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SB-0240 Appendix P - SBI060.400.0003 Huckins&Lathe Phase II Report (
November 24, 2010 Ms. Ann Kolata Senior Redevelopment Specialist City of South Bend Department of Community and Economic Development 227 West Jefferson Blvd, 12th Floor South Bend, Indiana 46601 RE: Letter Report for Phase II Environmental Site Assessment at the Former South Bend Lathe (Lathe) and Huckins Tool & Die (Huckins) Properties of the Former Studebaker Complex in South Bend, Indiana (the Site). SBI060.400.0003.Phase II Report.DOC Dear Ms. Kolata: Hull & Associates, Inc. (Hull) is pleased to submit this report documenting additional Phase II Environmental Site Assessment (ESA) activities conducted at the above Site. The objectives of this investigation were as follows: 1. to evaluate areas of the referenced parcels at the Site where samples collected during removal of underground storage tanks (USTs) indicated that chemicals of concern (COCs) remain in soils at concentrations exceeding the Indiana Department of Environmental Management (IDEM) 1996 Voluntary Remediation Program (VRP) Nonresidential Tier II Cleanup Goals; and 2. to evaluate the vertical and horizontal distribution of COCs in surface and subsurface soils where the IDEM 1996 VRP Nonresidential Tier II Cleanup Goals are exceeded in the vicinity of certain historical sampling locations. SCOPE OF WORK Based on previous Phase I ESA, Phase II ESA, and Phase III remedial activities completed to date, several areas of the former Lathe and Huckins parcels were identified as requiring additional assessment activities before a VRP Remediation Work Plan could be prepared for the Site. The areas that apply to the proposed additional Phase II ESA activities at the Lathe and Huckins parcels are further described below. Soil Boring SB-O1 (Lathe) - This historical soil boring is located in the east central portion of the former Lathe building. Elevated concentrations of total petroleum hydrocarbons (TPH) extended range organics (ERO) were previously detected in soil samples collected from this boring. Five soil borings were proposed to delineate the vertical and horizontal distribution of TPH-ERO in the vicinity of this boring. Soil Borings SB-SA1 through SB-SA3 (Lathe) – These historical soil borings are located in the northwest portion of the former Lathe building. Elevated concentrations of 6435 Castleway West Drive, Suite 119, Indianapolis, Indiana 46250 800.241.7173 614.793.9070 fax www.hullinc.com Ms. Ann Kolata November 24, 2010 SBI060.400.0003 Page 2 TPH-ERO were previously detected in soil samples collected from these borings. Five soil borings were proposed to delineate the vertical and horizontal distribution of TPH- ERO in this area. Former UST 72-A (Lathe) - One soil sample collected during the closure of this UST exhibited a concentration of TPH-ERO exceeding the soil migration to groundwater pathway. Five additional borings were proposed to delineate the vertical and horizontal distribution of TPH-ERO in this area. Former UST B-1 (Huckins) – Three soil samples collected during the closure of this UST exhibited elevated concentrations of TPH-ERO. An additional five soil borings were proposed to delineate the vertical and horizontal distribution of TPH-ERO in this area. The specific locations of the borings installed during the present investigation are shown on Figure 1. FIELD INVESTIGATION The field work was completed from August 19 through August 20, 2010. Specifically, the field work included the following tasks: 1. Installation of five soil borings located in the east central portion of the former South Bend Lathe building; 2. Installation of five soil borings located in the northwest portion of the former South Bend Lathe building; 3. Installation of five soil borings located west of the perimeter of the former South Bend Lathe building; and 4. Installation of eight soil borings located west of the perimeter of the former South Bend Lathe building near the Huckins property (additional boring locations were added in this area during the investigation based on field observations, as discussed below). Collection of Soil Samples From August 19 through August 20, 2010, under the supervision of Hull, D & T Drilling, Inc. (D & T) installed soil borings (HSB-O101 through HSB-O105, HSB-SA01 through HSB-SA05, HSB- 72A01 through HSB-72A05, and HSB-B101 through HSB-B108) at the locations shown on Figure 1. Soil borings were advanced using a direct-push Geoprobe rig. The borings extended to depths of approximately 15 to 20 feet below ground surface (bgs). Up to two samples were collected from each soil boring and submitted under appropriate chain-of-custody procedures to Pace Analytical Laboratories in Indianapolis, Indiana (Pace) for chemical analyses as follows: 1. HSB-O101 through HSB-O105, HSB-SA01 through HSB-SA05, HSB-72A01 through HSB-72A05, and HSB-B101 through HSB-B108 - TPH-ERO in accordance with U.S. EPA Method 8015M; and 2. HSB-B0102, HSB-B103, and HSB-B104 – volatile organic compounds (VOCs) in accordance with U.S. EPA Method 8260 (collected in accordance with U.S. EPA Method 5035). Ms. Ann Kolata November 24, 2010 SBI060.400.0003 Page 3 Hull’s field representative screened each sample using a photoionization detector (PID). The driller was required to decontaminate all down-hole equipment between sampling intervals using a non-phosphatic detergent (e.g., Liquinox) and rinsing with distilled water. Soil samples were selected based on Hull’s field observations. In general, those samples exhibiting the highest PID readings or other evidence of potential impact were selected for chemical analyses. In addition, a second (deeper) soil sample may have been selected and submitted to the laboratory to evaluate the vertical extent of potential contamination. Soil descriptions, PID readings, and sample intervals are described in further detail on the soil boring logs included in Appendix A. Unused soil cuttings were placed in a Department of Transportation (DOT)-approved 55-gallon drum. The driller decommissioned the borings by filling the boreholes to grade with bentonite chips. FINDINGS Forty-six soil samples and three duplicates were analyzed at Pace. Soil chemical analytical results are summarized in Table 1 and compared to the IDEM 1996 VRP Nonresidential Tier II Cleanup Goals. Alternatively, in the case of TPH parameters, for which there are no VRP Tier II Cleanup Goals, data were compared to Indiana Risk Integrated System of Closure (RISC) Commercial/Industrial Default Closure Levels (IDCLs). Soil sample results exceeding laboratory detection limits and 1996 VRP Nonresidential Tier II Cleanup Goals or RISC IDCLs are shown on Figure 2. Laboratory analytical reports for soil samples are included in Appendix B. The soil samples collected from HSB-B102 (10-11.4’ bgs) and HSB-B103 (10-11.2’ bgs) exhibited concentrations of TPH-ERO exceeding RISC IDCLs. All other soil concentrations were either below VRP Nonresidential Tier II Cleanup Goals or RISC IDCLs, and/or laboratory detection limits. Lithology of the soils logged during this stage of investigation is consistent with that observed during previous investigations. The soils underlying the Site consist primarily of a loose brown/black medium grained sand and gravel, slightly moist, to a depth of fifteen feet. Groundwater appears to be encountered at depths ranging from approximately 15 to 20 feet bgs. Groundwater samples were not collected from the Site during the August 2010 assessment activities. DISCUSSION AND RECOMMENDATIONS While most analytes were not detected above laboratory reporting limits during this investigation, TPH-ERO was detected at an elevated concentration (i.e., 3,360 mg/kg) in soil boring HSB-B102 (10 to 11.4 feet bgs) as shown on Figure 2. This concentration is above the IDEM IDEM RISC IDCL (2,300 mg/kg) for the direct contact exposure pathway but is below the IDEM RISC IDCL (5,800 mg/kg) for the migration to groundwater exposure pathway. The fact that this soil sample interval was collected at a depth beneath which the direct contact exposure pathway is considered complete effectively eliminates cause for concern at present. However, considering that construction and/or redevelopment plans for this portion of the Site are not currently known, this sampling location may require remediation at some point in the future. TPH-ERO was also detected at an elevated concentration (i.e., 6,720 mg/kg) in soil boring HSB- B103 (10-11.2 feet bgs) as shown on Figure 2. This concentration is above the IDEM RISC Ms. Ann Kolata November 24, 2010 SBI060.400.0003 Page 4 IDCL for both the direct contact and migration to groundwater exposure pathways. Although IDEM no longer requires evaluation of TPH parameters in groundwater, this source area may require additional assessment to evaluate its potential impact to groundwater as plans to develop a comprehensive VRP Remediation Work Plan are developed for the Site. During the course of field activities, petroleum odors and/or elevated PID readings were noted during the installation of soil borings HSB-B102 and HSB-B103 (where RISC IDCLs for TPH- ERO were exceeded). For this reason, additional soil borings HSB-B107 and HSB-B108 were installed in an attempt to delineate COCs in this area of the Site. The installation of these additional soil borings appears to have defined the vertical and horizontal extent of TPH-ERO in soils in this portion of the Site. Ultimately, all data collected at the Site (including the adjacent Allied Stamping Plant and Studebaker Foundry facilities) will be compiled into a Remediation Work Plan for the Site. At the time this report was prepared, given the fact that IDEM has requested that the Site’s Voluntary Remediation Agreement be amended to include groundwater, and given the fact that the adjacent Studebaker Foundry is slated for demolition and additional environmental assessment activities in 2011, the extent to which additional assessment activities will be required is not completely understood. As we have discussed, few, if any, of the previously- installed monitoring wells remain, and a network of monitoring wells to evaluate source areas and potentially complete pathways to future on-Site and/or downgradient receptors will likely be necessary prior to preparation of a Remediation Work Plan. We trust this information meets your needs at this time. If necessary, Hull will be happy to assist the City of South Bend with any communication about this report with the Indiana Voluntary Remediation Program. Should you have any questions about this investigation or our recommendations, please do not hesitate to contact either of the undersigned at (800) 241- 7173. Respectfully, Ryan M. France Project Scientist Douglas G. Stuart, CHMM Senior Project Manager Attachments: Tables Figures Appendix A – Soil Boring Logs Appendix B – Laboratory Analytical Reports TABLE PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-O101 HSB-O101 HSB-O102 HSB-O102 HSB-O103 HSB-O103Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-O101:S005020SBI060:HSB-O101:S020040SBI060:HSB-O102:S0050070SBI060:HSB-O102:S005020SBI060:HSB-O103:S005020SBI060:HSB-O103:S050070Sample Depth:0.5 - 2 2 - 4 0.5 - 0.7 0.5 - 2 0.5 - 2 5 - 7TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 843c293 340 730 737 125VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNTdNT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene ---e--- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NT1996 VRP Non Residential Subsurface Soilb1996 VRP