24/12 18:49 11097-69-104/24/12 15:050.52 PCB-1260 (Aroclor 1260)ND ug/L 1 04/24/12 18:49 11096-82-504/24/12 15:050.52 Surrogates Tetrachloro-m-xylene (S)93 %.1 04/24/12 18:49 877-09-804/24/12 15:0539-110 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 21:12 83-32-904/24/12 10:001.1 Acenaphthylene ND ug/L 1 04/25/12 21:12 208-96-804/24/12 10:001.1 Anthracene ND ug/L 1 04/25/12 21:12 120-12-704/24/12 10:000.11 Benzo(a)anthracene ND ug/L 1 04/25/12 21:12 56-55-304/24/12 10:000.11 Benzo(a)pyrene ND ug/L 1 04/25/12 21:12 50-32-804/24/12 10:000.11 Benzo(b)fluoranthene ND ug/L 1 04/25/12 21:12 205-99-204/24/12 10:000.11 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 21:12 191-24-204/24/12 10:000.11 Benzo(k)fluoranthene ND ug/L 1 04/25/12 21:12 207-08-904/24/12 10:000.11 Chrysene ND ug/L 1 04/25/12 21:12 218-01-904/24/12 10:000.53 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 21:12 53-70-304/24/12 10:000.11 Fluoranthene ND ug/L 1 04/25/12 21:12 206-44-004/24/12 10:001.1 Fluorene ND ug/L 1 04/25/12 21:12 86-73-704/24/12 10:001.1 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 21:12 193-39-504/24/12 10:000.11 2-Methylnaphthalene ND ug/L 1 04/25/12 21:12 91-57-604/24/12 10:001.1 Naphthalene ND ug/L 1 04/25/12 21:12 91-20-304/24/12 10:001.1 Phenanthrene ND ug/L 1 04/25/12 21:12 85-01-804/24/12 10:001.1 Pyrene ND ug/L 1 04/25/12 21:12 129-00-004/24/12 10:001.1 Surrogates 2-Fluorobiphenyl (S)68 %.1 04/25/12 21:12 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)92 %.1 04/25/12 21:12 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 05:53 100-51-604/24/12 10:0021.1 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 05:53 101-55-304/24/12 10:0010.5 Butylbenzylphthalate ND ug/L 1 04/25/12 05:53 85-68-704/24/12 10:0010.5 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 05:53 59-50-704/24/12 10:0021.1 4-Chloroaniline ND ug/L 1 04/25/12 05:53 106-47-804/24/12 10:0021.1 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 05:53 111-91-104/24/12 10:0010.5 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 05:53 111-44-404/24/12 10:0010.5 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 05:53 108-60-104/24/12 10:005.3 2-Chloronaphthalene ND ug/L 1 04/25/12 05:53 91-58-704/24/12 10:0010.5 2-Chlorophenol ND ug/L 1 04/25/12 05:53 95-57-804/24/12 10:0010.5 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 05:53 7005-72-304/24/12 10:0010.5 Dibenzofuran ND ug/L 1 04/25/12 05:53 132-64-904/24/12 10:0010.5 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 05:53 91-94-104/24/12 10:0021.1 2,4-Dichlorophenol ND ug/L 1 04/25/12 05:53 120-83-204/24/12 10:0010.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 24 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W041912 Lab ID:5061800007 Collected:04/19/12 17:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate ND ug/L 1 04/25/12 05:53 84-66-204/24/12 10:0010.5 2,4-Dimethylphenol ND ug/L 1 04/25/12 05:53 105-67-904/24/12 10:0010.5 Dimethylphthalate ND ug/L 1 04/25/12 05:53 131-11-304/24/12 10:0010.5 Di-n-butylphthalate ND ug/L 1 04/25/12 05:53 84-74-204/24/12 10:0010.5 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 05:53 534-52-104/24/12 10:0052.6 2,4-Dinitrophenol ND ug/L 1 04/25/12 05:53 51-28-504/24/12 10:0052.6 2,4-Dinitrotoluene ND ug/L 1 04/25/12 05:53 121-14-204/24/12 10:0010.5 2,6-Dinitrotoluene ND ug/L 1 04/25/12 05:53 606-20-204/24/12 10:0010.5 Di-n-octylphthalate ND ug/L 1 04/25/12 05:53 117-84-004/24/12 10:0010.5 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 05:53 117-81-704/24/12 10:005.3 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 05:53 87-68-304/24/12 10:005.3 Hexachlorobenzene ND ug/L 1 04/25/12 05:53 118-74-104/24/12 10:0010.5 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 05:53 77-47-404/24/12 10:0026.3 Hexachloroethane ND ug/L 1 04/25/12 05:53 67-72-104/24/12 10:0010.5 Isophorone ND ug/L 1 04/25/12 05:53 78-59-104/24/12 10:0010.5 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 05:53 95-48-704/24/12 10:0010.5 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 05:5304/24/12 10:0021.1 2-Nitroaniline ND ug/L 1 04/25/12 05:53 88-74-404/24/12 10:0052.6 3-Nitroaniline ND ug/L 1 04/25/12 05:53 99-09-204/24/12 10:0052.6 4-Nitroaniline ND ug/L 1 04/25/12 05:53 100-01-604/24/12 10:0052.6 Nitrobenzene ND ug/L 1 04/25/12 05:53 98-95-304/24/12 10:0010.5 2-Nitrophenol ND ug/L 1 04/25/12 05:53 88-75-504/24/12 10:0010.5 4-Nitrophenol ND ug/L 1 04/25/12 05:53 100-02-704/24/12 10:0052.6 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 05:53 621-64-704/24/12 10:0010.5 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 05:53 86-30-604/24/12 10:0010.5 Pentachlorophenol ND ug/L 1 04/25/12 05:53 87-86-504/24/12 10:0052.6 Phenol ND ug/L 1 04/25/12 05:53 108-95-204/24/12 10:0010.5 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 05:53 95-95-404/24/12 10:0010.5 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 05:53 88-06-204/24/12 10:0010.5 Surrogates Nitrobenzene-d5 (S)80 %.1 04/25/12 05:53 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)22 %.1 04/25/12 05:53 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)39 %.1 04/25/12 05:53 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)101 %.1 04/25/12 05:53 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 06:14 67-64-1100 Acrolein ND ug/L 1 04/24/12 06:14 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 06:14 107-13-1100 Benzene ND ug/L 1 04/24/12 06:14 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 06:14 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 06:14 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 06:14 75-27-45.0 Bromoform ND ug/L 1 04/24/12 06:14 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 06:14 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 06:14 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 06:14 104-51-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 25 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W041912 Lab ID:5061800007 Collected:04/19/12 17:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 sec-Butylbenzene ND ug/L 1 04/24/12 06:14 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 06:14 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 06:14 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 06:14 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 06:14 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 06:14 75-00-35.0 Chloroform ND ug/L 1 04/24/12 06:14 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 06:14 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 06:14 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 06:14 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 06:14 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 06:14 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 06:14 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 06:14 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 06:14 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 06:14 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 06:14 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 06:14 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 06:14 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 06:14 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 06:14 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 06:14 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 06:14 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 06:14 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 06:14 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 06:14 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 06:14 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 06:14 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 06:14 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 06:14 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 06:14 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 06:14 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 06:14 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 06:14 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 06:14 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 06:14 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 06:14 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 06:14 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 06:14 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 06:14 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 06:14 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 06:14 103-65-15.0 Styrene ND ug/L 1 04/24/12 06:14 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 06:14 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 06:14 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 06:14 127-18-45.0 Toluene ND ug/L 1 04/24/12 06:14 108-88-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 26 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W041912 Lab ID:5061800007 Collected:04/19/12 17:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 06:14 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 06:14 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 06:14 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 06:14 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 06:14 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 06:14 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 06:14 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 06:14 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 06:14 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 06:14 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 06:14 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 06:14 1330-20-710.0 Surrogates Dibromofluoromethane (S)106 %.1 04/24/12 06:14 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/24/12 06:14 460-00-472-125 Toluene-d8 (S)92 %.1 04/24/12 06:14 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 27 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G350390 Lab ID:5061800008 Collected:04/20/12 08:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 21:30 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 21:30 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 21:30 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 21:30 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 21:30 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 21:30 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 21:30 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene ND ug/L 1 04/25/12 21:30 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 21:30 218-01-904/24/12 10:000.52 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 21:30 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 21:30 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 21:30 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 21:30 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 21:30 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 21:30 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 21:30 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 21:30 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)66 %.1 04/25/12 21:30 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)87 %.1 04/25/12 21:30 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 06:14 100-51-604/24/12 10:0020.8 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 06:14 101-55-304/24/12 10:0010.4 Butylbenzylphthalate ND ug/L 1 04/25/12 06:14 85-68-704/24/12 10:0010.4 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 06:14 59-50-704/24/12 10:0020.8 4-Chloroaniline ND ug/L 1 04/25/12 06:14 106-47-804/24/12 10:0020.8 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 06:14 111-91-104/24/12 10:0010.4 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 06:14 111-44-404/24/12 10:0010.4 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 06:14 108-60-104/24/12 10:005.2 2-Chloronaphthalene ND ug/L 1 04/25/12 06:14 91-58-704/24/12 10:0010.4 2-Chlorophenol ND ug/L 1 04/25/12 06:14 95-57-804/24/12 10:0010.4 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 06:14 7005-72-304/24/12 10:0010.4 Dibenzofuran ND ug/L 1 04/25/12 06:14 132-64-904/24/12 10:0010.4 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 06:14 91-94-104/24/12 10:0020.8 2,4-Dichlorophenol ND ug/L 1 04/25/12 06:14 120-83-204/24/12 10:0010.4 Diethylphthalate ND ug/L 1 04/25/12 06:14 84-66-204/24/12 10:0010.4 2,4-Dimethylphenol ND ug/L 1 04/25/12 06:14 105-67-904/24/12 10:0010.4 Dimethylphthalate ND ug/L 1 04/25/12 06:14 131-11-304/24/12 10:0010.4 Di-n-butylphthalate ND ug/L 1 04/25/12 06:14 84-74-204/24/12 10:0010.4 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 06:14 534-52-104/24/12 10:0052.1 2,4-Dinitrophenol ND ug/L 1 04/25/12 06:14 51-28-504/24/12 10:0052.1 2,4-Dinitrotoluene ND ug/L 1 04/25/12 06:14 121-14-204/24/12 10:0010.4 2,6-Dinitrotoluene ND ug/L 1 04/25/12 06:14 606-20-204/24/12 10:0010.4 Di-n-octylphthalate ND ug/L 1 04/25/12 06:14 117-84-004/24/12 10:0010.4 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 06:14 117-81-704/24/12 10:005.2 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 06:14 87-68-304/24/12 10:005.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 28 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G350390 Lab ID:5061800008 Collected:04/20/12 08:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/25/12 06:14 118-74-104/24/12 10:0010.4 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 06:14 77-47-404/24/12 10:0026.0 Hexachloroethane ND ug/L 1 04/25/12 06:14 67-72-104/24/12 10:0010.4 Isophorone ND ug/L 1 04/25/12 06:14 78-59-104/24/12 10:0010.4 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 06:14 95-48-704/24/12 10:0010.4 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 06:1404/24/12 10:0020.8 2-Nitroaniline ND ug/L 1 04/25/12 06:14 88-74-404/24/12 10:0052.1 3-Nitroaniline ND ug/L 1 04/25/12 06:14 99-09-204/24/12 10:0052.1 4-Nitroaniline ND ug/L 1 04/25/12 06:14 100-01-604/24/12 10:0052.1 Nitrobenzene ND ug/L 1 04/25/12 06:14 98-95-304/24/12 10:0010.4 2-Nitrophenol ND ug/L 1 04/25/12 06:14 88-75-504/24/12 10:0010.4 4-Nitrophenol ND ug/L 1 04/25/12 06:14 100-02-704/24/12 10:0052.1 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 06:14 621-64-704/24/12 10:0010.4 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 06:14 86-30-604/24/12 10:0010.4 Pentachlorophenol ND ug/L 1 04/25/12 06:14 87-86-504/24/12 10:0052.1 Phenol ND ug/L 1 04/25/12 06:14 108-95-204/24/12 10:0010.4 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 06:14 95-95-404/24/12 10:0010.4 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 06:14 88-06-204/24/12 10:0010.4 Surrogates Nitrobenzene-d5 (S)77 %.1 04/25/12 06:14 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)17 %.1 04/25/12 06:14 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)30 %.1 04/25/12 06:14 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)101 %.1 04/25/12 06:14 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 20:01 67-64-1100 Acrolein ND ug/L 1 04/24/12 20:01 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 20:01 107-13-1100 Benzene ND ug/L 1 04/24/12 20:01 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 20:01 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 20:01 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 20:01 75-27-45.0 Bromoform ND ug/L 1 04/24/12 20:01 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 20:01 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 20:01 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 20:01 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/24/12 20:01 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 20:01 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 20:01 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 20:01 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 20:01 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 20:01 75-00-35.0 Chloroform ND ug/L 1 04/24/12 20:01 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 20:01 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 20:01 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 20:01 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 20:01 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 29 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G350390 Lab ID:5061800008 Collected:04/20/12 08:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 20:01 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 20:01 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 20:01 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 20:01 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 20:01 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 20:01 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 20:01 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 20:01 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 20:01 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 20:01 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 20:01 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 20:01 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 20:01 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 20:01 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 20:01 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 20:01 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 20:01 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 20:01 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 20:01 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 20:01 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 20:01 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 20:01 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 20:01 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 20:01 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 20:01 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 20:01 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 20:01 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 20:01 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 20:01 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 20:01 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 20:01 103-65-15.0 Styrene ND ug/L 1 04/24/12 20:01 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 20:01 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 20:01 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 20:01 127-18-45.0 Toluene ND ug/L 1 04/24/12 20:01 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 20:01 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 20:01 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 20:01 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 20:01 79-00-55.0 Trichloroethene 6.4 ug/L 1 04/24/12 20:01 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 20:01 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 20:01 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 20:01 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 20:01 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 20:01 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 20:01 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 30 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G350390 Lab ID:5061800008 Collected:04/20/12 08:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/24/12 20:01 1330-20-710.0 Surrogates Dibromofluoromethane (S)99 %.1 04/24/12 20:01 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/24/12 20:01 460-00-472-125 Toluene-d8 (S)102 %.1 04/24/12 20:01 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 31 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300 Lab ID:5061800009 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 22:24 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 22:24 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 22:24 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 22:24 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 22:24 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 22:24 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 22:24 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene ND ug/L 1 04/25/12 22:24 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 22:24 218-01-904/24/12 10:000.51 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 22:24 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 22:24 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 22:24 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 22:24 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 22:24 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 22:24 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 22:24 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 22:24 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)55 %.1 04/25/12 22:24 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)92 %.1 04/25/12 22:24 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 07:16 100-51-604/24/12 10:0020.4 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 07:16 101-55-304/24/12 10:0010.2 Butylbenzylphthalate ND ug/L 1 04/25/12 07:16 85-68-704/24/12 10:0010.2 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 07:16 59-50-704/24/12 10:0020.4 4-Chloroaniline ND ug/L 1 04/25/12 07:16 106-47-804/24/12 10:0020.4 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 07:16 111-91-104/24/12 10:0010.2 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 07:16 111-44-404/24/12 10:0010.2 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 07:16 108-60-104/24/12 10:005.1 2-Chloronaphthalene ND ug/L 1 04/25/12 07:16 91-58-704/24/12 10:0010.2 2-Chlorophenol ND ug/L 1 04/25/12 07:16 95-57-804/24/12 10:0010.2 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 07:16 7005-72-304/24/12 10:0010.2 Dibenzofuran ND ug/L 1 04/25/12 07:16 132-64-904/24/12 10:0010.2 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 07:16 91-94-104/24/12 10:0020.4 2,4-Dichlorophenol ND ug/L 1 04/25/12 07:16 120-83-204/24/12 10:0010.2 Diethylphthalate ND ug/L 1 04/25/12 07:16 84-66-204/24/12 10:0010.2 2,4-Dimethylphenol ND ug/L 1 04/25/12 07:16 105-67-904/24/12 10:0010.2 Dimethylphthalate ND ug/L 1 04/25/12 07:16 131-11-304/24/12 10:0010.2 Di-n-butylphthalate ND ug/L 1 04/25/12 07:16 84-74-204/24/12 10:0010.2 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 07:16 534-52-104/24/12 10:0051.0 2,4-Dinitrophenol ND ug/L 1 04/25/12 07:16 51-28-504/24/12 10:0051.0 2,4-Dinitrotoluene ND ug/L 1 04/25/12 07:16 121-14-204/24/12 10:0010.2 2,6-Dinitrotoluene ND ug/L 1 04/25/12 07:16 606-20-204/24/12 10:0010.2 Di-n-octylphthalate ND ug/L 1 04/25/12 07:16 117-84-004/24/12 10:0010.2 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 07:16 117-81-704/24/12 10:005.1 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 07:16 87-68-304/24/12 10:005.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 32 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300 Lab ID:5061800009 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/25/12 07:16 118-74-104/24/12 10:0010.2 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 07:16 77-47-404/24/12 10:0025.5 Hexachloroethane ND ug/L 1 04/25/12 07:16 67-72-104/24/12 10:0010.2 Isophorone ND ug/L 1 04/25/12 07:16 78-59-104/24/12 10:0010.2 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 07:16 95-48-704/24/12 10:0010.2 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 07:1604/24/12 10:0020.4 2-Nitroaniline ND ug/L 1 04/25/12 07:16 88-74-404/24/12 10:0051.0 3-Nitroaniline ND ug/L 1 04/25/12 07:16 99-09-204/24/12 10:0051.0 4-Nitroaniline ND ug/L 1 04/25/12 07:16 100-01-604/24/12 10:0051.0 Nitrobenzene ND ug/L 1 04/25/12 07:16 98-95-304/24/12 10:0010.2 2-Nitrophenol ND ug/L 1 04/25/12 07:16 88-75-504/24/12 10:0010.2 4-Nitrophenol ND ug/L 1 04/25/12 07:16 100-02-704/24/12 10:0051.0 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 07:16 621-64-704/24/12 10:0010.2 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 07:16 86-30-604/24/12 10:0010.2 Pentachlorophenol ND ug/L 1 04/25/12 07:16 87-86-504/24/12 10:0051.0 Phenol ND ug/L 1 04/25/12 07:16 108-95-204/24/12 10:0010.2 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 07:16 95-95-404/24/12 10:0010.2 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 07:16 88-06-204/24/12 10:0010.2 Surrogates Nitrobenzene-d5 (S)58 %.1 04/25/12 07:16 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)17 %.1 04/25/12 07:16 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)28 %.1 04/25/12 07:16 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)87 %.1 04/25/12 07:16 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 10:40 67-64-1100 Acrolein ND ug/L 1 04/25/12 10:40 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 10:40 107-13-1100 Benzene ND ug/L 1 04/25/12 10:40 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 10:40 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 10:40 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 10:40 75-27-45.0 Bromoform ND ug/L 1 04/25/12 10:40 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 10:40 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 10:40 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 10:40 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 10:40 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 10:40 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 10:40 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 10:40 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 10:40 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 10:40 75-00-35.0 Chloroform ND ug/L 1 04/25/12 10:40 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 10:40 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 10:40 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 10:40 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 10:40 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 33 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300 Lab ID:5061800009 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 10:40 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 10:40 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 10:40 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 10:40 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 10:40 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 10:40 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 10:40 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 10:40 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 10:40 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 10:40 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 10:40 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 10:40 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 10:40 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 10:40 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 10:40 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 10:40 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 10:40 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 10:40 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 10:40 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 10:40 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 10:40 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 10:40 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 10:40 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 10:40 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 10:40 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 10:40 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 10:40 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 10:40 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 10:40 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 10:40 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 10:40 103-65-15.0 Styrene ND ug/L 1 04/25/12 10:40 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 10:40 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 10:40 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 10:40 127-18-45.0 Toluene ND ug/L 1 04/25/12 10:40 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 10:40 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 10:40 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 10:40 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 10:40 79-00-55.0 Trichloroethene 6.4 ug/L 1 04/25/12 10:40 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 10:40 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 10:40 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 10:40 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 10:40 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 10:40 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 10:40 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 34 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300 Lab ID:5061800009 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 10:40 1330-20-710.0 Surrogates Dibromofluoromethane (S)106 %.1 04/25/12 10:40 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/25/12 10:40 460-00-472-125 Toluene-d8 (S)99 %.1 04/25/12 10:40 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 35 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300A Lab ID:5061800010 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 22:42 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 22:42 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 22:42 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 22:42 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 22:42 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 22:42 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 22:42 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene ND ug/L 1 04/25/12 22:42 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 22:42 218-01-904/24/12 10:000.51 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 22:42 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 22:42 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 22:42 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 22:42 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 22:42 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 22:42 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 22:42 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 22:42 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)68 %.1 04/25/12 22:42 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)94 %.1 04/25/12 22:42 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 07:36 100-51-604/24/12 10:0020.2 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 07:36 101-55-304/24/12 10:0010.1 Butylbenzylphthalate ND ug/L 1 04/25/12 07:36 85-68-704/24/12 10:0010.1 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 07:36 59-50-704/24/12 10:0020.2 4-Chloroaniline ND ug/L 1 04/25/12 07:36 106-47-804/24/12 10:0020.2 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 07:36 111-91-104/24/12 10:0010.1 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 07:36 111-44-404/24/12 10:0010.1 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 07:36 108-60-104/24/12 10:005.1 2-Chloronaphthalene ND ug/L 1 04/25/12 07:36 91-58-704/24/12 10:0010.1 2-Chlorophenol ND ug/L 1 04/25/12 07:36 95-57-804/24/12 10:0010.1 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 07:36 7005-72-304/24/12 10:0010.1 Dibenzofuran ND ug/L 1 04/25/12 07:36 132-64-904/24/12 10:0010.1 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 07:36 91-94-104/24/12 10:0020.2 2,4-Dichlorophenol ND ug/L 1 04/25/12 07:36 120-83-204/24/12 10:0010.1 Diethylphthalate ND ug/L 1 04/25/12 07:36 84-66-204/24/12 10:0010.1 2,4-Dimethylphenol ND ug/L 1 04/25/12 07:36 105-67-904/24/12 10:0010.1 Dimethylphthalate ND ug/L 1 04/25/12 07:36 131-11-304/24/12 10:0010.1 Di-n-butylphthalate ND ug/L 1 04/25/12 07:36 84-74-204/24/12 10:0010.1 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 07:36 534-52-104/24/12 10:0050.5 2,4-Dinitrophenol ND ug/L 1 04/25/12 07:36 51-28-504/24/12 10:0050.5 2,4-Dinitrotoluene ND ug/L 1 04/25/12 07:36 121-14-204/24/12 10:0010.1 2,6-Dinitrotoluene ND ug/L 1 04/25/12 07:36 606-20-204/24/12 10:0010.1 Di-n-octylphthalate ND ug/L 1 04/25/12 07:36 117-84-004/24/12 10:0010.1 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 07:36 117-81-704/24/12 10:005.1 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 07:36 87-68-304/24/12 10:005.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 36 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300A Lab ID:5061800010 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/25/12 07:36 118-74-104/24/12 10:0010.1 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 07:36 77-47-404/24/12 10:0025.3 Hexachloroethane ND ug/L 1 04/25/12 07:36 67-72-104/24/12 10:0010.1 Isophorone ND ug/L 1 04/25/12 07:36 78-59-104/24/12 10:0010.1 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 07:36 95-48-704/24/12 10:0010.1 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 07:3604/24/12 10:0020.2 2-Nitroaniline ND ug/L 1 04/25/12 07:36 88-74-404/24/12 10:0050.5 3-Nitroaniline ND ug/L 1 04/25/12 07:36 99-09-204/24/12 10:0050.5 4-Nitroaniline ND ug/L 1 04/25/12 07:36 100-01-604/24/12 10:0050.5 Nitrobenzene ND ug/L 1 04/25/12 07:36 98-95-304/24/12 10:0010.1 2-Nitrophenol ND ug/L 1 04/25/12 07:36 88-75-504/24/12 10:0010.1 4-Nitrophenol ND ug/L 1 04/25/12 07:36 100-02-704/24/12 10:0050.5 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 07:36 621-64-704/24/12 10:0010.1 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 07:36 86-30-604/24/12 10:0010.1 Pentachlorophenol ND ug/L 1 04/25/12 07:36 87-86-504/24/12 10:0050.5 Phenol ND ug/L 1 04/25/12 07:36 108-95-204/24/12 10:0010.1 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 07:36 95-95-404/24/12 10:0010.1 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 07:36 88-06-204/24/12 10:0010.1 Surrogates Nitrobenzene-d5 (S)76 %.1 04/25/12 07:36 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)20 %.1 04/25/12 07:36 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)36 %.1 04/25/12 07:36 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)96 %.1 04/25/12 07:36 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 11:14 67-64-1100 Acrolein ND ug/L 1 04/25/12 11:14 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 11:14 107-13-1100 Benzene ND ug/L 1 04/25/12 11:14 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 11:14 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 11:14 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 11:14 75-27-45.0 Bromoform ND ug/L 1 04/25/12 11:14 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 11:14 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 11:14 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 11:14 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 11:14 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 11:14 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 11:14 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 11:14 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 11:14 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 11:14 75-00-35.0 Chloroform ND ug/L 1 04/25/12 11:14 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 11:14 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 11:14 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 11:14 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 11:14 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 37 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300A Lab ID:5061800010 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 11:14 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 11:14 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 11:14 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 11:14 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 11:14 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 11:14 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 11:14 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 11:14 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 11:14 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 11:14 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 11:14 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 11:14 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 11:14 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 11:14 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 11:14 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 11:14 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 11:14 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 11:14 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 11:14 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 11:14 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 11:14 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 11:14 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 11:14 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 11:14 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 11:14 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 11:14 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 11:14 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 11:14 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 11:14 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 11:14 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 11:14 103-65-15.0 Styrene ND ug/L 1 04/25/12 11:14 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 11:14 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 11:14 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 11:14 127-18-45.0 Toluene ND ug/L 1 04/25/12 11:14 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 11:14 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 11:14 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 11:14 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 11:14 79-00-55.0 Trichloroethene 5.8 ug/L 1 04/25/12 11:14 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 11:14 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 11:14 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 11:14 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 11:14 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 11:14 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 11:14 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 38 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB5:G260300A Lab ID:5061800010 Collected:04/20/12 09:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 11:14 1330-20-710.0 Surrogates Dibromofluoromethane (S)98 %.1 04/25/12 11:14 1868-53-783-123 4-Bromofluorobenzene (S)105 %.1 04/25/12 11:14 460-00-472-125 Toluene-d8 (S)103 %.1 04/25/12 11:14 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 39 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G450490 Lab ID:5061800011 Collected:04/20/12 10:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 01:55 67-64-1100 Acrolein ND ug/L 1 04/25/12 01:55 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 01:55 107-13-1100 Benzene ND ug/L 1 04/25/12 01:55 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 01:55 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 01:55 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 01:55 75-27-45.0 Bromoform ND ug/L 1 04/25/12 01:55 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 01:55 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 01:55 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 01:55 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 01:55 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 01:55 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 01:55 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 01:55 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 01:55 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 01:55 75-00-35.0 Chloroform ND ug/L 1 04/25/12 01:55 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 01:55 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 01:55 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 01:55 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 01:55 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 01:55 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 01:55 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 01:55 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 01:55 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 01:55 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 01:55 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 01:55 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 01:55 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 01:55 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 01:55 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 01:55 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 01:55 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 01:55 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 01:55 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 01:55 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 01:55 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 01:55 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 01:55 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 01:55 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 01:55 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 01:55 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 01:55 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 01:55 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 01:55 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 01:55 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 40 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G450490 Lab ID:5061800011 Collected:04/20/12 10:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/25/12 01:55 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 01:55 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 01:55 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 01:55 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 01:55 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 01:55 103-65-15.0 Styrene ND ug/L 1 04/25/12 01:55 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 01:55 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 01:55 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 01:55 127-18-45.0 Toluene ND ug/L 1 04/25/12 01:55 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 01:55 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 01:55 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 01:55 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 01:55 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 01:55 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 01:55 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 01:55 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 01:55 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 01:55 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 01:55 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 01:55 75-01-42.0 Xylene (Total)ND ug/L 1 04/25/12 01:55 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/25/12 01:55 1868-53-783-123 4-Bromofluorobenzene (S)106 %.1 04/25/12 01:55 460-00-472-125 Toluene-d8 (S)103 %.1 04/25/12 01:55 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 41 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G350390 Lab ID:5061800012 Collected:04/20/12 11:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 02:29 67-64-1100 Acrolein ND ug/L 1 04/25/12 02:29 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 02:29 107-13-1100 Benzene ND ug/L 1 04/25/12 02:29 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 02:29 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 02:29 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 02:29 75-27-45.0 Bromoform ND ug/L 1 04/25/12 02:29 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 02:29 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 02:29 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 02:29 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 02:29 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 02:29 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 02:29 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 02:29 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 02:29 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 02:29 75-00-35.0 Chloroform ND ug/L 1 04/25/12 02:29 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 02:29 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 02:29 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 02:29 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 02:29 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 02:29 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 02:29 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 02:29 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 02:29 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 02:29 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 02:29 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 02:29 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 02:29 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 02:29 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 02:29 75-35-45.0 cis-1,2-Dichloroethene 19.7 ug/L 1 04/25/12 02:29 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 02:29 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 02:29 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 02:29 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 02:29 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 02:29 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 02:29 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 02:29 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 02:29 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 02:29 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 02:29 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 02:29 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 02:29 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 02:29 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 02:29 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 42 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G350390 Lab ID:5061800012 Collected:04/20/12 11:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/25/12 02:29 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 02:29 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 02:29 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 02:29 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 02:29 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 02:29 103-65-15.0 Styrene ND ug/L 1 04/25/12 02:29 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 02:29 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 02:29 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 02:29 127-18-45.0 Toluene ND ug/L 1 04/25/12 02:29 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 02:29 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 02:29 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 02:29 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 02:29 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 02:29 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 02:29 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 02:29 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 02:29 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 02:29 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 02:29 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 02:29 75-01-42.0 Xylene (Total)ND ug/L 1 04/25/12 02:29 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/25/12 02:29 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/25/12 02:29 460-00-472-125 Toluene-d8 (S)102 %.1 04/25/12 02:29 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 43 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W042012 Lab ID:5061800013 Collected:04/20/12 12:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/25/12 23:01 83-32-904/24/12 10:001.0 Acenaphthylene ND ug/L 1 04/25/12 23:01 208-96-804/24/12 10:001.0 Anthracene ND ug/L 1 04/25/12 23:01 120-12-704/24/12 10:000.10 Benzo(a)anthracene ND ug/L 1 04/25/12 23:01 56-55-304/24/12 10:000.10 Benzo(a)pyrene ND ug/L 1 04/25/12 23:01 50-32-804/24/12 10:000.10 Benzo(b)fluoranthene ND ug/L 1 04/25/12 23:01 205-99-204/24/12 10:000.10 Benzo(g,h,i)perylene ND ug/L 1 04/25/12 23:01 191-24-204/24/12 10:000.10 Benzo(k)fluoranthene ND ug/L 1 04/25/12 23:01 207-08-904/24/12 10:000.10 Chrysene ND ug/L 1 04/25/12 23:01 218-01-904/24/12 10:000.52 Dibenz(a,h)anthracene ND ug/L 1 04/25/12 23:01 53-70-304/24/12 10:000.10 Fluoranthene ND ug/L 1 04/25/12 23:01 206-44-004/24/12 10:001.0 Fluorene ND ug/L 1 04/25/12 23:01 86-73-704/24/12 10:001.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/25/12 23:01 193-39-504/24/12 10:000.10 2-Methylnaphthalene ND ug/L 1 04/25/12 23:01 91-57-604/24/12 10:001.0 Naphthalene ND ug/L 1 04/25/12 23:01 91-20-304/24/12 10:001.0 Phenanthrene ND ug/L 1 04/25/12 23:01 85-01-804/24/12 10:001.0 Pyrene ND ug/L 1 04/25/12 23:01 129-00-004/24/12 10:001.0 Surrogates 2-Fluorobiphenyl (S)70 %.1 04/25/12 23:01 321-60-804/24/12 10:0026-106 p-Terphenyl-d14 (S)85 %.1 04/25/12 23:01 1718-51-004/24/12 10:0016-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/25/12 07:57 100-51-604/24/12 10:0020.6 4-Bromophenylphenyl ether ND ug/L 1 04/25/12 07:57 101-55-304/24/12 10:0010.3 Butylbenzylphthalate ND ug/L 1 04/25/12 07:57 85-68-704/24/12 10:0010.3 4-Chloro-3-methylphenol ND ug/L 1 04/25/12 07:57 59-50-704/24/12 10:0020.6 4-Chloroaniline ND ug/L 1 04/25/12 07:57 106-47-804/24/12 10:0020.6 bis(2-Chloroethoxy)methane ND ug/L 1 04/25/12 07:57 111-91-104/24/12 10:0010.3 bis(2-Chloroethyl) ether ND ug/L 1 04/25/12 07:57 111-44-404/24/12 10:0010.3 bis(2chloro1methylethyl) ether ND ug/L 1 04/25/12 07:57 108-60-104/24/12 10:005.2 2-Chloronaphthalene ND ug/L 1 04/25/12 07:57 91-58-704/24/12 10:0010.3 2-Chlorophenol ND ug/L 1 04/25/12 07:57 95-57-804/24/12 10:0010.3 4-Chlorophenylphenyl ether ND ug/L 1 04/25/12 07:57 7005-72-304/24/12 10:0010.3 Dibenzofuran ND ug/L 1 04/25/12 07:57 132-64-904/24/12 10:0010.3 3,3'-Dichlorobenzidine ND ug/L 1 04/25/12 07:57 91-94-104/24/12 10:0020.6 2,4-Dichlorophenol ND ug/L 1 04/25/12 07:57 120-83-204/24/12 10:0010.3 Diethylphthalate ND ug/L 1 04/25/12 07:57 84-66-204/24/12 10:0010.3 2,4-Dimethylphenol ND ug/L 1 04/25/12 07:57 105-67-904/24/12 10:0010.3 Dimethylphthalate ND ug/L 1 04/25/12 07:57 131-11-304/24/12 10:0010.3 Di-n-butylphthalate ND ug/L 1 04/25/12 07:57 84-74-204/24/12 10:0010.3 4,6-Dinitro-2-methylphenol ND ug/L 1 04/25/12 07:57 534-52-104/24/12 10:0051.5 2,4-Dinitrophenol ND ug/L 1 04/25/12 07:57 51-28-504/24/12 10:0051.5 2,4-Dinitrotoluene ND ug/L 1 04/25/12 07:57 121-14-204/24/12 10:0010.3 2,6-Dinitrotoluene ND ug/L 1 04/25/12 07:57 606-20-204/24/12 10:0010.3 Di-n-octylphthalate ND ug/L 1 04/25/12 07:57 117-84-004/24/12 10:0010.3 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/25/12 07:57 117-81-704/24/12 10:005.2 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 07:57 87-68-304/24/12 10:005.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 44 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W042012 Lab ID:5061800013 Collected:04/20/12 12:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/25/12 07:57 118-74-104/24/12 10:0010.3 Hexachlorocyclopentadiene ND ug/L 1 04/25/12 07:57 77-47-404/24/12 10:0025.8 Hexachloroethane ND ug/L 1 04/25/12 07:57 67-72-104/24/12 10:0010.3 Isophorone ND ug/L 1 04/25/12 07:57 78-59-104/24/12 10:0010.3 2-Methylphenol(o-Cresol)ND ug/L 1 04/25/12 07:57 95-48-704/24/12 10:0010.3 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/25/12 07:5704/24/12 10:0020.6 2-Nitroaniline ND ug/L 1 04/25/12 07:57 88-74-404/24/12 10:0051.5 3-Nitroaniline ND ug/L 1 04/25/12 07:57 99-09-204/24/12 10:0051.5 4-Nitroaniline ND ug/L 1 04/25/12 07:57 100-01-604/24/12 10:0051.5 Nitrobenzene ND ug/L 1 04/25/12 07:57 98-95-304/24/12 10:0010.3 2-Nitrophenol ND ug/L 1 04/25/12 07:57 88-75-504/24/12 10:0010.3 4-Nitrophenol ND ug/L 1 04/25/12 07:57 100-02-704/24/12 10:0051.5 N-Nitroso-di-n-propylamine ND ug/L 1 04/25/12 07:57 621-64-704/24/12 10:0010.3 N-Nitrosodiphenylamine ND ug/L 1 04/25/12 07:57 86-30-604/24/12 10:0010.3 Pentachlorophenol ND ug/L 1 04/25/12 07:57 87-86-504/24/12 10:0051.5 Phenol ND ug/L 1 04/25/12 07:57 108-95-204/24/12 10:0010.3 2,4,5-Trichlorophenol ND ug/L 1 04/25/12 07:57 95-95-404/24/12 10:0010.3 2,4,6-Trichlorophenol ND ug/L 1 04/25/12 07:57 88-06-204/24/12 10:0010.3 Surrogates Nitrobenzene-d5 (S)76 %.1 04/25/12 07:57 4165-60-004/24/12 10:0033-108 Phenol-d5 (S)20 %.1 04/25/12 07:57 4165-62-204/24/12 10:0010-56 2-Fluorophenol (S)35 %.1 04/25/12 07:57 367-12-404/24/12 10:0010-74 2,4,6-Tribromophenol (S)94 %.1 04/25/12 07:57 118-79-604/24/12 10:0032-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 21:42 67-64-1100 Acrolein ND ug/L 1 04/24/12 21:42 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 21:42 107-13-1100 Benzene ND ug/L 1 04/24/12 21:42 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 21:42 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 21:42 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 21:42 75-27-45.0 Bromoform ND ug/L 1 04/24/12 21:42 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 21:42 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 21:42 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 21:42 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/24/12 21:42 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 21:42 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 21:42 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 21:42 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 21:42 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 21:42 75-00-35.0 Chloroform ND ug/L 1 04/24/12 21:42 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 21:42 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 21:42 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 21:42 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 21:42 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 45 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W042012 Lab ID:5061800013 Collected:04/20/12 12:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 21:42 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 21:42 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 21:42 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 21:42 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 21:42 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 21:42 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 21:42 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 21:42 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 21:42 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 21:42 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 21:42 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 21:42 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 21:42 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 21:42 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 21:42 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 21:42 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 21:42 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 21:42 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 21:42 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 21:42 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 21:42 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 21:42 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 21:42 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 21:42 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 21:42 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/24/12 21:42 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 21:42 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 21:42 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 21:42 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 21:42 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 21:42 103-65-15.0 Styrene ND ug/L 1 04/24/12 21:42 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 21:42 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 21:42 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 21:42 127-18-45.0 Toluene ND ug/L 1 04/24/12 21:42 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 21:42 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 21:42 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 21:42 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 21:42 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 21:42 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 21:42 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 21:42 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 21:42 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 21:42 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 21:42 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 21:42 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 46 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:FB1:W042012 Lab ID:5061800013 Collected:04/20/12 12:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/24/12 21:42 1330-20-710.0 Surrogates Dibromofluoromethane (S)100 %.1 04/24/12 21:42 1868-53-783-123 4-Bromofluorobenzene (S)105 %.1 04/24/12 21:42 460-00-472-125 Toluene-d8 (S)102 %.1 04/24/12 21:42 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 47 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G260300 Lab ID:5061800014 Collected:04/20/12 11:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 22:16 67-64-1100 Acrolein ND ug/L 1 04/24/12 22:16 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 22:16 107-13-1100 Benzene ND ug/L 1 04/24/12 22:16 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 22:16 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 22:16 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 22:16 75-27-45.0 Bromoform ND ug/L 1 04/24/12 22:16 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 22:16 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 22:16 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 22:16 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/24/12 22:16 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 22:16 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 22:16 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 22:16 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 22:16 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 22:16 75-00-35.0 Chloroform ND ug/L 1 04/24/12 22:16 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 22:16 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 22:16 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 22:16 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 22:16 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 22:16 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 22:16 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 22:16 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 22:16 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 22:16 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 22:16 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 22:16 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 22:16 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 22:16 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 22:16 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 22:16 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 22:16 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 22:16 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 22:16 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 22:16 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 22:16 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 22:16 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 22:16 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 22:16 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 22:16 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 22:16 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 22:16 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 22:16 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 22:16 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 22:16 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 48 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:HTB14:G260300 Lab ID:5061800014 Collected:04/20/12 11:30 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/24/12 22:16 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 22:16 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 22:16 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 22:16 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 22:16 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 22:16 103-65-15.0 Styrene ND ug/L 1 04/24/12 22:16 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 22:16 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 22:16 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 22:16 127-18-45.0 Toluene ND ug/L 1 04/24/12 22:16 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 22:16 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 22:16 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 22:16 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 22:16 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 22:16 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 22:16 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 22:16 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 22:16 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 22:16 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 22:16 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 22:16 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 22:16 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/24/12 22:16 1868-53-783-123 4-Bromofluorobenzene (S)105 %.1 04/24/12 22:16 460-00-472-125 Toluene-d8 (S)104 %.1 04/24/12 22:16 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 49 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:TB:W041912 Lab ID:5061800015 Collected:04/19/12 08:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/24/12 22:50 67-64-1100 Acrolein ND ug/L 1 04/24/12 22:50 107-02-8100 Acrylonitrile ND ug/L 1 04/24/12 22:50 107-13-1100 Benzene ND ug/L 1 04/24/12 22:50 71-43-25.0 Bromobenzene ND ug/L 1 04/24/12 22:50 108-86-15.0 Bromochloromethane ND ug/L 1 04/24/12 22:50 74-97-55.0 Bromodichloromethane ND ug/L 1 04/24/12 22:50 75-27-45.0 Bromoform ND ug/L 1 04/24/12 22:50 75-25-25.0 Bromomethane ND ug/L 1 04/24/12 22:50 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/24/12 22:50 78-93-325.0 n-Butylbenzene ND ug/L 1 04/24/12 22:50 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/24/12 22:50 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/24/12 22:50 98-06-65.0 Carbon disulfide ND ug/L 1 04/24/12 22:50 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/24/12 22:50 56-23-55.0 Chlorobenzene ND ug/L 1 04/24/12 22:50 108-90-75.0 Chloroethane ND ug/L 1 04/24/12 22:50 75-00-35.0 Chloroform ND ug/L 1 04/24/12 22:50 67-66-35.0 Chloromethane ND ug/L 1 04/24/12 22:50 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/24/12 22:50 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/24/12 22:50 106-43-45.0 Dibromochloromethane ND ug/L 1 04/24/12 22:50 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/24/12 22:50 106-93-45.0 Dibromomethane ND ug/L 1 04/24/12 22:50 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/24/12 22:50 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/24/12 22:50 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/24/12 22:50 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/24/12 22:50 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/24/12 22:50 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/24/12 22:50 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/24/12 22:50 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/24/12 22:50 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/24/12 22:50 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/24/12 22:50 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/24/12 22:50 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/24/12 22:50 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/24/12 22:50 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/24/12 22:50 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/24/12 22:50 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/24/12 22:50 10061-02-65.0 Ethylbenzene ND ug/L 1 04/24/12 22:50 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/24/12 22:50 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/24/12 22:50 87-68-35.0 n-Hexane ND ug/L 1 04/24/12 22:50 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/24/12 22:50 591-78-625.0 Iodomethane ND ug/L 1 04/24/12 22:50 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/24/12 22:50 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 50 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061800 SBI067 Sample:SBI067:TB:W041912 Lab ID:5061800015 Collected:04/19/12 08:00 Received:04/21/12 10:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/24/12 22:50 99-87-65.0 Methylene Chloride ND ug/L 1 04/24/12 22:50 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/24/12 22:50 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/24/12 22:50 1634-04-44.0 Naphthalene ND ug/L 1 04/24/12 22:50 91-20-35.0 n-Propylbenzene ND ug/L 1 04/24/12 22:50 103-65-15.0 Styrene ND ug/L 1 04/24/12 22:50 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/24/12 22:50 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/24/12 22:50 79-34-55.0 Tetrachloroethene ND ug/L 1 04/24/12 22:50 127-18-45.0 Toluene ND ug/L 1 04/24/12 22:50 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/24/12 22:50 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/24/12 22:50 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/24/12 22:50 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/24/12 22:50 79-00-55.0 Trichloroethene ND ug/L 1 04/24/12 22:50 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/24/12 22:50 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/24/12 22:50 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/24/12 22:50 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/24/12 22:50 108-67-85.0 Vinyl acetate ND ug/L 1 04/24/12 22:50 108-05-450.0 Vinyl chloride ND ug/L 1 04/24/12 22:50 75-01-42.0 Xylene (Total)ND ug/L 1 04/24/12 22:50 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/24/12 22:50 1868-53-783-123 4-Bromofluorobenzene (S)103 %.1 04/24/12 22:50 460-00-472-125 Toluene-d8 (S)102 %.1 04/24/12 22:50 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 51 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41537 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061800003, 5061800004, 5061800006, 5061800007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724450 Associated Lab Samples:5061800003, 5061800004, 5061800006, 5061800007 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/24/12 00:31 1,1,1-Trichloroethane ug/L ND 5.0 04/24/12 00:31 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/24/12 00:31 1,1,2-Trichloroethane ug/L ND 5.0 04/24/12 00:31 1,1-Dichloroethane ug/L ND 5.0 04/24/12 00:31 1,1-Dichloroethene ug/L ND 5.0 04/24/12 00:31 1,1-Dichloropropene ug/L ND 5.0 04/24/12 00:31 1,2,3-Trichlorobenzene ug/L ND 5.0 04/24/12 00:31 1,2,3-Trichloropropane ug/L ND 5.0 04/24/12 00:31 1,2,4-Trichlorobenzene ug/L ND 5.0 04/24/12 00:31 1,2,4-Trimethylbenzene ug/L ND 5.0 04/24/12 00:31 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/24/12 00:31 1,2-Dichlorobenzene ug/L ND 5.0 04/24/12 00:31 1,2-Dichloroethane ug/L ND 5.0 04/24/12 00:31 1,2-Dichloropropane ug/L ND 5.0 04/24/12 00:31 1,3,5-Trimethylbenzene ug/L ND 5.0 04/24/12 00:31 1,3-Dichlorobenzene ug/L ND 5.0 04/24/12 00:31 1,3-Dichloropropane ug/L ND 5.0 04/24/12 00:31 1,4-Dichlorobenzene ug/L ND 5.0 04/24/12 00:31 2,2-Dichloropropane ug/L ND 5.0 04/24/12 00:31 2-Butanone (MEK)ug/L ND 25.0 04/24/12 00:31 2-Chlorotoluene ug/L ND 5.0 04/24/12 00:31 2-Hexanone ug/L ND 25.0 04/24/12 00:31 4-Chlorotoluene ug/L ND 5.0 04/24/12 00:31 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/24/12 00:31 Acetone ug/L ND 100 04/24/12 00:31 Acrolein ug/L ND 100 04/24/12 00:31 Acrylonitrile ug/L ND 100 04/24/12 00:31 Benzene ug/L ND 5.0 04/24/12 00:31 Bromobenzene ug/L ND 5.0 04/24/12 00:31 Bromochloromethane ug/L ND 5.0 04/24/12 00:31 Bromodichloromethane ug/L ND 5.0 04/24/12 00:31 Bromoform ug/L ND 5.0 04/24/12 00:31 Bromomethane ug/L ND 5.0 04/24/12 00:31 Carbon disulfide ug/L ND 10.0 04/24/12 00:31 Carbon tetrachloride ug/L ND 5.0 04/24/12 00:31 Chlorobenzene ug/L ND 5.0 04/24/12 00:31 Chloroethane ug/L ND 5.0 04/24/12 00:31 Chloroform ug/L ND 5.0 04/24/12 00:31 Chloromethane ug/L ND 5.0 04/24/12 00:31 cis-1,2-Dichloroethene ug/L ND 5.0 04/24/12 00:31 cis-1,3-Dichloropropene ug/L ND 5.0 04/24/12 00:31 Dibromochloromethane ug/L ND 5.0 04/24/12 00:31 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 52 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724450 Associated Lab Samples:5061800003, 5061800004, 5061800006, 5061800007 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 04/24/12 00:31 Dichlorodifluoromethane ug/L ND 5.0 04/24/12 00:31 Ethyl methacrylate ug/L ND 100 04/24/12 00:31 Ethylbenzene ug/L ND 5.0 04/24/12 00:31 Hexachloro-1,3-butadiene ug/L ND 5.0 04/24/12 00:31 Iodomethane ug/L ND 10.0 04/24/12 00:31 Isopropylbenzene (Cumene)ug/L ND 5.0 04/24/12 00:31 Methyl-tert-butyl ether ug/L ND 4.0 04/24/12 00:31 Methylene Chloride ug/L ND 5.0 04/24/12 00:31 n-Butylbenzene ug/L ND 5.0 04/24/12 00:31 n-Hexane ug/L ND 5.0 N204/24/12 00:31 n-Propylbenzene ug/L ND 5.0 04/24/12 00:31 Naphthalene ug/L ND 5.0 04/24/12 00:31 p-Isopropyltoluene ug/L ND 5.0 04/24/12 00:31 sec-Butylbenzene ug/L ND 5.0 04/24/12 00:31 Styrene ug/L ND 5.0 04/24/12 00:31 tert-Butylbenzene ug/L ND 5.0 04/24/12 00:31 Tetrachloroethene ug/L ND 5.0 04/24/12 00:31 Toluene ug/L ND 5.0 04/24/12 00:31 trans-1,2-Dichloroethene ug/L ND 5.0 04/24/12 00:31 trans-1,3-Dichloropropene ug/L ND 5.0 04/24/12 00:31 trans-1,4-Dichloro-2-butene ug/L ND 100 04/24/12 00:31 Trichloroethene ug/L ND 5.0 04/24/12 00:31 Trichlorofluoromethane ug/L ND 5.0 04/24/12 00:31 Vinyl acetate ug/L ND 50.0 04/24/12 00:31 Vinyl chloride ug/L ND 2.0 04/24/12 00:31 Xylene (Total)ug/L ND 10.0 04/24/12 00:31 4-Bromofluorobenzene (S)%.101 72-125 04/24/12 00:31 Dibromofluoromethane (S)%.110 83-123 04/24/12 00:31 Toluene-d8 (S)%.90 81-114 04/24/12 00:31 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724451LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.250 96 69-122 1,1,1-Trichloroethane ug/L 48.650 97 69-126 1,1,2,2-Tetrachloroethane ug/L 43.550 87 68-134 1,1,2-Trichloroethane ug/L 42.450 85 77-129 1,1-Dichloroethane ug/L 40.150 80 70-127 1,1-Dichloroethene ug/L 56.150 112 75-145 1,1-Dichloropropene ug/L 45.350 91 75-126 1,2,3-Trichlorobenzene ug/L 51.650 103 63-130 1,2,3-Trichloropropane ug/L 65.3 L35013145-121 1,2,4-Trichlorobenzene ug/L 55.050 110 64-122 1,2,4-Trimethylbenzene ug/L 57.550 115 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 53 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724451LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 43.750 87 77-123 1,2-Dichlorobenzene ug/L 54.150 108 74-123 1,2-Dichloroethane ug/L 50.250 100 71-127 1,2-Dichloropropane ug/L 40.850 82 75-126 1,3,5-Trimethylbenzene ug/L 53.750 107 69-129 1,3-Dichlorobenzene ug/L 55.250 110 76-123 1,3-Dichloropropane ug/L 37.2 L0507477-126 1,4-Dichlorobenzene ug/L 48.250 96 77-121 2,2-Dichloropropane ug/L 42.150 84 45-138 2-Butanone (MEK)ug/L 244250 98 42-177 2-Chlorotoluene ug/L 52.250 104 74-129 2-Hexanone ug/L 186250 74 57-162 4-Chlorotoluene ug/L 47.950 96 70-125 4-Methyl-2-pentanone (MIBK)ug/L 183250 73 64-135 Acetone ug/L 318250 127 10-200 Acrolein ug/L 17801000 178 10-200 Acrylonitrile ug/L 9331000 93 59-144 Benzene ug/L 41.850 84 76-123 Bromobenzene ug/L 43.850 88 67-130 Bromochloromethane ug/L 42.650 85 58-153 Bromodichloromethane ug/L 52.050 104 71-124 Bromoform ug/L 35.850 72 64-116 Bromomethane ug/L 73.550 147 23-197 Carbon disulfide ug/L 124100 124 55-146 Carbon tetrachloride ug/L 44.950 90 65-125 Chlorobenzene ug/L 45.450 91 78-120 Chloroethane ug/L 60.850 122 56-163 Chloroform ug/L 52.050 104 73-122 Chloromethane ug/L 56.750 113 46-146 cis-1,2-Dichloroethene ug/L 40.950 82 79-129 cis-1,3-Dichloropropene ug/L 40.250 80 66-123 Dibromochloromethane ug/L 39.150 78 70-123 Dibromomethane ug/L 47.950 96 73-123 Dichlorodifluoromethane ug/L 58.950 118 19-200 Ethyl methacrylate ug/L 145200 73 70-127 Ethylbenzene ug/L 47.450 95 75-120 Hexachloro-1,3-butadiene ug/L 50.650 101 64-131 Iodomethane ug/L 142100 142 16-181 Isopropylbenzene (Cumene)ug/L 52.250 104 73-123 Methyl-tert-butyl ether ug/L 98.5100 98 66-128 Methylene Chloride ug/L 56.950 114 61-138 n-Butylbenzene ug/L 49.650 99 69-130 n-Hexane ug/L 43.7 N2508767-142 n-Propylbenzene ug/L 43.350 87 71-132 Naphthalene ug/L 49.950 100 62-130 p-Isopropyltoluene ug/L 52.250 104 71-126 sec-Butylbenzene ug/L 48.750 97 69-130 Styrene ug/L 54.350 109 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 54 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724451LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 46.250 92 49-114 Tetrachloroethene ug/L 42.450 85 57-125 Toluene ug/L 48.750 97 72-124 trans-1,2-Dichloroethene ug/L 58.050 116 71-145 trans-1,3-Dichloropropene ug/L 41.950 84 58-118 trans-1,4-Dichloro-2-butene ug/L 159200 79 50-121 Trichloroethene ug/L 47.050 94 77-122 Trichlorofluoromethane ug/L 66.050 132 56-159 Vinyl acetate ug/L 236200 118 27-119 Vinyl chloride ug/L 64.850 130 61-146 Xylene (Total)ug/L 158150 105 72-126 4-Bromofluorobenzene (S)%.99 72-125 Dibromofluoromethane (S)%.108 83-123 Toluene-d8 (S)%.91 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 724454MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800006 724455 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 97 30-12292 5 2050ND48.5 45.9 1,1,1-Trichloroethane ug/L 50 96 37-13696 .02 2050ND48.0 48.0 1,1,2,2-Tetrachloroethane ug/L 50 90 47-13283 8 2050ND44.8 41.4 1,1,2-Trichloroethane ug/L 50 78 53-13172 7 2050ND38.9 36.2 1,1-Dichloroethane ug/L 50 81 47-13878 3 2050ND40.5 39.2 1,1-Dichloroethene ug/L 50 106 54-152107 .5 2050ND53.1 53.3 1,1-Dichloropropene ug/L 50 84 47-13682 2 2050ND41.9 40.9 1,2,3-Trichlorobenzene ug/L 50 95 15-13288 7 2050ND47.3 44.1 1,2,3-Trichloropropane ug/L M05012524-108124 .7 2050ND62.6 62.2 1,2,4-Trichlorobenzene ug/L 50 89 10-13085 4 2050ND44.3 42.6 1,2,4-Trimethylbenzene ug/L 50 106 10-14198 7 2050ND52.9 49.2 1,2-Dibromoethane (EDB)ug/L 50 87 49-13078 10 2050ND43.4 39.2 1,2-Dichlorobenzene ug/L 50 102 20-13796 6 2050ND51.0 48.1 1,2-Dichloroethane ug/L 50 100 42-13996 4 2050ND49.9 48.1 1,2-Dichloropropane ug/L 50 82 50-13177 6 2050ND40.8 38.5 1,3,5-Trimethylbenzene ug/L 50 99 10-14593 6 2050ND49.4 46.4 1,3-Dichlorobenzene ug/L 50 99 13-14395 4 2050ND49.6 47.6 1,3-Dichloropropane ug/L 50 80 53-13071 11 2050ND39.9 35.7 1,4-Dichlorobenzene ug/L 50 88 13-14083 6 2050ND44.0 41.6 2,2-Dichloropropane ug/L 50 79 13-14279 .9 2050ND39.7 39.4 2-Butanone (MEK)ug/L 250 100 43-14296 4 20250ND250240 2-Chlorotoluene ug/L 50 96 15-14590 6 2050ND48.0 45.1 2-Hexanone ug/L 250 82 46-13977 7 20250ND205192 4-Chlorotoluene ug/L 50 88 12-14383 5 2050ND43.9 41.7 4-Methyl-2-pentanone (MIBK)ug/L 250 76 43-14072 6 20250ND191180 Acetone ug/L 250 116 38-155121 4 20250ND290302 Acrolein ug/L 1000 138 11-200136 1 201000ND13801360 Acrylonitrile ug/L 1000 90 42-15089 1 201000ND903894 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 55 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724454MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800006 724455 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 77 52-13477 .1 2050ND38.7 38.6 Bromobenzene ug/L 50 100 25-14093 7 2050ND50.1 46.6 Bromochloromethane ug/L 50 88 54-14485 4 2050ND44.1 42.4 Bromodichloromethane ug/L 50 102 42-128100 2 2050ND51.2 50.1 Bromoform ug/L 50 69 34-11667 3 2050ND34.7 33.7 Bromomethane ug/L 50 140 10-200140 .3 2050ND69.8 70.0 Carbon disulfide ug/L 100 115 43-144111 3 20100ND115111 Carbon tetrachloride ug/L 50 89 26-13691 3 2050ND44.3 45.6 Chlorobenzene ug/L 50 90 33-13683 8 2050ND45.1 41.7 Chloroethane ug/L 50 110 21-200106 5 2050ND55.2 52.8 Chloroform ug/L 50 103 50-13499 4 2050ND51.7 49.6 Chloromethane ug/L 50 89 32-16088 2 2050ND44.6 43.8 cis-1,2-Dichloroethene ug/L 50 80 48-14579 1 2050ND41.0 40.6 cis-1,3-Dichloropropene ug/L 50 75 35-11668 9 2050ND37.3 34.2 Dibromochloromethane ug/L 50 77 39-12273 6 2050ND38.6 36.5 Dibromomethane ug/L 50 98 49-13492 6 2050ND49.1 46.1 Dichlorodifluoromethane ug/L 50 74 35-20074 .3 2050ND36.9 36.8 Ethyl methacrylate ug/L 200 78 54-12376 2 20200ND155152 Ethylbenzene ug/L 50 90 29-13283 8 2050ND44.9 41.3 Hexachloro-1,3-butadiene ug/L 50 90 10-14685 6 2050ND45.1 42.6 Iodomethane ug/L 100 127 10-171131 3 20100ND127131 Isopropylbenzene (Cumene)ug/L 50 101 11-14693 8 2050ND50.4 46.7 Methyl-tert-butyl ether ug/L 100 101 39-13799 1 20100ND10199.1 Methylene Chloride ug/L 50 107 47-141104 3 2050ND53.6 52.0 n-Butylbenzene ug/L 50 84 10-15682 3 2050ND43.6 42.3 n-Hexane ug/L N2507951-13777 2 2050ND39.5 38.7 n-Propylbenzene ug/L 50 80 10-14875 6 2050ND40.2 38.0 Naphthalene ug/L 50 102 40-12497 5 2050ND50.8 48.5 p-Isopropyltoluene ug/L 50 94 10-15092 3 2050ND47.7 46.4 sec-Butylbenzene ug/L 50 92 10-15088 4 2050ND47.7 45.9 Styrene ug/L 50 103 20-14395 8 2050ND51.5 47.3 tert-Butylbenzene ug/L 50 88 10-12384 5 2050ND44.1 42.1 Tetrachloroethene ug/L 50 81 30-12474 8 2050ND40.3 37.2 Toluene ug/L 50 90 42-13083 8 2050ND44.9 41.4 trans-1,2-Dichloroethene ug/L 50 105 48-144105 .4 2050ND52.5 52.3 trans-1,3-Dichloropropene ug/L 50 76 24-11472 5 2050ND37.9 36.0 trans-1,4-Dichloro-2-butene ug/L 200 73 22-12069 7 20200ND147137 Trichloroethene ug/L 50 87 44-13088 .8 2050ND45.9 46.3 Trichlorofluoromethane ug/L 50 121 17-200120 .4 2050ND60.4 60.2 Vinyl acetate ug/L 200 80 10-11580 .3 20200ND160161 Vinyl chloride ug/L 50 100 45-15998 3 2050ND50.1 48.8 Xylene (Total)ug/L 150 101 29-13193 8 20150ND151140 4-Bromofluorobenzene (S)%.104 72-125102 20 Dibromofluoromethane (S)%.105 83-123112 20 Toluene-d8 (S)%.89 81-11487 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 56 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41563 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061800008, 5061800013, 5061800014, 5061800015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724946 Associated Lab Samples:5061800008, 5061800013, 5061800014, 5061800015 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/24/12 19:28 1,1,1-Trichloroethane ug/L ND 5.0 04/24/12 19:28 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/24/12 19:28 1,1,2-Trichloroethane ug/L ND 5.0 04/24/12 19:28 1,1-Dichloroethane ug/L ND 5.0 04/24/12 19:28 1,1-Dichloroethene ug/L ND 5.0 04/24/12 19:28 1,1-Dichloropropene ug/L ND 5.0 04/24/12 19:28 1,2,3-Trichlorobenzene ug/L ND 5.0 04/24/12 19:28 1,2,3-Trichloropropane ug/L ND 5.0 04/24/12 19:28 1,2,4-Trichlorobenzene ug/L ND 5.0 04/24/12 19:28 1,2,4-Trimethylbenzene ug/L ND 5.0 04/24/12 19:28 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/24/12 19:28 1,2-Dichlorobenzene ug/L ND 5.0 04/24/12 19:28 1,2-Dichloroethane ug/L ND 5.0 04/24/12 19:28 1,2-Dichloropropane ug/L ND 5.0 04/24/12 19:28 1,3,5-Trimethylbenzene ug/L ND 5.0 04/24/12 19:28 1,3-Dichlorobenzene ug/L ND 5.0 04/24/12 19:28 1,3-Dichloropropane ug/L ND 5.0 04/24/12 19:28 1,4-Dichlorobenzene ug/L ND 5.0 04/24/12 19:28 2,2-Dichloropropane ug/L ND 5.0 04/24/12 19:28 2-Butanone (MEK)ug/L ND 25.0 04/24/12 19:28 2-Chlorotoluene ug/L ND 5.0 04/24/12 19:28 2-Hexanone ug/L ND 25.0 04/24/12 19:28 4-Chlorotoluene ug/L ND 5.0 04/24/12 19:28 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/24/12 19:28 Acetone ug/L ND 100 04/24/12 19:28 Acrolein ug/L ND 100 04/24/12 19:28 Acrylonitrile ug/L ND 100 04/24/12 19:28 Benzene ug/L ND 5.0 04/24/12 19:28 Bromobenzene ug/L ND 5.0 04/24/12 19:28 Bromochloromethane ug/L ND 5.0 04/24/12 19:28 Bromodichloromethane ug/L ND 5.0 04/24/12 19:28 Bromoform ug/L ND 5.0 04/24/12 19:28 Bromomethane ug/L ND 5.0 04/24/12 19:28 Carbon disulfide ug/L ND 10.0 04/24/12 19:28 Carbon tetrachloride ug/L ND 5.0 04/24/12 19:28 Chlorobenzene ug/L ND 5.0 04/24/12 19:28 Chloroethane ug/L ND 5.0 04/24/12 19:28 Chloroform ug/L ND 5.0 04/24/12 19:28 Chloromethane ug/L ND 5.0 04/24/12 19:28 cis-1,2-Dichloroethene ug/L ND 5.0 04/24/12 19:28 cis-1,3-Dichloropropene ug/L ND 5.0 04/24/12 19:28 Dibromochloromethane ug/L ND 5.0 04/24/12 19:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 57 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724946 Associated Lab Samples:5061800008, 5061800013, 5061800014, 5061800015 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 04/24/12 19:28 Dichlorodifluoromethane ug/L ND 5.0 04/24/12 19:28 Ethyl methacrylate ug/L ND 100 04/24/12 19:28 Ethylbenzene ug/L ND 5.0 04/24/12 19:28 Hexachloro-1,3-butadiene ug/L ND 5.0 04/24/12 19:28 Iodomethane ug/L ND 10.0 04/24/12 19:28 Isopropylbenzene (Cumene)ug/L ND 5.0 04/24/12 19:28 Methyl-tert-butyl ether ug/L ND 4.0 04/24/12 19:28 Methylene Chloride ug/L ND 5.0 04/24/12 19:28 n-Butylbenzene ug/L ND 5.0 04/24/12 19:28 n-Hexane ug/L ND 5.0 N204/24/12 19:28 n-Propylbenzene ug/L ND 5.0 04/24/12 19:28 Naphthalene ug/L ND 5.0 04/24/12 19:28 p-Isopropyltoluene ug/L ND 5.0 04/24/12 19:28 sec-Butylbenzene ug/L ND 5.0 04/24/12 19:28 Styrene ug/L ND 5.0 04/24/12 19:28 tert-Butylbenzene ug/L ND 5.0 04/24/12 19:28 Tetrachloroethene ug/L ND 5.0 04/24/12 19:28 Toluene ug/L ND 5.0 04/24/12 19:28 trans-1,2-Dichloroethene ug/L ND 5.0 04/24/12 19:28 trans-1,3-Dichloropropene ug/L ND 5.0 04/24/12 19:28 trans-1,4-Dichloro-2-butene ug/L ND 100 04/24/12 19:28 Trichloroethene ug/L ND 5.0 04/24/12 19:28 Trichlorofluoromethane ug/L ND 5.0 04/24/12 19:28 Vinyl acetate ug/L ND 50.0 04/24/12 19:28 Vinyl chloride ug/L ND 2.0 04/24/12 19:28 Xylene (Total)ug/L ND 10.0 04/24/12 19:28 4-Bromofluorobenzene (S)%.100 72-125 04/24/12 19:28 Dibromofluoromethane (S)%.105 83-123 04/24/12 19:28 Toluene-d8 (S)%.101 81-114 04/24/12 19:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724947LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 46.850 94 69-122 1,1,1-Trichloroethane ug/L 47.450 95 69-126 1,1,2,2-Tetrachloroethane ug/L 41.450 83 68-134 1,1,2-Trichloroethane ug/L 41.650 83 77-129 1,1-Dichloroethane ug/L 42.150 84 70-127 1,1-Dichloroethene ug/L 46.250 92 75-145 1,1-Dichloropropene ug/L 47.550 95 75-126 1,2,3-Trichlorobenzene ug/L 38.750 77 63-130 1,2,3-Trichloropropane ug/L 70.5 L35014145-121 1,2,4-Trichlorobenzene ug/L 38.650 77 64-122 1,2,4-Trimethylbenzene ug/L 50.950 102 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 58 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724947LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 41.950 84 77-123 1,2-Dichlorobenzene ug/L 39.150 78 74-123 1,2-Dichloroethane ug/L 44.050 88 71-127 1,2-Dichloropropane ug/L 42.550 85 75-126 1,3,5-Trimethylbenzene ug/L 50.250 100 69-129 1,3-Dichlorobenzene ug/L 47.250 94 76-123 1,3-Dichloropropane ug/L 42.150 84 77-126 1,4-Dichlorobenzene ug/L 39.350 79 77-121 2,2-Dichloropropane ug/L 47.750 95 45-138 2-Butanone (MEK)ug/L 270250 108 42-177 2-Chlorotoluene ug/L 48.850 98 74-129 2-Hexanone ug/L 219250 88 57-162 4-Chlorotoluene ug/L 41.650 83 70-125 4-Methyl-2-pentanone (MIBK)ug/L 219250 88 64-135 Acetone ug/L 245250 98 10-200 Acrolein ug/L 14001000 140 10-200 Acrylonitrile ug/L 8171000 82 59-144 Benzene ug/L 42.750 85 76-123 Bromobenzene ug/L 48.250 96 67-130 Bromochloromethane ug/L 49.450 99 58-153 Bromodichloromethane ug/L 42.850 86 71-124 Bromoform ug/L 39.650 79 64-116 Bromomethane ug/L 64.550 129 23-197 Carbon disulfide ug/L 94.8100 95 55-146 Carbon tetrachloride ug/L 42.050 84 65-125 Chlorobenzene ug/L 49.950 100 78-120 Chloroethane ug/L 60.250 120 56-163 Chloroform ug/L 42.550 85 73-122 Chloromethane ug/L 56.050 112 46-146 cis-1,2-Dichloroethene ug/L 49.950 100 79-129 cis-1,3-Dichloropropene ug/L 45.150 90 66-123 Dibromochloromethane ug/L 39.950 80 70-123 Dibromomethane ug/L 46.050 92 73-123 Dichlorodifluoromethane ug/L 50.950 102 19-200 Ethyl methacrylate ug/L 174200 87 70-127 Ethylbenzene ug/L 52.450 105 75-120 Hexachloro-1,3-butadiene ug/L 40.850 82 64-131 Iodomethane ug/L 104100 104 16-181 Isopropylbenzene (Cumene)ug/L 50.650 101 73-123 Methyl-tert-butyl ether ug/L 95.5100 96 66-128 Methylene Chloride ug/L 46.250 92 61-138 n-Butylbenzene ug/L 51.350 103 69-130 n-Hexane ug/L 40.1 N2508067-142 n-Propylbenzene ug/L 52.150 104 71-132 Naphthalene ug/L 40.650 81 62-130 p-Isopropyltoluene ug/L 50.450 101 71-126 sec-Butylbenzene ug/L 51.350 103 69-130 Styrene ug/L 50.950 102 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 59 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724947LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 39.550 79 49-114 Tetrachloroethene ug/L 38.550 77 57-125 Toluene ug/L 50.150 100 72-124 trans-1,2-Dichloroethene ug/L 46.450 93 71-145 trans-1,3-Dichloropropene ug/L 42.450 85 58-118 trans-1,4-Dichloro-2-butene ug/L 154200 77 50-121 Trichloroethene ug/L 44.350 89 77-122 Trichlorofluoromethane ug/L 53.450 107 56-159 Vinyl acetate ug/L 276 L320013827-119 Vinyl chloride ug/L 58.450 117 61-146 Xylene (Total)ug/L 148150 99 72-126 4-Bromofluorobenzene (S)%.97 72-125 Dibromofluoromethane (S)%.100 83-123 Toluene-d8 (S)%.102 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 724948MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800008 724949 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 97 30-12290 7 2050ND48.5 45.2 1,1,1-Trichloroethane ug/L 50 101 37-13696 5 2050ND50.5 48.0 1,1,2,2-Tetrachloroethane ug/L 50 94 47-13287 8 2050ND47.0 43.4 1,1,2-Trichloroethane ug/L 50 88 53-13187 .6 2050ND43.8 43.6 1,1-Dichloroethane ug/L 50 95 47-13893 2 2050ND47.7 46.5 1,1-Dichloroethene ug/L 50 106 54-15298 8 2050ND52.8 49.0 1,1-Dichloropropene ug/L 50 103 47-13698 4 2050ND51.3 49.1 1,2,3-Trichlorobenzene ug/L 50 75 15-13276 2 2050ND37.3 37.8 1,2,3-Trichloropropane ug/L M05013924-108135 3 2050ND69.3 67.4 1,2,4-Trichlorobenzene ug/L 50 69 10-13068 2 2050ND34.6 33.9 1,2,4-Trimethylbenzene ug/L 50 107 10-141102 4 2050ND53.5 51.1 1,2-Dibromoethane (EDB)ug/L 50 90 49-13088 1 2050ND44.8 44.1 1,2-Dichlorobenzene ug/L 50 82 20-13779 4 2050ND41.0 39.4 1,2-Dichloroethane ug/L 50 96 42-13989 8 2050ND48.2 44.6 1,2-Dichloropropane ug/L 50 91 50-13187 4 2050ND45.4 43.7 1,3,5-Trimethylbenzene ug/L 50 105 10-145100 5 2050ND52.7 50.2 1,3-Dichlorobenzene ug/L 50 96 13-14392 4 2050ND48.1 46.1 1,3-Dichloropropane ug/L 50 91 53-13085 7 2050ND45.3 42.3 1,4-Dichlorobenzene ug/L 50 79 13-14076 4 2050ND39.6 38.1 2,2-Dichloropropane ug/L 50 91 13-14287 5 2050ND45.7 43.4 2-Butanone (MEK)ug/L 250 116 43-142111 5 20250ND290277 2-Chlorotoluene ug/L 50 102 15-14597 5 2050ND50.8 48.5 2-Hexanone ug/L 250 93 46-13989 4 20250ND233223 4-Chlorotoluene ug/L 50 85 12-14380 6 2050ND42.7 40.2 4-Methyl-2-pentanone (MIBK)ug/L 250 94 43-14090 4 20250ND235226 Acetone ug/L 250 109 38-155104 5 20250ND274260 Acrolein ug/L 1000 138 11-200130 6 201000ND13801300 Acrylonitrile ug/L 1000 88 42-15081 8 201000ND881812 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 60 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724948MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800008 724949 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 94 52-13488 6 2050ND47.1 44.2 Bromobenzene ug/L 50 114 25-14096 18 2050ND57.1 47.8 Bromochloromethane ug/L 50 109 54-14497 12 2050ND54.6 48.5 Bromodichloromethane ug/L 50 89 42-12886 4 2050ND44.4 42.9 Bromoform ug/L 50 80 34-11680 .04 2050ND39.8 39.9 Bromomethane ug/L 50 117 10-200124 6 2050ND58.5 62.0 Carbon disulfide ug/L 100 100 43-14496 5 20100ND10096.1 Carbon tetrachloride ug/L 50 85 26-13685 .6 2050ND42.5 42.3 Chlorobenzene ug/L 50 106 33-136100 6 2050ND52.9 49.8 Chloroethane ug/L 50 138 21-200125 10 2050ND68.9 62.6 Chloroform ug/L 50 92 50-13490 2 2050ND46.0 45.0 Chloromethane ug/L 50 116 32-160111 4 2050ND57.8 55.7 cis-1,2-Dichloroethene ug/L 50 108 48-145103 5 2050ND54.1 51.3 cis-1,3-Dichloropropene ug/L 50 89 35-11687 2 2050ND44.4 43.5 Dibromochloromethane ug/L 50 88 39-12284 4 2050ND43.8 42.0 Dibromomethane ug/L 50 101 49-13497 4 2050ND50.6 48.6 Dichlorodifluoromethane ug/L 50 109 35-20099 9 2050ND55.2 50.6 Ethyl methacrylate ug/L 200 87 54-12387 .04 