Non Residential Surface Soila Reporting UnitsHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA1 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-O101 HSB-O101 HSB-O102 HSB-O102 HSB-O103 HSB-O103Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-O101:S005020SBI060:HSB-O101:S020040SBI060:HSB-O102:S0050070SBI060:HSB-O102:S005020SBI060:HSB-O103:S005020SBI060:HSB-O103:S050070Sample Depth:0.5 - 2 2 - 4 0.5 - 0.7 0.5 - 2 0.5 - 2 5 - 71996 VRP Non Residential Subsurface Soilb1996 VRP Non Residential Surface Soila Reporting UnitsChlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA2 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-O103 HSB-O104 HSB-O104 HSB-O105 HSB-O105 HSB-72A01Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-O103:S050070ASBI060:HSB-O104:S005020SBI060:HSB-O104:S005070SBI060:HSB-O105:S005020SBI060:HSB-O105:S170187SBI060:HSB-72A01:S005020Sample Depth:5 - 7 0.5 - 2 0.5 - 7 0.5 - 2 17 - 18.7 0.5 - 2TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 101 1350 106 667<10.493.6VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NT1996 VRP Non Residential Subsurface SoilbReporting Units1996 VRP Non Residential Surface Soila HULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA3 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-O103 HSB-O104 HSB-O104 HSB-O105 HSB-O105 HSB-72A01Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-O103:S050070ASBI060:HSB-O104:S005020SBI060:HSB-O104:S005070SBI060:HSB-O105:S005020SBI060:HSB-O105:S170187SBI060:HSB-72A01:S005020Sample Depth:5 - 7 0.5 - 2 0.5 - 7 0.5 - 2 17 - 18.7 0.5 - 21996 VRP Non Residential Subsurface SoilbReporting Units1996 VRP Non Residential Surface Soila Chlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA4 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-72A01 HSB-72A02 HSB-72A02 HSB-72A03 HSB-72A03 HSB-72A04Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-72A01:S050070SBI060:HSB-72A02:S005020SBI060:HSB-72A02:S020040SBI060:HSB-72A03:S005020SBI060:HSB-72A03:S050070SBI060:HSB-72A04:S005020Sample Depth:5 - 7 0.5 - 2 2 - 4 0.5 - 2 5 - 7 0.5 - 2TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 685 304 61.4 118 231 313VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NTReporting Units1996 VRP Non Residential Surface Soila1996 VRP Non Residential Subsurface SoilbHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA5 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-72A01 HSB-72A02 HSB-72A02 HSB-72A03 HSB-72A03 HSB-72A04Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-72A01:S050070SBI060:HSB-72A02:S005020SBI060:HSB-72A02:S020040SBI060:HSB-72A03:S005020SBI060:HSB-72A03:S050070SBI060:HSB-72A04:S005020Sample Depth:5 - 7 0.5 - 2 2 - 4 0.5 - 2 5 - 7 0.5 - 2Reporting Units1996 VRP Non Residential Surface Soila1996 VRP Non Residential Subsurface SoilbChlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA6 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-72A04 HSB-72A05 HSB-72A05 HSB-B101 HSB-B101 HSB-B102Sample Date:8/19/2010 8/19/2010 8/19/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-72A04:S020040SBI060:HSB-72A05:S005020SBI060:HSB-72A05:S050070SBI060:HSB-B101:S005020SBI060:HSB-B101:S070080SBI060:HSB-B102:S005020Sample Depth:2 - 4 0.5 - 2 5 - 7 0.5 - 2 7 - 8 0.5 - 2TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 270 137 304 877 746 178VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NT1996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA7 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-72A04 HSB-72A05 HSB-72A05 HSB-B101 HSB-B101 HSB-B102Sample Date:8/19/2010 8/19/2010 8/19/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-72A04:S020040SBI060:HSB-72A05:S005020SBI060:HSB-72A05:S050070SBI060:HSB-B101:S005020SBI060:HSB-B101:S070080SBI060:HSB-B102:S005020Sample Depth:2 - 4 0.5 - 2 5 - 7 0.5 - 2 7 - 8 0.5 - 21996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsChlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA8 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B102 HSB-B103 HSB-B103 HSB-B103 HSB-B104 HSB-B104Sample Date:8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-B102:S100114SBI060:HSB-B103:S005020SBI060:HSB-B103:S100112SBI060:HSB-B103:S100112ASBI060:HSB-B104:S005020SBI060:HSB-B104:S020040Sample Depth:10 - 11.4 0.5 - 2 10 - 11.2 10 - 11.2 0.5 - 2 2 - 4TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg3360f5296720NT303 509VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1,1-Trichloroethane 1000 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1,2,2-Tetrachloroethane 75.41 0.21 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1,2-Trichloroethane 22.74 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1-Dichloroethane 973.47 0.08 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1-Dichloroethene 0.15 1405.37 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,1-Dichloropropene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2,3-Trichlorobenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2,3-Trichloropropane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2,4-Trichlorobenzene 10000 10000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2,4-Trimethylbenzene --- --- mg/kg 0.0044NT0.388 0.386NT <0.0041,2-Dibromoethane (EDB) --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2-Dichlorobenzene 10000 0.37 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2-Dichloroethane 5.27 34.67 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,2-Dichloropropane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,3,5-Trimethylbenzene --- --- mg/kg<0.0038 NT0.175 0.169NT <0.0041,3-Dichlorobenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,3-Dichloropropane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041,4-Dichlorobenzene 2416.67 1.05 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0042,2-Dichloropropane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0042-Butanone (MEK) 1000 146.24 mg/kg<0.019 NT <0.476 <0.47 NT <0.02022-Chlorotoluene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0042-Hexanone --- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.0814-Chlorotoluene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0044-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kg<0.019 NT <0.476 <0.47 NT <0.0202Acetone 1000 136.29 mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Acrolein --- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Acrylonitrile--- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Benzene 16.63 4.77 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Bromobenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Bromochloromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Bromodichloromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Bromoform --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Bromomethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Carbon Disulfide --- --- mg/kg<0.0076 NT <0.19 <0.188 NT <0.0081Carbon Tetrachloride --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.0041996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA9 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B102 HSB-B103 HSB-B103 HSB-B103 HSB-B104 HSB-B104Sample Date:8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-B102:S100114SBI060:HSB-B103:S005020SBI060:HSB-B103:S100112SBI060:HSB-B103:S100112ASBI060:HSB-B104:S005020SBI060:HSB-B104:S020040Sample Depth:10 - 11.4 0.5 - 2 10 - 11.2 10 - 11.2 0.5 - 2 2 - 41996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsChlorobenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Chloroethane 1000 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Chloroform 5.28 20.33 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Chloromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Cis-1,2-Dichloroethene 1000 102.49 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Cis-1,3-Dichloropropene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Dibromochloromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Dibromomethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Dichlorodifluoromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Ethyl Methacrylate--- --- mg/kg<0.0076 NT <0.19 <0.188 NT <0.0081Ethylbenzene 1000 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Hexachloro-1,3-Butadiene 1.78 31.18 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Iodomethane --- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Isopropyl Benzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Methylene Chloride --- --- mg/kg<0.0152 NT <0.381 <0.376 NT <0.0162Methyl-Tert-Butyl Ether--- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Naphthalene 10000 10000 mg/kg<0.0038 NT0.41 0.403NT <0.004N-Butylbenzene--- --- mg/kg<0.0038 NT0.165 0.164NT <0.004N-Hexane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004N-Propylbenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004P-Isopropyltoluene--- --- mg/kg<0.0038 NT0.112 0.109NT <0.004Sec-Butylbenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Styrene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Tert-Butylbenzene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Tetrachloroethene 101.23 8.01 mg/kg0.0038 NT <0.0952 <0.094 NT <0.004Toluene 1000 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Trans-1,2-Dichloroethene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Trans-1,3-Dichloropropene --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Trans-1,4-Dichloro-2-Butene --- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Trichloroethene 24.97 25.73 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Trichlorofluoromethane --- --- mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Vinyl Acetate--- --- mg/kg<0.0758 NT <1.9 <1.88 NT <0.081Vinyl Chloride 1000 1000 mg/kg<0.0038 NT <0.0952 <0.094 NT <0.004Xylene (Total) 1000 1000 mg/kg<0.0076 NT <0.19 <0.188 NT <0.0081HULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA10 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B105 HSB-B105 HSB-B105 HSB-B106 HSB-B106 HSB-B107Sample Date:8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-B105:S005020SBI060:HSB-B105:S005020ASBI060:HSB-B105:S020040SBI060:HSB-B106:S005020SBI060:HSB-B106:S020040SBI060:HSB-B107:S005020Sample Depth:0.5 - 2 0.5 - 2 2 - 4 0.5 - 2 2 - 4 0.5 - 2TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 391 254 146 350 155 218VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NT1996 VRP Non Residential Subsurface SoilbReporting Units1996 VRP Non Residential Surface SoilaHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA11 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B105 HSB-B105 HSB-B105 HSB-B106 HSB-B106 HSB-B107Sample Date:8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010 8/20/2010Laboratory Identication:SBI060:HSB-B105:S005020SBI060:HSB-B105:S005020ASBI060:HSB-B105:S020040SBI060:HSB-B106:S005020SBI060:HSB-B106:S020040SBI060:HSB-B107:S005020Sample Depth:0.5 - 2 0.5 - 2 2 - 4 0.5 - 2 2 - 4 0.5 - 21996 VRP Non Residential Subsurface SoilbReporting Units1996 VRP Non Residential Surface SoilaChlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA12 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B107 HSB-B108 HSB-B108 HSB-SA01 HSB-SA01 HSB-SA02Sample Date:8/20/2010 8/20/2010 8/20/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-B107:S100120SBI060:HSB-B108:S005020SBI060:HSB-B108:S100120SBI060:HSB-SA01:S005020SBI060:HSB-SA01:S020040SBI060:HSB-SA02:S005020Sample Depth:10 - 12 0.5 - 2 10 - 12 0.5 - 2 2 - 4 0.5 - 2TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg<10.6182<10.8165 298 138VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NTReporting Units1996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA13 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-B107 HSB-B108 HSB-B108 HSB-SA01 HSB-SA01 HSB-SA02Sample Date:8/20/2010 8/20/2010 8/20/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-B107:S100120SBI060:HSB-B108:S005020SBI060:HSB-B108:S100120SBI060:HSB-SA01:S005020SBI060:HSB-SA01:S020040SBI060:HSB-SA02:S005020Sample Depth:10 - 12 0.5 - 2 10 - 12 0.5 - 2 2 - 4 0.5 - 2Reporting Units1996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbChlorobenzene --- --- mg/kgNT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NTHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA14 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-SA02 HSB-SA03 HSB-SA03 HSB-SA04 HSB-SA04 HSB-SA05 HSB-SA05Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-SA02:S020040SBI060:HSB-SA03:S005020SBI060:HSB-SA03:S020039SBI060:HSB-SA04:S005020SBI060:HSB-SA04:S020040SBI060:HSB-SA05:S005020SBI060:HSB-SA05:S0170181Sample Depth:2 - 4 0.5 - 2 2 - 3.9 0.5 - 2 2 - 4 0.5 - 2 1.7 - 1.8TPH (Method 8015)Extended Range Organics 5800 2300 mg/kg 583 697 632 66.6 305 272<10.4VOCs (Method 8260)1,1,1,2-Tetrachloroethane 75.91 7.24 mg/kgNT NT NT NT NT NT NT1,1,1-Trichloroethane 1000 1000 mg/kgNT NT NT NT NT NT NT1,1,2,2-Tetrachloroethane 75.41 0.21 mg/kgNT NT NT NT NT NT NT1,1,2-Trichloroethane 22.74 1000 mg/kgNT NT NT NT NT NT NT1,1-Dichloroethane 973.47 0.08 mg/kgNT NT NT NT NT NT NT1,1-Dichloroethene 0.15 1405.37 mg/kgNT NT NT NT NT NT NT1,1-Dichloropropene --- --- mg/kgNT NT NT NT NT NT NT1,2,3-Trichlorobenzene --- --- mg/kgNT NT NT NT NT NT NT1,2,3-Trichloropropane --- --- mg/kgNT NT NT NT NT NT NT1,2,4-Trichlorobenzene 10000 10000 mg/kgNT NT NT NT NT NT NT1,2,4-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT NT1,2-Dibromoethane (EDB) --- --- mg/kgNT NT NT NT NT NT NT1,2-Dichlorobenzene 10000 0.37 mg/kgNT NT NT NT NT NT NT1,2-Dichloroethane 5.27 34.67 mg/kgNT NT NT NT NT NT NT1,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT NT1,3,5-Trimethylbenzene --- --- mg/kgNT NT NT NT NT NT NT1,3-Dichlorobenzene --- --- mg/kgNT NT NT NT NT NT NT1,3-Dichloropropane --- --- mg/kgNT NT NT NT NT NT NT1,4-Dichlorobenzene 2416.67 1.05 mg/kgNT NT NT NT NT NT NT2,2-Dichloropropane --- --- mg/kgNT NT NT NT NT NT NT2-Butanone (MEK) 1000 146.24 mg/kgNT NT NT NT NT NT NT2-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT NT2-Hexanone --- --- mg/kgNT NT NT NT NT NT NT4-Chlorotoluene --- --- mg/kgNT NT NT NT NT NT NT4-Methyl-2-Pentanone (MIBK) 10000 427.24 mg/kgNT NT NT NT NT NT NTAcetone 1000 136.29 mg/kgNT NT NT NT NT NT NTAcrolein --- --- mg/kgNT NT NT NT NT NT NTAcrylonitrile--- --- mg/kgNT NT NT NT NT NT NTBenzene 16.63 4.77 mg/kgNT NT NT NT NT NT NTBromobenzene --- --- mg/kgNT NT NT NT NT NT NTBromochloromethane --- --- mg/kgNT NT NT NT NT NT NTBromodichloromethane --- --- mg/kgNT NT NT NT NT NT NTBromoform --- --- mg/kgNT NT NT NT NT NT NTBromomethane --- --- mg/kgNT NT NT NT NT NT NTCarbon Disulfide --- --- mg/kgNT NT NT NT NT NT NTCarbon Tetrachloride --- --- mg/kgNT NT NT NT NT NT NT1996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsHULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA15 of 16NOVEMBER 2010SBI060.400.0002 PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER SOUTH BEND LATHE AND HUCKINS TOOL DIE PROPERTIESSOUTH BEND, INDIANATABLE 1SOIL LABORATORY ANALYSES(mg/kg)Sample Identification:HSB-SA02 HSB-SA03 HSB-SA03 HSB-SA04 HSB-SA04 HSB-SA05 HSB-SA05Sample Date:8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010 8/19/2010Laboratory Identication:SBI060:HSB-SA02:S020040SBI060:HSB-SA03:S005020SBI060:HSB-SA03:S020039SBI060:HSB-SA04:S005020SBI060:HSB-SA04:S020040SBI060:HSB-SA05:S005020SBI060:HSB-SA05:S0170181Sample Depth:2 - 4 0.5 - 2 2 - 3.9 0.5 - 2 2 - 4 0.5 - 2 1.7 - 1.81996 VRP Non Residential Surface Soila 1996 VRP Non Residential Subsurface SoilbReporting UnitsChlorobenzene --- --- mg/kgNT NT NT NT NT NT NTChloroethane 1000 1000 mg/kgNT NT NT NT NT NT NTChloroform 5.28 20.33 mg/kgNT NT NT NT NT NT NTChloromethane --- --- mg/kgNT NT NT NT NT NT NTCis-1,2-Dichloroethene 1000 102.49 mg/kgNT NT NT NT NT NT NTCis-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NT NTDibromochloromethane --- --- mg/kgNT NT NT NT NT NT NTDibromomethane --- --- mg/kgNT NT NT NT NT NT NTDichlorodifluoromethane --- --- mg/kgNT NT NT NT NT NT NTEthyl Methacrylate--- --- mg/kgNT NT NT NT NT NT NTEthylbenzene 1000 1000 mg/kgNT NT NT NT NT NT NTHexachloro-1,3-Butadiene 1.78 31.18 mg/kgNT NT NT NT NT NT NTIodomethane --- --- mg/kgNT NT NT NT NT NT NTIsopropyl Benzene --- --- mg/kgNT NT NT NT NT NT NTMethylene Chloride --- --- mg/kgNT NT NT NT NT NT NTMethyl-Tert-Butyl Ether--- --- mg/kgNT NT NT NT NT NT NTNaphthalene 10000 10000 mg/kgNT NT NT NT NT NT NTN-Butylbenzene--- --- mg/kgNT NT NT NT NT NT NTN-Hexane --- --- mg/kgNT NT NT NT NT NT NTN-Propylbenzene --- --- mg/kgNT NT NT NT NT NT NTP-Isopropyltoluene--- --- mg/kgNT NT NT NT NT NT NTSec-Butylbenzene --- --- mg/kgNT NT NT NT NT NT NTStyrene --- --- mg/kgNT NT NT NT NT NT NTTert-Butylbenzene --- --- mg/kgNT NT NT NT NT NT NTTetrachloroethene 101.23 8.01 mg/kgNT NT NT NT NT NT NTToluene 1000 1000 mg/kgNT NT NT NT NT NT NTTrans-1,2-Dichloroethene --- --- mg/kgNT NT NT NT NT NT NTTrans-1,3-Dichloropropene --- --- mg/kgNT NT NT NT NT NT NTTrans-1,4-Dichloro-2-Butene --- --- mg/kgNT NT NT NT NT NT NTTrichloroethene 24.97 25.73 mg/kgNT NT NT NT NT NT NTTrichlorofluoromethane --- --- mg/kgNT NT NT NT NT NT NTVinyl Acetate--- --- mg/kgNT NT NT NT NT NT NTVinyl Chloride 1000 1000 mg/kgNT NT NT NT NT NT NTXylene (Total) 1000 1000 mg/kgNT NT NT NT NT NT NTNotes:a. For TPH-ERO, results are compared to the IDEM RISC IDCL for the direct contact exposure pathway.b. For TPH-ERO, results are compared to the IDEM RISC IDCL for the migration to ground water exposure pathway.c. Values shown in bold indicate detection of parameter by laboratory at concentration above laboratory detection limit.d. NT - Not tested.e. -- No standard.f. Values shown in bold and italics indicate that value exceeds the 1996 VRP Non-Residential Closure Level or the IDEM RISC IDCL.HULL & ASSOCIATES, INC.INDIANAPOLIS, INDIANA16 of 16NOVEMBER 2010SBI060.400.0002 FIGURES SAMPLE STREET SOUTH BEND LATHE (PROPERTY C) MUNICIPAL SERVICES BLDG B-5 B-7 B-6B-4 B-3 B-1 B-2 TB-10 MW-11D MW-11S HMW-31D HMW-15D HMW-16D HMW-30DHMW-29DHMW-28D HMW-5S HMW-3S HMW-4S HMW-31IHMW-31SHMW-30I HMW-29IHMW-28S HMW-18S HMW-15S HMW-34S HMW-14S GB-3 GB-2 GB-1 GB-9 GB-13 GB-12GB-10 GB-11SB-2 3-1 5-4 7-1 4A-2 4C-2 4B-1 5-3 7-2 6-1 5-1 6-2 5-2 4C-14B-2 4A-1 95019500 HSB-O105 HSB-O103 HSB-O104 HSB-O101 HSB-O102 HSB-SA05 HSB-SA04 HSB-SA02 HSB-SA03 HSB-SA01 HSB-72A05 HSB-72A03 HSB-72A04 HSB-72A01 HSB-72A02 SB-C2 SB-C1 SB-G1 SB-G2 SB-Y1 SB-Y2 SB-H2 SB-H3 SB-H4 SB-H5 SB-H6 SB-H7 SB-H8 SB-M1 SB-M2 SB-M3 SB-U2 SB-T3SB-P1SB-L4SB-L2SB-L1SB-F8SB-F7SB-F6SB-F5SB-F4SB-F3SB-F2SB-F1 SB-E1 SB-E2 SB-E3 SB-E4 SB-E5 SB-E6 SB-K1 SB-K2 SB-K3 SB-O1 SB-R2SB-N1SB-J4SB-J3SB-J2SB-D6SB-D5SB-D4SB-D3SB-D2 SB-D1 SB-A1 SB-SS3 SB-SS2SB-SS1 SB-SA3 SB-SA2 SB-SA1 SB/B2-S11 SB/B2-S05 SB/B2-S03SB/B2-S08 SB/B2-S10 SB/B2-S02 SB/B2-S07SB/B2-S01SB/B2-S09 SB/B2-S06SB/B2-S04 SB/72A-S04 SB/B12-S06 SB/B12-S08SB/B12-S02 SB/B12-S01 SB/B12-S07 SB/B12-S05 SB/B12-S04 SB/72A-S01SB/72A-S09 SB/72A-S07 SB/72A-S02 SB/72A-S10SB/72A-S11SB/72A-S03 SB/72A-S08SB/72A-S05 SB/CSTSC-S08SB/CSTSC-S07SB/CSTSC-S05SB/CSTSC-S06SB/CSTSC-S01SB/CSTSC-S02 SB/CSTSC-S03SB/CSTSC-S04 SB-U3/U4 DUP SB-L3/L5 DUP SB-A2/A3 DUP SB-S2/S3 DUP SB-H1(MS/MSD) SB-J1/J5 DUP (MS/MSD) Produced using ArcGIS 9.3.1 SP1 and EnviroSpase 2008 LegendHull Soil Boring Installed Aug. 2010Post-Demolition Soil Samples (Collected by Weaver-Bros)Area A - Pre-2002 Assessments7/1992 Soil Borings and Monitoring Wells Installed by EIS (B-#)5/1995 Monitoring Wells Installed by APT, Inc. (TB-#,MW-#S/D)5/1995 Soil Borings Installed by APT, Inc. (HP-#)Dry WellArea A - 9/2002 Hull Soil Borings and Monitoring WellsDeep Monitoring Well Locations (HMW-#D)Monitoring Well Nest Locations, S=Shallow, I=Intermediate (HMW-#S/I)Soil Boring to 4 Feet (GB-#)Soil Boring to 25 Feet (SB-#)Weaver-Boos Sample LocationsApproximate Core Location with Core Only (March 2008 through August 2009)Approximate Core Location with Boring (March 2008 through August 2009) SamplingLocations Additional Phase II ESA South Bend, St. Joseph County, Indiana 1Figure November 2010 6435 Castleway West Dr.Suite 119Indianapolis, IN 46250 Phone: (800) 241-7173 Fax: (614) 793.9070www.hullinc.com 0 40 8020Feet 1:960 © 2010, Hull & Associates, Inc. File Name:SBI060_A_Fig01_SampLocs.mxd Edited: 11/24/2010 By: jsliferGeodatabase:HAIGIS.mdb HSB-B108 HSB-B107 HSB-B106 HSB-B105 HSB-B104HSB-B103 HSB-B102HSB-B101 SB-F1 SB/B1-S01 SB/B1-S06 SB/B1-S04 SB/B1-S09 SB/B1-S02 SB/B1-S07 SB/B1-S10 SB/B1-S08 SB/B1-S03 SB/B1-S11 SB/B1-S05 HMW-6D HMW-6S SB-1 Inset Scale: 1"=20' SAMPLE STREET SOUTH BEND LATHE (PROPERTY C) B-5 B-7 B-6B-4 B-3 B-1 B-2 TB-10 MW-11D MW-11SHMW-15D HMW-16D HMW-28D HMW-5S HMW-3S HMW-4S HMW-18S HMW-15S HMW-34S HMW-14S GB-3 GB-2 GB-1 GB-9 GB-13 GB-12GB-10 GB-11SB-2 3-1 5-4 7-1 4A-2 4C-2 4B-1 5-3 7-2 6-1 5-1 6-2 5-2 4C-14B-2 4A-1 950195006030 HSB-O105 HSB-O103 HSB-O104 HSB-O101 HSB-O102 HSB-SA05 HSB-SA04 HSB-SA02 HSB-SA03 HSB-SA01 HSB-72A05 HSB-72A03 HSB-72A04 HSB-72A01 HSB-72A02 SB-C2 SB-C1 SB-G1 SB-G2 SB-Y1 SB-Y2 SB-H2 SB-H3 SB-H4 SB-H5 SB-H6 SB-H7 SB-H8 SB-M1 SB-U2 SB-T3SB-P1SB-L4SB-L2SB-L1SB-F8SB-F7SB-F6SB-F5SB-F4SB-F3SB-F2SB-F1 SB-E1 SB-E2 SB-E3 SB-E4 SB-E5 SB-E6 SB-K1 SB-K2 SB-K3 SB-O1 SB-R2SB-N1SB-J4SB-J3SB-J2SB-D6SB-D5SB-D4SB-D3SB-D2 SB-D1 SB-A1 SB-SS3 SB-SS2SB-SS1 SB-SA3 SB-SA2 SB-SA1 SB/B2-S11 SB/B2-S05 SB/B2-S03SB/B2-S08 SB/B2-S10 SB/B2-S02 SB/B2-S07SB/B2-S01SB/B2-S09 SB/B2-S06SB/B2-S04 SB/72A-S04 SB/B12-S06 SB/B12-S08SB/B12-S02 SB/B12-S01 SB/B12-S07 SB/B12-S05 SB/B12-S04 SB/72A-S01SB/72A-S09 SB/72A-S07 SB/72A-S02 SB/72A-S10SB/72A-S11SB/72A-S03 SB/72A-S08SB/72A-S05 SB/CSTSC-S08 SB/CSTSC-S07 SB/CSTSC-S05 SB/CSTSC-S06 SB/CSTSC-S01SB/CSTSC-S02 SB/CSTSC-S03SB/CSTSC-S04 SB-L3/L5 DUP SB-A2/A3 DUP SB-S2/S3 DUP SB-H1(MS/MSD) SB-J1/J5 DUP (MS/MSD) HSB-72A04 8/19/2010 0.5-2' 2-4' ___________________________ TPH-ERO: 313 270 HSB-72A05 8/19/2010 0.5-2' 5-7' ___________________________ TPH-ERO 137 304 HSB-72A01 8/19/2010 0.5-2' 5-7' ___________________________ TPH-ERO: 93.6 685 HSB-72A03 8/19/2010 0.5-2' 5-7' ___________________________ TPH-ERO 118 231 HSB-72A02 8/19/2010 0.5-2' 2-4' ____________________________ TPH-ERO 304 61.4 HSB-SA04 8/19/2010 0.5-2' 2-4' ___________________________ TPH-ERO 66.6 305 HSB-SA05 8/19/2010 0.5-2' ____________________ TPH-ERO 272 HSB-SA03 8/19/2010 0.5-2' 2-3.9' _____________________________ TPH-ERO 697 632 HSB-SA01 8/19/2010 0.5-2' 2-4' ___________________________ TPH-ERO 165 298 HSB-SA02 8/19/2010 0.5-2' 2-4' ___________________________ TPH-ERO 138 583 HSB-O104 8/19/2010 0.5-2' 0.5-7' _____________________________ TPH-ERO 1350 106 HSB-O101 8/19/2010 0.5-2' 2-4' ___________________________ TPH-ERO 843 293 HSB-O103 8/19/2010 0.5-2' 5-7' 5-7' __________________________________ TPH-ERO 737 125 101 HSB-O105 8/19/2010 0.5-2' ____________________ TPH-ERO 667 HSB-O102 8/19/2010 0.5-0.7' 0.5-2' _______________________________ TPH-ERO 340 730 Produced using ArcGIS 9.3.1 SP1 and EnviroSpase 2008 Legend Hull Soil Boring Installed Aug. 2010 Post-Demolition Soil Samples (Collected by Weaver-Bros) Area A - Pre-2002 Assessments 7/1992 Soil Borings and Monitoring Wells Installed by EIS (B-#) 5/1995 Monitoring Wells Installed by APT, Inc. (TB-#,MW-#S/D) 5/1995 Soil Borings Installed by APT, Inc. (HP-#) Dry Well Area A - 9/2002 Hull Soil