20200ND175175 Ethylbenzene ug/L 50 112 29-132104 7 2050ND56.1 52.1 Hexachloro-1,3-butadiene ug/L 50 81 10-14678 3 2050ND40.3 39.2 Iodomethane ug/L 100 104 10-171104 .4 20100ND104104 Isopropylbenzene (Cumene)ug/L 50 108 11-146102 5 2050ND54.0 51.2 Methyl-tert-butyl ether ug/L 100 106 39-137103 2 20100ND106103 Methylene Chloride ug/L 50 87 47-14188 1 2050ND43.4 44.0 n-Butylbenzene ug/L 50 97 10-15695 2 2050ND48.5 47.5 n-Hexane ug/L N2509051-13783 9 2050ND45.1 41.3 n-Propylbenzene ug/L 50 109 10-148103 6 2050ND54.7 51.5 Naphthalene ug/L 50 85 40-12482 4 2050ND42.6 41.1 p-Isopropyltoluene ug/L 50 103 10-15099 4 2050ND51.6 49.5 sec-Butylbenzene ug/L 50 110 10-150102 7 2050ND54.9 51.1 Styrene ug/L 50 106 20-143103 3 2050ND52.9 51.4 tert-Butylbenzene ug/L 50 85 10-12379 7 2050ND42.6 39.6 Tetrachloroethene ug/L 50 83 30-12479 5 2050ND41.6 39.6 Toluene ug/L 50 108 42-130101 7 2050ND54.2 50.4 trans-1,2-Dichloroethene ug/L 50 95 48-14494 .7 2050ND47.4 47.1 trans-1,3-Dichloropropene ug/L 50 84 24-11480 5 2050ND41.9 40.0 trans-1,4-Dichloro-2-butene ug/L 200 75 22-12073 2 20200ND149147 Trichloroethene ug/L 50 96 44-13088 7 20506.4 54.3 50.4 Trichlorofluoromethane ug/L 50 117 17-200110 6 2050ND58.4 54.8 Vinyl acetate ug/L 200 109 10-115106 2 20200ND218212 Vinyl chloride ug/L 50 121 45-159117 4 2050ND60.7 58.3 Xylene (Total)ug/L 150 103 29-13199 4 20150ND155148 4-Bromofluorobenzene (S)%.100 72-125100 20 Dibromofluoromethane (S)%.100 83-123101 20 Toluene-d8 (S)%.99 81-114100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 61 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41564 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061800011, 5061800012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724950 Associated Lab Samples:5061800011, 5061800012 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/25/12 01:21 1,1,1-Trichloroethane ug/L ND 5.0 04/25/12 01:21 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/25/12 01:21 1,1,2-Trichloroethane ug/L ND 5.0 04/25/12 01:21 1,1-Dichloroethane ug/L ND 5.0 04/25/12 01:21 1,1-Dichloroethene ug/L ND 5.0 04/25/12 01:21 1,1-Dichloropropene ug/L ND 5.0 04/25/12 01:21 1,2,3-Trichlorobenzene ug/L ND 5.0 04/25/12 01:21 1,2,3-Trichloropropane ug/L ND 5.0 04/25/12 01:21 1,2,4-Trichlorobenzene ug/L ND 5.0 04/25/12 01:21 1,2,4-Trimethylbenzene ug/L ND 5.0 04/25/12 01:21 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/25/12 01:21 1,2-Dichlorobenzene ug/L ND 5.0 04/25/12 01:21 1,2-Dichloroethane ug/L ND 5.0 04/25/12 01:21 1,2-Dichloropropane ug/L ND 5.0 04/25/12 01:21 1,3,5-Trimethylbenzene ug/L ND 5.0 04/25/12 01:21 1,3-Dichlorobenzene ug/L ND 5.0 04/25/12 01:21 1,3-Dichloropropane ug/L ND 5.0 04/25/12 01:21 1,4-Dichlorobenzene ug/L ND 5.0 04/25/12 01:21 2,2-Dichloropropane ug/L ND 5.0 04/25/12 01:21 2-Butanone (MEK)ug/L ND 25.0 04/25/12 01:21 2-Chlorotoluene ug/L ND 5.0 04/25/12 01:21 2-Hexanone ug/L ND 25.0 04/25/12 01:21 4-Chlorotoluene ug/L ND 5.0 04/25/12 01:21 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/25/12 01:21 Acetone ug/L ND 100 04/25/12 01:21 Acrolein ug/L ND 100 04/25/12 01:21 Acrylonitrile ug/L ND 100 04/25/12 01:21 Benzene ug/L ND 5.0 04/25/12 01:21 Bromobenzene ug/L ND 5.0 04/25/12 01:21 Bromochloromethane ug/L ND 5.0 04/25/12 01:21 Bromodichloromethane ug/L ND 5.0 04/25/12 01:21 Bromoform ug/L ND 5.0 04/25/12 01:21 Bromomethane ug/L ND 5.0 04/25/12 01:21 Carbon disulfide ug/L ND 10.0 04/25/12 01:21 Carbon tetrachloride ug/L ND 5.0 04/25/12 01:21 Chlorobenzene ug/L ND 5.0 04/25/12 01:21 Chloroethane ug/L ND 5.0 04/25/12 01:21 Chloroform ug/L ND 5.0 04/25/12 01:21 Chloromethane ug/L ND 5.0 04/25/12 01:21 cis-1,2-Dichloroethene ug/L ND 5.0 04/25/12 01:21 cis-1,3-Dichloropropene ug/L ND 5.0 04/25/12 01:21 Dibromochloromethane ug/L ND 5.0 04/25/12 01:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 62 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724950 Associated Lab Samples:5061800011, 5061800012 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 04/25/12 01:21 Dichlorodifluoromethane ug/L ND 5.0 04/25/12 01:21 Ethyl methacrylate ug/L ND 100 04/25/12 01:21 Ethylbenzene ug/L ND 5.0 04/25/12 01:21 Hexachloro-1,3-butadiene ug/L ND 5.0 04/25/12 01:21 Iodomethane ug/L ND 10.0 04/25/12 01:21 Isopropylbenzene (Cumene)ug/L ND 5.0 04/25/12 01:21 Methyl-tert-butyl ether ug/L ND 4.0 04/25/12 01:21 Methylene Chloride ug/L ND 5.0 04/25/12 01:21 n-Butylbenzene ug/L ND 5.0 04/25/12 01:21 n-Hexane ug/L ND 5.0 N204/25/12 01:21 n-Propylbenzene ug/L ND 5.0 04/25/12 01:21 Naphthalene ug/L ND 5.0 04/25/12 01:21 p-Isopropyltoluene ug/L ND 5.0 04/25/12 01:21 sec-Butylbenzene ug/L ND 5.0 04/25/12 01:21 Styrene ug/L ND 5.0 04/25/12 01:21 tert-Butylbenzene ug/L ND 5.0 04/25/12 01:21 Tetrachloroethene ug/L ND 5.0 04/25/12 01:21 Toluene ug/L ND 5.0 04/25/12 01:21 trans-1,2-Dichloroethene ug/L ND 5.0 04/25/12 01:21 trans-1,3-Dichloropropene ug/L ND 5.0 04/25/12 01:21 trans-1,4-Dichloro-2-butene ug/L ND 100 04/25/12 01:21 Trichloroethene ug/L ND 5.0 04/25/12 01:21 Trichlorofluoromethane ug/L ND 5.0 04/25/12 01:21 Vinyl acetate ug/L ND 50.0 04/25/12 01:21 Vinyl chloride ug/L ND 2.0 04/25/12 01:21 Xylene (Total)ug/L ND 10.0 04/25/12 01:21 4-Bromofluorobenzene (S)%.103 72-125 04/25/12 01:21 Dibromofluoromethane (S)%.104 83-123 04/25/12 01:21 Toluene-d8 (S)%.101 81-114 04/25/12 01:21 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724951LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 43.650 87 69-122 1,1,1-Trichloroethane ug/L 43.750 87 69-126 1,1,2,2-Tetrachloroethane ug/L 48.950 98 68-134 1,1,2-Trichloroethane ug/L 46.450 93 77-129 1,1-Dichloroethane ug/L 52.450 105 70-127 1,1-Dichloroethene ug/L 47.150 94 75-145 1,1-Dichloropropene ug/L 45.950 92 75-126 1,2,3-Trichlorobenzene ug/L 42.450 85 63-130 1,2,3-Trichloropropane ug/L 66.0 L35013245-121 1,2,4-Trichlorobenzene ug/L 33.950 68 64-122 1,2,4-Trimethylbenzene ug/L 45.650 91 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 63 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724951LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 41.050 82 77-123 1,2-Dichlorobenzene ug/L 44.950 90 74-123 1,2-Dichloroethane ug/L 42.350 85 71-127 1,2-Dichloropropane ug/L 47.350 95 75-126 1,3,5-Trimethylbenzene ug/L 43.250 86 69-129 1,3-Dichlorobenzene ug/L 40.350 81 76-123 1,3-Dichloropropane ug/L 40.650 81 77-126 1,4-Dichlorobenzene ug/L 39.950 80 77-121 2,2-Dichloropropane ug/L 44.150 88 45-138 2-Butanone (MEK)ug/L 261250 104 42-177 2-Chlorotoluene ug/L 43.750 87 74-129 2-Hexanone ug/L 215250 86 57-162 4-Chlorotoluene ug/L 45.250 90 70-125 4-Methyl-2-pentanone (MIBK)ug/L 213250 85 64-135 Acetone ug/L 268250 107 10-200 Acrolein ug/L 13401000 134 10-200 Acrylonitrile ug/L 8101000 81 59-144 Benzene ug/L 45.650 91 76-123 Bromobenzene ug/L 46.550 93 67-130 Bromochloromethane ug/L 50.950 102 58-153 Bromodichloromethane ug/L 42.050 84 71-124 Bromoform ug/L 36.750 73 64-116 Bromomethane ug/L 55.450 111 23-197 Carbon disulfide ug/L 101100 101 55-146 Carbon tetrachloride ug/L 41.150 82 65-125 Chlorobenzene ug/L 47.550 95 78-120 Chloroethane ug/L 61.550 123 56-163 Chloroform ug/L 44.250 88 73-122 Chloromethane ug/L 49.150 98 46-146 cis-1,2-Dichloroethene ug/L 46.750 93 79-129 cis-1,3-Dichloropropene ug/L 41.650 83 66-123 Dibromochloromethane ug/L 39.250 78 70-123 Dibromomethane ug/L 46.750 93 73-123 Dichlorodifluoromethane ug/L 50.150 100 19-200 Ethyl methacrylate ug/L 184200 92 70-127 Ethylbenzene ug/L 45.350 91 75-120 Hexachloro-1,3-butadiene ug/L 40.250 80 64-131 Iodomethane ug/L 84.8100 85 16-181 Isopropylbenzene (Cumene)ug/L 37.950 76 73-123 Methyl-tert-butyl ether ug/L 101100 101 66-128 Methylene Chloride ug/L 44.550 89 61-138 n-Butylbenzene ug/L 41.550 83 69-130 n-Hexane ug/L 38.4 N2507767-142 n-Propylbenzene ug/L 44.650 89 71-132 Naphthalene ug/L 44.950 90 62-130 p-Isopropyltoluene ug/L 45.150 90 71-126 sec-Butylbenzene ug/L 45.250 90 69-130 Styrene ug/L 37.450 75 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 64 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724951LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 37.250 74 49-114 Tetrachloroethene ug/L 34.750 69 57-125 Toluene ug/L 47.150 94 72-124 trans-1,2-Dichloroethene ug/L 44.750 89 71-145 trans-1,3-Dichloropropene ug/L 38.750 77 58-118 trans-1,4-Dichloro-2-butene ug/L 150200 75 50-121 Trichloroethene ug/L 44.450 89 77-122 Trichlorofluoromethane ug/L 52.350 105 56-159 Vinyl acetate ug/L 260 L320013027-119 Vinyl chloride ug/L 52.750 105 61-146 Xylene (Total)ug/L 134150 89 72-126 4-Bromofluorobenzene (S)%.96 72-125 Dibromofluoromethane (S)%.101 83-123 Toluene-d8 (S)%.99 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 724952MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061826005 724953 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 94 30-12293 2 2050ND47.1 46.4 1,1,1-Trichloroethane ug/L 50 96 37-13696 .6 2050ND48.1 47.8 1,1,2,2-Tetrachloroethane ug/L 50 108 47-132110 2 2050ND54.1 55.0 1,1,2-Trichloroethane ug/L 50 109 53-131103 5 2050ND54.5 51.7 1,1-Dichloroethane ug/L 50 117 47-138117 .2 2050ND58.7 58.6 1,1-Dichloroethene ug/L 50 102 54-152101 1 2050ND51.0 50.5 1,1-Dichloropropene ug/L 50 106 47-13698 8 2050ND53.2 49.1 1,2,3-Trichlorobenzene ug/L 50 94 15-13297 3 2050ND46.9 48.3 1,2,3-Trichloropropane ug/L M05014424-108148 3 2050ND71.9 73.9 1,2,4-Trichlorobenzene ug/L 50 75 10-13078 4 2050ND37.5 39.0 1,2,4-Trimethylbenzene ug/L 50 97 10-14195 2 2050ND48.5 47.4 1,2-Dibromoethane (EDB)ug/L 50 91 49-13089 3 2050ND45.4 44.3 1,2-Dichlorobenzene ug/L 50 104 20-137104 .1 2050ND51.8 51.9 1,2-Dichloroethane ug/L 50 95 42-13995 1 2050ND47.3 47.7 1,2-Dichloropropane ug/L 50 111 50-131103 7 2050ND55.3 51.6 1,3,5-Trimethylbenzene ug/L 50 91 10-14590 1 2050ND45.7 45.0 1,3-Dichlorobenzene ug/L 50 94 13-14392 1 2050ND46.8 46.2 1,3-Dichloropropane ug/L 50 92 53-13088 4 2050ND45.8 43.9 1,4-Dichlorobenzene ug/L 50 91 13-14091 .6 2050ND45.6 45.3 2,2-Dichloropropane ug/L 50 87 13-14289 3 2050ND43.3 44.5 2-Butanone (MEK)ug/L 250 125 43-142114 9 20250ND313286 2-Chlorotoluene ug/L 50 98 15-14598 .3 2050ND48.8 49.0 2-Hexanone ug/L 250 95 46-13994 2 20250ND238234 4-Chlorotoluene ug/L 50 102 12-14399 3 2050ND51.2 49.7 4-Methyl-2-pentanone (MIBK)ug/L 250 95 43-14094 2 20250ND238234 Acetone ug/L 250 120 38-155130 8 20250ND332359 Acrolein ug/L 1000 135 11-200131 3 201000ND13501310 Acrylonitrile ug/L 1000 90 42-15090 1 201000ND904895 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 65 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724952MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061826005 724953 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 107 52-134100 6 2050ND53.3 50.2 Bromobenzene ug/L 50 107 25-140122 14 2050ND53.3 61.2 Bromochloromethane ug/L 50 117 54-144104 12 2050ND58.5 52.1 Bromodichloromethane ug/L 50 93 42-12889 4 2050ND46.4 44.5 Bromoform ug/L 50 74 34-11678 6 2050ND36.8 39.2 Bromomethane ug/L 50 101 10-200119 17 2050ND50.4 59.5 Carbon disulfide ug/L 100 117 43-144112 5 20100ND117112 Carbon tetrachloride ug/L 50 83 26-13687 5 2050ND41.4 43.3 Chlorobenzene ug/L 50 112 33-136107 5 2050ND56.2 53.3 Chloroethane ug/L 50 131 21-200119 10 2050ND65.6 59.6 Chloroform ug/L 50 104 50-134102 3 2050ND52.2 50.9 Chloromethane ug/L 50 103 32-16085 19 2050ND51.3 42.5 cis-1,2-Dichloroethene ug/L 50 109 48-145109 .1 2050ND54.6 54.5 cis-1,3-Dichloropropene ug/L 50 89 35-11687 3 2050ND44.6 43.4 Dibromochloromethane ug/L 50 83 39-12280 4 2050ND41.4 39.9 Dibromomethane ug/L 50 105 49-134106 .2 2050ND52.7 52.8 Dichlorodifluoromethane ug/L 50 117 35-200109 7 2050ND58.5 54.4 Ethyl methacrylate ug/L 200 101 54-12396 5 20200ND203192 Ethylbenzene ug/L 50 101 29-13297 4 2050ND50.5 48.7 Hexachloro-1,3-butadiene ug/L 50 89 10-14680 11 2050ND44.7 40.2 Iodomethane ug/L 100 78 10-17182 4 20100ND78.0 81.5 Isopropylbenzene (Cumene)ug/L 50 88 11-14682 6 2050ND43.8 41.2 Methyl-tert-butyl ether ug/L 100 115 39-137113 2 20100ND115113 Methylene Chloride ug/L 50 88 47-14188 .8 2050ND44.2 43.8 n-Butylbenzene ug/L 50 93 10-15690 4 2050ND46.7 44.9 n-Hexane ug/L N2508351-13786 4 2050ND41.4 42.9 n-Propylbenzene ug/L 50 99 10-14897 2 2050ND49.7 48.5 Naphthalene ug/L 50 95 40-12495 .003 2050ND47.6 47.6 p-Isopropyltoluene ug/L 50 99 10-15096 3 2050ND49.5 47.9 sec-Butylbenzene ug/L 50 100 10-15096 4 2050ND50.2 48.2 Styrene ug/L 50 81 20-14377 5 2050ND40.3 38.4 tert-Butylbenzene ug/L 50 82 10-12380 2 2050ND41.2 40.2 Tetrachloroethene ug/L 50 83 30-12477 8 2050ND41.7 38.5 Toluene ug/L 50 109 42-130104 4 2050ND54.5 52.2 trans-1,2-Dichloroethene ug/L 50 103 48-14498 5 2050ND51.5 48.9 trans-1,3-Dichloropropene ug/L 50 83 24-11486 4 2050ND41.7 43.2 trans-1,4-Dichloro-2-butene ug/L 200 82 22-12084 3 20200ND165169 Trichloroethene ug/L 50 99 44-13098 2 2050ND49.6 48.8 Trichlorofluoromethane ug/L 50 120 17-200114 5 2050ND60.1 57.0 Vinyl acetate ug/L 200 98 10-11599 1 20200ND196198 Vinyl chloride ug/L 50 120 45-159114 5 2050ND59.9 56.8 Xylene (Total)ug/L 150 102 29-13196 6 20150ND153144 4-Bromofluorobenzene (S)%.101 72-12599 20 Dibromofluoromethane (S)%.102 83-123101 20 Toluene-d8 (S)%.103 81-11497 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 66 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41568 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061800001, 5061800002, 5061800009, 5061800010 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724962 Associated Lab Samples:5061800001, 5061800002, 5061800009, 5061800010 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/25/12 01:38 1,1,1-Trichloroethane ug/L ND 5.0 04/25/12 01:38 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/25/12 01:38 1,1,2-Trichloroethane ug/L ND 5.0 04/25/12 01:38 1,1-Dichloroethane ug/L ND 5.0 04/25/12 01:38 1,1-Dichloroethene ug/L ND 5.0 04/25/12 01:38 1,1-Dichloropropene ug/L ND 5.0 04/25/12 01:38 1,2,3-Trichlorobenzene ug/L ND 5.0 04/25/12 01:38 1,2,3-Trichloropropane ug/L ND 5.0 04/25/12 01:38 1,2,4-Trichlorobenzene ug/L ND 5.0 04/25/12 01:38 1,2,4-Trimethylbenzene ug/L ND 5.0 04/25/12 01:38 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/25/12 01:38 1,2-Dichlorobenzene ug/L ND 5.0 04/25/12 01:38 1,2-Dichloroethane ug/L ND 5.0 04/25/12 01:38 1,2-Dichloropropane ug/L ND 5.0 04/25/12 01:38 1,3,5-Trimethylbenzene ug/L ND 5.0 04/25/12 01:38 1,3-Dichlorobenzene ug/L ND 5.0 04/25/12 01:38 1,3-Dichloropropane ug/L ND 5.0 04/25/12 01:38 1,4-Dichlorobenzene ug/L ND 5.0 04/25/12 01:38 2,2-Dichloropropane ug/L ND 5.0 04/25/12 01:38 2-Butanone (MEK)ug/L ND 25.0 04/25/12 01:38 2-Chlorotoluene ug/L ND 5.0 04/25/12 01:38 2-Hexanone ug/L ND 25.0 04/25/12 01:38 4-Chlorotoluene ug/L ND 5.0 04/25/12 01:38 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/25/12 01:38 Acetone ug/L ND 100 04/25/12 01:38 Acrolein ug/L ND 100 04/25/12 01:38 Acrylonitrile ug/L ND 100 04/25/12 01:38 Benzene ug/L ND 5.0 04/25/12 01:38 Bromobenzene ug/L ND 5.0 04/25/12 01:38 Bromochloromethane ug/L ND 5.0 04/25/12 01:38 Bromodichloromethane ug/L ND 5.0 04/25/12 01:38 Bromoform ug/L ND 5.0 04/25/12 01:38 Bromomethane ug/L ND 5.0 04/25/12 01:38 Carbon disulfide ug/L ND 10.0 04/25/12 01:38 Carbon tetrachloride ug/L ND 5.0 04/25/12 01:38 Chlorobenzene ug/L ND 5.0 04/25/12 01:38 Chloroethane ug/L ND 5.0 04/25/12 01:38 Chloroform ug/L ND 5.0 04/25/12 01:38 Chloromethane ug/L ND 5.0 04/25/12 01:38 cis-1,2-Dichloroethene ug/L ND 5.0 04/25/12 01:38 cis-1,3-Dichloropropene ug/L ND 5.0 04/25/12 01:38 Dibromochloromethane ug/L ND 5.0 04/25/12 01:38 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 67 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724962 Associated Lab Samples:5061800001, 5061800002, 5061800009, 5061800010 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 04/25/12 01:38 Dichlorodifluoromethane ug/L ND 5.0 04/25/12 01:38 Ethyl methacrylate ug/L ND 100 04/25/12 01:38 Ethylbenzene ug/L ND 5.0 04/25/12 01:38 Hexachloro-1,3-butadiene ug/L ND 5.0 04/25/12 01:38 Iodomethane ug/L ND 10.0 04/25/12 01:38 Isopropylbenzene (Cumene)ug/L ND 5.0 04/25/12 01:38 Methyl-tert-butyl ether ug/L ND 4.0 04/25/12 01:38 Methylene Chloride ug/L ND 5.0 04/25/12 01:38 n-Butylbenzene ug/L ND 5.0 04/25/12 01:38 n-Hexane ug/L ND 5.0 N204/25/12 01:38 n-Propylbenzene ug/L ND 5.0 04/25/12 01:38 Naphthalene ug/L ND 5.0 04/25/12 01:38 p-Isopropyltoluene ug/L ND 5.0 04/25/12 01:38 sec-Butylbenzene ug/L ND 5.0 04/25/12 01:38 Styrene ug/L ND 5.0 04/25/12 01:38 tert-Butylbenzene ug/L ND 5.0 04/25/12 01:38 Tetrachloroethene ug/L ND 5.0 04/25/12 01:38 Toluene ug/L ND 5.0 04/25/12 01:38 trans-1,2-Dichloroethene ug/L ND 5.0 04/25/12 01:38 trans-1,3-Dichloropropene ug/L ND 5.0 04/25/12 01:38 trans-1,4-Dichloro-2-butene ug/L ND 100 04/25/12 01:38 Trichloroethene ug/L ND 5.0 04/25/12 01:38 Trichlorofluoromethane ug/L ND 5.0 04/25/12 01:38 Vinyl acetate ug/L ND 50.0 04/25/12 01:38 Vinyl chloride ug/L ND 2.0 04/25/12 01:38 Xylene (Total)ug/L ND 10.0 04/25/12 01:38 4-Bromofluorobenzene (S)%.100 72-125 04/25/12 01:38 Dibromofluoromethane (S)%.97 83-123 04/25/12 01:38 Toluene-d8 (S)%.102 81-114 04/25/12 01:38 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724963LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.050 96 69-122 1,1,1-Trichloroethane ug/L 47.750 95 69-126 1,1,2,2-Tetrachloroethane ug/L 47.750 95 68-134 1,1,2-Trichloroethane ug/L 41.750 83 77-129 1,1-Dichloroethane ug/L 47.650 95 70-127 1,1-Dichloroethene ug/L 51.350 103 75-145 1,1-Dichloropropene ug/L 51.650 103 75-126 1,2,3-Trichlorobenzene ug/L 39.950 80 63-130 1,2,3-Trichloropropane ug/L 71.9 L35014445-121 1,2,4-Trichlorobenzene ug/L 37.450 75 64-122 1,2,4-Trimethylbenzene ug/L 54.250 108 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 68 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724963LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 46.550 93 77-123 1,2-Dichlorobenzene ug/L 40.650 81 74-123 1,2-Dichloroethane ug/L 48.350 97 71-127 1,2-Dichloropropane ug/L 45.950 92 75-126 1,3,5-Trimethylbenzene ug/L 52.650 105 69-129 1,3-Dichlorobenzene ug/L 49.350 99 76-123 1,3-Dichloropropane ug/L 45.150 90 77-126 1,4-Dichlorobenzene ug/L 40.350 81 77-121 2,2-Dichloropropane ug/L 47.450 95 45-138 2-Butanone (MEK)ug/L 287250 115 42-177 2-Chlorotoluene ug/L 50.250 100 74-129 2-Hexanone ug/L 240250 96 57-162 4-Chlorotoluene ug/L 43.050 86 70-125 4-Methyl-2-pentanone (MIBK)ug/L 230250 92 64-135 Acetone ug/L 275250 110 10-200 Acrolein ug/L 15401000 154 10-200 Acrylonitrile ug/L 8671000 87 59-144 Benzene ug/L 45.350 91 76-123 Bromobenzene ug/L 50.250 100 67-130 Bromochloromethane ug/L 51.750 103 58-153 Bromodichloromethane ug/L 45.350 91 71-124 Bromoform ug/L 42.950 86 64-116 Bromomethane ug/L 61.350 123 23-197 Carbon disulfide ug/L 99.1100 99 55-146 Carbon tetrachloride ug/L 44.750 89 65-125 Chlorobenzene ug/L 50.350 101 78-120 Chloroethane ug/L 67.150 134 56-163 Chloroform ug/L 45.050 90 73-122 Chloromethane ug/L 56.150 112 46-146 cis-1,2-Dichloroethene ug/L 51.550 103 79-129 cis-1,3-Dichloropropene ug/L 45.450 91 66-123 Dibromochloromethane ug/L 45.050 90 70-123 Dibromomethane ug/L 47.350 95 73-123 Dichlorodifluoromethane ug/L 53.550 107 19-200 Ethyl methacrylate ug/L 181200 90 70-127 Ethylbenzene ug/L 54.350 109 75-120 Hexachloro-1,3-butadiene ug/L 42.650 85 64-131 Iodomethane ug/L 97.7100 98 16-181 Isopropylbenzene (Cumene)ug/L 52.450 105 73-123 Methyl-tert-butyl ether ug/L 108100 108 66-128 Methylene Chloride ug/L 48.550 97 61-138 n-Butylbenzene ug/L 50.550 101 69-130 n-Hexane ug/L 41.7 N2508367-142 n-Propylbenzene ug/L 53.550 107 71-132 Naphthalene ug/L 45.850 92 62-130 p-Isopropyltoluene ug/L 52.650 105 71-126 sec-Butylbenzene ug/L 54.250 108 69-130 Styrene ug/L 53.550 107 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 69 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724963LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 41.550 83 49-114 Tetrachloroethene ug/L 38.550 77 57-125 Toluene ug/L 51.850 104 72-124 trans-1,2-Dichloroethene ug/L 48.550 97 71-145 trans-1,3-Dichloropropene ug/L 43.350 87 58-118 trans-1,4-Dichloro-2-butene ug/L 160200 80 50-121 Trichloroethene ug/L 46.850 94 77-122 Trichlorofluoromethane ug/L 57.150 114 56-159 Vinyl acetate ug/L 282 L320014127-119 Vinyl chloride ug/L 60.450 121 61-146 Xylene (Total)ug/L 151150 101 72-126 4-Bromofluorobenzene (S)%.100 72-125 Dibromofluoromethane (S)%.103 83-123 Toluene-d8 (S)%.97 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 724964MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800002 724965 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 89 30-12284 5 2050ND44.5 42.1 1,1,1-Trichloroethane ug/L 50 94 37-13687 8 2050ND47.1 43.6 1,1,2,2-Tetrachloroethane ug/L 50 96 47-13293 4 2050ND48.2 46.5 1,1,2-Trichloroethane ug/L 50 95 53-13188 8 2050ND47.6 44.0 1,1-Dichloroethane ug/L 50 99 47-13889 11 2050ND49.7 44.7 1,1-Dichloroethene ug/L 50 101 54-15291 10 2050ND50.7 45.6 1,1-Dichloropropene ug/L 50 104 47-13690 15 2050ND51.9 44.8 1,2,3-Trichlorobenzene ug/L 50 81 15-13275 7 2050ND40.5 37.7 1,2,3-Trichloropropane ug/L M05013624-108131 4 2050ND68.0 65.5 1,2,4-Trichlorobenzene ug/L 50 75 10-13068 10 2050ND37.6 34.0 1,2,4-Trimethylbenzene ug/L 50 108 10-14192 16 2050ND54.0 46.1 1,2-Dibromoethane (EDB)ug/L 50 91 49-13089 2 2050ND45.4 44.7 1,2-Dichlorobenzene ug/L 50 85 20-13779 7 2050ND42.4 39.5 1,2-Dichloroethane ug/L 50 101 42-13997 4 2050ND50.4 48.6 1,2-Dichloropropane ug/L 50 94 50-13188 7 2050ND46.8 43.8 1,3,5-Trimethylbenzene ug/L 50 104 10-14589 16 2050ND51.9 44.4 1,3-Dichlorobenzene ug/L 50 99 13-14390 9 2050ND49.6 45.1 1,3-Dichloropropane ug/L 50 93 53-13087 7 2050ND46.6 43.4 1,4-Dichlorobenzene ug/L 50 82 13-14074 10 2050ND40.9 37.1 2,2-Dichloropropane ug/L 50 86 13-14279 8 2050ND43.0 39.7 2-Butanone (MEK)ug/L 250 126 43-142124 2 20250ND315310 2-Chlorotoluene ug/L 50 106 15-14591 15 2050ND52.8 45.4 2-Hexanone ug/L 250 99 46-13994 6 20250ND248234 4-Chlorotoluene ug/L 50 88 12-14378 12 2050ND44.0 39.2 4-Methyl-2-pentanone (MIBK)ug/L 250 100 43-14091 10 20250ND250227 Acetone ug/L 250 116 38-155120 4 20250ND290301 Acrolein ug/L 1000 143 11-200139 3 201000ND14301390 Acrylonitrile ug/L 1000 89 42-15091 3 201000ND886914 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 70 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724964MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800002 724965 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 95 52-13487 10 2050ND47.7 43.3 Bromobenzene ug/L R15012125-14093 26 2050ND60.6 46.7 Bromochloromethane ug/L 50 114 54-144101 12 2050ND57.0 50.7 Bromodichloromethane ug/L 50 86 42-12885 .2 2050ND42.8 42.7 Bromoform ug/L 50 70 34-11674 5 2050ND35.2 37.1 Bromomethane ug/L 50 119 10-200116 3 2050ND59.7 58.1 Carbon disulfide ug/L 100 102 43-14490 12 20100ND10289.9 Carbon tetrachloride ug/L 50 76 26-13674 4 2050ND38.2 36.9 Chlorobenzene ug/L 50 108 33-13695 13 2050ND54.1 47.5 Chloroethane ug/L 50 137 21-200118 14 2050ND68.4 59.2 Chloroform ug/L 50 97 50-13489 8 2050ND48.4 44.7 Chloromethane ug/L 50 113 32-160107 6 2050ND56.7 53.3 cis-1,2-Dichloroethene ug/L 50 114 48-145105 9 2050ND57.1 52.3 cis-1,3-Dichloropropene ug/L 50 87 35-11681 8 2050ND43.5 40.3 Dibromochloromethane ug/L 50 76 39-12278 3 2050ND38.1 39.1 Dibromomethane ug/L 50 105 49-134102 3 2050ND52.4 50.9 Dichlorodifluoromethane ug/L 50 109 35-20095 14 2050ND54.5 47.3 Ethyl methacrylate ug/L 200 92 54-12385 8 20200ND185171 Ethylbenzene ug/L 50 118 29-13298 19 2050ND59.0 48.9 Hexachloro-1,3-butadiene ug/L 50 84 10-14674 14 2050ND42.2 36.8 Iodomethane ug/L 100 105 10-17196 9 20100ND10596.3 Isopropylbenzene (Cumene)ug/L 50 112 11-14694 18 2050ND56.2 46.8 Methyl-tert-butyl ether ug/L 100 112 39-137109 3 20100ND112109 Methylene Chloride ug/L 50 94 47-14190 5 2050ND47.2 45.1 n-Butylbenzene ug/L 50 102 10-15687 16 2050ND51.0 43.5 n-Hexane ug/L N2508851-13776 15 2050ND44.1 38.1 n-Propylbenzene ug/L 50 110 10-14894 16 2050ND55.0 47.0 Naphthalene ug/L 50 88 40-12482 7 2050ND44.0 41.1 p-Isopropyltoluene ug/L 50 107 10-15089 18 2050ND53.4 44.5 sec-Butylbenzene ug/L 50 110 10-15092 18 2050ND55.2 46.2 Styrene ug/L 50 106 20-14393 13 2050ND52.9 46.4 tert-Butylbenzene ug/L 50 84 10-12373 14 2050ND42.0 36.4 Tetrachloroethene ug/L 50 89 30-12472 20 2050ND47.2 38.5 Toluene ug/L 50 110 42-13093 17 2050ND54.9 46.5 trans-1,2-Dichloroethene ug/L 50 103 48-14492 11 2050ND51.7 46.1 trans-1,3-Dichloropropene ug/L 50 81 24-11478 4 2050ND40.7 39.0 trans-1,4-Dichloro-2-butene ug/L 200 75 22-12071 6 20200ND149141 Trichloroethene ug/L 50 96 44-13084 12 20508.2 56.2 50.0 Trichlorofluoromethane ug/L 50 118 17-20099 17 2050ND58.8 49.7 Vinyl acetate ug/L 200 97 10-115100 3 20200ND195200 Vinyl chloride ug/L 50 125 45-159109 14 2050ND62.5 54.3 Xylene (Total)ug/L 150 107 29-13191 17 20150ND161136 4-Bromofluorobenzene (S)%.101 72-125101 20 Dibromofluoromethane (S)%.98 83-123106 20 Toluene-d8 (S)%.101 81-11497 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 71 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/29416 EPA 3510 EPA 8082 8082 GCS PCB Mod Associated Lab Samples:5061800001, 5061800002, 5061800003, 5061800004, 5061800006, 5061800007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724549 Associated Lab Samples:5061800001, 5061800002, 5061800003, 5061800004, 5061800006, 5061800007 Matrix:Water Analyzed PCB-1016 (Aroclor 1016)ug/L ND 0.50 04/24/12 17:50 PCB-1221 (Aroclor 1221)ug/L ND 0.50 04/24/12 17:50 PCB-1232 (Aroclor 1232)ug/L ND 0.50 04/24/12 17:50 PCB-1242 (Aroclor 1242)ug/L ND 0.50 04/24/12 17:50 PCB-1248 (Aroclor 1248)ug/L ND 0.50 04/24/12 17:50 PCB-1254 (Aroclor 1254)ug/L ND 0.50 04/24/12 17:50 PCB-1260 (Aroclor 1260)ug/L ND 0.50 04/24/12 17:50 Tetrachloro-m-xylene (S)%.86 39-110 04/24/12 17:50 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724550LABORATORY CONTROL SAMPLE: LCSSpike PCB-1016 (Aroclor 1016)ug/L 4.85 97 49-110 PCB-1260 (Aroclor 1260)ug/L 5.25 104 57-108 Tetrachloro-m-xylene (S)%.89 39-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 724551MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800002 724552 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. PCB-1016 (Aroclor 1016)ug/L 10.3 87 61-10193 7 2010.3ND 9.0 9.6 PCB-1260 (Aroclor 1260)ug/L 10.3 97 61-10499 3 2010.3ND 10 10.2 Tetrachloro-m-xylene (S)%.81 39-11086 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 72 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/29415 EPA 3510 EPA 8270 by SIM 8270 Water PAH Associated Lab Samples:5061800003, 5061800004, 5061800005, 5061800006, 5061800007, 5061800008, 5061800009, 5061800010, 5061800013 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724543 Associated Lab Samples:5061800003, 5061800004, 5061800005, 5061800006, 5061800007, 5061800008, 5061800009, 5061800010, 5061800013 Matrix:Water Analyzed 2-Methylnaphthalene ug/L ND 1.0 04/25/12 18:47 Acenaphthene ug/L ND 1.0 04/25/12 18:47 Acenaphthylene ug/L ND 1.0 04/25/12 18:47 Anthracene ug/L ND 0.10 04/25/12 18:47 Benzo(a)anthracene ug/L ND 0.10 04/25/12 18:47 Benzo(a)pyrene ug/L ND 0.10 04/25/12 18:47 Benzo(b)fluoranthene ug/L ND 0.10 04/25/12 18:47 Benzo(g,h,i)perylene ug/L ND 0.10 04/25/12 18:47 Benzo(k)fluoranthene ug/L ND 0.10 04/25/12 18:47 Chrysene ug/L ND 0.50 04/25/12 18:47 Dibenz(a,h)anthracene ug/L ND 0.10 04/25/12 18:47 Fluoranthene ug/L ND 1.0 04/25/12 18:47 Fluorene ug/L ND 1.0 04/25/12 18:47 Indeno(1,2,3-cd)pyrene ug/L ND 0.10 04/25/12 18:47 Naphthalene ug/L ND 1.0 04/25/12 18:47 Phenanthrene ug/L ND 1.0 04/25/12 18:47 Pyrene ug/L ND 1.0 04/25/12 18:47 2-Fluorobiphenyl (S)%.77 26-106 04/25/12 18:47 p-Terphenyl-d14 (S)%.101 16-111 04/25/12 18:47 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724544LABORATORY CONTROL SAMPLE: LCSSpike 2-Methylnaphthalene ug/L 7.510 75 24-104 Acenaphthene ug/L 8.310 83 31-108 Acenaphthylene ug/L 8.410 84 33-111 Anthracene ug/L 8.910 89 45-120 Benzo(a)anthracene ug/L 8.810 88 51-119 Benzo(a)pyrene ug/L 8.910 89 52-124 Benzo(b)fluoranthene ug/L 7.710 77 51-122 Benzo(g,h,i)perylene ug/L 8.810 88 48-112 Benzo(k)fluoranthene ug/L 10.210 102 53-123 Chrysene ug/L 9.610 96 54-118 Dibenz(a,h)anthracene ug/L 9.210 92 49-114 Fluoranthene ug/L 8.410 84 52-122 Fluorene ug/L 8.310 83 38-113 Indeno(1,2,3-cd)pyrene ug/L 9.010 90 49-114 Naphthalene ug/L 7.510 75 27-103 Phenanthrene ug/L 8.210 82 43-112 Pyrene ug/L 9.610 96 51-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 73 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724544LABORATORY CONTROL SAMPLE: LCSSpike 2-Fluorobiphenyl (S)%.78 26-106 p-Terphenyl-d14 (S)%.97 16-111 Parameter Units MS Result % Rec Limits Qual% RecConc. 724545MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800006 724546 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Methylnaphthalene ug/L 20.4 70 10-13061 14 2020.4ND 14.3 12.5 Acenaphthene ug/L 20.4 67 32-10263 6 2020.4ND 13.7 12.9 Acenaphthylene ug/L 20.4 72 25-11869 3 2020.4ND 14.6 14.2 Anthracene ug/L 20.4 74 46-11672 2 2020.4ND 15.0 14.7 Benzo(a)anthracene ug/L 20.4 70 31-10271 .9 2020.4ND 14.4 14.5 Benzo(a)pyrene ug/L 20.4 63 10-9368 7 2020.4ND 12.9 13.9 Benzo(b)fluoranthene ug/L 20.4 60 11-9363 5 2020.4ND 12.2 12.9 Benzo(g,h,i)perylene ug/L 20.4 54 10-7765 18 2020.4ND 11.1 13.3 Benzo(k)fluoranthene ug/L 20.4 76 12-9180 6 2020.4ND 15.4 16.4 Chrysene ug/L 20.4 80 34-9984 5 2020.4ND 16.3 17.1 Dibenz(a,h)anthracene ug/L 20.4 57 10-7968 17 2020.4ND 11.6 13.9 Fluoranthene ug/L 20.4 75 48-11675 .4 2020.4ND 15.4 15.3 Fluorene ug/L 20.4 71 41-10867 5 2020.4ND 14.5 13.7 Indeno(1,2,3-cd)pyrene ug/L 20.4 56 10-7967 18 2020.4ND 11.4 13.6 Naphthalene ug/L 20.4 67 23-10762 7 2020.4ND 13.6 12.7 Phenanthrene ug/L 20.4 75 46-10772 3 2020.4ND 15.3 14.8 Pyrene ug/L 20.4 80 46-11579 .9 2020.4ND 16.3 16.1 2-Fluorobiphenyl (S)%.65 26-10662 20 p-Terphenyl-d14 (S)%.82 16-11182 20 Parameter Units MS Result % Rec Limits Qual% RecConc. 724547MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800008 724548 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Methylnaphthalene ug/L 20.6 67 10-13068 2 2020.6ND 13.8 14.1 Acenaphthene ug/L 20.6 72 32-10269 4 2020.6ND 14.8 14.3 Acenaphthylene ug/L 20.6 75 25-11870 6 2020.6ND 15.4 14.5 Anthracene ug/L 20.6 82 46-11682 .07 2020.6ND 16.9 16.9 Benzo(a)anthracene ug/L 20.6 75 31-10277 3 2020.6ND 15.5 15.9 Benzo(a)pyrene ug/L 20.6 70 10-9373 3 2020.6ND 14.5 15.0 Benzo(b)fluoranthene ug/L 20.6 63 11-9364 1 2020.6ND 13.1 13.2 Benzo(g,h,i)perylene ug/L 20.6 60 10-7764 5 2020.6ND 12.4 13.1 Benzo(k)fluoranthene ug/L 20.6 81 12-9184 4 2020.6ND 16.7 17.4 Chrysene ug/L 20.6 85 34-9990 6 2020.6ND 17.4 18.5 Dibenz(a,h)anthracene ug/L 20.6 62 10-7964 3 2020.6ND 12.7 13.2 Fluoranthene ug/L 20.6 77 48-11678 2 2020.6ND 15.8 16.1 Fluorene ug/L 20.6 73 41-10871 3 2020.6ND 15.0 14.6 Indeno(1,2,3-cd)pyrene ug/L 20.6 62 10-7965 4 2020.6ND 12.8 13.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 74 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724547MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800008 724548 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Naphthalene ug/L 20.6 67 23-10763 7 2020.6ND 13.9 13.0 Phenanthrene ug/L 20.6 75 46-10775 .5 2020.6ND 15.4 15.5 Pyrene ug/L 20.6 86 46-11589 3 2020.6ND 17.7 18.3 2-Fluorobiphenyl (S)%.67 26-10665 20 p-Terphenyl-d14 (S)%.84 16-11185 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 75 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/29414 EPA 3510 EPA 8270 8270 Water Scan Associated Lab Samples:5061800003, 5061800004, 5061800005, 5061800006, 5061800007, 5061800008, 5061800009, 5061800010, 5061800013 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724537 Associated Lab Samples:5061800003, 5061800004, 5061800005, 5061800006, 5061800007, 5061800008, 5061800009, 5061800010, 5061800013 Matrix:Water Analyzed 2,4,5-Trichlorophenol ug/L ND 10.0 04/25/12 03:08 2,4,6-Trichlorophenol ug/L ND 10.0 04/25/12 03:08 2,4-Dichlorophenol ug/L ND 10.0 04/25/12 03:08 2,4-Dimethylphenol ug/L ND 10.0 04/25/12 03:08 2,4-Dinitrophenol ug/L ND 50.0 04/25/12 03:08 2,4-Dinitrotoluene ug/L ND 10.0 04/25/12 03:08 2,6-Dinitrotoluene ug/L ND 10.0 04/25/12 03:08 2-Chloronaphthalene ug/L ND 10.0 04/25/12 03:08 2-Chlorophenol ug/L ND 10.0 04/25/12 03:08 2-Methylphenol(o-Cresol)ug/L ND 10.0 04/25/12 03:08 2-Nitroaniline ug/L ND 50.0 04/25/12 03:08 2-Nitrophenol ug/L ND 10.0 04/25/12 03:08 3&4-Methylphenol(m&p Cresol)ug/L ND 20.0 04/25/12 03:08 3,3'-Dichlorobenzidine ug/L ND 20.0 04/25/12 03:08 3-Nitroaniline ug/L ND 50.0 04/25/12 03:08 4,6-Dinitro-2-methylphenol ug/L ND 50.0 04/25/12 03:08 4-Bromophenylphenyl ether ug/L ND 10.0 04/25/12 03:08 4-Chloro-3-methylphenol ug/L ND 20.0 04/25/12 03:08 4-Chloroaniline ug/L ND 20.0 04/25/12 03:08 4-Chlorophenylphenyl ether ug/L ND 10.0 04/25/12 03:08 4-Nitroaniline ug/L ND 50.0 04/25/12 03:08 4-Nitrophenol ug/L ND 50.0 04/25/12 03:08 Benzyl alcohol ug/L ND 20.0 04/25/12 03:08 bis(2-Chloroethoxy)methane ug/L ND 10.0 04/25/12 03:08 bis(2-Chloroethyl) ether ug/L ND 10.0 04/25/12 03:08 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/25/12 03:08 bis(2chloro1methylethyl) ether ug/L ND 5.0 04/25/12 03:08 Butylbenzylphthalate ug/L ND 10.0 04/25/12 03:08 Di-n-butylphthalate ug/L ND 10.0 04/25/12 03:08 Di-n-octylphthalate ug/L ND 10.0 04/25/12 03:08 Dibenzofuran ug/L ND 10.0 04/25/12 03:08 Diethylphthalate ug/L ND 10.0 04/25/12 03:08 Dimethylphthalate ug/L ND 10.0 04/25/12 03:08 Hexachloro-1,3-butadiene ug/L ND 5.0 04/25/12 03:08 Hexachlorobenzene ug/L ND 10.0 04/25/12 03:08 Hexachlorocyclopentadiene ug/L ND 25.0 04/25/12 03:08 Hexachloroethane ug/L ND 10.0 04/25/12 03:08 Isophorone ug/L ND 10.0 04/25/12 03:08 N-Nitroso-di-n-propylamine ug/L ND 10.0 04/25/12 03:08 N-Nitrosodiphenylamine ug/L ND 10.0 04/25/12 03:08 Nitrobenzene ug/L ND 10.0 04/25/12 03:08 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 76 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:724537 Associated Lab Samples:5061800003, 5061800004, 5061800005, 5061800006, 5061800007, 5061800008, 5061800009, 5061800010, 5061800013 Matrix:Water Analyzed Pentachlorophenol ug/L ND 50.0 04/25/12 03:08 Phenol ug/L ND 10.0 04/25/12 03:08 2,4,6-Tribromophenol (S)%.99 32-124 04/25/12 03:08 2-Fluorophenol (S)%.38 10-74 04/25/12 03:08 Nitrobenzene-d5 (S)%.76 33-108 04/25/12 03:08 Phenol-d5 (S)%.22 10-56 04/25/12 03:08 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 724538LABORATORY CONTROL SAMPLE: LCSSpike 2,4-Dinitrotoluene ug/L 88.3100 88 38-119 2-Chlorophenol ug/L 78.3100 78 37-106 4-Chloro-3-methylphenol ug/L 85.3100 85 43-115 4-Nitrophenol ug/L 27.1J100 27 10-57 N-Nitroso-di-n-propylamine ug/L 89.8100 90 43-112 Pentachlorophenol ug/L 101100 101 14-131 Phenol ug/L 24.8100 25 14-50 2,4,6-Tribromophenol (S)%.105 32-124 2-Fluorophenol (S)%.43 10-74 Nitrobenzene-d5 (S)%.85 33-108 Phenol-d5 (S)%.25 10-56 Parameter Units MS Result % Rec Limits Qual% RecConc. 724539MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800006 724540 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2,4-Dinitrotoluene ug/L 204 74 37-11473 .3 20204ND150150 2-Chlorophenol ug/L 204 63 43-10266 4 20204ND128134 4-Chloro-3-methylphenol ug/L 204 59 49-10868 14 20204ND121139 4-Nitrophenol ug/L 204 37 10-9936 20204ND74.7J 74.4J N-Nitroso-di-n-propylamine ug/L 204 67 43-10773 9 20204ND137150 Pentachlorophenol ug/L 204 83 25-11784 2 20204ND169172 Phenol ug/L 204 30 28-7432 6 20204ND62.1 66.1 2,4,6-Tribromophenol (S)%.84 32-12485 20 2-Fluorophenol (S)%.44 10-7447 20 Nitrobenzene-d5 (S)%.66 33-10870 20 Phenol-d5 (S)%.30 10-5631 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 77 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061800 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 724541MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061800008 724542 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2,4-Dinitrotoluene ug/L 206 73 37-11475 3 20206ND151155 2-Chlorophenol ug/L 206 64 43-10262 4 20206ND132127 4-Chloro-3-methylphenol ug/L 206 70 49-10869 1 20206ND144142 4-Nitrophenol ug/L 206 33 10-9937 20206ND68.9J 75.6J N-Nitroso-di-n-propylamine ug/L 206 73 43-10766 9 20206ND150137 Pentachlorophenol ug/L 206 79 25-11783 5 20206ND163171 Phenol ug/L 206 30 28-7431 2 20206ND62.8 64.1 2,4,6-Tribromophenol (S)%.86 32-12485 20 2-Fluorophenol (S)%.46 10-7446 20 Nitrobenzene-d5 (S)%.68 33-10865 20 Phenol-d5 (S)%.29 10-5630 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 78 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5061800 SBI067 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 79 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5061800 SBI067 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5061800001 OEXT/29416 GCSV/9256SBI067:HTB17:G350390 EPA 3510 EPA 8082 5061800002 OEXT/29416 GCSV/9256SBI067:HTB17:G260300 EPA 3510 EPA 8082 5061800003 OEXT/29416 GCSV/9256SBI067:HTB18:G450490 EPA 3510 EPA 8082 5061800004 OEXT/29416 GCSV/9256SBI067:HTB18:G350390 EPA 3510 EPA 8082 5061800006 OEXT/29416 GCSV/9256SBI067:HTB18:G260300 EPA 3510 EPA 8082 5061800007 OEXT/29416 GCSV/9256SBI067:FB1:W041912 EPA 3510 EPA 8082 5061800003 OEXT/29415 MSSV/10029SBI067:HTB18:G450490 EPA 3510 EPA 8270 by SIM 5061800004 OEXT/29415 MSSV/10029SBI067:HTB18:G350390 EPA 3510 EPA 8270 by SIM 5061800005 OEXT/29415 MSSV/10029SBI067:HTB18:G350390A EPA 3510 EPA 8270 by SIM 5061800006 OEXT/29415 MSSV/10029SBI067:HTB18:G260300 EPA 3510 EPA 8270 by SIM 5061800007 OEXT/29415 MSSV/10029SBI067:FB1:W041912 EPA 3510 EPA 8270 by SIM 5061800008 OEXT/29415 MSSV/10029SBI067:HTB5:G350390 EPA 3510 EPA 8270 by SIM 5061800009 OEXT/29415 MSSV/10029SBI067:HTB5:G260300 EPA 3510 EPA 8270 by SIM 5061800010 OEXT/29415 MSSV/10029SBI067:HTB5:G260300A EPA 3510 EPA 8270 by SIM 5061800013 OEXT/29415 MSSV/10029SBI067:FB1:W042012 EPA 3510 EPA 8270 by SIM 5061800003 OEXT/29414 MSSV/10024SBI067:HTB18:G450490 EPA 3510 EPA 8270 5061800004 OEXT/29414 MSSV/10024SBI067:HTB18:G350390 EPA 3510 EPA 8270 5061800005 OEXT/29414 MSSV/10024SBI067:HTB18:G350390A EPA 3510 EPA 8270 5061800006 OEXT/29414 MSSV/10024SBI067:HTB18:G260300 EPA 3510 EPA 8270 5061800007 OEXT/29414 MSSV/10024SBI067:FB1:W041912 EPA 3510 EPA 8270 5061800008 OEXT/29414 MSSV/10024SBI067:HTB5:G350390 EPA 3510 EPA 8270 5061800009 OEXT/29414 MSSV/10024SBI067:HTB5:G260300 EPA 3510 EPA 8270 5061800010 OEXT/29414 MSSV/10024SBI067:HTB5:G260300A EPA 3510 EPA 8270 5061800013 OEXT/29414 MSSV/10024SBI067:FB1:W042012 EPA 3510 EPA 8270 5061800001 MSV/41568SBI067:HTB17:G350390 EPA 8260 5061800002 MSV/41568SBI067:HTB17:G260300 EPA 8260 5061800003 MSV/41537SBI067:HTB18:G450490 EPA 8260 5061800004 MSV/41537SBI067:HTB18:G350390 EPA 8260 5061800006 MSV/41537SBI067:HTB18:G260300 EPA 8260 5061800007 MSV/41537SBI067:FB1:W041912 EPA 8260 5061800008 MSV/41563SBI067:HTB5:G350390 EPA 8260 5061800009 MSV/41568SBI067:HTB5:G260300 EPA 8260 5061800010 MSV/41568SBI067:HTB5:G260300A EPA 8260 5061800011 MSV/41564SBI067:HTB14:G450490 EPA 8260 5061800012 MSV/41564SBI067:HTB14:G350390 EPA 8260 5061800013 MSV/41563SBI067:FB1:W042012 EPA 8260 5061800014 MSV/41563SBI067:HTB14:G260300 EPA 8260 5061800015 MSV/41563SBI067:TB:W041912 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/26/2012 04:19 PM Page 80 of 80 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 April 30, 2012 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5061952 5061952 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 6435 Castleway West Drive Suite 119 Indianapolis, IN 46250 SBI067 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tina Sayer for Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 CERTIFICATIONS Pace Project No.: Project: 5061952 SBI067 Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074 Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042 Louisiana/NELAC Certification #: 04076Ohio VAP: CL0065 Pennsylvania: 68-04991West Virginia Certification #: 330 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE SUMMARY Pace Project No.: Project: 5061952 SBI067 Lab ID Sample ID Matrix Date Collected Date Received 5061952001 SBI067:HTB10:G450490 Water 04/23/12 09:00 04/25/12 12:43 5061952002 SBI067:HTB10:G350390 Water 04/23/12 09:40 04/25/12 12:43 5061952003 SBI067:HTB10:G260300 Water 04/23/12 10:10 04/25/12 12:43 5061952004 SBI067:HTB12:G450490 Water 04/23/12 11:10 04/25/12 12:43 5061952005 SBI067:HTB12:G350390 Water 04/23/12 11:40 04/25/12 12:43 5061952006 SBI067:HTB12:G260300 Water 04/23/12 12:15 04/25/12 12:43 5061952007 SBI067:HTB12:G260300A Water 04/23/12 12:15 04/25/12 12:43 5061952008 SBI067:HTB15:G450490 Water 04/23/12 13:20 04/25/12 12:43 5061952009 SBI067:HTB15:G350390 Water 04/23/12 13:45 04/25/12 12:43 5061952010 SBI067:HTB15:G260300 Water 04/23/12 14:00 04/25/12 12:43 5061952011 SBI067:HTB8:G450490 Water 04/23/12 14:50 04/25/12 12:43 5061952012 SBI067:HTB8:G450490A Water 04/23/12 14:50 04/25/12 12:43 5061952013 SBI067:HTB8:G350390 Water 04/23/12 15:25 04/25/12 12:43 5061952014 SBI067:HTB8:G260300 Water 04/23/12 16:25 04/25/12 12:43 5061952015 SBI067:FBI:W042312 Water 04/23/12 17:00 04/25/12 12:43 5061952016 SBI067:HTB16:G450490 Water 04/24/12 09:00 04/25/12 12:43 5061952017 SBI067:HTB16:G350390 Water 04/24/12 09:30 04/25/12 12:43 5061952018 SBI067:HTB16:G260300 Water 04/24/12 10:00 04/25/12 12:43 5061952019 SBI067:HTB13:G450490 Water 04/24/12 10:40 04/25/12 12:43 5061952020 SBI067:HTB13:G350390 Water 04/24/12 11:15 04/25/12 12:43 5061952021 SBI067:HTB13:G350390A Water 04/24/12 11:15 04/25/12 12:43 5061952022 SBI067:HTB13:G260300 Water 04/24/12 11:40 04/25/12 12:43 5061952023 SBI067:HTB11:G450490 Water 04/24/12 12:40 04/25/12 12:43 5061952024 SBI067:HTB11:G350390 Water 04/24/12 13:00 04/25/12 12:43 5061952025 SBI067:HTB11:G260300 Water 04/24/12 13:30 04/25/12 12:43 5061952026 SBI067:HTB22:G450490 Water 04/24/12 14:25 04/25/12 12:43 5061952027 SBI067:HTB22:G350390 Water 04/24/12 14:50 04/25/12 12:43 5061952028 SBI067:HTB22:G260300 Water 04/24/12 15:30 04/25/12 12:43 5061952029 SBI067:FB1:W042412 Water 04/24/12 16:00 04/25/12 12:43 5061952030 SBI067:TRIP BLANK:W042412 Water 04/23/12 08:00 04/25/12 12:43 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5061952 SBI067 Lab ID Sample ID Method Analytes ReportedAnalysts 5061952001 SBI067:HTB10:G450490 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952002 SBI067:HTB10:G350390 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952003 SBI067:HTB10:G260300 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952004 SBI067:HTB12:G450490 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952005 SBI067:HTB12:G350390 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952006 SBI067:HTB12:G260300 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952007 SBI067:HTB12:G260300A EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8260 73GRM 5061952008 SBI067:HTB15:G450490 EPA 8260 73GRM 5061952009 SBI067:HTB15:G350390 EPA 8260 73GRM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5061952 SBI067 Lab ID Sample ID Method Analytes ReportedAnalysts 5061952010 SBI067:HTB15:G260300 EPA 8260 73GRM 5061952011 SBI067:HTB8:G450490 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73GRM 5061952012 SBI067:HTB8:G450490A EPA 8270 by SIM 19CEM EPA 8270 47KES 5061952013 SBI067:HTB8:G350390 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73GRM 5061952014 SBI067:HTB8:G260300 EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73GRM 5061952015 SBI067:FBI:W042312 EPA 6010 7LLB EPA 6010 7LLB EPA 7470 1LLB EPA 7470 1LLB EPA 8270 by SIM 19CEM EPA 8270 47KES EPA 8260 73GRM 5061952016 SBI067:HTB16:G450490 EPA 8260 73GRM 5061952017 SBI067:HTB16:G350390 EPA 8260 73GRM 5061952018 SBI067:HTB16:G260300 EPA 8260 73GRM 5061952019 SBI067:HTB13:G450490 EPA 8260 73GRM 5061952020 SBI067:HTB13:G350390 EPA 8260 73GRM 5061952021 SBI067:HTB13:G350390A EPA 8260 73GRM 5061952022 SBI067:HTB13:G260300 EPA 8260 73GRM 5061952023 SBI067:HTB11:G450490 EPA 8260 73GRM 5061952024 SBI067:HTB11:G350390 EPA 8260 73GRM 5061952025 SBI067:HTB11:G260300 EPA 8260 73GRM 5061952026 SBI067:HTB22:G450490 EPA 8260 73GRM 5061952027 SBI067:HTB22:G350390 EPA 8260 73GRM 5061952028 SBI067:HTB22:G260300 EPA 8260 73GRM 5061952029 SBI067:FB1:W042412 EPA 8260 73GRM 5061952030 SBI067:TRIP BLANK:W042412 EPA 8260 73GRM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G450490 Lab ID:5061952001 Collected:04/23/12 09:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 0.12 mg/L 1 04/27/12 13:17 7440-38-204/26/12 12:000.010 Barium 0.47 mg/L 1 04/27/12 13:17 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:17 7440-43-904/26/12 12:000.0050 Chromium 0.21 mg/L 1 04/27/12 13:17 7440-47-304/26/12 12:000.010 Lead 0.11 mg/L 1 04/27/12 13:17 