Borings and Monitoring Wells Deep Monitoring Well Locations (HMW-#D) Monitoring Well Nest Locations, S=Shallow, I=Intermediate (HMW-#S/I) Soil Boring to 4 Feet (GB-#) Soil Boring to 25 Feet (SB-#) Weaver-Boos Sample LocationsApproximate Core Location with Core Only (March 2008 through August 2009)Approximate Core Location with Boring (March 2008 through August 2009) Concentrations of COCsin Soil (mg/kg) Additional Phase II ESA South Bend, St. Joseph County, Indiana 2Figure November 2010 6435 Castleway West Dr.Suite 119Indianapolis, IN 46250 Phone: (800) 241-7173 Fax: (614) 793.9070www.hullinc.com 0 40 8020Feet 1:960 © 2010, Hull & Associates, Inc. File Name:SBI060_A_Fig02_COCsSoil.mxd Edited: 11/24/2010 By: jsliferGeodatabase:HAIGIS.mdb HSB-B101 8/20/2010 0.5-2' 7-8' _______________________ TPH-ERO 877 746 HSB-B102 8/20/2010 0.5-2' 10-11.4' _________________________________________ TPH-ERO 178 3360 1,2,4-Trimethyl-benzene: 0.0044 HSB-B108 8/20/2010 0.5-2' __________________ TPH-ERO 182 HSB-B103 8/20/2010 0.5-2' 10-11.2' 10-11.2' __________________________________________________ TPH-ERO 529 6720 1,2,4-Trimethyl-benzene: 0.388 0.386 1,3,5-Trimethylbenzene: 0.175 0.169 4-Isopropyltoluene: 0.112 0.109 Butylbenzene: 0.165 0.164 Naphthalene: 0.41 0.403 HSB-B107 8/20/2010 0.5-2' __________________ TPH-ERO 218 HSB-B104 8/20/2010 0.5-2' 2-4' ________________________ TPH-ERO 303 509 HSB-B105 8/20/2010 0.5-2' 0.5-2' 2-4' _____________________________ TPH-ERO 391 254 146 HSB-B106 8/20/2010 0.5-2' 2-4' ______________________ TPH-ERO 350 155 HMW-6D HMW-6S SB-1 HSB-B103 HSB-B108 HSB-B107 HSB-B106 HSB-B105 HSB-B104HSB-B102HSB-B101 SB/B1-S02 SB-F1 SB/B1-S01SB/B1-S06 SB/B1-S04 SB/B1-S09 SB/B1-S07 SB/B1-S10 SB/B1-S08 SB/B1-S03 SB/B1-S11 SB/B1-S05 SB/72A-S11Inset Scale: 1"=30' Note: Results shown in red exceed the 96 VRP Nonresidential Closure Levelor the IDEM RISC IDCL (for TPH-ERO). APPENDIX A Soil Boring Logs 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA05.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA05:S005020 and SBI060:HSBSA05:S170181 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 24.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA05 (Page 1 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/3.8 5.0/3.5 5.0/3.3 5.0/3.1 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 DP4//SS7 PID/FID (ppm)0.1 0.3 0.1 0.0 0.0 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 3.8 - Loose dark brown medium grain SAND & GRAVEL, dry. 5.0 to 8.5 - Loose brown medium grain SAND, few gravel, dry. 10.0 to 13.3 - Same As Above (SAA) 15.0 to 18.1 - SAA 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA05.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA05:S005020 and SBI060:HSBSA05:S170181 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 24.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA05 (Page 2 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 Sample Interval/Sample Recovery5.0/2.3 Sampler Type/Sample NumberDP4/SS8 DP5/SS9 PID/FID (ppm)0.0 0.0 Blow Count(6"-6"-6"-6")NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 20.0 to 24.0 - SAA, wet @ 20.0 End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A01.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:72A01:S005020 and SBI060:HSB72A01:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A01 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/3.6 5.0/3.0 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.2 0.1 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.1 - Loose dark brown medium grain SAND & GRAVEL, slightly moist, staining 2-4'. 5.0 to 8.6 - Same As Above (SAA): staining 6.5 - 7.0' 10.0 to 12.0 - SAA, brown and black. 12.0 to 13.0 - Loose light brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A02.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSB72A02:S005020 and SBI060:HSB72A02:S020042 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A02 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.7 5.0/3.4 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.1 0.0 0.0 0.1 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.2 - Loose brown and black medium grain SAND & GRAVEL, slightly moist, stained black. 5.0 to 8.7 - Loose brown medium grain SAND & GRAVEL, slightly moist. 10.0 to 13.4 - Same As Above (SAA) End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A03.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:72A03:S005020 and SBI060:HSB72A03:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A03 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.0 5.0/3.4 5.0/3.1 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.1 0.0 0.2 0.0 0.1 0.1 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.0 - Loose brown and black medium grain SAND & GRAVEL, dry. 5.0 to 8.7 - Same As Above (SAA) 10.0 to 13.1 - Loose brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A04.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:72A04:S005020 and SBI060:HSB72A04:S020042 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A04 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/2.7 5.0/3.0 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.0 0.1 0.0 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.2 - Loose dark brown and black medium grain SAND & GRAVEL, slightly moist to dry, crushed brick @ 3.2', possible staining 2-4'. 5.0 to 7.7 - Loose brown medium grain SAND & GRAVEL, dry. 10.0 to 13.0 - Same As Above (SAA) End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A05.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSB72A05:S005020 and SBI060:HSB72A05:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A05 (Page 1 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/3.0 5.0/2.8 5.0/3.2 5.0/4.2 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP4/SS6 PID/FID (ppm)0.0 0.1 0.1 0.1 NA NA Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 3.0 - Loose dark brown medium grain SAND & GRAVEL, slightly moist. 5.0 to 7.8 - Same As Above (SAA): brown @ 7.6', possible staining 5-7'. 10.0 to 13.2 - Loose brown to light brown medium grain SAND & GRAVEL, dry. 15.0 to 19.2 - Loose light brown medium to coarse grain SAND & GRAVEL, wet @ 18.5'. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-72A05.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSB72A05:S005020 and SBI060:HSB72A05:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-72A05 (Page 2 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 Sample Interval/Sample RecoverySampler Type/Sample NumberPID/FID (ppm)Blow Count(6"-6"-6"-6")SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-0101.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSB0101:S005020 and SBI060:HSB0101:S020041 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-0101 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/3.8 5.0/3.6 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.2 0.1 0.2 0.1 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 TO 0.5 - TOPSOIL/FILL. 0.5 to 4.1 - Loose brown to dark brown medium grain SOIL & GRAVEL, slightly moist, staining possible 3-4'. 5.0 to 8.5 - Same As Above (SAA). 10.0 to 13.6 - Loose light brown medium grain SOIL & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-0102.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBO102:S005020 and SBI060:HSBO102:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-O102 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.1 5.0/3.2 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.0 0.3 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.2 - Loose dark brown medium grain SAND & GRAVEL, slightly moist. 5.0 to 8.1 - Same As Above (SAA): staining 5-7' 10.0 to 13.2 - Loose light brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-0104.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBO104:S005020 and SBI060:HSBO104:S050070 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-O104 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.8 5.0/3.5 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.3 0.2 0.1 0.1 0.0 0.1 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.2 - Loose dark brown medium grain SAND & GRAVEL, slightly moist. 5.0 to 8.8 - Same As Above (SAA) : possible staining 5-7' 10.0 to 13.5 - Loose light brown medium grain SAND & GRAVEL, dry. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-0105.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBO105:S005020 and SBI060:HSBO105:S017020 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-O105 (Page 1 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/3.8 5.0/3.3 5.0/3.7 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP2/SS5 DP3/SS6 DP3/SS7 DP4/SS8 PID/FID (ppm)0.2 0.7 0.2 0.3 0.5 0.3 0.2 0.3 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - FILL/ROOTS/TOPSOIL 0.5 to 4.1 - Loose brown medium grain SAND & GRAVEL, slightly moist, trace silty clay. 5.0 to 8.8 - Same As Above (SAA): dark brown. 10.0 to 10.9 SAA 10.9 to 12.7 - Loose brown medium to coarse grain SAND & GRAVEL, slightly moist. 12.7 to 13.3 - Loose brown medium to coarse grain SAND, few gravel, slightly moist. 15.0 to 18.7 - Loose brown medium grain SOIL & GRAVEL, slightly moist. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-0105.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBO105:S005020 and SBI060:HSBO105:S017020 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-O105 (Page 2 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 Sample Interval/Sample RecoverySampler Type/Sample NumberDP4/SS9 PID/FID (ppm)0.2 Blow Count(6"-6"-6"-6")NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B101.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB101:S005020 and SBI060:HSBB101:S070080 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B101 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.3 5.0/3.0 5.0/2.2 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 PID/FID (ppm)0.0 0.1 0.0 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.3 - Loose brown and black SAND & GRAVEL, stained, slightly moist. 5.0 to 8.0 - Same As Above (SAA): stained. 10.0 to 10.9 - Loose brown medium grain SAND. 10.9 to 11.4 - Crushed CONCRETE. 11.4 to 12.2 - Loose brown medium grain SOIL & GRAVEL, slightly moist to dry. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B102.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB102:S005020 and SBI060:HSBB102:S100114 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B102 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.6 5.0/2.6 5.0/3.2 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.2 0.1 0.1 0.1 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.6 - Loose brown and black medium grain SAND & GRAVEL, slightly moist, staining @ 2-4'. 5.0 to 8.0 - Same As Above (SAA): stained thoughout, slight petroleum odor. 10.0 to 11.4 - SAA, dark stained. 11.4 to 13.2 - Loose light brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B103.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB103:S005020 and SBI060:HSBB103:S100112 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B103 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.8 5.0/2.5 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.3 0.0 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.2 - Loose brown and black medium grain SAND & GRAVEL, slightly moist, odor and staining @ 2-4'. 5.0 to 8.8 - Same As Above (SAA): dark stained, petroleum odor. 10.0 to 11.2 - Loose brown and black medium grain SAND, strong petroleum odor, very moist, very stained. 11.2 to 11.4 - Crushed CONCRETE. 11.4 to 12.5 - Loose brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B104.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB104:S005020 and SBI060:HSBB104:S020035 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B104 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/3.5 5.0/3.2 5.0/2.0 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 PID/FID (ppm)0.0 0.0 0.1 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 3.5 - Loose brown and black medium grain SAND & GRAVEL, slightly moist. 5.0 to 8.2 - Loose light brown medium grain SAND, slightly moist. 10.0 to 12.0 - Same As Above (SAA) End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B105.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB105:S005020 and SBI060:HSBB105:S020041 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0 S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B105 (Page 1 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/4.0 5.0/2.2 5.0/3.1 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 DP4/SS7 PID/FID (ppm)0.1 0.0 0.2 0.1 0.0 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.1 - Loose brown and black medium grain SAND, moist, staining @ 2-4'. 5.0 to 8.0 - Loose brown medium grain SAND, slightly moist. 10.0 to 12.2 - Same As Above (SAA) 15.0 to 18.1 - Loose medium grain SAND & GRAVEL, wet @ 17.5'. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B105.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB105:S005020 and SBI060:HSBB105:S020041 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0 S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B105 (Page 2 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 Sample Interval/Sample RecoverySampler Type/Sample NumberDP4/SS8 PID/FID (ppm)0.0 Blow Count(6"-6"-6"-6")NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B106.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB106:S005020 and SBI060:HSBB106:S020042 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B106 (Page 1 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.2 5.0/3.6 5.0/2.3 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 DP4/SS7 PID/FID (ppm)0.1 0.2 0.3 0.1 0.0 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.2 - Loose brown and black medium grain SAND & GRAVEL, slightly moist, crushed concrete. 5.0 to 8.2 - Loose light brown medium grain SAND, slightly moist. 10.0 to 13.0 - Loose light brown medium grain SAND, dry. 13.0 to 15.0 - Loose brown medium grain SAND & GRAVEL, dry. 15.0 to 17.3 - Loose brown medium grain SAND & GRAVEL, dry, wet @ 17'. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B106.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB106:S005020 and SBI060:HSBB106:S020042 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 20.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B106 (Page 2 of 2) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 Sample Interval/Sample RecoverySampler Type/Sample NumberDP4/SS8 PID/FID (ppm)0.0 Blow Count(6"-6"-6"-6")NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B107.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB107:S005020 and SBI060:HSBB107:S100120 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B107 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.0 5.0/3.5 5.0/4.3 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.1 0.0 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 4.2 - Loose brown and black medium grain SAND & GRAVEL, slightly moist. 5.0 to 7.0 - Loose light brown medium grain SAND, dry. 10.0 to 14.3 - Same As Above (SAA). End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-B108.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBB108:S005020 and SBI060:HSBB108:S100120 were sent to laboratory for analysis. Date Started : 08/20/2010 Date Completed : 08/20/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-B108 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/3.8 5.0/3.8 5.0/4.1 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.2 0.1 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL 0.5 to 3.8 - Loose brown medium grain SAND & GRAVEL, slightly moist. 5.0 to 8.8 - Loose light brown medium grain SAND, slightly moist to dry. 10.0 to 14.1 - Same As Above (SAA). End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-O101.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBO101:S005020 and SBI060:HSBO101:S020041 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-O101 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/3.8 5.0/3.6 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.2 0.1 0.2 0.1 0.1 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 TO 0.5 - TOPSOIL/FILL. 0.5 to 4.1 - Loose brown to dark brown medium grain SOIL & GRAVEL, slightly moist, staining possible 3-4'. 5.0 to 8.5 - Same As Above (SAA). 10.0 to 13.6 - Loose light brown medium grain SOIL & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA01.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA01:S005020 and SBI060:HSBSA01:S020040 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA01 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.0 5.0/3.2 5.0/3.4 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.0 0.1 0.2 0.1 0.0 0.1 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.0 - Loose dark brown medium grain SAND & GRAVEL, slightly moist, staining 2-4'. 5.0 to 8.2 - Same As Above (SAA): grades to brown @ 7'. 10.0 to 13.4 - Loose light brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA02.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA02:S005020 and SBI060:HSBSA02:S020041 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA02 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.1 5.0/3.2 5.0/2.5 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.6 0.1 0.0 0.1 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.1 - Loose dark brown medium grain SAND & GRAVEL, dry, odor and staining 2-4'. 5.0 to 8.2 - Same As Above (SAA): grades to light brown @ 6.5'. 10.0 to 12.5 - Loose light brown medium grain SAND & GRAVEL, slightly moist. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA03.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA03:S005020 and SBI060:HSBSA03:S020039 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA03 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/3.9 5.0/2.4 5.0/3.8 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.1 0.3 0.1 0.0 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 3.9 - Loose dark brown medium grain SAND & GRAVEL, slightly moist, staining @ 3.9'. 5.0 to 7.4 - Loose brown medium grain SAND & GRAVEL, slightly moist. 10.0 to 13.8 - Same As Above (SAA): light brown. End of boring. 11-23-2010 J:\CLIENTS\SBI\SBI060 - Area A Additional Asmt. for VRP\LOGS\HSB-SA04.borProject Number: SBI060 Project Manager: Doug Stuart South Bend, IN Former Studebaker Site Remarks: Soil samples SBI060:HSBSA04:S005020 and SBI060:HSBSA04:S020042 were sent to laboratory for analysis. Date Started : 08/19/2010 Date Completed : 08/19/2010 Logged By : S. Sojda Reviewed By : Doug Stuart Drilling Contractor : D&T Drilling Method : Geoprobe Sampling Method : Macrocore Total Depth : 15.0' S. Water Level Date : NA S. Water Level (ft) : NA LOG OF BORING HSB-SA04 (Page 1 of 1) G. Elev. (ft USGS) : NA PID/FID Model : MiniRae 2000 PID/FID Calibration : 100ppm Isobutylene Depth in Feet 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Sample Interval/Sample Recovery5.0/4.2 5.0/3.2 5.0/2.3 Sampler Type/Sample NumberDP1/SS1 DP1/SS2 DP2/SS3 DP2/SS4 DP3/SS5 DP3/SS6 PID/FID (ppm)0.2 0.3 0.1 0.1 0.0 0.0 Blow Count(6"-6"-6"-6")NA NA NA NA NA NA SamplesGRAPHICDESCRIPTION Soil Samples Sample Interval Lab Sample Water Levels Static During drilling 0.0 to 0.5 - TOPSOIL/FILL. 0.5 to 4.2 - Loose dark brown medium grain SAND & GRAVEL, slightly moist, staining 2-4'. 5.0 to 8.2 - Loose brown medium grain SAND & GRAVEL, slightly moist. 10.0 to 12.3 - Loose brown medium grain SAND & GRAVEL, slightly moist. End of boring. APPENDIX B Laboratory Analytical Report September 02, 2010 LIMS USE: FR - DOUG STUART LIMS OBJECT ID: 5040522 5040522 Project: Pace Project No.: RE: Mr. Doug Stuart Hull & Associates 6435 Castleway West Drive Suite 119 Indianapolis, IN 46250 SBI060 Dear Mr. Stuart: Enclosed are the analytical results for sample(s) received by the laboratory on August 20, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kenneth Hunt kenneth.hunt@pacelabs.com Project Manager Illinois/NELAC Certification #: 100418 Indiana Certification #: C-49-06 Kansas Certification #: E-10247 Kentucky Certification #: 0042 Ohio VAP: CL0065 Pennsylvania: 68-00791 West Virginia Certification #: 330 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE SUMMARY Pace Project No.: Project: 5040522 SBI060 Lab ID Sample ID Matrix Date Collected Date Received 5040522001 SBI060:HSB-0105:S005020 Solid 08/19/10 09:20 08/20/10 15:17 5040522002 SBI060:HSB-0105:S170187 Solid 08/19/10 10:00 08/20/10 15:17 5040522003 SBI060:HSB-0103:S005020 Solid 08/19/10 10:10 08/20/10 15:17 5040522004 SBI060:HSB-0103:S050070 Solid 08/19/10 10:25 08/20/10 15:17 5040522005 SBI060:HSB-0103:S050070A Solid 08/19/10 10:25 08/20/10 15:17 5040522006 SBI060:HSB-0104:S005020 Solid 08/19/10 10:35 08/20/10 15:17 5040522007 SBI060:HSB-0104:S005070 Solid 08/19/10 10:45 08/20/10 15:17 5040522008 SBI060:HSB-0101:S005020 Solid 08/19/10 10:55 08/20/10 15:17 5040522009 SBI060:HSB-0101:S020040 Solid 08/19/10 11:05 08/20/10 15:17 5040522010 SBI060:HSB-0102:S005020 Solid 08/19/10 11:20 08/20/10 15:17 5040522011 SBI060:HSB-0102:S0050070 Solid 08/19/10 11:25 08/20/10 15:17 5040522012 SBI060:HSB-SA05:S005020 Solid 08/19/10 12:35 08/20/10 15:17 5040522013 SBI060:HSB-SA05:S0170181 Solid 08/19/10 13:00 08/20/10 15:17 5040522014 SBI060:HSB-SA01:S005020 Solid 08/19/10 13:15 08/20/10 15:17 5040522015 SBI060:HSB-SA01:S020040 Solid 08/19/10 13:22 08/20/10 15:17 5040522016 SBI060:HSB-SA02:S005020 Solid 08/19/10 13:40 08/20/10 15:17 5040522017 SBI060:HSB-SA02:S020040 Solid 08/19/10 13:50 08/20/10 15:17 5040522018 SBI060:HSB-SA03:S005020 Solid 08/19/10 14:05 08/20/10 15:17 5040522019 SBI060:HSB-SA03:S020039 Solid 08/19/10 14:17 08/20/10 15:17 5040522020 SBI060:HSB-SA04:S005020 Solid 08/19/10 14:25 08/20/10 15:17 5040522021 SBI060:HSB-SA04:S020040 Solid 08/19/10 14:40 08/20/10 15:17 5040522022 SBI060:HSB-72A05:S005020 Solid 08/19/10 15:05 08/20/10 15:17 5040522023 SBI060:HSB-72A05:S050070 Solid 08/19/10 15:20 08/20/10 15:17 5040522024 SBI060:HSB-72A04:S005020 Solid 08/19/10 15:35 08/20/10 15:17 5040522025 SBI060:HSB-72A04:S020040 Solid 08/19/10 15:50 08/20/10 15:17 5040522026 SBI060:HSB-72A01:S005020 Solid 08/19/10 16:00 08/20/10 15:17 5040522027 SBI060:HSB-72A01:S050070 Solid 08/19/10 16:10 08/20/10 15:17 5040522028 SBI060:HSB-72A02:S005020 Solid 08/19/10 16:25 08/20/10 15:17 5040522029 SBI060:HSB-72A02:S020040 Solid 08/19/10 16:35 08/20/10 15:17 5040522030 SBI060:HSB-72A03:S005020 Solid 08/19/10 16:45 08/20/10 15:17 5040522031 SBI060:HSB-72A03:S050070 Solid 08/19/10 16:55 08/20/10 15:17 5040522032 SBI060:EB1:W081910 Water 08/19/10 17:00 08/20/10 15:17 5040522033 SBI060:HSB-B106:S005020 Solid 08/20/10 08:00 08/20/10 15:17 5040522034 SBI060:HSB-B106:S020040 Solid 08/20/10 08:25 08/20/10 15:17 5040522035 SBI060:HSB-B105:S005020 Solid 08/20/10 08:35 08/20/10 15:17 5040522036 SBI060:HSB-B105:S020040 Solid 08/20/10 08:45 08/20/10 15:17 5040522037 SBI060:HSB-B105:S005020A Solid 08/20/10 08:35 08/20/10 15:17 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE SUMMARY Pace Project No.: Project: 5040522 SBI060 Lab ID Sample ID Matrix Date Collected Date Received 5040522038 SBI060:HSB-B104:S005020 Solid 08/20/10 09:02 08/20/10 15:17 5040522039 SBI060:HSB-B104:S020040 Solid 08/20/10 09:15 08/20/10 15:17 