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:17 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:17 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 11:35 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 11:35 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 11:35 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 11:35 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 11:35 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 11:35 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 11:35 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:21 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 13:27 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 20:05 67-64-1100 Acrolein ND ug/L 1 04/25/12 20:05 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 20:05 107-13-1100 Benzene ND ug/L 1 04/25/12 20:05 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 20:05 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 20:05 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 20:05 75-27-45.0 Bromoform ND ug/L 1 04/25/12 20:05 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 20:05 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 20:05 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 20:05 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 20:05 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 20:05 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 20:05 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 20:05 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 20:05 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 20:05 75-00-35.0 Chloroform ND ug/L 1 04/25/12 20:05 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 20:05 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 20:05 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 20:05 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 20:05 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 6 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G450490 Lab ID:5061952001 Collected:04/23/12 09:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 20:05 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 20:05 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 20:05 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 20:05 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 20:05 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 20:05 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 20:05 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 20:05 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 20:05 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 20:05 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 20:05 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 20:05 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 20:05 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 20:05 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 20:05 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 20:05 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 20:05 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 20:05 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 20:05 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 20:05 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 20:05 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 20:05 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 20:05 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 20:05 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 20:05 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 20:05 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 20:05 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 20:05 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 20:05 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 20:05 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 20:05 103-65-15.0 Styrene ND ug/L 1 04/25/12 20:05 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 20:05 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 20:05 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 20:05 127-18-45.0 Toluene ND ug/L 1 04/25/12 20:05 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 20:05 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 20:05 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 20:05 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 20:05 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 20:05 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 20:05 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 20:05 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 20:05 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 20:05 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 20:05 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 20:05 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 7 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G450490 Lab ID:5061952001 Collected:04/23/12 09:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 20:05 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/25/12 20:05 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/25/12 20:05 460-00-472-125 Toluene-d8 (S)99 %.1 04/25/12 20:05 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 8 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G350390 Lab ID:5061952002 Collected:04/23/12 09:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 0.018 mg/L 1 04/27/12 13:20 7440-38-204/26/12 12:000.010 Barium 0.11 mg/L 1 04/27/12 13:20 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:20 7440-43-904/26/12 12:000.0050 Chromium 0.046 mg/L 1 04/27/12 13:20 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 13:20 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:20 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:20 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 11:39 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 11:39 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 11:39 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 11:39 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 11:39 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 11:39 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 11:39 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:23 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 13:30 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 20:37 67-64-1100 Acrolein ND ug/L 1 04/25/12 20:37 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 20:37 107-13-1100 Benzene ND ug/L 1 04/25/12 20:37 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 20:37 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 20:37 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 20:37 75-27-45.0 Bromoform ND ug/L 1 04/25/12 20:37 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 20:37 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 20:37 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 20:37 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 20:37 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 20:37 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 20:37 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 20:37 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 20:37 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 20:37 75-00-35.0 Chloroform ND ug/L 1 04/25/12 20:37 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 20:37 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 20:37 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 20:37 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 20:37 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 9 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G350390 Lab ID:5061952002 Collected:04/23/12 09:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 20:37 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 20:37 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 20:37 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 20:37 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 20:37 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 20:37 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 20:37 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 20:37 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 20:37 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 20:37 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 20:37 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 20:37 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 20:37 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 20:37 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 20:37 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 20:37 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 20:37 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 20:37 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 20:37 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 20:37 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 20:37 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 20:37 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 20:37 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 20:37 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 20:37 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 20:37 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 20:37 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 20:37 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 20:37 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 20:37 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 20:37 103-65-15.0 Styrene ND ug/L 1 04/25/12 20:37 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 20:37 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 20:37 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 20:37 127-18-45.0 Toluene ND ug/L 1 04/25/12 20:37 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 20:37 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 20:37 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 20:37 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 20:37 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 20:37 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 20:37 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 20:37 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 20:37 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 20:37 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 20:37 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 20:37 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 10 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G350390 Lab ID:5061952002 Collected:04/23/12 09:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 20:37 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/25/12 20:37 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 04/25/12 20:37 460-00-472-125 Toluene-d8 (S)98 %.1 04/25/12 20:37 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 11 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G260300 Lab ID:5061952003 Collected:04/23/12 10:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 1 04/27/12 13:24 7440-38-204/26/12 12:000.010 Barium ND mg/L 1 04/27/12 13:24 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:24 7440-43-904/26/12 12:000.0050 Chromium ND mg/L 1 04/27/12 13:24 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 13:24 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:24 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:24 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 11:43 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 11:43 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 11:43 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 11:43 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 11:43 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 11:43 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 11:43 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:25 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 13:32 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 21:10 67-64-1100 Acrolein ND ug/L 1 04/25/12 21:10 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 21:10 107-13-1100 Benzene ND ug/L 1 04/25/12 21:10 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 21:10 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 21:10 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 21:10 75-27-45.0 Bromoform ND ug/L 1 04/25/12 21:10 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 21:10 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 21:10 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 21:10 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 21:10 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 21:10 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 21:10 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 21:10 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 21:10 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 21:10 75-00-35.0 Chloroform ND ug/L 1 04/25/12 21:10 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 21:10 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 21:10 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 21:10 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 21:10 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 12 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G260300 Lab ID:5061952003 Collected:04/23/12 10:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 21:10 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 21:10 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 21:10 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 21:10 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 21:10 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 21:10 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 21:10 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 21:10 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 21:10 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 21:10 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 21:10 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 21:10 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 21:10 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 21:10 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 21:10 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 21:10 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 21:10 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 21:10 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 21:10 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 21:10 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 21:10 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 21:10 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 21:10 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 21:10 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 21:10 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 21:10 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 21:10 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 21:10 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 21:10 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 21:10 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 21:10 103-65-15.0 Styrene ND ug/L 1 04/25/12 21:10 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 21:10 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 21:10 79-34-55.0 Tetrachloroethene 8.0 ug/L 1 04/25/12 21:10 127-18-45.0 Toluene ND ug/L 1 04/25/12 21:10 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 21:10 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 21:10 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 21:10 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 21:10 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 21:10 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 21:10 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 21:10 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 21:10 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 21:10 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 21:10 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 21:10 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 13 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB10:G260300 Lab ID:5061952003 Collected:04/23/12 10:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 21:10 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/25/12 21:10 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/25/12 21:10 460-00-472-125 Toluene-d8 (S)98 %.1 04/25/12 21:10 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 14 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G450490 Lab ID:5061952004 Collected:04/23/12 11:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 0.045 mg/L 1 04/27/12 13:27 7440-38-204/26/12 12:000.010 Barium 0.12 mg/L 1 04/27/12 13:27 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:27 7440-43-904/26/12 12:000.0050 Chromium 0.13 mg/L 1 04/27/12 13:27 7440-47-304/26/12 12:000.010 Lead 0.011 mg/L 1 04/27/12 13:27 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:27 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:27 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 11:46 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 11:46 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 11:46 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 11:46 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 11:46 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 11:46 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 11:46 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:27 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 14:32 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 21:42 67-64-1100 Acrolein ND ug/L 1 04/25/12 21:42 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 21:42 107-13-1100 Benzene ND ug/L 1 04/25/12 21:42 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 21:42 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 21:42 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 21:42 75-27-45.0 Bromoform ND ug/L 1 04/25/12 21:42 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 21:42 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 21:42 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 21:42 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 21:42 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 21:42 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 21:42 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 21:42 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 21:42 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 21:42 75-00-35.0 Chloroform ND ug/L 1 04/25/12 21:42 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 21:42 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 21:42 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 21:42 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 21:42 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 15 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G450490 Lab ID:5061952004 Collected:04/23/12 11:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 21:42 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 21:42 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 21:42 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 21:42 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 21:42 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 21:42 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 21:42 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 21:42 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 21:42 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 21:42 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/25/12 21:42 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 21:42 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 21:42 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 21:42 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 21:42 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 21:42 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 21:42 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 21:42 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 21:42 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 21:42 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 21:42 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 21:42 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 21:42 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 21:42 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 21:42 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 21:42 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 21:42 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 21:42 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 21:42 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 21:42 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 21:42 103-65-15.0 Styrene ND ug/L 1 04/25/12 21:42 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 21:42 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 21:42 79-34-55.0 Tetrachloroethene 23.4 ug/L 1 04/25/12 21:42 127-18-45.0 Toluene ND ug/L 1 04/25/12 21:42 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 21:42 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 21:42 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 21:42 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 21:42 79-00-55.0 Trichloroethene ND ug/L 1 04/25/12 21:42 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 21:42 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 21:42 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 21:42 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 21:42 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 21:42 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 21:42 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 16 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G450490 Lab ID:5061952004 Collected:04/23/12 11:10 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 21:42 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 04/25/12 21:42 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/25/12 21:42 460-00-472-125 Toluene-d8 (S)98 %.1 04/25/12 21:42 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 17 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G350390 Lab ID:5061952005 Collected:04/23/12 11:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 1 04/27/12 13:51 7440-38-204/26/12 12:000.010 Barium ND mg/L 1 04/27/12 13:51 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:51 7440-43-904/26/12 12:000.0050 Chromium ND mg/L 1 04/27/12 13:51 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 13:51 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:51 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:51 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 12:07 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 12:07 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 12:07 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 12:07 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 12:07 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 12:07 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 12:07 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:33 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 14:38 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/25/12 23:19 67-64-1100 Acrolein ND ug/L 1 04/25/12 23:19 107-02-8100 Acrylonitrile ND ug/L 1 04/25/12 23:19 107-13-1100 Benzene ND ug/L 1 04/25/12 23:19 71-43-25.0 Bromobenzene ND ug/L 1 04/25/12 23:19 108-86-15.0 Bromochloromethane ND ug/L 1 04/25/12 23:19 74-97-55.0 Bromodichloromethane ND ug/L 1 04/25/12 23:19 75-27-45.0 Bromoform ND ug/L 1 04/25/12 23:19 75-25-25.0 Bromomethane ND ug/L 1 04/25/12 23:19 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/25/12 23:19 78-93-325.0 n-Butylbenzene ND ug/L 1 04/25/12 23:19 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/25/12 23:19 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/25/12 23:19 98-06-65.0 Carbon disulfide ND ug/L 1 04/25/12 23:19 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/25/12 23:19 56-23-55.0 Chlorobenzene ND ug/L 1 04/25/12 23:19 108-90-75.0 Chloroethane ND ug/L 1 04/25/12 23:19 75-00-35.0 Chloroform ND ug/L 1 04/25/12 23:19 67-66-35.0 Chloromethane ND ug/L 1 04/25/12 23:19 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/25/12 23:19 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/25/12 23:19 106-43-45.0 Dibromochloromethane ND ug/L 1 04/25/12 23:19 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 18 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G350390 Lab ID:5061952005 Collected:04/23/12 11:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/25/12 23:19 106-93-45.0 Dibromomethane ND ug/L 1 04/25/12 23:19 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/25/12 23:19 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/25/12 23:19 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/25/12 23:19 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/25/12 23:19 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/25/12 23:19 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/25/12 23:19 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/25/12 23:19 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/25/12 23:19 75-35-45.0 cis-1,2-Dichloroethene 7.4 ug/L 1 04/25/12 23:19 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/25/12 23:19 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/25/12 23:19 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/25/12 23:19 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/25/12 23:19 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/25/12 23:19 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/25/12 23:19 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/25/12 23:19 10061-02-65.0 Ethylbenzene ND ug/L 1 04/25/12 23:19 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/25/12 23:19 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/25/12 23:19 87-68-35.0 n-Hexane ND ug/L 1 04/25/12 23:19 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/25/12 23:19 591-78-625.0 Iodomethane ND ug/L 1 04/25/12 23:19 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/25/12 23:19 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/25/12 23:19 99-87-65.0 Methylene Chloride ND ug/L 1 04/25/12 23:19 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/25/12 23:19 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/25/12 23:19 1634-04-44.0 Naphthalene ND ug/L 1 04/25/12 23:19 91-20-35.0 n-Propylbenzene ND ug/L 1 04/25/12 23:19 103-65-15.0 Styrene ND ug/L 1 04/25/12 23:19 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/25/12 23:19 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/25/12 23:19 79-34-55.0 Tetrachloroethene ND ug/L 1 04/25/12 23:19 127-18-45.0 Toluene ND ug/L 1 04/25/12 23:19 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/25/12 23:19 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/25/12 23:19 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/25/12 23:19 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/25/12 23:19 79-00-55.0 Trichloroethene 10.3 ug/L 1 04/25/12 23:19 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/25/12 23:19 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/25/12 23:19 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/25/12 23:19 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/25/12 23:19 108-67-85.0 Vinyl acetate ND ug/L 1 04/25/12 23:19 108-05-450.0 Vinyl chloride ND ug/L 1 04/25/12 23:19 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 19 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G350390 Lab ID:5061952005 Collected:04/23/12 11:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/25/12 23:19 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 04/25/12 23:19 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/25/12 23:19 460-00-472-125 Toluene-d8 (S)99 %.1 04/25/12 23:19 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 20 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300 Lab ID:5061952006 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 1 04/27/12 13:55 7440-38-204/26/12 12:000.010 Barium ND mg/L 1 04/27/12 13:55 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:55 7440-43-904/26/12 12:000.0050 Chromium ND mg/L 1 04/27/12 13:55 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 13:55 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:55 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:55 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 12:17 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 12:17 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 12:17 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 12:17 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 12:17 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 12:17 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 12:17 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 11:35 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 14:40 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 02:01 67-64-1100 Acrolein ND ug/L 1 04/26/12 02:01 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 02:01 107-13-1100 Benzene ND ug/L 1 04/26/12 02:01 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 02:01 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 02:01 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 02:01 75-27-45.0 Bromoform ND ug/L 1 04/26/12 02:01 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 02:01 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 02:01 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 02:01 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 02:01 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 02:01 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 02:01 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 02:01 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 02:01 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 02:01 75-00-35.0 Chloroform ND ug/L 1 04/26/12 02:01 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 02:01 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 02:01 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 02:01 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 02:01 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 21 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300 Lab ID:5061952006 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 02:01 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 02:01 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 02:01 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 02:01 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 02:01 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 02:01 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 02:01 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 02:01 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 02:01 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 02:01 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 02:01 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 02:01 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 02:01 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 02:01 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 02:01 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 02:01 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 02:01 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 02:01 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 02:01 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 02:01 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 02:01 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 02:01 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 02:01 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 02:01 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 02:01 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 02:01 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 02:01 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 02:01 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 02:01 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 02:01 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 02:01 103-65-15.0 Styrene ND ug/L 1 04/26/12 02:01 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 02:01 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 02:01 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 02:01 127-18-45.0 Toluene ND ug/L 1 04/26/12 02:01 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 02:01 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 02:01 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 02:01 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 02:01 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 02:01 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 02:01 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 02:01 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 02:01 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 02:01 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 02:01 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 02:01 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 22 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300 Lab ID:5061952006 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/26/12 02:01 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/26/12 02:01 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 02:01 460-00-472-125 Toluene-d8 (S)99 %.1 04/26/12 02:01 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 23 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300A Lab ID:5061952007 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 1 04/27/12 13:59 7440-38-204/26/12 12:000.010 Barium ND mg/L 1 04/27/12 13:59 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 13:59 7440-43-904/26/12 12:000.0050 Chromium ND mg/L 1 04/27/12 13:59 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 13:59 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 13:59 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 13:59 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 12:21 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 12:21 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 12:21 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 12:21 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 12:21 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 12:21 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 12:21 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 12:48 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 14:42 7439-97-604/26/12 12:212.0 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 02:33 67-64-1100 Acrolein ND ug/L 1 04/26/12 02:33 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 02:33 107-13-1100 Benzene ND ug/L 1 04/26/12 02:33 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 02:33 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 02:33 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 02:33 75-27-45.0 Bromoform ND ug/L 1 04/26/12 02:33 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 02:33 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 02:33 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 02:33 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 02:33 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 02:33 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 02:33 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 02:33 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 02:33 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 02:33 75-00-35.0 Chloroform ND ug/L 1 04/26/12 02:33 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 02:33 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 02:33 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 02:33 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 02:33 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 24 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300A Lab ID:5061952007 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 02:33 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 02:33 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 02:33 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 02:33 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 02:33 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 02:33 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 02:33 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 02:33 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 02:33 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 02:33 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 02:33 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 02:33 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 02:33 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 02:33 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 02:33 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 02:33 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 02:33 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 02:33 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 02:33 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 02:33 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 02:33 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 02:33 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 02:33 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 02:33 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 02:33 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 02:33 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 02:33 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 02:33 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 02:33 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 02:33 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 02:33 103-65-15.0 Styrene ND ug/L 1 04/26/12 02:33 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 02:33 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 02:33 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 02:33 127-18-45.0 Toluene ND ug/L 1 04/26/12 02:33 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 02:33 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 02:33 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 02:33 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 02:33 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 02:33 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 02:33 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 02:33 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 02:33 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 02:33 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 02:33 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 02:33 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 25 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB12:G260300A Lab ID:5061952007 Collected:04/23/12 12:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/26/12 02:33 1330-20-710.0 Surrogates Dibromofluoromethane (S)105 %.1 04/26/12 02:33 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 02:33 460-00-472-125 Toluene-d8 (S)99 %.1 04/26/12 02:33 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 26 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G450490 Lab ID:5061952008 Collected:04/23/12 13:20 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 03:05 67-64-1100 Acrolein ND ug/L 1 04/26/12 03:05 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 03:05 107-13-1100 Benzene ND ug/L 1 04/26/12 03:05 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 03:05 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 03:05 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 03:05 75-27-45.0 Bromoform ND ug/L 1 04/26/12 03:05 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 03:05 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 03:05 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 03:05 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 03:05 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 03:05 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 03:05 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 03:05 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 03:05 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 03:05 75-00-35.0 Chloroform ND ug/L 1 04/26/12 03:05 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 03:05 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 03:05 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 03:05 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 03:05 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 03:05 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 03:05 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 03:05 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 03:05 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 03:05 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 03:05 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 03:05 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 03:05 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 03:05 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 03:05 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 03:05 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 03:05 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 03:05 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 03:05 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 03:05 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 03:05 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 03:05 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 03:05 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 03:05 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 03:05 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 03:05 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 03:05 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 03:05 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 03:05 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 03:05 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 27 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G450490 Lab ID:5061952008 Collected:04/23/12 13:20 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 03:05 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 03:05 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 03:05 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 03:05 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 03:05 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 03:05 103-65-15.0 Styrene ND ug/L 1 04/26/12 03:05 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 03:05 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 03:05 79-34-55.0 Tetrachloroethene 95.3 ug/L 1 04/26/12 03:05 127-18-45.0 Toluene ND ug/L 1 04/26/12 03:05 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 03:05 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 03:05 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 03:05 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 03:05 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 03:05 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 03:05 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 03:05 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 03:05 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 03:05 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 03:05 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 03:05 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 03:05 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 04/26/12 03:05 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 04/26/12 03:05 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 03:05 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 28 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G350390 Lab ID:5061952009 Collected:04/23/12 13:45 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 