5040522040 SBI060:HSB-B103:S005020 Solid 08/20/10 09:30 08/20/10 15:17 5040522041 SBI060:HSB-B103:S100112 Solid 08/20/10 09:40 08/20/10 15:17 5040522042 SBI060:HSB-B103:S100112A Solid 08/20/10 09:40 08/20/10 15:17 5040522043 SBI060:HSB-B102:S005020 Solid 08/20/10 09:53 08/20/10 15:17 5040522044 SBI060:HSB-B102:S100114 Solid 08/20/10 10:05 08/20/10 15:17 5040522045 SBI060:HSB-B101:S005020 Solid 08/20/10 10:15 08/20/10 15:17 5040522046 SBI060:HSB-B101:S070080 Solid 08/20/10 10:30 08/20/10 15:17 5040522047 SBI060:EB1:W082010 Water 08/20/10 11:00 08/20/10 15:17 5040522048 TRIP BLANK Water 08/19/10 08:00 08/20/10 15:17 5040522049 SBI060:HSB-B107:S005020 Solid 08/20/10 11:10 08/20/10 15:17 5040522050 SBI060:HSB-B107:S100120 Solid 08/20/10 11:20 08/20/10 15:17 5040522051 SBI060:HSB-B108:S005020 Solid 08/20/10 11:25 08/20/10 15:17 5040522052 SBI060:HSB-B108:S100120 Solid 08/20/10 11:30 08/20/10 15:17 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5040522 SBI060 Lab ID Sample ID Method Analytes ReportedAnalysts 5040522001 SBI060:HSB-0105:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522002 SBI060:HSB-0105:S170187 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522003 SBI060:HSB-0103:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522004 SBI060:HSB-0103:S050070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522005 SBI060:HSB-0103:S050070A EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522006 SBI060:HSB-0104:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522007 SBI060:HSB-0104:S005070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522008 SBI060:HSB-0101:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522009 SBI060:HSB-0101:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522010 SBI060:HSB-0102:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522011 SBI060:HSB-0102:S0050070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522012 SBI060:HSB-SA05:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522013 SBI060:HSB-SA05:S0170181 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522014 SBI060:HSB-SA01:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522015 SBI060:HSB-SA01:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522016 SBI060:HSB-SA02:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522017 SBI060:HSB-SA02:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522018 SBI060:HSB-SA03:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522019 SBI060:HSB-SA03:S020039 EPA 8015 Mod Ext 2EDD REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5040522 SBI060 Lab ID Sample ID Method Analytes ReportedAnalysts ASTM D2974-87 1TPD 5040522020 SBI060:HSB-SA04:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522021 SBI060:HSB-SA04:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522022 SBI060:HSB-72A05:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522023 SBI060:HSB-72A05:S050070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522024 SBI060:HSB-72A04:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522025 SBI060:HSB-72A04:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522026 SBI060:HSB-72A01:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522027 SBI060:HSB-72A01:S050070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522028 SBI060:HSB-72A02:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522029 SBI060:HSB-72A02:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522030 SBI060:HSB-72A03:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522031 SBI060:HSB-72A03:S050070 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522032 SBI060:EB1:W081910 EPA 8015 Mod Ext 2EDD 5040522033 SBI060:HSB-B106:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522034 SBI060:HSB-B106:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522035 SBI060:HSB-B105:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522036 SBI060:HSB-B105:S020040 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522037 SBI060:HSB-B105:S005020A EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522038 SBI060:HSB-B104:S005020 EPA 8015 Mod Ext 2EDD REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 SAMPLE ANALYTE COUNT Pace Project No.: Project: 5040522 SBI060 Lab ID Sample ID Method Analytes ReportedAnalysts ASTM D2974-87 1TPD 5040522039 SBI060:HSB-B104:S020040 EPA 8015 Mod Ext 2EDD EPA 8260 73JLF ASTM D2974-87 1TPD 5040522040 SBI060:HSB-B103:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522041 SBI060:HSB-B103:S100112 EPA 8015 Mod Ext 2EDD EPA 8260 73JLF ASTM D2974-87 1TPD 5040522042 SBI060:HSB-B103:S100112A EPA 8260 73JLF ASTM D2974-87 1TPD 5040522043 SBI060:HSB-B102:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522044 SBI060:HSB-B102:S100114 EPA 8015 Mod Ext 2EDD EPA 8260 73JLF ASTM D2974-87 1TPD 5040522045 SBI060:HSB-B101:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522046 SBI060:HSB-B101:S070080 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522047 SBI060:EB1:W082010 EPA 8015 Mod Ext 2EDD EPA 8260 73JLF 5040522048 TRIP BLANK EPA 8260 73JLF 5040522049 SBI060:HSB-B107:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522050 SBI060:HSB-B107:S100120 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522051 SBI060:HSB-B108:S005020 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD 5040522052 SBI060:HSB-B108:S100120 EPA 8015 Mod Ext 2EDD ASTM D2974-87 1TPD REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0105:S005020 Lab ID:5040522001 Collected:08/19/10 09:20 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)667 mg/kg 5 08/25/10 18:5208/21/10 12:1053.5 n-Pentacosane (S)0 %5 08/25/10 18:52 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 08/23/10 13:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 7 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0105:S170187 Lab ID:5040522002 Collected:08/19/10 10:00 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)ND mg/kg 1 08/24/10 19:5008/21/10 12:1010.4 n-Pentacosane (S)71 %1 08/24/10 19:50 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.0 %1 08/23/10 13:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 8 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0103:S005020 Lab ID:5040522003 Collected:08/19/10 10:10 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)737 mg/kg 5 08/24/10 21:5808/21/10 12:1052.5 n-Pentacosane (S)0 %5 08/24/10 21:58 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.8 %1 08/23/10 13:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 9 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0103:S050070 Lab ID:5040522004 Collected:08/19/10 10:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)125 mg/kg 5 08/25/10 16:5108/21/10 12:1054.2 n-Pentacosane (S)0 %5 08/25/10 16:51 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.7 %1 08/23/10 13:180.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 10 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 0103:S050070A Lab ID:5040522005 Collected:08/19/10 10:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)101 mg/kg 1 08/24/10 19:5708/21/10 12:1010.8 n-Pentacosane (S)119 %1 08/24/10 19:57 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.5 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 11 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0104:S005020 Lab ID:5040522006 Collected:08/19/10 10:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)1350 mg/kg 5 08/24/10 21:4308/21/10 12:1052.7 n-Pentacosane (S)0 %5 08/24/10 21:43 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.2 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 12 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0104:S005070 Lab ID:5040522007 Collected:08/19/10 10:45 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)106 mg/kg 1 08/24/10 20:0508/21/10 12:1010.9 n-Pentacosane (S)129 %1 08/24/10 20:05 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.9 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 13 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0101:S005020 Lab ID:5040522008 Collected:08/19/10 10:55 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)843 mg/kg 5 08/24/10 21:3608/21/10 12:1052.7 n-Pentacosane (S)0 %5 08/24/10 21:36 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.1 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 14 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0101:S020040 Lab ID:5040522009 Collected:08/19/10 11:05 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)293 mg/kg 5 08/24/10 21:2908/21/10 12:1053.4 n-Pentacosane (S)0 %5 08/24/10 21:29 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 15 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-0102:S005020 Lab ID:5040522010 Collected:08/19/10 11:20 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)730 mg/kg 5 08/24/10 21:2208/21/10 12:1052.4 n-Pentacosane (S)0 %5 08/24/10 21:22 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.6 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 16 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 0102:S0050070 Lab ID:5040522011 Collected:08/19/10 11:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)340 mg/kg 1 08/24/10 20:1208/21/10 12:1010.8 n-Pentacosane (S)194 %1 08/24/10 20:12 629-99-2 3d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.8 %1 08/23/10 13:190.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 17 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA05:S005020 Lab ID:5040522012 Collected:08/19/10 12:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)272 mg/kg 1 08/24/10 20:4008/21/10 12:1011.0 n-Pentacosane (S)250 %1 08/24/10 20:40 629-99-2 3d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.2 %1 08/24/10 14:120.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 18 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- SA05:S0170181 Lab ID:5040522013 Collected:08/19/10 13:00 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)ND mg/kg 1 08/24/10 20:1908/21/10 12:1010.4 n-Pentacosane (S)78 %1 08/24/10 20:19 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.5 %1 08/23/10 13:200.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 19 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA01:S005020 Lab ID:5040522014 Collected:08/19/10 13:15 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)165 mg/kg 1 08/24/10 20:2608/21/10 12:1010.6 n-Pentacosane (S)184 %1 08/24/10 20:26 629-99-2 3d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.4 %1 08/23/10 13:200.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 20 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA01:S020040 Lab ID:5040522015 Collected:08/19/10 13:22 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)298 mg/kg 5 08/24/10 21:1508/21/10 12:1054.5 n-Pentacosane (S)0 %5 08/24/10 21:15 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.2 %1 08/23/10 13:200.