03:38 67-64-1100 Acrolein ND ug/L 1 04/26/12 03:38 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 03:38 107-13-1100 Benzene ND ug/L 1 04/26/12 03:38 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 03:38 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 03:38 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 03:38 75-27-45.0 Bromoform ND ug/L 1 04/26/12 03:38 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 03:38 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 03:38 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 03:38 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 03:38 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 03:38 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 03:38 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 03:38 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 03:38 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 03:38 75-00-35.0 Chloroform ND ug/L 1 04/26/12 03:38 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 03:38 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 03:38 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 03:38 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 03:38 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 03:38 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 03:38 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 03:38 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 03:38 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 03:38 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 03:38 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 03:38 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 03:38 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 03:38 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 03:38 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 03:38 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 03:38 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 03:38 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 03:38 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 03:38 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 03:38 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 03:38 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 03:38 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 03:38 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 03:38 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 03:38 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 03:38 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 03:38 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 03:38 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 03:38 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 29 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G350390 Lab ID:5061952009 Collected:04/23/12 13:45 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 03:38 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 03:38 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 03:38 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 03:38 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 03:38 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 03:38 103-65-15.0 Styrene ND ug/L 1 04/26/12 03:38 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 03:38 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 03:38 79-34-55.0 Tetrachloroethene 616 ug/L 10 04/26/12 14:43 127-18-450.0 Toluene ND ug/L 1 04/26/12 03:38 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 03:38 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 03:38 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 03:38 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 03:38 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 03:38 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 03:38 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 03:38 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 03:38 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 03:38 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 03:38 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 03:38 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 03:38 1330-20-710.0 Surrogates Dibromofluoromethane (S)106 %.1 04/26/12 03:38 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 03:38 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 03:38 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 30 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G260300 Lab ID:5061952010 Collected:04/23/12 14:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 04:10 67-64-1100 Acrolein ND ug/L 1 04/26/12 04:10 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 04:10 107-13-1100 Benzene ND ug/L 1 04/26/12 04:10 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 04:10 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 04:10 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 04:10 75-27-45.0 Bromoform ND ug/L 1 04/26/12 04:10 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 04:10 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 04:10 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 04:10 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 04:10 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 04:10 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 04:10 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 04:10 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 04:10 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 04:10 75-00-35.0 Chloroform ND ug/L 1 04/26/12 04:10 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 04:10 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 04:10 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 04:10 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 04:10 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 04:10 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 04:10 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 04:10 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 04:10 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 04:10 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 04:10 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 04:10 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 04:10 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 04:10 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 04:10 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 04:10 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 04:10 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 04:10 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 04:10 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 04:10 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 04:10 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 04:10 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 04:10 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 04:10 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 04:10 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 04:10 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 04:10 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 04:10 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 04:10 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 04:10 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 31 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB15:G260300 Lab ID:5061952010 Collected:04/23/12 14:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 04:10 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 04:10 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 04:10 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 04:10 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 04:10 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 04:10 103-65-15.0 Styrene ND ug/L 1 04/26/12 04:10 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 04:10 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 04:10 79-34-55.0 Tetrachloroethene 76.0 ug/L 1 04/26/12 04:10 127-18-45.0 Toluene ND ug/L 1 04/26/12 04:10 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 04:10 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 04:10 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 04:10 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 04:10 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 04:10 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 04:10 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 04:10 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 04:10 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 04:10 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 04:10 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 04:10 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 04:10 1330-20-710.0 Surrogates Dibromofluoromethane (S)100 %.1 04/26/12 04:10 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 04:10 460-00-472-125 Toluene-d8 (S)97 %.1 04/26/12 04:10 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 32 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490 Lab ID:5061952011 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/28/12 06:16 83-32-904/26/12 10:351.0 Acenaphthylene ND ug/L 1 04/28/12 06:16 208-96-804/26/12 10:351.0 Anthracene ND ug/L 1 04/28/12 06:16 120-12-704/26/12 10:350.10 Benzo(a)anthracene ND ug/L 1 04/28/12 06:16 56-55-304/26/12 10:350.10 Benzo(a)pyrene ND ug/L 1 04/28/12 06:16 50-32-804/26/12 10:350.10 Benzo(b)fluoranthene ND ug/L 1 04/28/12 06:16 205-99-204/26/12 10:350.10 Benzo(g,h,i)perylene ND ug/L 1 04/28/12 06:16 191-24-204/26/12 10:350.10 Benzo(k)fluoranthene ND ug/L 1 04/28/12 06:16 207-08-904/26/12 10:350.10 Chrysene ND ug/L 1 04/28/12 06:16 218-01-904/26/12 10:350.52 Dibenz(a,h)anthracene ND ug/L 1 04/28/12 06:16 53-70-304/26/12 10:350.10 Fluoranthene ND ug/L 1 04/28/12 06:16 206-44-004/26/12 10:351.0 Fluorene ND ug/L 1 04/28/12 06:16 86-73-704/26/12 10:351.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/28/12 06:16 193-39-504/26/12 10:350.10 2-Methylnaphthalene ND ug/L 1 04/28/12 06:16 91-57-604/26/12 10:351.0 Naphthalene ND ug/L 1 04/28/12 06:16 91-20-304/26/12 10:351.0 Phenanthrene ND ug/L 1 04/28/12 06:16 85-01-804/26/12 10:351.0 Pyrene ND ug/L 1 04/28/12 06:16 129-00-004/26/12 10:351.0 Surrogates 2-Fluorobiphenyl (S)56 %.1 04/28/12 06:16 321-60-804/26/12 10:3526-106 p-Terphenyl-d14 (S)76 %.1 04/28/12 06:16 1718-51-004/26/12 10:3516-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/26/12 17:25 100-51-604/26/12 10:3520.8 4-Bromophenylphenyl ether ND ug/L 1 04/26/12 17:25 101-55-304/26/12 10:3510.4 Butylbenzylphthalate ND ug/L 1 04/26/12 17:25 85-68-704/26/12 10:3510.4 4-Chloro-3-methylphenol ND ug/L 1 04/26/12 17:25 59-50-704/26/12 10:3520.8 4-Chloroaniline ND ug/L 1 04/26/12 17:25 106-47-804/26/12 10:3520.8 bis(2-Chloroethoxy)methane ND ug/L 1 04/26/12 17:25 111-91-104/26/12 10:3510.4 bis(2-Chloroethyl) ether ND ug/L 1 04/26/12 17:25 111-44-404/26/12 10:3510.4 bis(2chloro1methylethyl) ether ND ug/L 1 04/26/12 17:25 108-60-104/26/12 10:355.2 2-Chloronaphthalene ND ug/L 1 04/26/12 17:25 91-58-704/26/12 10:3510.4 2-Chlorophenol ND ug/L 1 04/26/12 17:25 95-57-804/26/12 10:3510.4 4-Chlorophenylphenyl ether ND ug/L 1 04/26/12 17:25 7005-72-304/26/12 10:3510.4 Dibenzofuran ND ug/L 1 04/26/12 17:25 132-64-904/26/12 10:3510.4 3,3'-Dichlorobenzidine ND ug/L 1 04/26/12 17:25 91-94-104/26/12 10:3520.8 2,4-Dichlorophenol ND ug/L 1 04/26/12 17:25 120-83-204/26/12 10:3510.4 Diethylphthalate ND ug/L 1 04/26/12 17:25 84-66-204/26/12 10:3510.4 2,4-Dimethylphenol ND ug/L 1 04/26/12 17:25 105-67-904/26/12 10:3510.4 Dimethylphthalate ND ug/L 1 04/26/12 17:25 131-11-304/26/12 10:3510.4 Di-n-butylphthalate ND ug/L 1 04/26/12 17:25 84-74-204/26/12 10:3510.4 4,6-Dinitro-2-methylphenol ND ug/L 1 04/26/12 17:25 534-52-104/26/12 10:3552.1 2,4-Dinitrophenol ND ug/L 1 04/26/12 17:25 51-28-504/26/12 10:3552.1 2,4-Dinitrotoluene ND ug/L 1 04/26/12 17:25 121-14-204/26/12 10:3510.4 2,6-Dinitrotoluene ND ug/L 1 04/26/12 17:25 606-20-204/26/12 10:3510.4 Di-n-octylphthalate ND ug/L 1 04/26/12 17:25 117-84-004/26/12 10:3510.4 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/26/12 17:25 117-81-704/26/12 10:355.2 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 17:25 87-68-304/26/12 10:355.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 33 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490 Lab ID:5061952011 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/26/12 17:25 118-74-104/26/12 10:3510.4 Hexachlorocyclopentadiene ND ug/L 1 04/26/12 17:25 77-47-404/26/12 10:3526.0 Hexachloroethane ND ug/L 1 04/26/12 17:25 67-72-104/26/12 10:3510.4 Isophorone ND ug/L 1 04/26/12 17:25 78-59-104/26/12 10:3510.4 2-Methylphenol(o-Cresol)ND ug/L 1 04/26/12 17:25 95-48-704/26/12 10:3510.4 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/26/12 17:2504/26/12 10:3520.8 2-Nitroaniline ND ug/L 1 04/26/12 17:25 88-74-404/26/12 10:3552.1 3-Nitroaniline ND ug/L 1 04/26/12 17:25 99-09-204/26/12 10:3552.1 4-Nitroaniline ND ug/L 1 04/26/12 17:25 100-01-604/26/12 10:3552.1 Nitrobenzene ND ug/L 1 04/26/12 17:25 98-95-304/26/12 10:3510.4 2-Nitrophenol ND ug/L 1 04/26/12 17:25 88-75-504/26/12 10:3510.4 4-Nitrophenol ND ug/L 1 04/26/12 17:25 100-02-704/26/12 10:3552.1 N-Nitroso-di-n-propylamine ND ug/L 1 04/26/12 17:25 621-64-704/26/12 10:3510.4 N-Nitrosodiphenylamine ND ug/L 1 04/26/12 17:25 86-30-604/26/12 10:3510.4 Pentachlorophenol ND ug/L 1 04/26/12 17:25 87-86-504/26/12 10:3552.1 Phenol ND ug/L 1 04/26/12 17:25 108-95-204/26/12 10:3510.4 2,4,5-Trichlorophenol ND ug/L 1 04/26/12 17:25 95-95-404/26/12 10:3510.4 2,4,6-Trichlorophenol ND ug/L 1 04/26/12 17:25 88-06-204/26/12 10:3510.4 Surrogates Nitrobenzene-d5 (S)59 %.1 04/26/12 17:25 4165-60-004/26/12 10:3533-108 Phenol-d5 (S)12 %.1 04/26/12 17:25 4165-62-204/26/12 10:3510-56 2-Fluorophenol (S)22 %.1 04/26/12 17:25 367-12-404/26/12 10:3510-74 2,4,6-Tribromophenol (S)70 %.1 04/26/12 17:25 118-79-604/26/12 10:3532-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 04:42 67-64-1100 Acrolein ND ug/L 1 04/26/12 04:42 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 04:42 107-13-1100 Benzene ND ug/L 1 04/26/12 04:42 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 04:42 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 04:42 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 04:42 75-27-45.0 Bromoform ND ug/L 1 04/26/12 04:42 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 04:42 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 04:42 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 04:42 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 04:42 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 04:42 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 04:42 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 04:42 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 04:42 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 04:42 75-00-35.0 Chloroform ND ug/L 1 04/26/12 04:42 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 04:42 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 04:42 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 04:42 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 04:42 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 34 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490 Lab ID:5061952011 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 04:42 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 04:42 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 04:42 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 04:42 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 04:42 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 04:42 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 04:42 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 04:42 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 04:42 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 04:42 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 04:42 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 04:42 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 04:42 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 04:42 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 04:42 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 04:42 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 04:42 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 04:42 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 04:42 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 04:42 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 04:42 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 04:42 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 04:42 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 04:42 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 04:42 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 04:42 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 04:42 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 04:42 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 04:42 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 04:42 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 04:42 103-65-15.0 Styrene ND ug/L 1 04/26/12 04:42 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 04:42 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 04:42 79-34-55.0 Tetrachloroethene 15.9 ug/L 1 04/26/12 04:42 127-18-45.0 Toluene ND ug/L 1 04/26/12 04:42 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 04:42 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 04:42 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 04:42 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 04:42 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 04:42 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 04:42 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 04:42 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 04:42 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 04:42 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 04:42 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 04:42 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 35 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490 Lab ID:5061952011 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/26/12 04:42 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/26/12 04:42 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/26/12 04:42 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 04:42 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 36 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490A Lab ID:5061952012 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/28/12 06:34 83-32-904/26/12 10:351.0 Acenaphthylene ND ug/L 1 04/28/12 06:34 208-96-804/26/12 10:351.0 Anthracene ND ug/L 1 04/28/12 06:34 120-12-704/26/12 10:350.10 Benzo(a)anthracene ND ug/L 1 04/28/12 06:34 56-55-304/26/12 10:350.10 Benzo(a)pyrene ND ug/L 1 04/28/12 06:34 50-32-804/26/12 10:350.10 Benzo(b)fluoranthene ND ug/L 1 04/28/12 06:34 205-99-204/26/12 10:350.10 Benzo(g,h,i)perylene ND ug/L 1 04/28/12 06:34 191-24-204/26/12 10:350.10 Benzo(k)fluoranthene ND ug/L 1 04/28/12 06:34 207-08-904/26/12 10:350.10 Chrysene ND ug/L 1 04/28/12 06:34 218-01-904/26/12 10:350.52 Dibenz(a,h)anthracene ND ug/L 1 04/28/12 06:34 53-70-304/26/12 10:350.10 Fluoranthene ND ug/L 1 04/28/12 06:34 206-44-004/26/12 10:351.0 Fluorene ND ug/L 1 04/28/12 06:34 86-73-704/26/12 10:351.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/28/12 06:34 193-39-504/26/12 10:350.10 2-Methylnaphthalene ND ug/L 1 04/28/12 06:34 91-57-604/26/12 10:351.0 Naphthalene ND ug/L 1 04/28/12 06:34 91-20-304/26/12 10:351.0 Phenanthrene ND ug/L 1 04/28/12 06:34 85-01-804/26/12 10:351.0 Pyrene ND ug/L 1 04/28/12 06:34 129-00-004/26/12 10:351.0 Surrogates 2-Fluorobiphenyl (S)70 %.1 04/28/12 06:34 321-60-804/26/12 10:3526-106 p-Terphenyl-d14 (S)86 %.1 04/28/12 06:34 1718-51-004/26/12 10:3516-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/26/12 17:45 100-51-604/26/12 10:3520.8 4-Bromophenylphenyl ether ND ug/L 1 04/26/12 17:45 101-55-304/26/12 10:3510.4 Butylbenzylphthalate ND ug/L 1 04/26/12 17:45 85-68-704/26/12 10:3510.4 4-Chloro-3-methylphenol ND ug/L 1 04/26/12 17:45 59-50-704/26/12 10:3520.8 4-Chloroaniline ND ug/L 1 04/26/12 17:45 106-47-804/26/12 10:3520.8 bis(2-Chloroethoxy)methane ND ug/L 1 04/26/12 17:45 111-91-104/26/12 10:3510.4 bis(2-Chloroethyl) ether ND ug/L 1 04/26/12 17:45 111-44-404/26/12 10:3510.4 bis(2chloro1methylethyl) ether ND ug/L 1 04/26/12 17:45 108-60-104/26/12 10:355.2 2-Chloronaphthalene ND ug/L 1 04/26/12 17:45 91-58-704/26/12 10:3510.4 2-Chlorophenol ND ug/L 1 04/26/12 17:45 95-57-804/26/12 10:3510.4 4-Chlorophenylphenyl ether ND ug/L 1 04/26/12 17:45 7005-72-304/26/12 10:3510.4 Dibenzofuran ND ug/L 1 04/26/12 17:45 132-64-904/26/12 10:3510.4 3,3'-Dichlorobenzidine ND ug/L 1 04/26/12 17:45 91-94-104/26/12 10:3520.8 2,4-Dichlorophenol ND ug/L 1 04/26/12 17:45 120-83-204/26/12 10:3510.4 Diethylphthalate ND ug/L 1 04/26/12 17:45 84-66-204/26/12 10:3510.4 2,4-Dimethylphenol ND ug/L 1 04/26/12 17:45 105-67-904/26/12 10:3510.4 Dimethylphthalate ND ug/L 1 04/26/12 17:45 131-11-304/26/12 10:3510.4 Di-n-butylphthalate ND ug/L 1 04/26/12 17:45 84-74-204/26/12 10:3510.4 4,6-Dinitro-2-methylphenol ND ug/L 1 04/26/12 17:45 534-52-104/26/12 10:3552.1 2,4-Dinitrophenol ND ug/L 1 04/26/12 17:45 51-28-504/26/12 10:3552.1 2,4-Dinitrotoluene ND ug/L 1 04/26/12 17:45 121-14-204/26/12 10:3510.4 2,6-Dinitrotoluene ND ug/L 1 04/26/12 17:45 606-20-204/26/12 10:3510.4 Di-n-octylphthalate ND ug/L 1 04/26/12 17:45 117-84-004/26/12 10:3510.4 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/26/12 17:45 117-81-704/26/12 10:355.2 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 17:45 87-68-304/26/12 10:355.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 37 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G450490A Lab ID:5061952012 Collected:04/23/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/26/12 17:45 118-74-104/26/12 10:3510.4 Hexachlorocyclopentadiene ND ug/L 1 04/26/12 17:45 77-47-404/26/12 10:3526.0 Hexachloroethane ND ug/L 1 04/26/12 17:45 67-72-104/26/12 10:3510.4 Isophorone ND ug/L 1 04/26/12 17:45 78-59-104/26/12 10:3510.4 2-Methylphenol(o-Cresol)ND ug/L 1 04/26/12 17:45 95-48-704/26/12 10:3510.4 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/26/12 17:4504/26/12 10:3520.8 2-Nitroaniline ND ug/L 1 04/26/12 17:45 88-74-404/26/12 10:3552.1 3-Nitroaniline ND ug/L 1 04/26/12 17:45 99-09-204/26/12 10:3552.1 4-Nitroaniline ND ug/L 1 04/26/12 17:45 100-01-604/26/12 10:3552.1 Nitrobenzene ND ug/L 1 04/26/12 17:45 98-95-304/26/12 10:3510.4 2-Nitrophenol ND ug/L 1 04/26/12 17:45 88-75-504/26/12 10:3510.4 4-Nitrophenol ND ug/L 1 04/26/12 17:45 100-02-704/26/12 10:3552.1 N-Nitroso-di-n-propylamine ND ug/L 1 04/26/12 17:45 621-64-704/26/12 10:3510.4 N-Nitrosodiphenylamine ND ug/L 1 04/26/12 17:45 86-30-604/26/12 10:3510.4 Pentachlorophenol ND ug/L 1 04/26/12 17:45 87-86-504/26/12 10:3552.1 Phenol ND ug/L 1 04/26/12 17:45 108-95-204/26/12 10:3510.4 2,4,5-Trichlorophenol ND ug/L 1 04/26/12 17:45 95-95-404/26/12 10:3510.4 2,4,6-Trichlorophenol ND ug/L 1 04/26/12 17:45 88-06-204/26/12 10:3510.4 Surrogates Nitrobenzene-d5 (S)71 %.1 04/26/12 17:45 4165-60-004/26/12 10:3533-108 Phenol-d5 (S)15 %.1 04/26/12 17:45 4165-62-204/26/12 10:3510-56 2-Fluorophenol (S)27 %.1 04/26/12 17:45 367-12-404/26/12 10:3510-74 2,4,6-Tribromophenol (S)83 %.1 04/26/12 17:45 118-79-604/26/12 10:3532-124 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 38 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G350390 Lab ID:5061952013 Collected:04/23/12 15:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/28/12 06:52 83-32-904/26/12 10:351.0 Acenaphthylene ND ug/L 1 04/28/12 06:52 208-96-804/26/12 10:351.0 Anthracene ND ug/L 1 04/28/12 06:52 120-12-704/26/12 10:350.10 Benzo(a)anthracene ND ug/L 1 04/28/12 06:52 56-55-304/26/12 10:350.10 Benzo(a)pyrene ND ug/L 1 04/28/12 06:52 50-32-804/26/12 10:350.10 Benzo(b)fluoranthene ND ug/L 1 04/28/12 06:52 205-99-204/26/12 10:350.10 Benzo(g,h,i)perylene ND ug/L 1 04/28/12 06:52 191-24-204/26/12 10:350.10 Benzo(k)fluoranthene ND ug/L 1 04/28/12 06:52 207-08-904/26/12 10:350.10 Chrysene ND ug/L 1 04/28/12 06:52 218-01-904/26/12 10:350.52 Dibenz(a,h)anthracene ND ug/L 1 04/28/12 06:52 53-70-304/26/12 10:350.10 Fluoranthene ND ug/L 1 04/28/12 06:52 206-44-004/26/12 10:351.0 Fluorene ND ug/L 1 04/28/12 06:52 86-73-704/26/12 10:351.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/28/12 06:52 193-39-504/26/12 10:350.10 2-Methylnaphthalene ND ug/L 1 04/28/12 06:52 91-57-604/26/12 10:351.0 Naphthalene ND ug/L 1 04/28/12 06:52 91-20-304/26/12 10:351.0 Phenanthrene ND ug/L 1 04/28/12 06:52 85-01-804/26/12 10:351.0 Pyrene ND ug/L 1 04/28/12 06:52 129-00-004/26/12 10:351.0 Surrogates 2-Fluorobiphenyl (S)68 %.1 04/28/12 06:52 321-60-804/26/12 10:3526-106 p-Terphenyl-d14 (S)85 %.1 04/28/12 06:52 1718-51-004/26/12 10:3516-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/26/12 18:06 100-51-604/26/12 10:3520.8 4-Bromophenylphenyl ether ND ug/L 1 04/26/12 18:06 101-55-304/26/12 10:3510.4 Butylbenzylphthalate ND ug/L 1 04/26/12 18:06 85-68-704/26/12 10:3510.4 4-Chloro-3-methylphenol ND ug/L 1 04/26/12 18:06 59-50-704/26/12 10:3520.8 4-Chloroaniline ND ug/L 1 04/26/12 18:06 106-47-804/26/12 10:3520.8 bis(2-Chloroethoxy)methane ND ug/L 1 04/26/12 18:06 111-91-104/26/12 10:3510.4 bis(2-Chloroethyl) ether ND ug/L 1 04/26/12 18:06 111-44-404/26/12 10:3510.4 bis(2chloro1methylethyl) ether ND ug/L 1 04/26/12 18:06 108-60-104/26/12 10:355.2 2-Chloronaphthalene ND ug/L 1 04/26/12 18:06 91-58-704/26/12 10:3510.4 2-Chlorophenol ND ug/L 1 04/26/12 18:06 95-57-804/26/12 10:3510.4 4-Chlorophenylphenyl ether ND ug/L 1 04/26/12 18:06 7005-72-304/26/12 10:3510.4 Dibenzofuran ND ug/L 1 04/26/12 18:06 132-64-904/26/12 10:3510.4 3,3'-Dichlorobenzidine ND ug/L 1 04/26/12 18:06 91-94-104/26/12 10:3520.8 2,4-Dichlorophenol ND ug/L 1 04/26/12 18:06 120-83-204/26/12 10:3510.4 Diethylphthalate ND ug/L 1 04/26/12 18:06 84-66-204/26/12 10:3510.4 2,4-Dimethylphenol ND ug/L 1 04/26/12 18:06 105-67-904/26/12 10:3510.4 Dimethylphthalate ND ug/L 1 04/26/12 18:06 131-11-304/26/12 10:3510.4 Di-n-butylphthalate ND ug/L 1 04/26/12 18:06 84-74-204/26/12 10:3510.4 4,6-Dinitro-2-methylphenol ND ug/L 1 04/26/12 18:06 534-52-104/26/12 10:3552.1 2,4-Dinitrophenol ND ug/L 1 04/26/12 18:06 51-28-504/26/12 10:3552.1 2,4-Dinitrotoluene ND ug/L 1 04/26/12 18:06 121-14-204/26/12 10:3510.4 2,6-Dinitrotoluene ND ug/L 1 04/26/12 18:06 606-20-204/26/12 10:3510.4 Di-n-octylphthalate ND ug/L 1 04/26/12 18:06 117-84-004/26/12 10:3510.4 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/26/12 18:06 117-81-704/26/12 10:355.2 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 18:06 87-68-304/26/12 10:355.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 39 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G350390 Lab ID:5061952013 Collected:04/23/12 15:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/26/12 18:06 118-74-104/26/12 10:3510.4 Hexachlorocyclopentadiene ND ug/L 1 04/26/12 18:06 77-47-404/26/12 10:3526.0 Hexachloroethane ND ug/L 1 04/26/12 18:06 67-72-104/26/12 10:3510.4 Isophorone ND ug/L 1 04/26/12 18:06 78-59-104/26/12 10:3510.4 2-Methylphenol(o-Cresol)ND ug/L 1 04/26/12 18:06 95-48-704/26/12 10:3510.4 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/26/12 18:0604/26/12 10:3520.8 2-Nitroaniline ND ug/L 1 04/26/12 18:06 88-74-404/26/12 10:3552.1 3-Nitroaniline ND ug/L 1 04/26/12 18:06 99-09-204/26/12 10:3552.1 4-Nitroaniline ND ug/L 1 04/26/12 18:06 100-01-604/26/12 10:3552.1 Nitrobenzene ND ug/L 1 04/26/12 18:06 98-95-304/26/12 10:3510.4 2-Nitrophenol ND ug/L 1 04/26/12 18:06 88-75-504/26/12 10:3510.4 4-Nitrophenol ND ug/L 1 04/26/12 18:06 100-02-704/26/12 10:3552.1 N-Nitroso-di-n-propylamine ND ug/L 1 04/26/12 18:06 621-64-704/26/12 10:3510.4 N-Nitrosodiphenylamine ND ug/L 1 04/26/12 18:06 86-30-604/26/12 10:3510.4 Pentachlorophenol ND ug/L 1 04/26/12 18:06 87-86-504/26/12 10:3552.1 Phenol ND ug/L 1 04/26/12 18:06 108-95-204/26/12 10:3510.4 2,4,5-Trichlorophenol ND ug/L 1 04/26/12 18:06 95-95-404/26/12 10:3510.4 2,4,6-Trichlorophenol ND ug/L 1 04/26/12 18:06 88-06-204/26/12 10:3510.4 Surrogates Nitrobenzene-d5 (S)70 %.1 04/26/12 18:06 4165-60-004/26/12 10:3533-108 Phenol-d5 (S)16 %.1 04/26/12 18:06 4165-62-204/26/12 10:3510-56 2-Fluorophenol (S)28 %.1 04/26/12 18:06 367-12-404/26/12 10:3510-74 2,4,6-Tribromophenol (S)87 %.1 04/26/12 18:06 118-79-604/26/12 10:3532-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 05:15 67-64-1100 Acrolein ND ug/L 1 04/26/12 05:15 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 05:15 107-13-1100 Benzene ND ug/L 1 04/26/12 05:15 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 05:15 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 05:15 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 05:15 75-27-45.0 Bromoform ND ug/L 1 04/26/12 05:15 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 05:15 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 05:15 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 05:15 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 05:15 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 05:15 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 05:15 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 05:15 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 05:15 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 05:15 75-00-35.0 Chloroform ND ug/L 1 04/26/12 05:15 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 05:15 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 05:15 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 05:15 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 05:15 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 40 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G350390 Lab ID:5061952013 Collected:04/23/12 15:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 05:15 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 05:15 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 05:15 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 05:15 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 05:15 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 05:15 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 05:15 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 05:15 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 05:15 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 05:15 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 05:15 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 05:15 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 05:15 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 05:15 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 05:15 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 05:15 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 05:15 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 05:15 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 05:15 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 05:15 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 05:15 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 05:15 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 05:15 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 05:15 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 05:15 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 05:15 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 05:15 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 05:15 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 05:15 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 05:15 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 05:15 103-65-15.0 Styrene ND ug/L 1 04/26/12 05:15 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 05:15 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 05:15 79-34-55.0 Tetrachloroethene 71.0 ug/L 1 04/26/12 05:15 127-18-45.0 Toluene ND ug/L 1 04/26/12 05:15 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 05:15 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 05:15 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 05:15 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 05:15 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 05:15 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 05:15 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 05:15 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 05:15 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 05:15 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 05:15 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 05:15 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 41 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G350390 Lab ID:5061952013 Collected:04/23/12 15:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/26/12 05:15 1330-20-710.0 Surrogates Dibromofluoromethane (S)105 %.1 04/26/12 05:15 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 05:15 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 05:15 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 42 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G260300 Lab ID:5061952014 Collected:04/23/12 16:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/28/12 07:47 83-32-904/26/12 10:351.1 Acenaphthylene ND ug/L 1 04/28/12 07:47 208-96-804/26/12 10:351.1 Anthracene ND ug/L 1 04/28/12 07:47 120-12-704/26/12 10:350.11 Benzo(a)anthracene ND ug/L 1 04/28/12 07:47 56-55-304/26/12 10:350.11 Benzo(a)pyrene ND ug/L 1 04/28/12 07:47 50-32-804/26/12 10:350.11 Benzo(b)fluoranthene ND ug/L 1 04/28/12 07:47 205-99-204/26/12 10:350.11 Benzo(g,h,i)perylene ND ug/L 1 04/28/12 07:47 191-24-204/26/12 10:350.11 Benzo(k)fluoranthene ND ug/L 1 04/28/12 07:47 207-08-904/26/12 10:350.11 Chrysene ND ug/L 1 04/28/12 07:47 218-01-904/26/12 10:350.53 Dibenz(a,h)anthracene ND ug/L 1 04/28/12 07:47 53-70-304/26/12 10:350.11 Fluoranthene ND ug/L 1 04/28/12 07:47 206-44-004/26/12 10:351.1 Fluorene ND ug/L 1 04/28/12 07:47 86-73-704/26/12 10:351.1 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/28/12 07:47 193-39-504/26/12 10:350.11 2-Methylnaphthalene ND ug/L 1 04/28/12 07:47 91-57-604/26/12 10:351.1 Naphthalene ND ug/L 1 04/28/12 07:47 91-20-304/26/12 10:351.1 Phenanthrene ND ug/L 1 04/28/12 07:47 85-01-804/26/12 10:351.1 Pyrene ND ug/L 1 04/28/12 07:47 129-00-004/26/12 10:351.1 Surrogates 2-Fluorobiphenyl (S)60 %.1 04/28/12 07:47 321-60-804/26/12 10:3526-106 p-Terphenyl-d14 (S)85 %.1 04/28/12 07:47 1718-51-004/26/12 10:3516-111 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/26/12 19:07 100-51-604/26/12 10:3521.3 4-Bromophenylphenyl ether ND ug/L 1 04/26/12 19:07 101-55-304/26/12 10:3510.6 Butylbenzylphthalate ND ug/L 1 04/26/12 19:07 85-68-704/26/12 10:3510.6 4-Chloro-3-methylphenol ND ug/L 1 04/26/12 19:07 59-50-704/26/12 10:3521.3 4-Chloroaniline ND ug/L 1 04/26/12 19:07 106-47-804/26/12 10:3521.3 bis(2-Chloroethoxy)methane ND ug/L 1 04/26/12 19:07 111-91-104/26/12 10:3510.6 bis(2-Chloroethyl) ether ND ug/L 1 04/26/12 19:07 111-44-404/26/12 10:3510.6 bis(2chloro1methylethyl) ether ND ug/L 1 04/26/12 19:07 108-60-104/26/12 10:355.3 2-Chloronaphthalene ND ug/L 1 04/26/12 19:07 91-58-704/26/12 10:3510.6 2-Chlorophenol ND ug/L 1 04/26/12 19:07 95-57-804/26/12 10:3510.6 4-Chlorophenylphenyl ether ND ug/L 1 04/26/12 19:07 7005-72-304/26/12 10:3510.6 Dibenzofuran ND ug/L 1 04/26/12 19:07 132-64-904/26/12 10:3510.6 3,3'-Dichlorobenzidine ND ug/L 1 04/26/12 19:07 91-94-104/26/12 10:3521.3 2,4-Dichlorophenol ND ug/L 1 04/26/12 19:07 120-83-204/26/12 10:3510.6 Diethylphthalate ND ug/L 1 04/26/12 19:07 84-66-204/26/12 10:3510.6 2,4-Dimethylphenol ND ug/L 1 04/26/12 19:07 105-67-904/26/12 10:3510.6 Dimethylphthalate ND ug/L 1 04/26/12 19:07 131-11-304/26/12 10:3510.6 Di-n-butylphthalate ND ug/L 1 04/26/12 19:07 84-74-204/26/12 10:3510.6 4,6-Dinitro-2-methylphenol ND ug/L 1 04/26/12 19:07 534-52-104/26/12 10:3553.2 2,4-Dinitrophenol ND ug/L 1 04/26/12 19:07 51-28-504/26/12 10:3553.2 2,4-Dinitrotoluene ND ug/L 1 04/26/12 19:07 121-14-204/26/12 10:3510.6 2,6-Dinitrotoluene ND ug/L 1 04/26/12 19:07 606-20-204/26/12 10:3510.6 Di-n-octylphthalate ND ug/L 1 04/26/12 19:07 117-84-004/26/12 10:3510.6 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/26/12 19:07 117-81-704/26/12 10:355.3 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 19:07 87-68-304/26/12 10:355.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 43 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G260300 Lab ID:5061952014 Collected:04/23/12 16:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Hexachlorobenzene ND ug/L 1 04/26/12 19:07 118-74-104/26/12 10:3510.6 Hexachlorocyclopentadiene ND ug/L 1 04/26/12 19:07 77-47-404/26/12 10:3526.6 Hexachloroethane ND ug/L 1 04/26/12 19:07 67-72-104/26/12 10:3510.6 Isophorone ND ug/L 1 04/26/12 19:07 78-59-104/26/12 10:3510.6 2-Methylphenol(o-Cresol)ND ug/L 1 04/26/12 19:07 95-48-704/26/12 10:3510.6 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/26/12 19:0704/26/12 10:3521.3 2-Nitroaniline ND ug/L 1 04/26/12 19:07 88-74-404/26/12 10:3553.2 3-Nitroaniline ND ug/L 1 04/26/12 19:07 99-09-204/26/12 10:3553.2 4-Nitroaniline ND ug/L 1 04/26/12 19:07 100-01-604/26/12 10:3553.2 Nitrobenzene ND ug/L 1 04/26/12 19:07 98-95-304/26/12 10:3510.6 2-Nitrophenol ND ug/L 1 04/26/12 19:07 88-75-504/26/12 10:3510.6 4-Nitrophenol ND ug/L 1 04/26/12 19:07 100-02-704/26/12 10:3553.2 N-Nitroso-di-n-propylamine ND ug/L 1 04/26/12 19:07 621-64-704/26/12 10:3510.6 N-Nitrosodiphenylamine ND ug/L 1 04/26/12 19:07 86-30-604/26/12 10:3510.6 Pentachlorophenol ND ug/L 1 04/26/12 19:07 87-86-504/26/12 10:3553.2 Phenol ND ug/L 1 04/26/12 19:07 108-95-204/26/12 10:3510.6 2,4,5-Trichlorophenol ND ug/L 1 04/26/12 19:07 95-95-404/26/12 10:3510.6 2,4,6-Trichlorophenol ND ug/L 1 04/26/12 19:07 88-06-204/26/12 10:3510.6 Surrogates Nitrobenzene-d5 (S)61 %.1 04/26/12 19:07 4165-60-004/26/12 10:3533-108 Phenol-d5 (S)14 %.1 04/26/12 19:07 4165-62-204/26/12 10:3510-56 2-Fluorophenol (S)23 %.1 04/26/12 19:07 367-12-404/26/12 10:3510-74 2,4,6-Tribromophenol (S)88 %.1 04/26/12 19:07 118-79-604/26/12 10:3532-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 05:47 67-64-1100 Acrolein ND ug/L 1 04/26/12 05:47 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 05:47 107-13-1100 Benzene ND ug/L 1 04/26/12 05:47 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 05:47 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 05:47 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 05:47 75-27-45.0 Bromoform ND ug/L 1 04/26/12 05:47 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 05:47 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 05:47 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 05:47 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 05:47 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 05:47 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 05:47 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 05:47 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 05:47 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 05:47 75-00-35.0 Chloroform ND ug/L 1 04/26/12 05:47 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 05:47 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 05:47 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 05:47 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 05:47 124-48-15.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 44 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G260300 Lab ID:5061952014 Collected:04/23/12 16:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 05:47 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 05:47 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 05:47 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 05:47 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 05:47 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 05:47 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 05:47 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 05:47 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 05:47 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 05:47 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 05:47 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 05:47 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 05:47 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 05:47 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 05:47 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 05:47 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 05:47 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 05:47 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 05:47 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 05:47 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 05:47 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 05:47 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 05:47 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 05:47 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 05:47 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 05:47 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 05:47 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 05:47 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 05:47 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 05:47 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 05:47 103-65-15.0 Styrene ND ug/L 1 04/26/12 05:47 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 05:47 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 05:47 79-34-55.0 Tetrachloroethene 77.6 ug/L 1 04/26/12 05:47 127-18-45.0 Toluene ND ug/L 1 04/26/12 05:47 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 05:47 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 05:47 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 05:47 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 05:47 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 05:47 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 05:47 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 05:47 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 05:47 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 05:47 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 05:47 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 05:47 75-01-42.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 45 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB8:G260300 Lab ID:5061952014 Collected:04/23/12 16:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Xylene (Total)ND ug/L 1 04/26/12 05:47 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 04/26/12 05:47 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 04/26/12 05:47 460-00-472-125 Toluene-d8 (S)97 %.1 04/26/12 05:47 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 46 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FBI:W042312 Lab ID:5061952015 Collected:04/23/12 17:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 1 04/27/12 14:02 7440-38-204/26/12 12:000.010 Barium ND mg/L 1 04/27/12 14:02 7440-39-304/26/12 12:000.10 Cadmium ND mg/L 1 04/27/12 14:02 7440-43-904/26/12 12:000.0050 Chromium ND mg/L 1 04/27/12 14:02 7440-47-304/26/12 12:000.010 Lead ND mg/L 1 04/27/12 14:02 7439-92-104/26/12 12:000.010 Selenium ND mg/L 1 04/27/12 14:02 7782-49-204/26/12 12:000.010 Silver ND mg/L 1 04/27/12 14:02 7440-22-404/26/12 12:000.050 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved ND ug/L 1 04/27/12 12:24 7440-38-204/26/12 12:0010.0 Barium, Dissolved ND ug/L 1 04/27/12 12:24 7440-39-304/26/12 12:00100 Cadmium, Dissolved ND ug/L 1 04/27/12 12:24 7440-43-904/26/12 12:005.0 Chromium, Dissolved ND ug/L 1 04/27/12 12:24 7440-47-304/26/12 12:0010.0 Lead, Dissolved ND ug/L 1 04/27/12 12:24 7439-92-104/26/12 12:005.0 Selenium, Dissolved ND ug/L 1 04/27/12 12:24 7782-49-204/26/12 12:0010.0 Silver, Dissolved ND ug/L 1 04/27/12 12:24 7440-22-404/26/12 12:0050.0 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND mg/L 1 04/27/12 12:51 7439-97-604/26/12 12:180.0020 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved ND ug/L 1 04/27/12 14:44 7439-97-604/26/12 12:212.0 8270 MSSV PAH Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 04/28/12 08:05 83-32-904/26/12 10:351.0 Acenaphthylene ND ug/L 1 04/28/12 08:05 208-96-804/26/12 10:351.0 Anthracene ND ug/L 1 04/28/12 08:05 120-12-704/26/12 10:350.10 Benzo(a)anthracene ND ug/L 1 04/28/12 08:05 56-55-304/26/12 10:350.10 Benzo(a)pyrene ND ug/L 1 04/28/12 08:05 50-32-804/26/12 10:350.10 Benzo(b)fluoranthene ND ug/L 1 04/28/12 08:05 205-99-204/26/12 10:350.10 Benzo(g,h,i)perylene ND ug/L 1 04/28/12 08:05 191-24-204/26/12 10:350.10 Benzo(k)fluoranthene ND ug/L 1 04/28/12 08:05 207-08-904/26/12 10:350.10 Chrysene ND ug/L 1 04/28/12 08:05 218-01-904/26/12 10:350.51 Dibenz(a,h)anthracene ND ug/L 1 04/28/12 08:05 53-70-304/26/12 10:350.10 Fluoranthene ND ug/L 1 04/28/12 08:05 206-44-004/26/12 10:351.0 Fluorene ND ug/L 1 04/28/12 08:05 86-73-704/26/12 10:351.