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 21 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA02:S005020 Lab ID:5040522016 Collected:08/19/10 13:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)138 mg/kg 5 08/24/10 21:0808/21/10 12:1052.5 n-Pentacosane (S)0 %5 08/24/10 21:08 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.8 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 22 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA02:S020040 Lab ID:5040522017 Collected:08/19/10 13:50 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)583 mg/kg 5 08/24/10 21:0108/21/10 12:1054.7 n-Pentacosane (S)0 %5 08/24/10 21:01 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.5 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 23 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA03:S005020 Lab ID:5040522018 Collected:08/19/10 14:05 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)697 mg/kg 5 08/24/10 20:5408/21/10 12:1053.4 n-Pentacosane (S)0 %5 08/24/10 20:54 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 24 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA03:S020039 Lab ID:5040522019 Collected:08/19/10 14:17 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)632 mg/kg 5 08/24/10 20:4708/21/10 12:1054.1 n-Pentacosane (S)0 %5 08/24/10 20:47 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.5 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 25 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA04:S005020 Lab ID:5040522020 Collected:08/19/10 14:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)66.6 mg/kg 1 08/24/10 20:3308/21/10 12:1010.8 n-Pentacosane (S)103 %1 08/24/10 20:33 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.3 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 26 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-SA04:S020040 Lab ID:5040522021 Collected:08/19/10 14:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)305 mg/kg 1 08/25/10 12:5108/21/10 12:1011.0 n-Pentacosane (S)298 %1 08/25/10 12:51 629-99-2 4d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.9 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 27 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A05:S005020 Lab ID:5040522022 Collected:08/19/10 15:05 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)137 mg/kg 1 08/26/10 14:3408/21/10 12:1010.4 n-Pentacosane (S)156 %1 08/26/10 14:34 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.2 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 28 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A05:S050070 Lab ID:5040522023 Collected:08/19/10 15:20 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)304 mg/kg 1 08/25/10 12:5808/21/10 12:1010.9 n-Pentacosane (S)280 %1 08/25/10 12:58 629-99-2 4d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.1 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 29 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A04:S005020 Lab ID:5040522024 Collected:08/19/10 15:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)313 mg/kg 1 08/25/10 13:1208/21/10 12:1010.7 n-Pentacosane (S)291 %1 08/25/10 13:12 629-99-2 4d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 30 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A04:S020040 Lab ID:5040522025 Collected:08/19/10 15:50 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)270 mg/kg 1 08/25/10 13:1908/21/10 12:1010.8 n-Pentacosane (S)229 %1 08/25/10 13:19 629-99-2 4d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.7 %1 08/23/10 13:210.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 31 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A01:S005020 Lab ID:5040522026 Collected:08/19/10 16:00 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)93.6 mg/kg 1 08/25/10 13:2608/21/10 12:1010.7 n-Pentacosane (S)139 %1 08/25/10 13:26 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 %1 08/23/10 13:220.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 32 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A01:S050070 Lab ID:5040522027 Collected:08/19/10 16:10 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)685 mg/kg 5 08/25/10 20:4508/21/10 12:1055.0 n-Pentacosane (S)0 %5 08/25/10 20:45 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.0 %1 08/23/10 13:220.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 33 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A02:S005020 Lab ID:5040522028 Collected:08/19/10 16:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)304 mg/kg 1 08/25/10 13:4008/21/10 12:1010.7 n-Pentacosane (S)240 %1 08/25/10 13:40 629-99-2 4d08/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 08/23/10 13:220.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 34 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A02:S020040 Lab ID:5040522029 Collected:08/19/10 16:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)61.4 mg/kg 1 08/25/10 13:4708/21/10 12:1010.8 n-Pentacosane (S)111 %1 08/25/10 13:47 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.7 %1 08/23/10 13:220.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 35 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A03:S005020 Lab ID:5040522030 Collected:08/19/10 16:45 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)118 mg/kg 1 08/26/10 14:4808/21/10 12:1010.7 n-Pentacosane (S)139 %1 08/26/10 14:48 629-99-208/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.2 %1 08/23/10 13:220.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 36 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- 72A03:S050070 Lab ID:5040522031 Collected:08/19/10 16:55 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)231 mg/kg 5 08/26/10 13:3008/21/10 12:1053.8 n-Pentacosane (S)0 %5 08/26/10 13:30 629-99-2 S408/21/10 12:1045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.1 %1 08/23/10 13:230.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 37 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:EB1:W081910 Lab ID:5040522032 Collected:08/19/10 17:00 Received:08/20/10 15:17 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3510 High End Organics (C8-C34)ND mg/L 1 08/24/10 11:2708/22/10 21:370.10 n-Pentacosane (S)87 %1 08/24/10 11:27 629-99-208/22/10 21:3740-156 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 38 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B106:S005020 Lab ID:5040522033 Collected:08/20/10 08:00 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)350 mg/kg 1 08/25/10 14:0908/21/10 12:2010.7 n-Pentacosane (S)277 %1 08/25/10 14:09 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 %1 08/23/10 13:230.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 39 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B106:S020040 Lab ID:5040522034 Collected:08/20/10 08:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)155 mg/kg 1 08/25/10 14:3708/21/10 12:2010.9 n-Pentacosane (S)182 %1 08/25/10 14:37 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.5 %1 08/23/10 13:230.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 40 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B105:S005020 Lab ID:5040522035 Collected:08/20/10 08:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)391 mg/kg 5 08/25/10 20:5208/21/10 12:2053.6 n-Pentacosane (S)0 %5 08/25/10 20:52 629-99-2 S408/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.7 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 41 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B105:S020040 Lab ID:5040522036 Collected:08/20/10 08:45 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)146 mg/kg 1 08/25/10 14:5108/21/10 12:2010.7 n-Pentacosane (S)162 %1 08/25/10 14:51 629-99-208/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.7 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 42 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- B105:S005020A Lab ID:5040522037 Collected:08/20/10 08:35 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)254 mg/kg 1 08/25/10 14:5808/21/10 12:2010.8 n-Pentacosane (S)202 %1 08/25/10 14:58 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.5 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 43 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B104:S005020 Lab ID:5040522038 Collected:08/20/10 09:02 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)303 mg/kg 1 08/25/10 15:0508/21/10 12:2010.7 n-Pentacosane (S)318 %1 08/25/10 15:05 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 44 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B104:S020040 Lab ID:5040522039 Collected:08/20/10 09:15 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)509 mg/kg 5 08/25/10 20:5908/21/10 12:2054.3 n-Pentacosane (S)0 %5 08/25/10 20:59 629-99-2 S408/21/10 12:2045-170 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 08/31/10 15:21 67-64-181.0 Acrolein ND ug/kg 1 08/31/10 15:21 107-02-881.0 Acrylonitrile ND ug/kg 1 08/31/10 15:21 107-13-181.0 Benzene ND ug/kg 1 08/31/10 15:21 71-43-24.0 Bromobenzene ND ug/kg 1 08/31/10 15:21 108-86-14.0 Bromochloromethane ND ug/kg 1 08/31/10 15:21 74-97-54.0 Bromodichloromethane ND ug/kg 1 08/31/10 15:21 75-27-44.0 Bromoform ND ug/kg 1 08/31/10 15:21 75-25-24.0 Bromomethane ND ug/kg 1 08/31/10 15:21 74-83-94.0 2-Butanone (MEK)ND ug/kg 1 08/31/10 15:21 78-93-320.2 n-Butylbenzene ND ug/kg 1 08/31/10 15:21 104-51-84.0 sec-Butylbenzene ND ug/kg 1 08/31/10 15:21 135-98-84.0 tert-Butylbenzene ND ug/kg 1 08/31/10 15:21 98-06-64.0 Carbon disulfide ND ug/kg 1 08/31/10 15:21 75-15-08.1 Carbon tetrachloride ND ug/kg 1 08/31/10 15:21 56-23-54.0 Chlorobenzene ND ug/kg 1 08/31/10 15:21 108-90-74.0 Chloroethane ND ug/kg 1 08/31/10 15:21 75-00-34.0 Chloroform ND ug/kg 1 08/31/10 15:21 67-66-34.0 Chloromethane ND ug/kg 1 08/31/10 15:21 74-87-34.0 2-Chlorotoluene ND ug/kg 1 08/31/10 15:21 95-49-84.0 4-Chlorotoluene ND ug/kg 1 08/31/10 15:21 106-43-44.0 Dibromochloromethane ND ug/kg 1 08/31/10 15:21 124-48-14.0 1,2-Dibromoethane (EDB)ND ug/kg 1 08/31/10 15:21 106-93-44.0 Dibromomethane ND ug/kg 1 08/31/10 15:21 74-95-34.0 1,2-Dichlorobenzene ND ug/kg 1 08/31/10 15:21 95-50-14.0 1,3-Dichlorobenzene ND ug/kg 1 08/31/10 15:21 541-73-14.0 1,4-Dichlorobenzene ND ug/kg 1 08/31/10 15:21 106-46-74.0 trans-1,4-Dichloro-2-butene ND ug/kg 1 08/31/10 15:21 110-57-681.0 Dichlorodifluoromethane ND ug/kg 1 08/31/10 15:21 75-71-84.0 1,1-Dichloroethane ND ug/kg 1 08/31/10 15:21 75-34-34.0 1,2-Dichloroethane ND ug/kg 1 08/31/10 15:21 107-06-24.0 1,1-Dichloroethene ND ug/kg 1 08/31/10 15:21 75-35-44.0 cis-1,2-Dichloroethene ND ug/kg 1 08/31/10 15:21 156-59-24.0 trans-1,2-Dichloroethene ND ug/kg 1 08/31/10 15:21 156-60-54.0 1,2-Dichloropropane ND ug/kg 1 08/31/10 15:21 78-87-54.0 1,3-Dichloropropane ND ug/kg 1 08/31/10 15:21 142-28-94.0 2,2-Dichloropropane ND ug/kg 1 08/31/10 15:21 594-20-74.0 1,1-Dichloropropene ND ug/kg 1 08/31/10 15:21 563-58-64.0 cis-1,3-Dichloropropene ND ug/kg 1 08/31/10 15:21 10061-01-54.0 trans-1,3-Dichloropropene ND ug/kg 1 08/31/10 15:21 10061-02-64.0 Ethylbenzene ND ug/kg 1 08/31/10 15:21 100-41-44.0 Ethyl methacrylate ND ug/kg 1 08/31/10 15:21 97-63-28.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 45 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B104:S020040 Lab ID:5040522039 Collected:08/20/10 09:15 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Hexachloro-1,3-butadiene ND ug/kg 1 08/31/10 15:21 87-68-34.0 n-Hexane ND ug/kg 1 08/31/10 15:21 110-54-34.0 2-Hexanone ND ug/kg 1 08/31/10 15:21 591-78-681.0 Iodomethane ND ug/kg 1 08/31/10 15:21 74-88-481.0 Isopropylbenzene (Cumene)ND ug/kg 1 08/31/10 15:21 98-82-84.0 p-Isopropyltoluene ND ug/kg 1 08/31/10 15:21 99-87-64.0 Methylene chloride ND ug/kg 1 08/31/10 15:21 75-09-216.2 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 08/31/10 15:21 108-10-120.2 Methyl-tert-butyl ether ND ug/kg 1 08/31/10 15:21 1634-04-44.0 Naphthalene ND ug/kg 1 08/31/10 15:21 91-20-34.0 n-Propylbenzene ND ug/kg 1 08/31/10 15:21 103-65-14.0 Styrene ND ug/kg 1 08/31/10 15:21 100-42-54.0 1,1,1,2-Tetrachloroethane ND ug/kg 1 08/31/10 15:21 630-20-64.0 1,1,2,2-Tetrachloroethane ND ug/kg 1 08/31/10 15:21 79-34-54.0 Tetrachloroethene ND ug/kg 1 08/31/10 15:21 127-18-44.0 Toluene ND ug/kg 1 08/31/10 15:21 108-88-34.0 1,2,3-Trichlorobenzene ND ug/kg 1 08/31/10 15:21 87-61-64.0 1,2,4-Trichlorobenzene ND ug/kg 1 08/31/10 15:21 120-82-14.0 1,1,1-Trichloroethane ND ug/kg 1 08/31/10 15:21 71-55-64.0 1,1,2-Trichloroethane ND ug/kg 1 08/31/10 15:21 79-00-54.0 Trichloroethene ND ug/kg 1 08/31/10 15:21 79-01-64.0 Trichlorofluoromethane ND ug/kg 1 08/31/10 15:21 75-69-44.0 1,2,3-Trichloropropane ND ug/kg 1 08/31/10 15:21 96-18-44.0 1,2,4-Trimethylbenzene ND ug/kg 1 08/31/10 15:21 95-63-64.0 1,3,5-Trimethylbenzene ND ug/kg 1 08/31/10 15:21 108-67-84.0 Vinyl acetate ND ug/kg 1 08/31/10 15:21 108-05-481.0 Vinyl chloride ND ug/kg 1 08/31/10 15:21 75-01-44.0 Xylene (Total)ND ug/kg 1 08/31/10 15:21 1330-20-78.1 Dibromofluoromethane (S)102 %1 08/31/10 15:21 1868-53-780-124 Toluene-d8 (S)111 %1 08/31/10 15:21 2037-26-558-145 4-Bromofluorobenzene (S)88 %1 08/31/10 15:21 460-00-461-131 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.0 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 46 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B103:S005020 Lab ID:5040522040 Collected:08/20/10 09:30 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)529 mg/kg 5 08/25/10 21:2008/21/10 12:2053.1 n-Pentacosane (S)0 %5 08/25/10 21:20 629-99-2 S408/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.8 %1 08/23/10 13:240.