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 04/28/12 08:05 193-39-504/26/12 10:350.10 2-Methylnaphthalene ND ug/L 1 04/28/12 08:05 91-57-604/26/12 10:351.0 Naphthalene ND ug/L 1 04/28/12 08:05 91-20-304/26/12 10:351.0 Phenanthrene ND ug/L 1 04/28/12 08:05 85-01-804/26/12 10:351.0 Pyrene ND ug/L 1 04/28/12 08:05 129-00-004/26/12 10:351.0 Surrogates 2-Fluorobiphenyl (S)77 %.1 04/28/12 08:05 321-60-804/26/12 10:3526-106 p-Terphenyl-d14 (S)92 %.1 04/28/12 08:05 1718-51-004/26/12 10:3516-111 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 47 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FBI:W042312 Lab ID:5061952015 Collected:04/23/12 17:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Benzyl alcohol ND ug/L 1 04/26/12 19:28 100-51-604/26/12 10:3520.4 4-Bromophenylphenyl ether ND ug/L 1 04/26/12 19:28 101-55-304/26/12 10:3510.2 Butylbenzylphthalate ND ug/L 1 04/26/12 19:28 85-68-704/26/12 10:3510.2 4-Chloro-3-methylphenol ND ug/L 1 04/26/12 19:28 59-50-704/26/12 10:3520.4 4-Chloroaniline ND ug/L 1 04/26/12 19:28 106-47-804/26/12 10:3520.4 bis(2-Chloroethoxy)methane ND ug/L 1 04/26/12 19:28 111-91-104/26/12 10:3510.2 bis(2-Chloroethyl) ether ND ug/L 1 04/26/12 19:28 111-44-404/26/12 10:3510.2 bis(2chloro1methylethyl) ether ND ug/L 1 04/26/12 19:28 108-60-104/26/12 10:355.1 2-Chloronaphthalene ND ug/L 1 04/26/12 19:28 91-58-704/26/12 10:3510.2 2-Chlorophenol ND ug/L 1 04/26/12 19:28 95-57-804/26/12 10:3510.2 4-Chlorophenylphenyl ether ND ug/L 1 04/26/12 19:28 7005-72-304/26/12 10:3510.2 Dibenzofuran ND ug/L 1 04/26/12 19:28 132-64-904/26/12 10:3510.2 3,3'-Dichlorobenzidine ND ug/L 1 04/26/12 19:28 91-94-104/26/12 10:3520.4 2,4-Dichlorophenol ND ug/L 1 04/26/12 19:28 120-83-204/26/12 10:3510.2 Diethylphthalate ND ug/L 1 04/26/12 19:28 84-66-204/26/12 10:3510.2 2,4-Dimethylphenol ND ug/L 1 04/26/12 19:28 105-67-904/26/12 10:3510.2 Dimethylphthalate ND ug/L 1 04/26/12 19:28 131-11-304/26/12 10:3510.2 Di-n-butylphthalate ND ug/L 1 04/26/12 19:28 84-74-204/26/12 10:3510.2 4,6-Dinitro-2-methylphenol ND ug/L 1 04/26/12 19:28 534-52-104/26/12 10:3551.0 2,4-Dinitrophenol ND ug/L 1 04/26/12 19:28 51-28-504/26/12 10:3551.0 2,4-Dinitrotoluene ND ug/L 1 04/26/12 19:28 121-14-204/26/12 10:3510.2 2,6-Dinitrotoluene ND ug/L 1 04/26/12 19:28 606-20-204/26/12 10:3510.2 Di-n-octylphthalate ND ug/L 1 04/26/12 19:28 117-84-004/26/12 10:3510.2 bis(2-Ethylhexyl)phthalate ND ug/L 1 04/26/12 19:28 117-81-704/26/12 10:355.1 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 19:28 87-68-304/26/12 10:355.1 Hexachlorobenzene ND ug/L 1 04/26/12 19:28 118-74-104/26/12 10:3510.2 Hexachlorocyclopentadiene ND ug/L 1 04/26/12 19:28 77-47-404/26/12 10:3525.5 Hexachloroethane ND ug/L 1 04/26/12 19:28 67-72-104/26/12 10:3510.2 Isophorone ND ug/L 1 04/26/12 19:28 78-59-104/26/12 10:3510.2 2-Methylphenol(o-Cresol)ND ug/L 1 04/26/12 19:28 95-48-704/26/12 10:3510.2 3&4-Methylphenol(m&p Cresol)ND ug/L 1 04/26/12 19:2804/26/12 10:3520.4 2-Nitroaniline ND ug/L 1 04/26/12 19:28 88-74-404/26/12 10:3551.0 3-Nitroaniline ND ug/L 1 04/26/12 19:28 99-09-204/26/12 10:3551.0 4-Nitroaniline ND ug/L 1 04/26/12 19:28 100-01-604/26/12 10:3551.0 Nitrobenzene ND ug/L 1 04/26/12 19:28 98-95-304/26/12 10:3510.2 2-Nitrophenol ND ug/L 1 04/26/12 19:28 88-75-504/26/12 10:3510.2 4-Nitrophenol ND ug/L 1 04/26/12 19:28 100-02-704/26/12 10:3551.0 N-Nitroso-di-n-propylamine ND ug/L 1 04/26/12 19:28 621-64-704/26/12 10:3510.2 N-Nitrosodiphenylamine ND ug/L 1 04/26/12 19:28 86-30-604/26/12 10:3510.2 Pentachlorophenol ND ug/L 1 04/26/12 19:28 87-86-504/26/12 10:3551.0 Phenol ND ug/L 1 04/26/12 19:28 108-95-204/26/12 10:3510.2 2,4,5-Trichlorophenol ND ug/L 1 04/26/12 19:28 95-95-404/26/12 10:3510.2 2,4,6-Trichlorophenol ND ug/L 1 04/26/12 19:28 88-06-204/26/12 10:3510.2 Surrogates Nitrobenzene-d5 (S)79 %.1 04/26/12 19:28 4165-60-004/26/12 10:3533-108 Phenol-d5 (S)16 %.1 04/26/12 19:28 4165-62-204/26/12 10:3510-56 2-Fluorophenol (S)30 %.1 04/26/12 19:28 367-12-404/26/12 10:3510-74 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 48 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FBI:W042312 Lab ID:5061952015 Collected:04/23/12 17:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV SCAN Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates 2,4,6-Tribromophenol (S)96 %.1 04/26/12 19:28 118-79-604/26/12 10:3532-124 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 06:20 67-64-1100 Acrolein ND ug/L 1 04/26/12 06:20 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 06:20 107-13-1100 Benzene ND ug/L 1 04/26/12 06:20 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 06:20 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 06:20 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 06:20 75-27-45.0 Bromoform ND ug/L 1 04/26/12 06:20 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 06:20 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 06:20 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 06:20 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 06:20 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 06:20 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 06:20 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 06:20 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 06:20 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 06:20 75-00-35.0 Chloroform ND ug/L 1 04/26/12 06:20 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 06:20 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 06:20 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 06:20 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 06:20 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 06:20 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 06:20 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 06:20 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 06:20 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 06:20 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 06:20 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 06:20 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 06:20 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 06:20 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 06:20 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 06:20 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 06:20 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 06:20 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 06:20 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 06:20 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 06:20 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 06:20 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 06:20 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 06:20 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 06:20 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 06:20 87-68-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 49 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FBI:W042312 Lab ID:5061952015 Collected:04/23/12 17:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 n-Hexane ND ug/L 1 04/26/12 06:20 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 06:20 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 06:20 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 06:20 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 06:20 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 06:20 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 06:20 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 06:20 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 06:20 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 06:20 103-65-15.0 Styrene ND ug/L 1 04/26/12 06:20 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 06:20 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 06:20 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 06:20 127-18-45.0 Toluene ND ug/L 1 04/26/12 06:20 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 06:20 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 06:20 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 06:20 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 06:20 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 06:20 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 06:20 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 06:20 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 06:20 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 06:20 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 06:20 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 06:20 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 06:20 1330-20-710.0 Surrogates Dibromofluoromethane (S)104 %.1 04/26/12 06:20 1868-53-783-123 4-Bromofluorobenzene (S)99 %.1 04/26/12 06:20 460-00-472-125 Toluene-d8 (S)97 %.1 04/26/12 06:20 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 50 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G450490 Lab ID:5061952016 Collected:04/24/12 09:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 06:52 67-64-1100 Acrolein ND ug/L 1 04/26/12 06:52 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 06:52 107-13-1100 Benzene ND ug/L 1 04/26/12 06:52 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 06:52 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 06:52 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 06:52 75-27-45.0 Bromoform ND ug/L 1 04/26/12 06:52 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 06:52 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 06:52 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 06:52 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 06:52 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 06:52 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 06:52 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 06:52 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 06:52 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 06:52 75-00-35.0 Chloroform ND ug/L 1 04/26/12 06:52 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 06:52 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 06:52 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 06:52 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 06:52 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 06:52 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 06:52 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 06:52 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 06:52 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 06:52 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 06:52 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 06:52 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 06:52 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 06:52 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 06:52 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 06:52 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 06:52 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 06:52 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 06:52 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 06:52 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 06:52 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 06:52 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 06:52 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 06:52 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 06:52 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 06:52 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 06:52 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 06:52 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 06:52 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 06:52 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 51 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G450490 Lab ID:5061952016 Collected:04/24/12 09:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 06:52 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 06:52 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 06:52 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 06:52 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 06:52 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 06:52 103-65-15.0 Styrene ND ug/L 1 04/26/12 06:52 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 06:52 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 06:52 79-34-55.0 Tetrachloroethene 6.0 ug/L 1 04/26/12 06:52 127-18-45.0 Toluene ND ug/L 1 04/26/12 06:52 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 06:52 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 06:52 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 06:52 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 06:52 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 06:52 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 06:52 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 06:52 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 06:52 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 06:52 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 06:52 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 06:52 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 06:52 1330-20-710.0 Surrogates Dibromofluoromethane (S)105 %.1 04/26/12 06:52 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/26/12 06:52 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 06:52 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 52 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G350390 Lab ID:5061952017 Collected:04/24/12 09:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 07:25 67-64-1100 Acrolein ND ug/L 1 04/26/12 07:25 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 07:25 107-13-1100 Benzene ND ug/L 1 04/26/12 07:25 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 07:25 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 07:25 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 07:25 75-27-45.0 Bromoform ND ug/L 1 04/26/12 07:25 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 07:25 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 07:25 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 07:25 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 07:25 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 07:25 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 07:25 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 07:25 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 07:25 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 07:25 75-00-35.0 Chloroform ND ug/L 1 04/26/12 07:25 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 07:25 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 07:25 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 07:25 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 07:25 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 07:25 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 07:25 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 07:25 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 07:25 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 07:25 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 07:25 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 07:25 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 07:25 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 07:25 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 07:25 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 07:25 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 07:25 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 07:25 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 07:25 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 07:25 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 07:25 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 07:25 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 07:25 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 07:25 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 07:25 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 07:25 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 07:25 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 07:25 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 07:25 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 07:25 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 53 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G350390 Lab ID:5061952017 Collected:04/24/12 09:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 07:25 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 07:25 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 07:25 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 07:25 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 07:25 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 07:25 103-65-15.0 Styrene ND ug/L 1 04/26/12 07:25 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 07:25 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 07:25 79-34-55.0 Tetrachloroethene 206 ug/L 1 04/26/12 07:25 127-18-45.0 Toluene ND ug/L 1 04/26/12 07:25 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 07:25 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 07:25 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 07:25 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 07:25 79-00-55.0 Trichloroethene 9.2 ug/L 1 04/26/12 07:25 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 07:25 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 07:25 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 07:25 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 07:25 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 07:25 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 07:25 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 07:25 1330-20-710.0 Surrogates Dibromofluoromethane (S)103 %.1 04/26/12 07:25 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/26/12 07:25 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 07:25 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 54 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G260300 Lab ID:5061952018 Collected:04/24/12 10:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 07:57 67-64-1100 Acrolein ND ug/L 1 04/26/12 07:57 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 07:57 107-13-1100 Benzene ND ug/L 1 04/26/12 07:57 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 07:57 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 07:57 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 07:57 75-27-45.0 Bromoform ND ug/L 1 04/26/12 07:57 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 07:57 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 07:57 78-93-325.0 n-Butylbenzene 5.5 ug/L 1 04/26/12 07:57 104-51-85.0 sec-Butylbenzene 8.8 ug/L 1 04/26/12 07:57 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 07:57 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 07:57 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 07:57 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 07:57 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 07:57 75-00-35.0 Chloroform ND ug/L 1 04/26/12 07:57 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 07:57 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 07:57 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 07:57 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 07:57 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 07:57 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 07:57 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 07:57 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 07:57 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 07:57 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 07:57 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 07:57 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 07:57 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 07:57 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 07:57 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 07:57 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 07:57 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 07:57 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 07:57 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 07:57 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 07:57 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 07:57 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 07:57 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 07:57 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 07:57 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 07:57 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 07:57 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 07:57 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 07:57 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 07:57 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 55 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB16:G260300 Lab ID:5061952018 Collected:04/24/12 10:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 07:57 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 07:57 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 07:57 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 07:57 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 07:57 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 07:57 103-65-15.0 Styrene ND ug/L 1 04/26/12 07:57 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 07:57 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 07:57 79-34-55.0 Tetrachloroethene 20.1 ug/L 1 04/26/12 07:57 127-18-45.0 Toluene ND ug/L 1 04/26/12 07:57 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 07:57 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 07:57 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 07:57 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 07:57 79-00-55.0 Trichloroethene 54.1 ug/L 1 04/26/12 07:57 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 07:57 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 07:57 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 07:57 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 07:57 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 07:57 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 07:57 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 07:57 1330-20-710.0 Surrogates Dibromofluoromethane (S)105 %.1 04/26/12 07:57 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/26/12 07:57 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 07:57 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 56 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G450490 Lab ID:5061952019 Collected:04/24/12 10:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 08:29 67-64-1100 Acrolein ND ug/L 1 04/26/12 08:29 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 08:29 107-13-1100 Benzene ND ug/L 1 04/26/12 08:29 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 08:29 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 08:29 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 08:29 75-27-45.0 Bromoform ND ug/L 1 04/26/12 08:29 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 08:29 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 08:29 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 08:29 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 08:29 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 08:29 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 08:29 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 08:29 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 08:29 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 08:29 75-00-35.0 Chloroform ND ug/L 1 04/26/12 08:29 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 08:29 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 08:29 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 08:29 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 08:29 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 08:29 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 08:29 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 08:29 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 08:29 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 08:29 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 08:29 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 08:29 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 08:29 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 08:29 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 08:29 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 08:29 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 08:29 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 08:29 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 08:29 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 08:29 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 08:29 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 08:29 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 08:29 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 08:29 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 08:29 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 08:29 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 08:29 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 08:29 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 08:29 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 08:29 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 57 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G450490 Lab ID:5061952019 Collected:04/24/12 10:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 08:29 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 08:29 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 08:29 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 08:29 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 08:29 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 08:29 103-65-15.0 Styrene ND ug/L 1 04/26/12 08:29 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 08:29 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 08:29 79-34-55.0 Tetrachloroethene 138 ug/L 1 04/26/12 08:29 127-18-45.0 Toluene ND ug/L 1 04/26/12 08:29 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 08:29 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 08:29 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 08:29 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 08:29 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 08:29 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 08:29 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 08:29 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 08:29 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 08:29 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 08:29 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 08:29 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 08:29 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/26/12 08:29 1868-53-783-123 4-Bromofluorobenzene (S)105 %.1 04/26/12 08:29 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 08:29 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 58 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G350390 Lab ID:5061952020 Collected:04/24/12 11:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 09:02 67-64-1100 Acrolein ND ug/L 1 04/26/12 09:02 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 09:02 107-13-1100 Benzene ND ug/L 1 04/26/12 09:02 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 09:02 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 09:02 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 09:02 75-27-45.0 Bromoform ND ug/L 1 04/26/12 09:02 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 09:02 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 09:02 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 09:02 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 09:02 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 09:02 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 09:02 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 09:02 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 09:02 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 09:02 75-00-35.0 Chloroform ND ug/L 1 04/26/12 09:02 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 09:02 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 09:02 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 09:02 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 09:02 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 09:02 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 09:02 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 09:02 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 09:02 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 09:02 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 09:02 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 09:02 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 09:02 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 09:02 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 09:02 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 09:02 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 09:02 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 09:02 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 09:02 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 09:02 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 09:02 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 09:02 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 09:02 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 09:02 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 09:02 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 09:02 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 09:02 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 09:02 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 09:02 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 09:02 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 59 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G350390 Lab ID:5061952020 Collected:04/24/12 11:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 09:02 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 09:02 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 09:02 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 09:02 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 09:02 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 09:02 103-65-15.0 Styrene ND ug/L 1 04/26/12 09:02 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 09:02 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 09:02 79-34-55.0 Tetrachloroethene 447 ug/L 10 04/26/12 15:15 127-18-450.0 Toluene ND ug/L 1 04/26/12 09:02 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 09:02 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 09:02 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 09:02 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 09:02 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 09:02 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 09:02 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 09:02 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 09:02 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 09:02 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 09:02 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 09:02 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 09:02 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/26/12 09:02 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 09:02 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 09:02 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 60 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G350390A Lab ID:5061952021 Collected:04/24/12 11:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 16:52 67-64-1100 Acrolein ND ug/L 1 04/26/12 16:52 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 16:52 107-13-1100 Benzene ND ug/L 1 04/26/12 16:52 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 16:52 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 16:52 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 16:52 75-27-45.0 Bromoform ND ug/L 1 04/26/12 16:52 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 16:52 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 16:52 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 16:52 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 16:52 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 16:52 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 16:52 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 16:52 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 16:52 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 16:52 75-00-35.0 Chloroform ND ug/L 1 04/26/12 16:52 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 16:52 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 16:52 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 16:52 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 16:52 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 16:52 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 16:52 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 16:52 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 16:52 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 16:52 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 16:52 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 16:52 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 16:52 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 16:52 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 16:52 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 16:52 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 16:52 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 16:52 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 16:52 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 16:52 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 16:52 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 16:52 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 16:52 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 16:52 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 16:52 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 16:52 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 16:52 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 16:52 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 16:52 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 16:52 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 61 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G350390A Lab ID:5061952021 Collected:04/24/12 11:15 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 16:52 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 16:52 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 16:52 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 16:52 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 16:52 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 16:52 103-65-15.0 Styrene ND ug/L 1 04/26/12 16:52 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 16:52 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 16:52 79-34-55.0 Tetrachloroethene 579 ug/L 10 04/30/12 10:59 127-18-450.0 Toluene ND ug/L 1 04/26/12 16:52 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 16:52 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 16:52 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 16:52 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 16:52 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 16:52 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 16:52 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 16:52 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 16:52 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 16:52 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 16:52 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 16:52 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 16:52 1330-20-710.0 Surrogates Dibromofluoromethane (S)100 %.1 04/26/12 16:52 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/26/12 16:52 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 16:52 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 62 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G260300 Lab ID:5061952022 Collected:04/24/12 11:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 17:24 67-64-1100 Acrolein ND ug/L 1 04/26/12 17:24 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 17:24 107-13-1100 Benzene ND ug/L 1 04/26/12 17:24 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 17:24 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 17:24 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 17:24 75-27-45.0 Bromoform ND ug/L 1 04/26/12 17:24 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 17:24 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 17:24 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 17:24 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 17:24 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 17:24 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 17:24 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 17:24 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 17:24 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 17:24 75-00-35.0 Chloroform ND ug/L 1 04/26/12 17:24 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 17:24 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 17:24 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 17:24 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 17:24 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 17:24 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 17:24 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 17:24 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 17:24 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 17:24 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 17:24 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 17:24 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 17:24 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 17:24 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 17:24 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 17:24 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 17:24 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 17:24 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 17:24 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 17:24 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 17:24 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 17:24 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 17:24 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 17:24 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 17:24 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 17:24 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 17:24 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 17:24 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 17:24 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 17:24 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 63 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB13:G260300 Lab ID:5061952022 Collected:04/24/12 11:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 17:24 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 17:24 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 17:24 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 17:24 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 17:24 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 17:24 103-65-15.0 Styrene ND ug/L 1 04/26/12 17:24 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 17:24 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 17:24 79-34-55.0 Tetrachloroethene 40.9 ug/L 1 04/26/12 17:24 127-18-45.0 Toluene ND ug/L 1 04/26/12 17:24 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 17:24 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 17:24 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 17:24 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 17:24 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 17:24 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 17:24 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 17:24 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 17:24 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 17:24 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 17:24 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 17:24 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 17:24 1330-20-710.0 Surrogates Dibromofluoromethane (S)102 %.1 04/26/12 17:24 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 17:24 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 17:24 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 64 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G450490 Lab ID:5061952023 Collected:04/24/12 12:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 17:56 67-64-1100 Acrolein ND ug/L 1 04/26/12 17:56 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 17:56 107-13-1100 Benzene ND ug/L 1 04/26/12 17:56 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 17:56 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 17:56 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 17:56 75-27-45.0 Bromoform ND ug/L 1 04/26/12 17:56 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 17:56 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 17:56 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 17:56 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 17:56 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 17:56 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 17:56 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 17:56 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 17:56 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 17:56 75-00-35.0 Chloroform ND ug/L 1 04/26/12 17:56 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 17:56 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 17:56 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 17:56 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 17:56 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 17:56 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 17:56 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 17:56 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 17:56 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 17:56 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 17:56 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 17:56 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 17:56 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 17:56 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 17:56 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 17:56 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 17:56 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 17:56 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 17:56 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 17:56 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 17:56 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 17:56 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 17:56 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 17:56 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 17:56 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 17:56 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 17:56 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 17:56 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 17:56 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 17:56 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 65 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G450490 Lab ID:5061952023 Collected:04/24/12 12:40 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 17:56 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 17:56 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 17:56 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 17:56 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 17:56 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 17:56 103-65-15.0 Styrene ND ug/L 1 04/26/12 17:56 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 17:56 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 17:56 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 17:56 127-18-45.0 Toluene ND ug/L 1 04/26/12 17:56 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 17:56 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 17:56 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 17:56 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 17:56 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 17:56 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 17:56 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 17:56 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 17:56 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 17:56 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 17:56 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 17:56 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 17:56 1330-20-710.0 Surrogates Dibromofluoromethane (S)99 %.1 04/26/12 17:56 1868-53-783-123 4-Bromofluorobenzene (S)98 %.1 04/26/12 17:56 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 17:56 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 66 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G350390 Lab ID:5061952024 Collected:04/24/12 13:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 09:34 67-64-1100 Acrolein ND ug/L 1 04/26/12 09:34 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 09:34 107-13-1100 Benzene ND ug/L 1 04/26/12 09:34 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 09:34 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 09:34 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 09:34 75-27-45.0 Bromoform ND ug/L 1 04/26/12 09:34 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 09:34 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 09:34 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 09:34 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 09:34 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 09:34 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 09:34 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 09:34 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 09:34 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 09:34 75-00-35.0 Chloroform ND ug/L 1 04/26/12 09:34 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 09:34 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 09:34 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 09:34 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 09:34 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 09:34 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 09:34 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 09:34 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 09:34 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 09:34 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 09:34 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 09:34 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 09:34 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 09:34 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 09:34 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 09:34 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 09:34 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 09:34 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 09:34 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 09:34 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 09:34 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 09:34 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 09:34 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 09:34 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 09:34 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 09:34 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 09:34 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 09:34 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 09:34 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 09:34 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 67 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G350390 Lab ID:5061952024 Collected:04/24/12 13:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 09:34 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 09:34 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 09:34 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 09:34 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 09:34 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 09:34 103-65-15.0 Styrene ND ug/L 1 04/26/12 09:34 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 09:34 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 09:34 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 09:34 127-18-45.0 Toluene ND ug/L 1 04/26/12 09:34 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 09:34 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 09:34 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 09:34 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 09:34 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 09:34 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 09:34 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 09:34 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 09:34 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 09:34 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 09:34 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 09:34 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 09:34 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/26/12 09:34 1868-53-783-123 4-Bromofluorobenzene (S)106 %.1 04/26/12 09:34 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 09:34 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 68 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G260300 Lab ID:5061952025 Collected:04/24/12 13:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 18:28 67-64-1100 Acrolein ND ug/L 1 04/26/12 18:28 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 18:28 107-13-1100 Benzene ND ug/L 1 04/26/12 18:28 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 18:28 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 18:28 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 18:28 75-27-45.0 Bromoform ND ug/L 1 04/26/12 18:28 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 18:28 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 18:28 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 18:28 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 18:28 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 18:28 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 18:28 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 18:28 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 18:28 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 18:28 75-00-35.0 Chloroform ND ug/L 1 04/26/12 18:28 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 18:28 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 18:28 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 18:28 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 18:28 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 18:28 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 18:28 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 18:28 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 18:28 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 18:28 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 18:28 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 18:28 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 18:28 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 18:28 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 18:28 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 18:28 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 18:28 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 18:28 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 18:28 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 18:28 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 18:28 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 18:28 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 18:28 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 18:28 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 18:28 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 18:28 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 18:28 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 18:28 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 18:28 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 18:28 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 69 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB11:G260300 Lab ID:5061952025 Collected:04/24/12 13:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 18:28 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 18:28 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 18:28 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 18:28 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 18:28 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 18:28 103-65-15.0 Styrene ND ug/L 1 04/26/12 18:28 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 18:28 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 18:28 79-34-55.0 Tetrachloroethene 6.9 ug/L 1 04/26/12 18:28 127-18-45.0 Toluene ND ug/L 1 04/26/12 18:28 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 18:28 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 18:28 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 18:28 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 18:28 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 18:28 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 18:28 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 18:28 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 18:28 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 18:28 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 18:28 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 18:28 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 18:28 1330-20-710.0 Surrogates Dibromofluoromethane (S)99 %.1 04/26/12 18:28 1868-53-783-123 4-Bromofluorobenzene (S)100 %.1 04/26/12 18:28 460-00-472-125 Toluene-d8 (S)98 %.1 04/26/12 18:28 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 70 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G450490 Lab ID:5061952026 Collected:04/24/12 14:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 19:00 67-64-1100 Acrolein ND ug/L 1 04/26/12 19:00 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 19:00 107-13-1100 Benzene ND ug/L 1 04/26/12 19:00 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 19:00 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 19:00 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 19:00 75-27-45.0 Bromoform ND ug/L 1 04/26/12 19:00 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 19:00 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 19:00 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 19:00 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 19:00 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 19:00 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 19:00 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 19:00 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 19:00 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 19:00 75-00-35.0 Chloroform ND ug/L 1 04/26/12 19:00 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 19:00 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 19:00 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 19:00 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 19:00 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 19:00 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 19:00 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 19:00 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 19:00 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 19:00 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 19:00 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 19:00 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 19:00 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 19:00 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 19:00 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 19:00 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 19:00 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 19:00 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 19:00 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 19:00 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 19:00 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 19:00 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 19:00 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 19:00 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 19:00 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 19:00 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 19:00 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 19:00 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 19:00 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 19:00 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 71 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G450490 Lab ID:5061952026 Collected:04/24/12 14:25 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 19:00 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 19:00 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 19:00 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 19:00 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 19:00 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 19:00 103-65-15.0 Styrene ND ug/L 1 04/26/12 19:00 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 19:00 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 19:00 79-34-55.0 Tetrachloroethene 970 ug/L 10 04/30/12 12:13 127-18-450.0 Toluene ND ug/L 1 04/26/12 19:00 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 19:00 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 19:00 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 19:00 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 19:00 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 19:00 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 19:00 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 19:00 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 19:00 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 19:00 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 19:00 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 19:00 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 19:00 1330-20-710.0 Surrogates Dibromofluoromethane (S)97 %.1 04/26/12 19:00 1868-53-783-123 4-Bromofluorobenzene (S)106 %.1 04/26/12 19:00 460-00-472-125 Toluene-d8 (S)93 %.1 04/26/12 19:00 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 72 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G350390 Lab ID:5061952027 Collected:04/24/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 19:32 67-64-1100 Acrolein ND ug/L 1 04/26/12 19:32 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 19:32 107-13-1100 Benzene ND ug/L 1 04/26/12 19:32 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 19:32 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 19:32 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 19:32 75-27-45.0 Bromoform ND ug/L 1 04/26/12 19:32 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 19:32 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 19:32 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 19:32 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 19:32 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 19:32 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 19:32 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 19:32 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 19:32 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 19:32 75-00-35.0 Chloroform ND ug/L 1 04/26/12 19:32 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 19:32 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 19:32 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 19:32 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 19:32 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 19:32 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 19:32 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 19:32 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 19:32 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 19:32 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 19:32 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 19:32 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 19:32 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 19:32 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 19:32 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 19:32 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 19:32 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 19:32 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 19:32 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 19:32 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 19:32 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 19:32 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 19:32 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 19:32 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 19:32 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 19:32 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 19:32 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 19:32 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 19:32 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 19:32 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 73 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G350390 Lab ID:5061952027 Collected:04/24/12 14:50 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 19:32 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 19:32 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 19:32 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 19:32 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 19:32 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 19:32 103-65-15.0 Styrene ND ug/L 1 04/26/12 19:32 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 19:32 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 19:32 79-34-55.0 Tetrachloroethene 1350 ug/L 10 04/30/12 12:50 127-18-450.0 Toluene ND ug/L 1 04/26/12 19:32 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 19:32 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 19:32 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 19:32 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 19:32 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 19:32 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 19:32 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 19:32 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 19:32 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 19:32 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 19:32 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 19:32 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 19:32 1330-20-710.0 Surrogates Dibromofluoromethane (S)98 %.1 04/26/12 19:32 1868-53-783-123 4-Bromofluorobenzene (S)107 %.1 04/26/12 19:32 460-00-472-125 Toluene-d8 (S)96 %.1 04/26/12 19:32 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 74 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G260300 Lab ID:5061952028 Collected:04/24/12 15:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 20:04 67-64-1100 Acrolein ND ug/L 1 04/26/12 20:04 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 20:04 107-13-1100 Benzene ND ug/L 1 04/26/12 20:04 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 20:04 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 20:04 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 20:04 75-27-45.0 Bromoform ND ug/L 1 04/26/12 20:04 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 20:04 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 20:04 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 20:04 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 20:04 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 20:04 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 20:04 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 20:04 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 20:04 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 20:04 75-00-35.0 Chloroform ND ug/L 1 04/26/12 20:04 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 20:04 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 20:04 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 20:04 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 20:04 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 20:04 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 20:04 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 20:04 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 20:04 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 20:04 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 20:04 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 20:04 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 20:04 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 20:04 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 20:04 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 20:04 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 20:04 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 20:04 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 20:04 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 20:04 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 20:04 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 20:04 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 20:04 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 20:04 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 20:04 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 20:04 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 20:04 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 20:04 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 20:04 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 20:04 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 75 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:HTB22:G260300 Lab ID:5061952028 Collected:04/24/12 15:30 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 20:04 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 20:04 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 20:04 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 20:04 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 20:04 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 20:04 103-65-15.0 Styrene ND ug/L 1 04/26/12 20:04 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 20:04 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 20:04 79-34-55.0 Tetrachloroethene 53.2 ug/L 1 04/26/12 20:04 127-18-45.0 Toluene ND ug/L 1 04/26/12 20:04 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 20:04 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 20:04 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 20:04 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 20:04 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 20:04 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 20:04 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 20:04 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 20:04 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 20:04 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 20:04 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 20:04 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 20:04 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/26/12 20:04 1868-53-783-123 4-Bromofluorobenzene (S)102 %.1 04/26/12 20:04 460-00-472-125 Toluene-d8 (S)100 %.1 04/26/12 20:04 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 76 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FB1:W042412 Lab ID:5061952029 Collected:04/24/12 16:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 20:37 67-64-1100 Acrolein ND ug/L 1 04/26/12 20:37 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 20:37 107-13-1100 Benzene ND ug/L 1 04/26/12 20:37 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 20:37 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 20:37 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 20:37 75-27-45.0 Bromoform ND ug/L 1 04/26/12 20:37 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 20:37 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 20:37 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 20:37 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 20:37 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 20:37 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 20:37 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 20:37 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 20:37 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 20:37 75-00-35.0 Chloroform ND ug/L 1 04/26/12 20:37 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 20:37 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 20:37 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 20:37 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 20:37 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 20:37 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 20:37 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 20:37 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 20:37 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 20:37 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 20:37 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 20:37 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 20:37 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 20:37 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 20:37 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 20:37 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 20:37 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 20:37 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 20:37 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 20:37 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 20:37 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 20:37 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 20:37 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 20:37 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 20:37 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 20:37 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 20:37 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 20:37 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 20:37 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 20:37 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 77 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:FB1:W042412 Lab ID:5061952029 Collected:04/24/12 16:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 04/26/12 20:37 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 20:37 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 20:37 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 20:37 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 20:37 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 20:37 103-65-15.0 Styrene ND ug/L 1 04/26/12 20:37 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 20:37 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 20:37 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 20:37 127-18-45.0 Toluene ND ug/L 1 04/26/12 20:37 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 20:37 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 20:37 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 20:37 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 20:37 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 20:37 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 20:37 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 20:37 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 20:37 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 20:37 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 20:37 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 20:37 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 20:37 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/26/12 20:37 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/26/12 20:37 460-00-472-125 Toluene-d8 (S)100 %.1 04/26/12 20:37 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 78 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:TRIP BLANK:W042412 Lab ID:5061952030 Collected:04/23/12 08:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 04/26/12 21:09 67-64-1100 Acrolein ND ug/L 1 04/26/12 21:09 107-02-8100 Acrylonitrile ND ug/L 1 04/26/12 21:09 107-13-1100 Benzene ND ug/L 1 04/26/12 21:09 71-43-25.0 Bromobenzene ND ug/L 1 04/26/12 21:09 108-86-15.0 Bromochloromethane ND ug/L 1 04/26/12 21:09 74-97-55.0 Bromodichloromethane ND ug/L 1 04/26/12 21:09 75-27-45.0 Bromoform ND ug/L 1 04/26/12 21:09 75-25-25.0 Bromomethane ND ug/L 1 04/26/12 21:09 74-83-95.0 2-Butanone (MEK)ND ug/L 1 04/26/12 21:09 78-93-325.0 n-Butylbenzene ND ug/L 1 04/26/12 21:09 104-51-85.0 sec-Butylbenzene ND ug/L 1 04/26/12 21:09 135-98-85.0 tert-Butylbenzene ND ug/L 1 04/26/12 21:09 98-06-65.0 Carbon disulfide ND ug/L 1 04/26/12 21:09 75-15-010.0 Carbon tetrachloride ND ug/L 1 04/26/12 21:09 56-23-55.0 Chlorobenzene ND ug/L 1 04/26/12 21:09 108-90-75.0 Chloroethane ND ug/L 1 04/26/12 21:09 75-00-35.0 Chloroform ND ug/L 1 04/26/12 21:09 67-66-35.0 Chloromethane ND ug/L 1 04/26/12 21:09 74-87-35.0 2-Chlorotoluene ND ug/L 1 04/26/12 21:09 95-49-85.0 4-Chlorotoluene ND ug/L 1 04/26/12 21:09 106-43-45.0 Dibromochloromethane ND ug/L 1 04/26/12 21:09 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 04/26/12 21:09 106-93-45.0 Dibromomethane ND ug/L 1 04/26/12 21:09 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 04/26/12 21:09 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 04/26/12 21:09 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 04/26/12 21:09 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 04/26/12 21:09 110-57-6100 Dichlorodifluoromethane ND ug/L 1 04/26/12 21:09 75-71-85.0 1,1-Dichloroethane ND ug/L 1 04/26/12 21:09 75-34-35.0 1,2-Dichloroethane ND ug/L 1 04/26/12 21:09 107-06-25.0 1,1-Dichloroethene ND ug/L 1 04/26/12 21:09 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 04/26/12 21:09 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 04/26/12 21:09 156-60-55.0 1,2-Dichloropropane ND ug/L 1 04/26/12 21:09 78-87-55.0 1,3-Dichloropropane ND ug/L 1 04/26/12 21:09 142-28-95.0 2,2-Dichloropropane ND ug/L 1 04/26/12 21:09 594-20-75.0 1,1-Dichloropropene ND ug/L 1 04/26/12 21:09 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 04/26/12 21:09 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 04/26/12 21:09 10061-02-65.0 Ethylbenzene ND ug/L 1 04/26/12 21:09 100-41-45.0 Ethyl methacrylate ND ug/L 1 04/26/12 21:09 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 04/26/12 21:09 87-68-35.0 n-Hexane ND ug/L 1 04/26/12 21:09 110-54-3 N25.0 2-Hexanone ND ug/L 1 04/26/12 21:09 591-78-625.0 Iodomethane ND ug/L 1 04/26/12 21:09 74-88-410.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 79 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 ANALYTICAL RESULTS Pace Project No.: Project: 5061952 SBI067 Sample:SBI067:TRIP BLANK:W042412 Lab ID:5061952030 Collected:04/23/12 08:00 Received:04/25/12 12:43 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Isopropylbenzene (Cumene)ND ug/L 1 04/26/12 21:09 98-82-85.0 p-Isopropyltoluene ND ug/L 1 04/26/12 21:09 99-87-65.0 Methylene Chloride ND ug/L 1 04/26/12 21:09 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 04/26/12 21:09 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 04/26/12 21:09 1634-04-44.0 Naphthalene ND ug/L 1 04/26/12 21:09 91-20-35.0 n-Propylbenzene ND ug/L 1 04/26/12 21:09 103-65-15.0 Styrene ND ug/L 1 04/26/12 21:09 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 04/26/12 21:09 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 04/26/12 21:09 79-34-55.0 Tetrachloroethene ND ug/L 1 04/26/12 21:09 127-18-45.0 Toluene ND ug/L 1 04/26/12 21:09 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 04/26/12 21:09 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 04/26/12 21:09 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 04/26/12 21:09 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 04/26/12 21:09 79-00-55.0 Trichloroethene ND ug/L 1 04/26/12 21:09 79-01-65.0 Trichlorofluoromethane ND ug/L 1 04/26/12 21:09 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 04/26/12 21:09 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 04/26/12 21:09 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 04/26/12 21:09 108-67-85.0 Vinyl acetate ND ug/L 1 04/26/12 21:09 108-05-450.0 Vinyl chloride ND ug/L 1 04/26/12 21:09 75-01-42.0 Xylene (Total)ND ug/L 1 04/26/12 21:09 1330-20-710.0 Surrogates Dibromofluoromethane (S)101 %.1 04/26/12 21:09 1868-53-783-123 4-Bromofluorobenzene (S)101 %.1 04/26/12 21:09 460-00-472-125 Toluene-d8 (S)100 %.1 04/26/12 21:09 2037-26-581-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 80 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MERP/3812 EPA 7470 EPA 7470 7470 Mercury Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725712 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Matrix:Water Analyzed Mercury mg/L ND 0.0020 04/27/12 11:17 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725713LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/L 0.0046.005 92 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 725714MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 725715 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/L .005 101 75-12598 3 20.005ND 0.0050 0.0049 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 81 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MERP/3813 EPA 7470 EPA 7470 7470 Mercury Dissolved Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725723 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Matrix:Water Analyzed Mercury, Dissolved ug/L ND 2.0 04/27/12 13:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725724LABORATORY CONTROL SAMPLE: LCSSpike Mercury, Dissolved ug/L 4.85 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 725725MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 725726 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury, Dissolved ug/L 5 99 75-12588 12 205ND4.9 4.4 Parameter Units MS Result % Rec Limits Qual% RecConc. 725727MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061841005 725728 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury, Dissolved ug/L 5 92 75-12592 .2 205ND4.6 4.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 82 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/9075 EPA 3010 EPA 6010 6010 MET Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725673 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Matrix:Water Analyzed Arsenic mg/L ND 0.010 04/27/12 13:10 Barium mg/L ND 0.10 04/27/12 13:10 Cadmium mg/L ND 0.0050 04/27/12 13:10 Chromium mg/L ND 0.010 04/27/12 13:10 Lead mg/L ND 0.010 04/27/12 13:10 Selenium mg/L ND 0.010 04/27/12 13:10 Silver mg/L ND 0.050 04/27/12 13:10 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725674LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/L 0.971 97 80-120 Barium mg/L 0.981 98 80-120 Cadmium mg/L 0.971 97 80-120 Chromium mg/L 1.01 101 80-120 Lead mg/L 0.941 94 80-120 Selenium mg/L 0.961 96 80-120 Silver mg/L 0.52.5 104 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 725675MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 725676 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/L 1 97 75-12596 1 2010.045 1.0 1.0 Barium mg/L 1 100 75-12598 2 2010.12 1.1 1.1 Cadmium mg/L 1 98 75-12597 1 201ND0.98 0.97 Chromium mg/L 1 97 75-12597 .09 2010.13 1.1 1.1 Lead mg/L 1 90 75-12589 1 2010.011 0.91 0.90 Selenium mg/L 1 96 75-12595 1 201ND0.97 0.95 Silver mg/L .5 105 75-125104 1 20.5ND 0.53 0.52 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 83 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/9079 EPA 3010 EPA 6010 6010 MET Dissolved Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:726219 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005, 5061952006, 5061952007, 5061952015 Matrix:Water Analyzed Arsenic, Dissolved ug/L ND 10.0 04/27/12 11:18 Barium, Dissolved ug/L ND 100 04/27/12 11:18 Cadmium, Dissolved ug/L ND 5.0 04/27/12 11:18 Chromium, Dissolved ug/L ND 10.0 04/27/12 11:18 Lead, Dissolved ug/L ND 5.0 04/27/12 11:18 Selenium, Dissolved ug/L ND 10.0 04/27/12 11:18 Silver, Dissolved ug/L ND 50.0 04/27/12 11:18 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 726220LABORATORY CONTROL SAMPLE: LCSSpike Arsenic, Dissolved ug/L 9731000 97 80-120 Barium, Dissolved ug/L 9811000 98 80-120 Cadmium, Dissolved ug/L 9721000 97 80-120 Chromium, Dissolved ug/L 10001000 100 80-120 Lead, Dissolved ug/L 9531000 95 80-120 Selenium, Dissolved ug/L 9781000 98 80-120 Silver, Dissolved ug/L 497500 99 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 726221MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 726222 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic, Dissolved ug/L 1000 96 75-12598 1 201000ND965976 Barium, Dissolved ug/L 1000 97 75-12597 .7 201000ND9941000 Cadmium, Dissolved ug/L 1000 97 75-12598 1 201000ND966976 Chromium, Dissolved ug/L 1000 97 75-12596 .6 201000ND969963 Lead, Dissolved ug/L 1000 92 75-12592 .2 201000ND922924 Selenium, Dissolved ug/L 1000 97 75-12597 .6 201000ND965972 Silver, Dissolved ug/L 500 96 75-125100 4 20500ND481501 Parameter Units MS Result % Rec Limits Qual% RecConc. 726223MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061841005 726224 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic, Dissolved ug/L 1000 98 75-12598 .1 201000ND978980 Barium, Dissolved ug/L 1000 98 75-12598 .6 201000ND10301020 Cadmium, Dissolved ug/L 1000 98 75-12598 .1 201000ND977975 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 84 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 726223MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061841005 726224 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Chromium, Dissolved ug/L 1000 99 75-12597 2 201000ND992970 Lead, Dissolved ug/L 1000 92 75-12592 .4 201000ND924920 Selenium, Dissolved ug/L 1000 98 75-12597 1 201000ND980968 Silver, Dissolved ug/L 500 100 75-125101 1 20500ND500505 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 85 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41620 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725803 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/25/12 14:02 1,1,1-Trichloroethane ug/L ND 5.0 04/25/12 14:02 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/25/12 14:02 1,1,2-Trichloroethane ug/L ND 5.0 04/25/12 14:02 1,1-Dichloroethane ug/L ND 5.0 04/25/12 14:02 1,1-Dichloroethene ug/L ND 5.0 04/25/12 14:02 1,1-Dichloropropene ug/L ND 5.0 04/25/12 14:02 1,2,3-Trichlorobenzene ug/L ND 5.0 04/25/12 14:02 1,2,3-Trichloropropane ug/L ND 5.0 04/25/12 14:02 1,2,4-Trichlorobenzene ug/L ND 5.0 04/25/12 14:02 1,2,4-Trimethylbenzene ug/L ND 5.0 04/25/12 14:02 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/25/12 14:02 1,2-Dichlorobenzene ug/L ND 5.0 04/25/12 14:02 1,2-Dichloroethane ug/L ND 5.0 04/25/12 14:02 1,2-Dichloropropane ug/L ND 5.0 04/25/12 14:02 1,3,5-Trimethylbenzene ug/L ND 5.0 04/25/12 14:02 1,3-Dichlorobenzene ug/L ND 5.0 04/25/12 14:02 1,3-Dichloropropane ug/L ND 5.0 04/25/12 14:02 1,4-Dichlorobenzene ug/L ND 5.0 04/25/12 14:02 2,2-Dichloropropane ug/L ND 5.0 04/25/12 14:02 2-Butanone (MEK)ug/L ND 25.0 04/25/12 14:02 2-Chlorotoluene ug/L ND 5.0 04/25/12 14:02 2-Hexanone ug/L ND 25.0 04/25/12 14:02 4-Chlorotoluene ug/L ND 5.0 04/25/12 14:02 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/25/12 14:02 Acetone ug/L ND 100 04/25/12 14:02 Acrolein ug/L ND 100 04/25/12 14:02 Acrylonitrile ug/L ND 100 04/25/12 14:02 Benzene ug/L ND 5.0 04/25/12 14:02 Bromobenzene ug/L ND 5.0 04/25/12 14:02 Bromochloromethane ug/L ND 5.0 04/25/12 14:02 Bromodichloromethane ug/L ND 5.0 04/25/12 14:02 Bromoform ug/L ND 5.0 04/25/12 14:02 Bromomethane ug/L ND 5.0 04/25/12 14:02 Carbon disulfide ug/L ND 10.0 04/25/12 14:02 Carbon tetrachloride ug/L ND 5.0 04/25/12 14:02 Chlorobenzene ug/L ND 5.0 04/25/12 14:02 Chloroethane ug/L ND 5.0 04/25/12 14:02 Chloroform ug/L ND 5.0 04/25/12 14:02 Chloromethane ug/L ND 5.0 04/25/12 14:02 cis-1,2-Dichloroethene ug/L ND 5.0 04/25/12 14:02 cis-1,3-Dichloropropene ug/L ND 5.0 04/25/12 14:02 Dibromochloromethane ug/L ND 5.0 04/25/12 14:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 86 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725803 Associated Lab Samples:5061952001, 5061952002, 5061952003, 5061952004, 5061952005 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 04/25/12 14:02 Dichlorodifluoromethane ug/L ND 5.0 04/25/12 14:02 Ethyl methacrylate ug/L ND 100 04/25/12 14:02 Ethylbenzene ug/L ND 5.0 04/25/12 14:02 Hexachloro-1,3-butadiene ug/L ND 5.0 04/25/12 14:02 Iodomethane ug/L ND 10.0 04/25/12 14:02 Isopropylbenzene (Cumene)ug/L ND 5.0 04/25/12 14:02 Methyl-tert-butyl ether ug/L ND 4.0 04/25/12 14:02 Methylene Chloride ug/L ND 5.0 04/25/12 14:02 n-Butylbenzene ug/L ND 5.0 04/25/12 14:02 n-Hexane ug/L ND 5.0 N204/25/12 14:02 n-Propylbenzene ug/L ND 5.0 04/25/12 14:02 Naphthalene ug/L ND 5.0 04/25/12 14:02 p-Isopropyltoluene ug/L ND 5.0 04/25/12 14:02 sec-Butylbenzene ug/L ND 5.0 04/25/12 14:02 Styrene ug/L ND 5.0 04/25/12 14:02 tert-Butylbenzene ug/L ND 5.0 04/25/12 14:02 Tetrachloroethene ug/L ND 5.0 04/25/12 14:02 Toluene ug/L ND 5.0 04/25/12 14:02 trans-1,2-Dichloroethene ug/L ND 5.0 04/25/12 14:02 trans-1,3-Dichloropropene ug/L ND 5.0 04/25/12 14:02 trans-1,4-Dichloro-2-butene ug/L ND 100 04/25/12 14:02 Trichloroethene ug/L ND 5.0 04/25/12 14:02 Trichlorofluoromethane ug/L ND 5.0 04/25/12 14:02 Vinyl acetate ug/L ND 50.0 04/25/12 14:02 Vinyl chloride ug/L ND 2.0 04/25/12 14:02 Xylene (Total)ug/L ND 10.0 04/25/12 14:02 4-Bromofluorobenzene (S)%.100 72-125 04/25/12 14:02 Dibromofluoromethane (S)%.101 83-123 04/25/12 14:02 Toluene-d8 (S)%.99 81-114 04/25/12 14:02 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725804LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 50.050 100 69-122 1,1,1-Trichloroethane ug/L 55.650 111 69-126 1,1,2,2-Tetrachloroethane ug/L 49.150 98 68-134 1,1,2-Trichloroethane ug/L 50.650 101 77-129 1,1-Dichloroethane ug/L 48.350 97 70-127 1,1-Dichloroethene ug/L 51.250 102 75-145 1,1-Dichloropropene ug/L 49.050 98 75-126 1,2,3-Trichlorobenzene ug/L 50.250 100 63-130 1,2,3-Trichloropropane ug/L 86.1 L35017245-121 1,2,4-Trichlorobenzene ug/L 50.250 100 64-122 1,2,4-Trimethylbenzene ug/L 48.350 97 68-129 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 87 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725804LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 50.250 100 77-123 1,2-Dichlorobenzene ug/L 48.750 97 74-123 1,2-Dichloroethane ug/L 52.550 105 71-127 1,2-Dichloropropane ug/L 50.050 100 75-126 1,3,5-Trimethylbenzene ug/L 47.650 95 69-129 1,3-Dichlorobenzene ug/L 48.450 97 76-123 1,3-Dichloropropane ug/L 44.750 89 77-126 1,4-Dichlorobenzene ug/L 48.250 96 77-121 2,2-Dichloropropane ug/L 47.950 96 45-138 2-Butanone (MEK)ug/L 241250 96 42-177 2-Chlorotoluene ug/L 46.450 93 74-129 2-Hexanone ug/L 237250 95 57-162 4-Chlorotoluene ug/L 47.750 95 70-125 4-Methyl-2-pentanone (MIBK)ug/L 236250 94 64-135 Acetone ug/L 267250 107 10-200 Acrolein ug/L 61J L01000610-200 Acrylonitrile ug/L 8981000 90 59-144 Benzene ug/L 44.650 89 76-123 Bromobenzene ug/L 47.450 95 67-130 Bromochloromethane ug/L 51.250 102 58-153 Bromodichloromethane ug/L 47.050 94 71-124 Bromoform ug/L 46.750 93 64-116 Bromomethane ug/L 47.450 95 23-197 Carbon disulfide ug/L 109100 109 55-146 Carbon tetrachloride ug/L 49.150 98 65-125 Chlorobenzene ug/L 47.350 95 78-120 Chloroethane ug/L 49.550 99 56-163 Chloroform ug/L 51.050 102 73-122 Chloromethane ug/L 36.350 73 46-146 cis-1,2-Dichloroethene ug/L 47.450 95 79-129 cis-1,3-Dichloropropene ug/L 44.550 89 66-123 Dibromochloromethane ug/L 46.650 93 70-123 Dibromomethane ug/L 48.350 97 73-123 Dichlorodifluoromethane ug/L 42.450 85 19-200 Ethyl methacrylate ug/L 177200 88 70-127 Ethylbenzene ug/L 48.150 96 75-120 Hexachloro-1,3-butadiene ug/L 50.050 100 64-131 Iodomethane ug/L 103100 103 16-181 Isopropylbenzene (Cumene)ug/L 49.250 98 73-123 Methyl-tert-butyl ether ug/L 95.7100 96 66-128 Methylene Chloride ug/L 45.250 90 61-138 n-Butylbenzene ug/L 49.350 99 69-130 n-Hexane ug/L 38.9 N2507867-142 n-Propylbenzene ug/L 47.550 95 71-132 Naphthalene ug/L 48.050 96 62-130 p-Isopropyltoluene ug/L 49.350 99 71-126 sec-Butylbenzene ug/L 48.350 97 69-130 Styrene ug/L 47.950 96 75-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 88 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725804LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 46.150 92 49-114 Tetrachloroethene ug/L 37.450 75 57-125 Toluene ug/L 46.250 92 72-124 trans-1,2-Dichloroethene ug/L 46.150 92 71-145 trans-1,3-Dichloropropene ug/L 44.950 90 58-118 trans-1,4-Dichloro-2-butene ug/L 171200 86 50-121 Trichloroethene ug/L 50.450 101 77-122 Trichlorofluoromethane ug/L 53.750 107 56-159 Vinyl acetate ug/L 221200 111 27-119 Vinyl chloride ug/L 46.750 93 61-146 Xylene (Total)ug/L 146150 97 72-126 4-Bromofluorobenzene (S)%.103 72-125 Dibromofluoromethane (S)%.109 83-123 Toluene-d8 (S)%.100 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 725805MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061663003 725806 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 84 30-12287 3 2050ND42.2 43.4 1,1,1-Trichloroethane ug/L 50 89 37-13691 2 2050ND44.5 45.6 1,1,2,2-Tetrachloroethane ug/L 50 89 47-13290 1 2050ND44.6 45.2 1,1,2-Trichloroethane ug/L 50 91 53-13197 6 2050ND45.7 48.7 1,1-Dichloroethane ug/L 50 82 47-13883 1 2050ND41.0 41.4 1,1-Dichloroethene ug/L 50 80 54-15280 .06 2050ND40.1 40.1 1,1-Dichloropropene ug/L 50 78 47-13680 2 2050ND39.2 40.1 1,2,3-Trichlorobenzene ug/L 50 76 15-13279 5 2050ND37.8 39.7 1,2,3-Trichloropropane ug/L M05014124-108143 2 2050ND70.3 71.5 1,2,4-Trichlorobenzene ug/L 50 70 10-13076 9 2050ND34.9 38.0 1,2,4-Trimethylbenzene ug/L 50 82 10-141109 29 2050ND41.7 55.5 1,2-Dibromoethane (EDB)ug/L 50 92 49-13095 4 2050ND46.0 47.7 1,2-Dichlorobenzene ug/L 50 80 20-13782 2 2050ND39.9 40.8 1,2-Dichloroethane ug/L 50 95 42-13998 2 2050ND47.7 48.8 1,2-Dichloropropane ug/L 50 87 50-13188 2 2050ND43.5 44.2 1,3,5-Trimethylbenzene ug/L 50 75 10-14586 13 2050ND37.5 42.8 1,3-Dichlorobenzene ug/L 50 75 13-14379 6 2050ND37.4 39.7 1,3-Dichloropropane ug/L 50 83 53-13085 3 2050ND41.4 42.6 1,4-Dichlorobenzene ug/L 50 74 13-14078 5 2050ND37.2 39.1 2,2-Dichloropropane ug/L 50 72 13-14272 .3 2050ND36.1 36.2 2-Butanone (MEK)ug/L 250 92 43-14296 4 20250ND231239 2-Chlorotoluene ug/L 50 75 15-14581 8 2050ND37.4 40.5 2-Hexanone ug/L 250 90 46-13993 3 20250ND226233 4-Chlorotoluene ug/L 50 73 12-14378 7 2050ND36.5 39.1 4-Methyl-2-pentanone (MIBK)ug/L 250 89 43-14092 4 20250ND222230 Acetone ug/L 250 104 38-155108 4 20250ND260271 Acrolein ug/L M01000511-2006 4 201000ND54.8J 57.2J Acrylonitrile ug/L 1000 87 42-15089 3 201000ND865891 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 89 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 725805MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061663003 725806 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/L 50 78 52-13484 8 2050ND38.9 42.2 Bromobenzene ug/L 50 79 25-14081 3 2050ND39.7 40.7 Bromochloromethane ug/L 50 92 54-14496 4 2050ND46.2 48.2 Bromodichloromethane ug/L 50 80 42-12882 3 2050ND40.1 41.2 Bromoform ug/L 50 79 34-11682 4 2050ND39.6 41.2 Bromomethane ug/L 50 76 10-20093 19 2050ND38.1 46.3 Carbon disulfide ug/L 100 84 43-14483 1 20100ND84.0 83.2 Carbon tetrachloride ug/L 50 77 26-13678 1 2050ND38.4 38.8 Chlorobenzene ug/L 50 79 33-13682 4 2050ND39.5 41.1 Chloroethane ug/L 50 82 21-20079 3 2050ND40.9 39.7 Chloroform ug/L 50 90 50-13493 3 2050ND45.2 46.6 Chloromethane ug/L 50 58 32-16060 4 2050ND29.0 30.0 cis-1,2-Dichloroethene ug/L 50 81 48-14581 .06 2050ND40.5 40.6 cis-1,3-Dichloropropene ug/L 50 74 35-11677 3 2050ND37.1 38.3 Dibromochloromethane ug/L 50 80 39-12283 4 2050ND39.8 41.3 Dibromomethane ug/L 50 88 49-13488 .09 2050ND44.2 44.2 Dichlorodifluoromethane ug/L 50 71 35-20070 2 2050ND35.6 35.0 Ethyl methacrylate ug/L 200 83 54-12385 2 20200ND166169 Ethylbenzene ug/L M0,R1509529-132152 46 2050ND49.1 78.0 Hexachloro-1,3-butadiene ug/L 50 65 10-14665 .04 2050ND32.4 32.4 Iodomethane ug/L 100 78 10-17185 9 20100ND77.6 84.8 Isopropylbenzene (Cumene)ug/L 50 78 11-14682 5 2050ND39.0 41.2 Methyl-tert-butyl ether ug/L 100 92 39-13793 2 20100ND91.6 93.5 Methylene Chloride ug/L 50 80 47-14183 4 2050ND40.1 41.7 n-Butylbenzene ug/L 50 64 10-15670 8 2050ND32.2 35.0 n-Hexane ug/L N2506351-13767 5 2050ND31.6 33.3 n-Propylbenzene ug/L 50 73 10-14881 11 2050ND36.4 40.5 Naphthalene ug/L 50 86 40-12498 13 2050ND43.0 48.9 p-Isopropyltoluene ug/L 50 71 10-15075 5 2050ND35.4 37.4 sec-Butylbenzene ug/L 50 72 10-15074 4 2050ND35.8 37.2 Styrene ug/L 50 80 20-14383 4 2050ND40.0 41.6 tert-Butylbenzene ug/L 50 73 10-12375 2 2050ND36.5 37.4 Tetrachloroethene ug/L 50 58 30-12461 5 2050ND29.1 30.7 Toluene ug/L 50 82 42-13099 19 2050ND41.1 49.8 trans-1,2-Dichloroethene ug/L 50 74 48-14475 2 2050ND37.1 37.7 trans-1,3-Dichloropropene ug/L 50 76 24-11478 3 2050ND38.0 38.9 trans-1,4-Dichloro-2-butene ug/L 200 70 22-12073 4 20200ND140146 Trichloroethene ug/L 50 82 44-13085 4 2050ND40.8 42.5 Trichlorofluoromethane ug/L 50 86 17-20086 .4 2050ND43.1 42.9 Vinyl acetate ug/L 200 95 10-11597 2 20200ND190194 Vinyl chloride ug/L 50 73 45-15972 2 2050ND36.6 36.0 Xylene (Total)ug/L ES,RS1509429-131141 40 20150ND141212 4-Bromofluorobenzene (S)%.102 72-125103 20 Dibromofluoromethane (S)%.109 83-123110 20 Toluene-d8 (S)%.100 81-114100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 90 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 725811MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 725812 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 95 30-122101 7 2050ND47.5 50.7 1,1,1-Trichloroethane ug/L 50 111 37-136116 5 2050ND55.3 58.0 1,1,2,2-Tetrachloroethane ug/L 50 95 47-132101 6 2050ND47.5 50.4 1,1,2-Trichloroethane ug/L 50 101 53-131106 5 2050ND50.5 53.2 1,1-Dichloroethane ug/L 50 96 47-138101 5 2050ND48.1 50.5 1,1-Dichloroethene ug/L 50 103 54-152103 .2 2050ND51.3 51.4 1,1-Dichloropropene ug/L 50 100 47-136103 3 2050ND49.8 51.3 1,2,3-Trichlorobenzene ug/L 50 96 15-132102 6 2050ND47.8 50.8 1,2,3-Trichloropropane ug/L M05015924-108174 9 2050ND79.6 86.9 1,2,4-Trichlorobenzene ug/L 50 97 10-130101 4 2050ND48.7 50.7 1,2,4-Trimethylbenzene ug/L 50 96 10-141102 6 2050ND47.9 50.9 1,2-Dibromoethane (EDB)ug/L 50 99 49-130104 5 2050ND49.6 52.1 1,2-Dichlorobenzene ug/L 50 95 20-137101 6 2050ND47.7 50.5 1,2-Dichloroethane ug/L 50 104 42-139109 5 2050ND52.1 54.7 1,2-Dichloropropane ug/L 50 101 50-131103 3 2050ND50.3 51.6 1,3,5-Trimethylbenzene ug/L 50 94 10-14599 5 2050ND47.2 49.7 1,3-Dichlorobenzene ug/L 50 96 13-143101 5 2050ND48.1 50.5 1,3-Dichloropropane ug/L 50 91 53-13095 4 2050ND45.5 47.5 1,4-Dichlorobenzene ug/L 50 95 13-140100 5 2050ND47.6 49.8 2,2-Dichloropropane ug/L 50 93 13-14299 7 2050ND46.4 49.5 2-Butanone (MEK)ug/L 250 95 43-14299 4 20250ND237247 2-Chlorotoluene ug/L 50 93 15-14597 4 2050ND46.3 48.3 2-Hexanone ug/L 250 93 46-13998 5 20250ND232245 4-Chlorotoluene ug/L 50 95 12-143101 6 2050ND47.5 50.3 4-Methyl-2-pentanone (MIBK)ug/L 250 91 43-14098 7 20250ND228244 Acetone ug/L 250 102 38-155107 5 20250ND255268 Acrolein ug/L M01000611-2006 2 201000ND59.6J 61J Acrylonitrile ug/L 1000 89 42-15092 3 201000ND894924 Benzene ug/L 50 90 52-13493 3 2050ND45.0 46.3 Bromobenzene ug/L 50 93 25-14099 6 2050ND46.5 49.6 Bromochloromethane ug/L 50 105 54-144108 3 2050ND52.3 53.9 Bromodichloromethane ug/L 50 90 42-12895 5 2050ND45.2 47.6 Bromoform ug/L 50 84 34-11691 8 2050ND42.1 45.4 Bromomethane ug/L 50 106 10-200112 5 2050ND53.1 56.0 Carbon disulfide ug/L 100 109 43-144112 3 20100ND109112 Carbon tetrachloride ug/L 50 92 26-136100 8 2050ND46.1 50.0 Chlorobenzene ug/L 50 94 33-13699 5 2050ND47.1 49.6 Chloroethane ug/L 50 101 21-200102 1 2050ND50.4 50.9 Chloroform ug/L 50 102 50-134106 4 2050ND51.0 53.0 Chloromethane ug/L 50 80 32-16083 4 2050ND40.2 41.7 cis-1,2-Dichloroethene ug/L 50 95 48-14598 3 2050ND47.6 48.9 cis-1,3-Dichloropropene ug/L 50 86 35-11693 7 2050ND43.1 46.3 Dibromochloromethane ug/L 50 87 39-12294 7 2050ND43.6 46.8 Dibromomethane ug/L 50 95 49-134101 5 2050ND47.7 50.4 Dichlorodifluoromethane ug/L 50 85 35-20088 3 2050ND42.4 43.9 Ethyl methacrylate ug/L 200 87 54-12392 6 20200ND173183 Ethylbenzene ug/L 50 98 29-132102 5 2050ND48.8 51.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 91 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 725811MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952004 725812 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Hexachloro-1,3-butadiene ug/L 50 99 10-146105 6 2050ND49.7 52.6 Iodomethane ug/L 100 98 10-171105 7 20100ND97.7 105 Isopropylbenzene (Cumene)ug/L 50 98 11-146103 5 2050ND49.0 51.3 Methyl-tert-butyl ether ug/L 100 95 39-137100 4 20100ND95.5 99.8 Methylene Chloride ug/L 50 92 47-14197 5 2050ND45.8 48.4 n-Butylbenzene ug/L 50 97 10-156102 5 2050ND48.4 51.0 n-Hexane ug/L N2507851-13782 4 2050ND39.1 40.8 n-Propylbenzene ug/L 50 94 10-148100 6 2050ND46.9 49.8 Naphthalene ug/L 50 93 40-12499 6 2050ND46.3 49.4 p-Isopropyltoluene ug/L 50 98 10-150104 5 2050ND49.2 51.8 sec-Butylbenzene ug/L 50 96 10-150101 5 2050ND48.1 50.5 Styrene ug/L 50 94 20-143100 6 2050ND47.2 50.0 tert-Butylbenzene ug/L 50 93 10-12398 6 2050ND46.3 49.2 Tetrachloroethene ug/L 50 73 30-12480 5 205023.4 60.1 63.2 Toluene ug/L 50 94 42-13099 5 2050ND46.9 49.4 trans-1,2-Dichloroethene ug/L 50 92 48-14496 3 2050ND46.2 47.9 trans-1,3-Dichloropropene ug/L 50 86 24-11493 8 2050ND42.9 46.6 trans-1,4-Dichloro-2-butene ug/L 200 83 22-12089 7 20200ND166178 Trichloroethene ug/L 50 102 44-130105 3 2050ND51.0 52.6 Trichlorofluoromethane ug/L 50 109 17-200109 .2 2050ND54.4 54.5 Vinyl acetate ug/L 200 103 10-115109 6 20200ND206219 Vinyl chloride ug/L 50 95 45-15998 3 2050ND47.5 49.1 Xylene (Total)ug/L 150 97 29-131103 5 20150ND146154 4-Bromofluorobenzene (S)%.102 72-125102 20 Dibromofluoromethane (S)%.109 83-123109 20 Toluene-d8 (S)%.98 81-114100 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 92 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41633 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061952006, 5061952007, 5061952008, 5061952009, 5061952010, 5061952011, 5061952013, 5061952014, 5061952015, 5061952016, 5061952017, 5061952018, 5061952019, 5061952020, 5061952024 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725970 Associated Lab Samples:5061952006, 5061952007, 5061952008, 5061952009, 5061952010, 5061952011, 5061952013, 5061952014, 5061952015, 5061952016, 5061952017, 5061952018, 5061952019, 5061952020, 5061952024 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/26/12 01:28 1,1,1-Trichloroethane ug/L ND 5.0 04/26/12 01:28 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/26/12 01:28 1,1,2-Trichloroethane ug/L ND 5.0 04/26/12 01:28 1,1-Dichloroethane ug/L ND 5.0 04/26/12 01:28 1,1-Dichloroethene ug/L ND 5.0 04/26/12 01:28 1,1-Dichloropropene ug/L ND 5.0 04/26/12 01:28 1,2,3-Trichlorobenzene ug/L ND 5.0 04/26/12 01:28 1,2,3-Trichloropropane ug/L ND 5.0 04/26/12 01:28 1,2,4-Trichlorobenzene ug/L ND 5.0 04/26/12 01:28 1,2,4-Trimethylbenzene ug/L ND 5.0 04/26/12 01:28 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/26/12 01:28 1,2-Dichlorobenzene ug/L ND 5.0 04/26/12 01:28 1,2-Dichloroethane ug/L ND 5.0 04/26/12 01:28 1,2-Dichloropropane ug/L ND 5.0 04/26/12 01:28 1,3,5-Trimethylbenzene ug/L ND 5.0 04/26/12 01:28 1,3-Dichlorobenzene ug/L ND 5.0 04/26/12 01:28 1,3-Dichloropropane ug/L ND 5.0 04/26/12 01:28 1,4-Dichlorobenzene ug/L ND 5.0 04/26/12 01:28 2,2-Dichloropropane ug/L ND 5.0 04/26/12 01:28 2-Butanone (MEK)ug/L ND 25.0 04/26/12 01:28 2-Chlorotoluene ug/L ND 5.0 04/26/12 01:28 2-Hexanone ug/L ND 25.0 04/26/12 01:28 4-Chlorotoluene ug/L ND 5.0 04/26/12 01:28 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/26/12 01:28 Acetone ug/L ND 100 04/26/12 01:28 Acrolein ug/L ND 100 04/26/12 01:28 Acrylonitrile ug/L ND 100 04/26/12 01:28 Benzene ug/L ND 5.0 04/26/12 01:28 Bromobenzene ug/L ND 5.0 04/26/12 01:28 Bromochloromethane ug/L ND 5.0 04/26/12 01:28 Bromodichloromethane ug/L ND 5.0 04/26/12 01:28 Bromoform ug/L ND 5.0 04/26/12 01:28 Bromomethane ug/L ND 5.0 04/26/12 01:28 Carbon disulfide ug/L ND 10.0 04/26/12 01:28 Carbon tetrachloride ug/L ND 5.0 04/26/12 01:28 Chlorobenzene ug/L ND 5.0 04/26/12 01:28 Chloroethane ug/L ND 5.0 04/26/12 01:28 Chloroform ug/L ND 5.0 04/26/12 01:28 Chloromethane ug/L ND 5.0 04/26/12 01:28 cis-1,2-Dichloroethene ug/L ND 5.0 04/26/12 01:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 93 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725970 Associated Lab Samples:5061952006, 5061952007, 5061952008, 5061952009, 5061952010, 5061952011, 5061952013, 5061952014, 5061952015, 5061952016, 5061952017, 5061952018, 5061952019, 5061952020, 5061952024 Matrix:Water Analyzed cis-1,3-Dichloropropene ug/L ND 5.0 04/26/12 01:28 Dibromochloromethane ug/L ND 5.0 04/26/12 01:28 Dibromomethane ug/L ND 5.0 04/26/12 01:28 Dichlorodifluoromethane ug/L ND 5.0 04/26/12 01:28 Ethyl methacrylate ug/L ND 100 04/26/12 01:28 Ethylbenzene ug/L ND 5.0 04/26/12 01:28 Hexachloro-1,3-butadiene ug/L ND 5.0 04/26/12 01:28 Iodomethane ug/L ND 10.0 04/26/12 01:28 Isopropylbenzene (Cumene)ug/L ND 5.0 04/26/12 01:28 Methyl-tert-butyl ether ug/L ND 4.0 04/26/12 01:28 Methylene Chloride ug/L ND 5.0 04/26/12 01:28 n-Butylbenzene ug/L ND 5.0 04/26/12 01:28 n-Hexane ug/L ND 5.0 N204/26/12 01:28 n-Propylbenzene ug/L ND 5.0 04/26/12 01:28 Naphthalene ug/L ND 5.0 04/26/12 01:28 p-Isopropyltoluene ug/L ND 5.0 04/26/12 01:28 sec-Butylbenzene ug/L ND 5.0 04/26/12 01:28 Styrene ug/L ND 5.0 04/26/12 01:28 tert-Butylbenzene ug/L ND 5.0 04/26/12 01:28 Tetrachloroethene ug/L ND 5.0 04/26/12 01:28 Toluene ug/L ND 5.0 04/26/12 01:28 trans-1,2-Dichloroethene ug/L ND 5.0 04/26/12 01:28 trans-1,3-Dichloropropene ug/L ND 5.0 04/26/12 01:28 trans-1,4-Dichloro-2-butene ug/L ND 100 04/26/12 01:28 Trichloroethene ug/L ND 5.0 04/26/12 01:28 Trichlorofluoromethane ug/L ND 5.0 04/26/12 01:28 Vinyl acetate ug/L ND 50.0 04/26/12 01:28 Vinyl chloride ug/L ND 2.0 04/26/12 01:28 Xylene (Total)ug/L ND 10.0 04/26/12 01:28 4-Bromofluorobenzene (S)%.100 72-125 04/26/12 01:28 Dibromofluoromethane (S)%.101 83-123 04/26/12 01:28 Toluene-d8 (S)%.100 81-114 04/26/12 01:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725971LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 49.550 99 69-122 1,1,1-Trichloroethane ug/L 56.550 113 69-126 1,1,2,2-Tetrachloroethane ug/L 48.750 97 68-134 1,1,2-Trichloroethane ug/L 50.850 102 77-129 1,1-Dichloroethane ug/L 48.850 98 70-127 1,1-Dichloroethene ug/L 51.650 103 75-145 1,1-Dichloropropene ug/L 50.050 100 75-126 1,2,3-Trichlorobenzene ug/L 48.350 97 63-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 94 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725971LABORATORY CONTROL SAMPLE: LCSSpike 1,2,3-Trichloropropane ug/L 84.0 L35016845-121 1,2,4-Trichlorobenzene ug/L 47.050 94 64-122 1,2,4-Trimethylbenzene ug/L 47.750 95 68-129 1,2-Dibromoethane (EDB)ug/L 50.650 101 77-123 1,2-Dichlorobenzene ug/L 48.050 96 74-123 1,2-Dichloroethane ug/L 51.850 104 71-127 1,2-Dichloropropane ug/L 50.650 101 75-126 1,3,5-Trimethylbenzene ug/L 47.150 94 69-129 1,3-Dichlorobenzene ug/L 47.450 95 76-123 1,3-Dichloropropane ug/L 45.650 91 77-126 1,4-Dichlorobenzene ug/L 46.850 94 77-121 2,2-Dichloropropane ug/L 47.750 95 45-138 2-Butanone (MEK)ug/L 239250 96 42-177 2-Chlorotoluene ug/L 46.050 92 74-129 2-Hexanone ug/L 236250 94 57-162 4-Chlorotoluene ug/L 46.850 94 70-125 4-Methyl-2-pentanone (MIBK)ug/L 231250 92 64-135 Acetone ug/L 265250 106 10-200 Acrolein ug/L 60J L01000610-200 Acrylonitrile ug/L 9001000 90 59-144 Benzene ug/L 44.950 90 76-123 Bromobenzene ug/L 46.650 93 67-130 Bromochloromethane ug/L 51.850 104 58-153 Bromodichloromethane ug/L 46.750 93 71-124 Bromoform ug/L 44.550 89 64-116 Bromomethane ug/L 57.150 114 23-197 Carbon disulfide ug/L 110100 110 55-146 Carbon tetrachloride ug/L 49.050 98 65-125 Chlorobenzene ug/L 47.250 94 78-120 Chloroethane ug/L 50.050 100 56-163 Chloroform ug/L 51.650 103 73-122 Chloromethane ug/L 37.550 75 46-146 cis-1,2-Dichloroethene ug/L 47.750 95 79-129 cis-1,3-Dichloropropene ug/L 44.650 89 66-123 Dibromochloromethane ug/L 45.550 91 70-123 Dibromomethane ug/L 48.250 96 73-123 Dichlorodifluoromethane ug/L 44.650 89 19-200 Ethyl methacrylate ug/L 176200 88 70-127 Ethylbenzene ug/L 48.750 97 75-120 Hexachloro-1,3-butadiene ug/L 49.150 98 64-131 Iodomethane ug/L 108100 108 16-181 Isopropylbenzene (Cumene)ug/L 49.650 99 73-123 Methyl-tert-butyl ether ug/L 96.7100 97 66-128 Methylene Chloride ug/L 45.950 92 61-138 n-Butylbenzene ug/L 47.450 95 69-130 n-Hexane ug/L 39.4 N2507967-142 n-Propylbenzene ug/L 47.050 94 71-132 Naphthalene ug/L 47.150 94 62-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 95 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725971LABORATORY CONTROL SAMPLE: LCSSpike p-Isopropyltoluene ug/L 49.050 98 71-126 sec-Butylbenzene ug/L 48.150 96 69-130 Styrene ug/L 47.950 96 75-125 tert-Butylbenzene ug/L 46.950 94 49-114 Tetrachloroethene ug/L 37.250 74 57-125 Toluene ug/L 46.750 93 72-124 trans-1,2-Dichloroethene ug/L 46.050 92 71-145 trans-1,3-Dichloropropene ug/L 44.950 90 58-118 trans-1,4-Dichloro-2-butene ug/L 167200 84 50-121 Trichloroethene ug/L 50.950 102 77-122 Trichlorofluoromethane ug/L 54.650 109 56-159 Vinyl acetate ug/L 222200 111 27-119 Vinyl chloride ug/L 47.950 96 61-146 Xylene (Total)ug/L 147150 98 72-126 4-Bromofluorobenzene (S)%.102 72-125 Dibromofluoromethane (S)%.110 83-123 Toluene-d8 (S)%.99 81-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 725972MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952024 725973 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 50 94 30-12265 36 2050ND46.8 32.5 1,1,1-Trichloroethane ug/L 50 110 37-13653 70 2050ND55.2 26.7 1,1,2,2-Tetrachloroethane ug/L 50 114 47-132110 4 2050ND57.0 54.8 1,1,2-Trichloroethane ug/L 50 105 53-13189 17 2050ND52.6 44.5 1,1-Dichloroethane ug/L 50 97 47-13861 45 2050ND48.4 30.5 1,1-Dichloroethene ug/L 50 99 54-15244 76 2050ND49.3 22.1 1,1-Dichloropropene ug/L 50 98 47-13646 72 2050ND48.9 23.0 1,2,3-Trichlorobenzene ug/L 50 92 15-13256 49 2050ND45.8 27.8 1,2,3-Trichloropropane ug/L M05015224-108122 22 2050ND76.1 61.1 1,2,4-Trichlorobenzene ug/L 50 88 10-13051 53 2050ND44.1 25.7 1,2,4-Trimethylbenzene ug/L 50 91 10-14151 56 2050ND45.3 25.5 1,2-Dibromoethane (EDB)ug/L 50 104 49-13088 16 2050ND51.9 44.1 1,2-Dichlorobenzene ug/L 50 92 20-13763 38 2050ND46.0 31.4 1,2-Dichloroethane ug/L 50 106 42-13990 17 2050ND53.1 45.0 1,2-Dichloropropane ug/L 50 100 50-13172 32 2050ND49.8 36.0 1,3,5-Trimethylbenzene ug/L 50 89 10-14547 61 2050ND44.6 23.6 1,3-Dichlorobenzene ug/L 50 90 13-14356 46 2050ND45.0 28.1 1,3-Dichloropropane ug/L 50 90 53-13077 16 2050ND45.0 38.3 1,4-Dichlorobenzene ug/L 50 89 13-14056 46 2050ND44.6 28.0 2,2-Dichloropropane ug/L 50 90 13-14245 67 2050ND45.0 22.5 2-Butanone (MEK)ug/L 250 100 43-142104 4 20250ND251260 2-Chlorotoluene ug/L 50 88 15-14550 54 2050ND44.0 25.2 2-Hexanone ug/L 250 99 46-13997 2 20250ND248243 4-Chlorotoluene ug/L 50 90 12-14351 55 2050ND44.8 25.6 4-Methyl-2-pentanone (MIBK)ug/L 250 98 43-14095 3 20250ND246238 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 96 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 725972MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952024 725973 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Acetone ug/L 250 106 38-155114 7 20250ND266284 Acrolein ug/L M01000511-2006 2 201000ND55J55.9J Acrylonitrile ug/L 1000 92 42-15094 3 201000ND917945 Benzene ug/L 50 90 52-13456 47 2050ND44.8 27.8 Bromobenzene ug/L 50 91 25-14067 31 2050ND45.7 33.5 Bromochloromethane ug/L 50 104 54-14488 17 2050ND52.2 44.0 Bromodichloromethane ug/L 50 89 42-12865 32 2050ND44.7 32.5 Bromoform ug/L 50 83 34-11669 18 2050ND41.5 34.7 Bromomethane ug/L 50 83 10-20049 51 2050ND41.4 24.5 Carbon disulfide ug/L 100 105 43-14450 71 20100ND10550.1 Carbon tetrachloride ug/L 50 91 26-13641 76 2050ND45.6 20.5 Chlorobenzene ug/L 50 91 33-13660 41 2050ND45.7 30.1 Chloroethane ug/L 50 98 21-20054 58 2050ND49.1 27.1 Chloroform ug/L 50 103 50-13470 39 2050ND51.6 34.9 Chloromethane ug/L 50 74 32-16041 57 2050ND37.2 20.6 cis-1,2-Dichloroethene ug/L 50 93 48-14563 39 2050ND46.7 31.4 cis-1,3-Dichloropropene ug/L 50 84 35-11660 33 2050ND42.0 30.1 Dibromochloromethane ug/L 50 84 39-12267 23 2050ND41.8 33.3 Dibromomethane ug/L 50 97 49-13484 15 2050ND48.6 42.1 Dichlorodifluoromethane ug/L 50 86 35-20035 84 2050ND43.2 17.6 Ethyl methacrylate ug/L 200 90 54-12382 9 20200ND180165 Ethylbenzene ug/L 50 96 29-13253 58 2050ND47.9 26.3 Hexachloro-1,3-butadiene ug/L 50 93 10-14626 112 2050ND46.5 13.2 Iodomethane ug/L 100 84 10-17147 56 20100ND84.4 47.4 Isopropylbenzene (Cumene)ug/L 50 97 11-14648 68 2050ND48.7 24.1 Methyl-tert-butyl ether ug/L 100 101 39-13792 9 20100ND10192.4 Methylene Chloride ug/L 50 88 47-14166 29 2050ND44.2 33.0 n-Butylbenzene ug/L 50 89 10-15635 88 2050ND44.7 17.3 n-Hexane ug/L N2507951-13731 88 2050ND39.4 15.4 n-Propylbenzene ug/L 50 90 10-14843 72 2050ND45.1 21.3 Naphthalene ug/L 50 95 40-12472 27 2050ND47.4 36.1 p-Isopropyltoluene ug/L 50 94 10-15041 78 2050ND47.0 20.6 sec-Butylbenzene ug/L 50 93 10-15039 82 2050ND46.3 19.3 Styrene ug/L 50 92 20-14360 42 2050ND45.9 29.9 tert-Butylbenzene ug/L 50 91 10-12343 71 2050ND45.4 21.6 Tetrachloroethene ug/L 50 74 30-12433 69 2050ND40.0 19.5 Toluene ug/L 50 93 42-13054 53 2050ND46.4 27.1 trans-1,2-Dichloroethene ug/L 50 90 48-14450 57 2050ND44.8 24.9 trans-1,3-Dichloropropene ug/L 50 83 24-11463 28 2050ND41.7 31.3 trans-1,4-Dichloro-2-butene ug/L 200 79 22-12072 9 20200ND158144 Trichloroethene ug/L 50 102 44-13055 61 2050ND51.1 27.3 Trichlorofluoromethane ug/L 50 108 17-20047 79 2050ND53.8 23.5 Vinyl acetate ug/L 200 87 10-11576 14 20200ND175152 Vinyl chloride ug/L 50 93 45-15944 72 2050ND46.3 21.9 Xylene (Total)ug/L 150 96 29-13153 57 20150ND14480.2 4-Bromofluorobenzene (S)%.104 72-125103 20 Dibromofluoromethane (S)%.1d11083-123107 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 97 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units MS Result % Rec Limits Qual% RecConc. 725972MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952024 725973 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Toluene-d8 (S)%.99 81-11498 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 98 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/41680 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5061952021, 5061952022, 5061952023, 5061952025, 5061952026, 5061952027, 5061952028, 5061952029, 5061952030 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:726761 Associated Lab Samples:5061952021, 5061952022, 5061952023, 5061952025, 5061952026, 5061952027, 5061952028, 5061952029, 5061952030 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/26/12 13:06 1,1,1-Trichloroethane ug/L ND 5.0 04/26/12 13:06 1,1,2,2-Tetrachloroethane ug/L ND 5.0 04/26/12 13:06 1,1,2-Trichloroethane ug/L ND 5.0 04/26/12 13:06 1,1-Dichloroethane ug/L ND 5.0 04/26/12 13:06 1,1-Dichloroethene ug/L ND 5.0 04/26/12 13:06 1,1-Dichloropropene ug/L ND 5.0 04/26/12 13:06 1,2,3-Trichlorobenzene ug/L ND 5.0 04/26/12 13:06 1,2,3-Trichloropropane ug/L ND 5.0 04/26/12 13:06 1,2,4-Trichlorobenzene ug/L ND 5.0 04/26/12 13:06 1,2,4-Trimethylbenzene ug/L ND 5.0 04/26/12 13:06 1,2-Dibromoethane (EDB)ug/L ND 5.0 04/26/12 13:06 1,2-Dichlorobenzene ug/L ND 5.0 04/26/12 13:06 1,2-Dichloroethane ug/L ND 5.0 04/26/12 13:06 1,2-Dichloropropane ug/L ND 5.0 04/26/12 13:06 1,3,5-Trimethylbenzene ug/L ND 5.0 04/26/12 13:06 1,3-Dichlorobenzene ug/L ND 5.0 04/26/12 13:06 1,3-Dichloropropane ug/L ND 5.0 04/26/12 13:06 1,4-Dichlorobenzene ug/L ND 5.0 04/26/12 13:06 2,2-Dichloropropane ug/L ND 5.0 04/26/12 13:06 2-Butanone (MEK)ug/L ND 25.0 04/26/12 13:06 2-Chlorotoluene ug/L ND 5.0 04/26/12 13:06 2-Hexanone ug/L ND 25.0 04/26/12 13:06 4-Chlorotoluene ug/L ND 5.0 04/26/12 13:06 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 04/26/12 13:06 Acetone ug/L ND 100 04/26/12 13:06 Acrolein ug/L ND 100 04/26/12 13:06 Acrylonitrile ug/L ND 100 04/26/12 13:06 Benzene ug/L ND 5.0 04/26/12 13:06 Bromobenzene ug/L ND 5.0 04/26/12 13:06 Bromochloromethane ug/L ND 5.0 04/26/12 13:06 Bromodichloromethane ug/L ND 5.0 04/26/12 13:06 Bromoform ug/L ND 5.0 04/26/12 13:06 Bromomethane ug/L ND 5.0 04/26/12 13:06 Carbon disulfide ug/L ND 10.0 04/26/12 13:06 Carbon tetrachloride ug/L ND 5.0 04/26/12 13:06 Chlorobenzene ug/L ND 5.0 04/26/12 13:06 Chloroethane ug/L ND 5.0 04/26/12 13:06 Chloroform ug/L ND 5.0 04/26/12 13:06 Chloromethane ug/L ND 5.0 04/26/12 13:06 cis-1,2-Dichloroethene ug/L ND 5.0 04/26/12 13:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 99 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:726761 Associated Lab Samples:5061952021, 5061952022, 5061952023, 5061952025, 5061952026, 5061952027, 5061952028, 5061952029, 5061952030 Matrix:Water Analyzed cis-1,3-Dichloropropene ug/L ND 5.0 04/26/12 13:06 Dibromochloromethane ug/L ND 5.0 04/26/12 13:06 Dibromomethane ug/L ND 5.0 04/26/12 13:06 Dichlorodifluoromethane ug/L ND 5.0 04/26/12 13:06 Ethyl methacrylate ug/L ND 100 04/26/12 13:06 Ethylbenzene ug/L ND 5.0 04/26/12 13:06 Hexachloro-1,3-butadiene ug/L ND 5.0 04/26/12 13:06 Iodomethane ug/L ND 10.0 04/26/12 13:06 Isopropylbenzene (Cumene)ug/L ND 5.0 04/26/12 13:06 Methyl-tert-butyl ether ug/L ND 4.0 04/26/12 13:06 Methylene Chloride ug/L ND 5.0 04/26/12 13:06 n-Butylbenzene ug/L ND 5.0 04/26/12 13:06 n-Hexane ug/L ND 5.0 N204/26/12 13:06 n-Propylbenzene ug/L ND 5.0 04/26/12 13:06 Naphthalene ug/L ND 5.0 04/26/12 13:06 p-Isopropyltoluene ug/L ND 5.0 04/26/12 13:06 sec-Butylbenzene ug/L ND 5.0 04/26/12 13:06 Styrene ug/L ND 5.0 04/26/12 13:06 tert-Butylbenzene ug/L ND 5.0 04/26/12 13:06 Tetrachloroethene ug/L ND 5.0 04/26/12 13:06 Toluene ug/L ND 5.0 04/26/12 13:06 trans-1,2-Dichloroethene ug/L ND 5.0 04/26/12 13:06 trans-1,3-Dichloropropene ug/L ND 5.0 04/26/12 13:06 trans-1,4-Dichloro-2-butene ug/L ND 100 04/26/12 13:06 Trichloroethene ug/L ND 5.0 04/26/12 13:06 Trichlorofluoromethane ug/L ND 5.0 04/26/12 13:06 Vinyl acetate ug/L ND 50.0 04/26/12 13:06 Vinyl chloride ug/L ND 2.0 04/26/12 13:06 Xylene (Total)ug/L ND 10.0 04/26/12 13:06 4-Bromofluorobenzene (S)%.100 72-125 04/26/12 13:06 Dibromofluoromethane (S)%.105 83-123 04/26/12 13:06 Toluene-d8 (S)%.99 81-114 04/26/12 13:06 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 726762LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.550 97 69-122 1,1,1-Trichloroethane ug/L 55.750 111 69-126 1,1,2,2-Tetrachloroethane ug/L 49.950 100 68-134 1,1,2-Trichloroethane ug/L 51.550 103 77-129 1,1-Dichloroethane ug/L 48.450 97 70-127 1,1-Dichloroethene ug/L 48.950 98 75-145 1,1-Dichloropropene ug/L 49.250 98 75-126 1,2,3-Trichlorobenzene ug/L 51.350 103 63-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 100 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 726762LABORATORY CONTROL SAMPLE: LCSSpike 1,2,3-Trichloropropane ug/L 86.5 L35017345-121 1,2,4-Trichlorobenzene ug/L 51.150 102 64-122 1,2,4-Trimethylbenzene ug/L 49.450 99 68-129 1,2-Dibromoethane (EDB)ug/L 50.250 100 77-123 1,2-Dichlorobenzene ug/L 49.250 98 74-123 1,2-Dichloroethane ug/L 51.950 104 71-127 1,2-Dichloropropane ug/L 49.750 99 75-126 1,3,5-Trimethylbenzene ug/L 48.550 97 69-129 1,3-Dichlorobenzene ug/L 49.250 98 76-123 1,3-Dichloropropane ug/L 44.850 90 77-126 1,4-Dichlorobenzene ug/L 49.150 98 77-121 2,2-Dichloropropane ug/L 48.350 97 45-138 2-Butanone (MEK)ug/L 244250 98 42-177 2-Chlorotoluene ug/L 47.050 94 74-129 2-Hexanone ug/L 241250 96 57-162 4-Chlorotoluene ug/L 49.050 98 70-125 4-Methyl-2-pentanone (MIBK)ug/L 239250 95 64-135 Acetone ug/L 268250 107 10-200 Acrolein ug/L 59.1J L01000610-200 Acrylonitrile ug/L 8921000 89 59-144 Benzene ug/L 44.850 90 76-123 Bromobenzene ug/L 46.950 94 67-130 Bromochloromethane ug/L 51.150 102 58-153 Bromodichloromethane ug/L 45.550 91 71-124 Bromoform ug/L 44.950 90 64-116 Bromomethane ug/L 52.050 104 23-197 Carbon disulfide ug/L 105100 105 55-146 Carbon tetrachloride ug/L 47.750 95 65-125 Chlorobenzene ug/L 47.350 95 78-120 Chloroethane ug/L 49.050 98 56-163 Chloroform ug/L 50.950 102 73-122 Chloromethane ug/L 35.850 72 46-146 cis-1,2-Dichloroethene ug/L 46.550 93 79-129 cis-1,3-Dichloropropene ug/L 44.450 89 66-123 Dibromochloromethane ug/L 44.450 89 70-123 Dibromomethane ug/L 47.150 94 73-123 Dichlorodifluoromethane ug/L 40.050 80 19-200 Ethyl methacrylate ug/L 178200 89 70-127 Ethylbenzene ug/L 48.550 97 75-120 Hexachloro-1,3-butadiene ug/L 52.150 104 64-131 Iodomethane ug/L 97.6100 98 16-181 Isopropylbenzene (Cumene)ug/L 49.450 99 73-123 Methyl-tert-butyl ether ug/L 97.3100 97 66-128 Methylene Chloride ug/L 45.150 90 61-138 n-Butylbenzene ug/L 50.550 101 69-130 n-Hexane ug/L 39.2 N2507867-142 n-Propylbenzene ug/L 48.750 97 71-132 Naphthalene ug/L 49.650 99 62-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 101 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 726762LABORATORY CONTROL SAMPLE: LCSSpike p-Isopropyltoluene ug/L 51.250 102 71-126 sec-Butylbenzene ug/L 49.150 98 69-130 Styrene ug/L 47.650 95 75-125 tert-Butylbenzene ug/L 47.350 95 49-114 Tetrachloroethene ug/L 37.550 75 57-125 Toluene ug/L 46.650 93 72-124 trans-1,2-Dichloroethene ug/L 45.750 91 71-145 trans-1,3-Dichloropropene ug/L 45.250 90 58-118 trans-1,4-Dichloro-2-butene ug/L 170200 85 50-121 Trichloroethene ug/L 50.450 101 77-122 Trichlorofluoromethane ug/L 51.850 104 56-159 Vinyl acetate ug/L 221200 110 27-119 Vinyl chloride ug/L 46.450 93 61-146 Xylene (Total)ug/L 146150 97 72-126 4-Bromofluorobenzene (S)%.101 72-125 Dibromofluoromethane (S)%.108 83-123 Toluene-d8 (S)%.99 81-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 102 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/29440 EPA 3510 EPA 8270 by SIM 8270 Water PAH Associated Lab Samples:5061952011, 5061952012, 5061952013, 5061952014, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725706 Associated Lab Samples:5061952011, 5061952012, 5061952013, 5061952014, 5061952015 Matrix:Water Analyzed 2-Methylnaphthalene ug/L ND 1.0 04/28/12 05:40 Acenaphthene ug/L ND 1.0 04/28/12 05:40 Acenaphthylene ug/L ND 1.0 04/28/12 05:40 Anthracene ug/L ND 0.10 04/28/12 05:40 Benzo(a)anthracene ug/L ND 0.10 04/28/12 05:40 Benzo(a)pyrene ug/L ND 0.10 04/28/12 05:40 Benzo(b)fluoranthene ug/L ND 0.10 04/28/12 05:40 Benzo(g,h,i)perylene ug/L ND 0.10 04/28/12 05:40 Benzo(k)fluoranthene ug/L ND 0.10 04/28/12 05:40 Chrysene ug/L ND 0.50 04/28/12 05:40 Dibenz(a,h)anthracene ug/L ND 0.10 04/28/12 05:40 Fluoranthene ug/L ND 1.0 04/28/12 05:40 Fluorene ug/L ND 1.0 04/28/12 05:40 Indeno(1,2,3-cd)pyrene ug/L ND 0.10 04/28/12 05:40 Naphthalene ug/L ND 1.0 04/28/12 05:40 Phenanthrene ug/L ND 1.0 04/28/12 05:40 Pyrene ug/L ND 1.0 04/28/12 05:40 2-Fluorobiphenyl (S)%.84 26-106 04/28/12 05:40 p-Terphenyl-d14 (S)%.98 16-111 04/28/12 05:40 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725707LABORATORY CONTROL SAMPLE: LCSSpike 2-Methylnaphthalene ug/L 8.910 89 24-104 Acenaphthene ug/L 9.010 90 31-108 Acenaphthylene ug/L 8.810 88 33-111 Anthracene ug/L 9.610 96 45-120 Benzo(a)anthracene ug/L 9.610 96 51-119 Benzo(a)pyrene ug/L 9.810 98 52-124 Benzo(b)fluoranthene ug/L 10.410 104 51-122 Benzo(g,h,i)perylene ug/L 9.610 96 48-112 Benzo(k)fluoranthene ug/L 9.510 95 53-123 Chrysene ug/L 10.010 100 54-118 Dibenz(a,h)anthracene ug/L 9.910 99 49-114 Fluoranthene ug/L 9.710 97 52-122 Fluorene ug/L 9.010 90 38-113 Indeno(1,2,3-cd)pyrene ug/L 9.610 96 49-114 Naphthalene ug/L 8.610 86 27-103 Phenanthrene ug/L 9.810 98 43-112 Pyrene ug/L 9.610 96 51-120 2-Fluorobiphenyl (S)%.87 26-106 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 103 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725707LABORATORY CONTROL SAMPLE: LCSSpike p-Terphenyl-d14 (S)%.102 16-111 Parameter Units MS Result % Rec Limits Qual% RecConc. 725710MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952013 725711 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2-Methylnaphthalene ug/L 20.8 78 10-13084 7 2020.8ND 16.2 17.4 Acenaphthene ug/L 20.8 76 32-10280 5 2020.8ND 15.9 16.7 Acenaphthylene ug/L 20.8 79 25-11881 3 2020.8ND 16.4 16.9 Anthracene ug/L 20.8 83 46-11687 4 2020.8ND 17.4 18.1 Benzo(a)anthracene ug/L 20.8 83 31-10287 5 2020.8ND 17.3 18.2 Benzo(a)pyrene ug/L 20.8 79 10-9384 6 2020.8ND 16.5 17.5 Benzo(b)fluoranthene ug/L 20.8 83 11-9387 5 2020.8ND 17.3 18.2 Benzo(g,h,i)perylene ug/L M020.8 73 10-7778 7 2020.8ND 15.2 16.2 Benzo(k)fluoranthene ug/L 20.8 78 12-9185 9 2020.8ND 16.3 17.8 Chrysene ug/L 20.8 88 34-9991 4 2020.8ND 18.3 19.0 Dibenz(a,h)anthracene ug/L 20.8 73 10-7977 6 2020.8ND 15.2 16.1 Fluoranthene ug/L 20.8 87 48-11690 4 2020.8ND 18.0 18.8 Fluorene ug/L 20.8 80 41-10880 .8 2020.8ND 16.6 16.7 Indeno(1,2,3-cd)pyrene ug/L 20.8 74 10-7978 6 2020.8ND 15.3 16.2 Naphthalene ug/L 20.8 75 23-10779 6 2020.8ND 15.6 16.5 Phenanthrene ug/L 20.8 86 46-10788 2 2020.8ND 17.9 18.2 Pyrene ug/L 20.8 85 46-11589 4 2020.8ND 17.7 18.5 2-Fluorobiphenyl (S)%.78 26-10679 20 p-Terphenyl-d14 (S)%.89 16-11192 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 104 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/29439 EPA 3510 EPA 8270 8270 Water Scan Associated Lab Samples:5061952011, 5061952012, 5061952013, 5061952014, 5061952015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725702 Associated Lab Samples:5061952011, 5061952012, 5061952013, 5061952014, 5061952015 Matrix:Water Analyzed 2,4,5-Trichlorophenol ug/L ND 10.0 04/26/12 16:44 2,4,6-Trichlorophenol ug/L ND 10.0 04/26/12 16:44 2,4-Dichlorophenol ug/L ND 10.0 04/26/12 16:44 2,4-Dimethylphenol ug/L ND 10.0 04/26/12 16:44 2,4-Dinitrophenol ug/L ND 50.0 04/26/12 16:44 2,4-Dinitrotoluene ug/L ND 10.0 04/26/12 16:44 2,6-Dinitrotoluene ug/L ND 10.0 04/26/12 16:44 2-Chloronaphthalene ug/L ND 10.0 04/26/12 16:44 2-Chlorophenol ug/L ND 10.0 04/26/12 16:44 2-Methylphenol(o-Cresol)ug/L ND 10.0 04/26/12 16:44 2-Nitroaniline ug/L ND 50.0 04/26/12 16:44 2-Nitrophenol ug/L ND 10.0 04/26/12 16:44 3&4-Methylphenol(m&p Cresol)ug/L ND 20.0 04/26/12 16:44 3,3'-Dichlorobenzidine ug/L ND 20.0 04/26/12 16:44 3-Nitroaniline ug/L ND 50.0 04/26/12 16:44 4,6-Dinitro-2-methylphenol ug/L ND 50.0 04/26/12 16:44 4-Bromophenylphenyl ether ug/L ND 10.0 04/26/12 16:44 4-Chloro-3-methylphenol ug/L ND 20.0 04/26/12 16:44 4-Chloroaniline ug/L ND 20.0 04/26/12 16:44 4-Chlorophenylphenyl ether ug/L ND 10.0 04/26/12 16:44 4-Nitroaniline ug/L ND 50.0 04/26/12 16:44 4-Nitrophenol ug/L ND 50.0 04/26/12 16:44 Benzyl alcohol ug/L ND 20.0 04/26/12 16:44 bis(2-Chloroethoxy)methane ug/L ND 10.0 04/26/12 16:44 bis(2-Chloroethyl) ether ug/L ND 10.0 04/26/12 16:44 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/26/12 16:44 bis(2chloro1methylethyl) ether ug/L ND 5.0 04/26/12 16:44 Butylbenzylphthalate ug/L ND 10.0 04/26/12 16:44 Di-n-butylphthalate ug/L ND 10.0 04/26/12 16:44 Di-n-octylphthalate ug/L ND 10.0 04/26/12 16:44 Dibenzofuran ug/L ND 10.0 04/26/12 16:44 Diethylphthalate ug/L ND 10.0 04/26/12 16:44 Dimethylphthalate ug/L ND 10.0 04/26/12 16:44 Hexachloro-1,3-butadiene ug/L ND 5.0 04/26/12 16:44 Hexachlorobenzene ug/L ND 10.0 04/26/12 16:44 Hexachlorocyclopentadiene ug/L ND 25.0 04/26/12 16:44 Hexachloroethane ug/L ND 10.0 04/26/12 16:44 Isophorone ug/L ND 10.0 04/26/12 16:44 N-Nitroso-di-n-propylamine ug/L ND 10.0 04/26/12 16:44 N-Nitrosodiphenylamine ug/L ND 10.0 04/26/12 16:44 Nitrobenzene ug/L ND 10.0 04/26/12 16:44 Pentachlorophenol ug/L ND 50.0 04/26/12 16:44 Phenol ug/L ND 10.0 04/26/12 16:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 105 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA Pace Project No.: Project: 5061952 SBI067 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:725702 Associated Lab Samples:5061952011, 5061952012, 5061952013, 5061952014, 5061952015 Matrix:Water Analyzed 2,4,6-Tribromophenol (S)%.95 32-124 04/26/12 16:44 2-Fluorophenol (S)%.31 10-74 04/26/12 16:44 Nitrobenzene-d5 (S)%.82 33-108 04/26/12 16:44 Phenol-d5 (S)%.17 10-56 04/26/12 16:44 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 725703LABORATORY CONTROL SAMPLE: LCSSpike 2,4-Dinitrotoluene ug/L 89.3100 89 38-119 2-Chlorophenol ug/L 72.1100 72 37-106 4-Chloro-3-methylphenol ug/L 79.5100 79 43-115 4-Nitrophenol ug/L ND100 20 10-57 N-Nitroso-di-n-propylamine ug/L 86.3100 86 43-112 Pentachlorophenol ug/L 106100 106 14-131 Phenol ug/L 18.6100 19 14-50 2,4,6-Tribromophenol (S)%.110 32-124 2-Fluorophenol (S)%.32 10-74 Nitrobenzene-d5 (S)%.85 33-108 Phenol-d5 (S)%.18 10-56 Parameter Units MS Result % Rec Limits Qual% RecConc. 725704MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5061952013 725705 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 2,4-Dinitrotoluene ug/L 208 80 37-11484 5 20208ND167176 2-Chlorophenol ug/L 208 71 43-10274 4 20208ND148154 4-Chloro-3-methylphenol ug/L 208 77 49-10880 5 20208ND159167 4-Nitrophenol ug/L 208 32 10-9937 20208ND67.2J 76.5J N-Nitroso-di-n-propylamine ug/L 208 74 43-10781 9 20208ND154168 Pentachlorophenol ug/L 208 87 25-117102 16 20208ND181213 Phenol ug/L 208 29 28-7432 10 20208ND60.5 67.2 2,4,6-Tribromophenol (S)%.93 32-124100 20 2-Fluorophenol (S)%.44 10-7451 20 Nitrobenzene-d5 (S)%.76 33-10882 20 Phenol-d5 (S)%.29 10-5633 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 106 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALIFIERS Pace Project No.: Project: 5061952 SBI067 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Several compounds are outside of acceptance limits for RPD value. Refer to the LCS for system control. grm 4-26-121d The reported result is estimated because one or more of the constituent results are qualified as such.ES Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 The lab does not hold TNI accreditation for this parameter.N2 RPD value was outside control limits.R1 The RPD value in one of the constituent analytes was outside the control limits.RS REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 107 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5061952 SBI067 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5061952001 MPRP/9075 ICP/9051SBI067:HTB10:G450490 EPA 3010 EPA 6010 5061952002 MPRP/9075 ICP/9051SBI067:HTB10:G350390 EPA 3010 EPA 6010 5061952003 MPRP/9075 ICP/9051SBI067:HTB10:G260300 EPA 3010 EPA 6010 5061952004 MPRP/9075 ICP/9051SBI067:HTB12:G450490 EPA 3010 EPA 6010 5061952005 MPRP/9075 ICP/9051SBI067:HTB12:G350390 EPA 3010 EPA 6010 5061952006 MPRP/9075 ICP/9051SBI067:HTB12:G260300 EPA 3010 EPA 6010 5061952007 MPRP/9075 ICP/9051SBI067:HTB12:G260300A EPA 3010 EPA 6010 5061952015 MPRP/9075 ICP/9051SBI067:FBI:W042312 EPA 3010 EPA 6010 5061952001 MPRP/9079 ICP/9050SBI067:HTB10:G450490 EPA 3010 EPA 6010 5061952002 MPRP/9079 ICP/9050SBI067:HTB10:G350390 EPA 3010 EPA 6010 5061952003 MPRP/9079 ICP/9050SBI067:HTB10:G260300 EPA 3010 EPA 6010 5061952004 MPRP/9079 ICP/9050SBI067:HTB12:G450490 EPA 3010 EPA 6010 5061952005 MPRP/9079 ICP/9050SBI067:HTB12:G350390 EPA 3010 EPA 6010 5061952006 MPRP/9079 ICP/9050SBI067:HTB12:G260300 EPA 3010 EPA 6010 5061952007 MPRP/9079 ICP/9050SBI067:HTB12:G260300A EPA 3010 EPA 6010 5061952015 MPRP/9079 ICP/9050SBI067:FBI:W042312 EPA 3010 EPA 6010 5061952001 MERP/3812 MERC/3742SBI067:HTB10:G450490 EPA 7470 EPA 7470 5061952002 MERP/3812 MERC/3742SBI067:HTB10:G350390 EPA 7470 EPA 7470 5061952003 MERP/3812 MERC/3742SBI067:HTB10:G260300 EPA 7470 EPA 7470 5061952004 MERP/3812 MERC/3742SBI067:HTB12:G450490 EPA 7470 EPA 7470 5061952005 MERP/3812 MERC/3742SBI067:HTB12:G350390 EPA 7470 EPA 7470 5061952006 MERP/3812 MERC/3742SBI067:HTB12:G260300 EPA 7470 EPA 7470 5061952007 MERP/3812 MERC/3742SBI067:HTB12:G260300A EPA 7470 EPA 7470 5061952015 MERP/3812 MERC/3742SBI067:FBI:W042312 EPA 7470 EPA 7470 5061952001 MERP/3813 MERC/3743SBI067:HTB10:G450490 EPA 7470 EPA 7470 5061952002 MERP/3813 MERC/3743SBI067:HTB10:G350390 EPA 7470 EPA 7470 5061952003 MERP/3813 MERC/3743SBI067:HTB10:G260300 EPA 7470 EPA 7470 5061952004 MERP/3813 MERC/3743SBI067:HTB12:G450490 EPA 7470 EPA 7470 5061952005 MERP/3813 MERC/3743SBI067:HTB12:G350390 EPA 7470 EPA 7470 5061952006 MERP/3813 MERC/3743SBI067:HTB12:G260300 EPA 7470 EPA 7470 5061952007 MERP/3813 MERC/3743SBI067:HTB12:G260300A EPA 7470 EPA 7470 5061952015 MERP/3813 MERC/3743SBI067:FBI:W042312 EPA 7470 EPA 7470 5061952011 OEXT/29440 MSSV/10039SBI067:HTB8:G450490 EPA 3510 EPA 8270 by SIM 5061952012 OEXT/29440 MSSV/10039SBI067:HTB8:G450490A EPA 3510 EPA 8270 by SIM 5061952013 OEXT/29440 MSSV/10039SBI067:HTB8:G350390 EPA 3510 EPA 8270 by SIM 5061952014 OEXT/29440 MSSV/10039SBI067:HTB8:G260300 EPA 3510 EPA 8270 by SIM 5061952015 OEXT/29440 MSSV/10039SBI067:FBI:W042312 EPA 3510 EPA 8270 by SIM 5061952011 OEXT/29439 MSSV/10035SBI067:HTB8:G450490 EPA 3510 EPA 8270 5061952012 OEXT/29439 MSSV/10035SBI067:HTB8:G450490A EPA 3510 EPA 8270 5061952013 OEXT/29439 MSSV/10035SBI067:HTB8:G350390 EPA 3510 EPA 8270 5061952014 OEXT/29439 MSSV/10035SBI067:HTB8:G260300 EPA 3510 EPA 8270 5061952015 OEXT/29439 MSSV/10035SBI067:FBI:W042312 EPA 3510 EPA 8270 5061952001 MSV/41620SBI067:HTB10:G450490 EPA 8260 5061952002 MSV/41620SBI067:HTB10:G350390 EPA 8260 5061952003 MSV/41620SBI067:HTB10:G260300 EPA 8260 5061952004 MSV/41620SBI067:HTB12:G450490 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 108 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 5061952 SBI067 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 5061952005 MSV/41620SBI067:HTB12:G350390 EPA 8260 5061952006 MSV/41633SBI067:HTB12:G260300 EPA 8260 5061952007 MSV/41633SBI067:HTB12:G260300A EPA 8260 5061952008 MSV/41633SBI067:HTB15:G450490 EPA 8260 5061952009 MSV/41633SBI067:HTB15:G350390 EPA 8260 5061952010 MSV/41633SBI067:HTB15:G260300 EPA 8260 5061952011 MSV/41633SBI067:HTB8:G450490 EPA 8260 5061952013 MSV/41633SBI067:HTB8:G350390 EPA 8260 5061952014 MSV/41633SBI067:HTB8:G260300 EPA 8260 5061952015 MSV/41633SBI067:FBI:W042312 EPA 8260 5061952016 MSV/41633SBI067:HTB16:G450490 EPA 8260 5061952017 MSV/41633SBI067:HTB16:G350390 EPA 8260 5061952018 MSV/41633SBI067:HTB16:G260300 EPA 8260 5061952019 MSV/41633SBI067:HTB13:G450490 EPA 8260 5061952020 MSV/41633SBI067:HTB13:G350390 EPA 8260 5061952021 MSV/41680SBI067:HTB13:G350390A EPA 8260 5061952022 MSV/41680SBI067:HTB13:G260300 EPA 8260 5061952023 MSV/41680SBI067:HTB11:G450490 EPA 8260 5061952024 MSV/41633SBI067:HTB11:G350390 EPA 8260 5061952025 MSV/41680SBI067:HTB11:G260300 EPA 8260 5061952026 MSV/41680SBI067:HTB22:G450490 EPA 8260 5061952027 MSV/41680SBI067:HTB22:G350390 EPA 8260 5061952028 MSV/41680SBI067:HTB22:G260300 EPA 8260 5061952029 MSV/41680SBI067:FB1:W042412 EPA 8260 5061952030 MSV/41680SBI067:TRIP BLANK:W042412 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 04/30/2012 03:35 PM Page 109 of 109 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 Pace Analytical Services, Inc. 1233 Dublin Road Columbus, OH 43215 (614)486-5421