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 47 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B103:S100112 Lab ID:5040522041 Collected:08/20/10 09:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)6720 mg/kg 50 08/26/10 15:1608/21/10 12:20556 n-Pentacosane (S)0 %50 08/26/10 15:16 629-99-2 S408/21/10 12:2045-170 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 25 08/31/10 17:14 67-64-11900 Acrolein ND ug/kg 25 08/31/10 17:14 107-02-81900 Acrylonitrile ND ug/kg 25 08/31/10 17:14 107-13-11900 Benzene ND ug/kg 25 08/31/10 17:14 71-43-2 1d95.2 Bromobenzene ND ug/kg 25 08/31/10 17:14 108-86-195.2 Bromochloromethane ND ug/kg 25 08/31/10 17:14 74-97-595.2 Bromodichloromethane ND ug/kg 25 08/31/10 17:14 75-27-495.2 Bromoform ND ug/kg 25 08/31/10 17:14 75-25-295.2 Bromomethane ND ug/kg 25 08/31/10 17:14 74-83-995.2 2-Butanone (MEK)ND ug/kg 25 08/31/10 17:14 78-93-3476 n-Butylbenzene 165 ug/kg 25 08/31/10 17:14 104-51-895.2 sec-Butylbenzene ND ug/kg 25 08/31/10 17:14 135-98-895.2 tert-Butylbenzene ND ug/kg 25 08/31/10 17:14 98-06-695.2 Carbon disulfide ND ug/kg 25 08/31/10 17:14 75-15-0190 Carbon tetrachloride ND ug/kg 25 08/31/10 17:14 56-23-595.2 Chlorobenzene ND ug/kg 25 08/31/10 17:14 108-90-795.2 Chloroethane ND ug/kg 25 08/31/10 17:14 75-00-395.2 Chloroform ND ug/kg 25 08/31/10 17:14 67-66-395.2 Chloromethane ND ug/kg 25 08/31/10 17:14 74-87-395.2 2-Chlorotoluene ND ug/kg 25 08/31/10 17:14 95-49-895.2 4-Chlorotoluene ND ug/kg 25 08/31/10 17:14 106-43-495.2 Dibromochloromethane ND ug/kg 25 08/31/10 17:14 124-48-195.2 1,2-Dibromoethane (EDB)ND ug/kg 25 08/31/10 17:14 106-93-495.2 Dibromomethane ND ug/kg 25 08/31/10 17:14 74-95-395.2 1,2-Dichlorobenzene ND ug/kg 25 08/31/10 17:14 95-50-195.2 1,3-Dichlorobenzene ND ug/kg 25 08/31/10 17:14 541-73-195.2 1,4-Dichlorobenzene ND ug/kg 25 08/31/10 17:14 106-46-795.2 trans-1,4-Dichloro-2-butene ND ug/kg 25 08/31/10 17:14 110-57-61900 Dichlorodifluoromethane ND ug/kg 25 08/31/10 17:14 75-71-895.2 1,1-Dichloroethane ND ug/kg 25 08/31/10 17:14 75-34-395.2 1,2-Dichloroethane ND ug/kg 25 08/31/10 17:14 107-06-295.2 1,1-Dichloroethene ND ug/kg 25 08/31/10 17:14 75-35-495.2 cis-1,2-Dichloroethene ND ug/kg 25 08/31/10 17:14 156-59-295.2 trans-1,2-Dichloroethene ND ug/kg 25 08/31/10 17:14 156-60-595.2 1,2-Dichloropropane ND ug/kg 25 08/31/10 17:14 78-87-595.2 1,3-Dichloropropane ND ug/kg 25 08/31/10 17:14 142-28-995.2 2,2-Dichloropropane ND ug/kg 25 08/31/10 17:14 594-20-795.2 1,1-Dichloropropene ND ug/kg 25 08/31/10 17:14 563-58-695.2 cis-1,3-Dichloropropene ND ug/kg 25 08/31/10 17:14 10061-01-595.2 trans-1,3-Dichloropropene ND ug/kg 25 08/31/10 17:14 10061-02-695.2 Ethylbenzene ND ug/kg 25 08/31/10 17:14 100-41-495.2 Ethyl methacrylate ND ug/kg 25 08/31/10 17:14 97-63-2190 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 48 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B103:S100112 Lab ID:5040522041 Collected:08/20/10 09:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Hexachloro-1,3-butadiene ND ug/kg 25 08/31/10 17:14 87-68-395.2 n-Hexane ND ug/kg 25 08/31/10 17:14 110-54-395.2 2-Hexanone ND ug/kg 25 08/31/10 17:14 591-78-61900 Iodomethane ND ug/kg 25 08/31/10 17:14 74-88-41900 Isopropylbenzene (Cumene)ND ug/kg 25 08/31/10 17:14 98-82-895.2 p-Isopropyltoluene 112 ug/kg 25 08/31/10 17:14 99-87-695.2 Methylene chloride ND ug/kg 25 08/31/10 17:14 75-09-2381 4-Methyl-2-pentanone (MIBK)ND ug/kg 25 08/31/10 17:14 108-10-1476 Methyl-tert-butyl ether ND ug/kg 25 08/31/10 17:14 1634-04-4 D395.2 Naphthalene 410 ug/kg 25 08/31/10 17:14 91-20-395.2 n-Propylbenzene ND ug/kg 25 08/31/10 17:14 103-65-195.2 Styrene ND ug/kg 25 08/31/10 17:14 100-42-595.2 1,1,1,2-Tetrachloroethane ND ug/kg 25 08/31/10 17:14 630-20-695.2 1,1,2,2-Tetrachloroethane ND ug/kg 25 08/31/10 17:14 79-34-595.2 Tetrachloroethene ND ug/kg 25 08/31/10 17:14 127-18-495.2 Toluene ND ug/kg 25 08/31/10 17:14 108-88-395.2 1,2,3-Trichlorobenzene ND ug/kg 25 08/31/10 17:14 87-61-695.2 1,2,4-Trichlorobenzene ND ug/kg 25 08/31/10 17:14 120-82-195.2 1,1,1-Trichloroethane ND ug/kg 25 08/31/10 17:14 71-55-695.2 1,1,2-Trichloroethane ND ug/kg 25 08/31/10 17:14 79-00-595.2 Trichloroethene ND ug/kg 25 08/31/10 17:14 79-01-695.2 Trichlorofluoromethane ND ug/kg 25 08/31/10 17:14 75-69-495.2 1,2,3-Trichloropropane ND ug/kg 25 08/31/10 17:14 96-18-495.2 1,2,4-Trimethylbenzene 388 ug/kg 25 08/31/10 17:14 95-63-695.2 1,3,5-Trimethylbenzene 175 ug/kg 25 08/31/10 17:14 108-67-895.2 Vinyl acetate ND ug/kg 25 08/31/10 17:14 108-05-41900 Vinyl chloride ND ug/kg 25 08/31/10 17:14 75-01-495.2 Xylene (Total)ND ug/kg 25 08/31/10 17:14 1330-20-7190 Dibromofluoromethane (S)91 %25 08/31/10 17:14 1868-53-780-124 Toluene-d8 (S)103 %25 08/31/10 17:14 2037-26-558-145 4-Bromofluorobenzene (S)103 %25 08/31/10 17:14 460-00-461-131 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.1 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 49 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- B103:S100112A Lab ID:5040522042 Collected:08/20/10 09:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 25 08/31/10 17:51 67-64-11880 Acrolein ND ug/kg 25 08/31/10 17:51 107-02-81880 Acrylonitrile ND ug/kg 25 08/31/10 17:51 107-13-11880 Benzene ND ug/kg 25 08/31/10 17:51 71-43-2 1d94.0 Bromobenzene ND ug/kg 25 08/31/10 17:51 108-86-194.0 Bromochloromethane ND ug/kg 25 08/31/10 17:51 74-97-594.0 Bromodichloromethane ND ug/kg 25 08/31/10 17:51 75-27-494.0 Bromoform ND ug/kg 25 08/31/10 17:51 75-25-294.0 Bromomethane ND ug/kg 25 08/31/10 17:51 74-83-994.0 2-Butanone (MEK)ND ug/kg 25 08/31/10 17:51 78-93-3470 n-Butylbenzene 164 ug/kg 25 08/31/10 17:51 104-51-894.0 sec-Butylbenzene ND ug/kg 25 08/31/10 17:51 135-98-894.0 tert-Butylbenzene ND ug/kg 25 08/31/10 17:51 98-06-694.0 Carbon disulfide ND ug/kg 25 08/31/10 17:51 75-15-0188 Carbon tetrachloride ND ug/kg 25 08/31/10 17:51 56-23-594.0 Chlorobenzene ND ug/kg 25 08/31/10 17:51 108-90-794.0 Chloroethane ND ug/kg 25 08/31/10 17:51 75-00-394.0 Chloroform ND ug/kg 25 08/31/10 17:51 67-66-394.0 Chloromethane ND ug/kg 25 08/31/10 17:51 74-87-394.0 2-Chlorotoluene ND ug/kg 25 08/31/10 17:51 95-49-894.0 4-Chlorotoluene ND ug/kg 25 08/31/10 17:51 106-43-494.0 Dibromochloromethane ND ug/kg 25 08/31/10 17:51 124-48-194.0 1,2-Dibromoethane (EDB)ND ug/kg 25 08/31/10 17:51 106-93-494.0 Dibromomethane ND ug/kg 25 08/31/10 17:51 74-95-394.0 1,2-Dichlorobenzene ND ug/kg 25 08/31/10 17:51 95-50-194.0 1,3-Dichlorobenzene ND ug/kg 25 08/31/10 17:51 541-73-194.0 1,4-Dichlorobenzene ND ug/kg 25 08/31/10 17:51 106-46-794.0 trans-1,4-Dichloro-2-butene ND ug/kg 25 08/31/10 17:51 110-57-61880 Dichlorodifluoromethane ND ug/kg 25 08/31/10 17:51 75-71-894.0 1,1-Dichloroethane ND ug/kg 25 08/31/10 17:51 75-34-394.0 1,2-Dichloroethane ND ug/kg 25 08/31/10 17:51 107-06-294.0 1,1-Dichloroethene ND ug/kg 25 08/31/10 17:51 75-35-494.0 cis-1,2-Dichloroethene ND ug/kg 25 08/31/10 17:51 156-59-294.0 trans-1,2-Dichloroethene ND ug/kg 25 08/31/10 17:51 156-60-594.0 1,2-Dichloropropane ND ug/kg 25 08/31/10 17:51 78-87-594.0 1,3-Dichloropropane ND ug/kg 25 08/31/10 17:51 142-28-994.0 2,2-Dichloropropane ND ug/kg 25 08/31/10 17:51 594-20-794.0 1,1-Dichloropropene ND ug/kg 25 08/31/10 17:51 563-58-694.0 cis-1,3-Dichloropropene ND ug/kg 25 08/31/10 17:51 10061-01-594.0 trans-1,3-Dichloropropene ND ug/kg 25 08/31/10 17:51 10061-02-694.0 Ethylbenzene ND ug/kg 25 08/31/10 17:51 100-41-494.0 Ethyl methacrylate ND ug/kg 25 08/31/10 17:51 97-63-2188 Hexachloro-1,3-butadiene ND ug/kg 25 08/31/10 17:51 87-68-394.0 n-Hexane ND ug/kg 25 08/31/10 17:51 110-54-394.0 2-Hexanone ND ug/kg 25 08/31/10 17:51 591-78-61880 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 50 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB- B103:S100112A Lab ID:5040522042 Collected:08/20/10 09:40 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Iodomethane ND ug/kg 25 08/31/10 17:51 74-88-41880 Isopropylbenzene (Cumene)ND ug/kg 25 08/31/10 17:51 98-82-894.0 p-Isopropyltoluene 109 ug/kg 25 08/31/10 17:51 99-87-694.0 Methylene chloride ND ug/kg 25 08/31/10 17:51 75-09-2376 4-Methyl-2-pentanone (MIBK)ND ug/kg 25 08/31/10 17:51 108-10-1470 Methyl-tert-butyl ether ND ug/kg 25 08/31/10 17:51 1634-04-4 D394.0 Naphthalene 403 ug/kg 25 08/31/10 17:51 91-20-394.0 n-Propylbenzene ND ug/kg 25 08/31/10 17:51 103-65-194.0 Styrene ND ug/kg 25 08/31/10 17:51 100-42-594.0 1,1,1,2-Tetrachloroethane ND ug/kg 25 08/31/10 17:51 630-20-694.0 1,1,2,2-Tetrachloroethane ND ug/kg 25 08/31/10 17:51 79-34-594.0 Tetrachloroethene ND ug/kg 25 08/31/10 17:51 127-18-494.0 Toluene ND ug/kg 25 08/31/10 17:51 108-88-394.0 1,2,3-Trichlorobenzene ND ug/kg 25 08/31/10 17:51 87-61-694.0 1,2,4-Trichlorobenzene ND ug/kg 25 08/31/10 17:51 120-82-194.0 1,1,1-Trichloroethane ND ug/kg 25 08/31/10 17:51 71-55-694.0 1,1,2-Trichloroethane ND ug/kg 25 08/31/10 17:51 79-00-594.0 Trichloroethene ND ug/kg 25 08/31/10 17:51 79-01-694.0 Trichlorofluoromethane ND ug/kg 25 08/31/10 17:51 75-69-494.0 1,2,3-Trichloropropane ND ug/kg 25 08/31/10 17:51 96-18-494.0 1,2,4-Trimethylbenzene 386 ug/kg 25 08/31/10 17:51 95-63-694.0 1,3,5-Trimethylbenzene 169 ug/kg 25 08/31/10 17:51 108-67-894.0 Vinyl acetate ND ug/kg 25 08/31/10 17:51 108-05-41880 Vinyl chloride ND ug/kg 25 08/31/10 17:51 75-01-494.0 Xylene (Total)ND ug/kg 25 08/31/10 17:51 1330-20-7188 Dibromofluoromethane (S)88 %25 08/31/10 17:51 1868-53-780-124 Toluene-d8 (S)100 %25 08/31/10 17:51 2037-26-558-145 4-Bromofluorobenzene (S)106 %25 08/31/10 17:51 460-00-461-131 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.4 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 51 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B102:S005020 Lab ID:5040522043 Collected:08/20/10 09:53 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)178 mg/kg 1 08/25/10 15:4008/21/10 12:2010.7 n-Pentacosane (S)164 %1 08/25/10 15:40 629-99-208/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 52 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B102:S100114 Lab ID:5040522044 Collected:08/20/10 10:05 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)3360 mg/kg 20 08/25/10 21:3408/21/10 12:20219 n-Pentacosane (S)0 %20 08/25/10 21:34 629-99-2 S408/21/10 12:2045-170 8260 MSV 5035A VOA Analytical Method: EPA 8260 Acetone ND ug/kg 1 08/31/10 18:29 67-64-175.8 Acrolein ND ug/kg 1 08/31/10 18:29 107-02-875.8 Acrylonitrile ND ug/kg 1 08/31/10 18:29 107-13-175.8 Benzene ND ug/kg 1 08/31/10 18:29 71-43-23.8 Bromobenzene ND ug/kg 1 08/31/10 18:29 108-86-13.8 Bromochloromethane ND ug/kg 1 08/31/10 18:29 74-97-53.8 Bromodichloromethane ND ug/kg 1 08/31/10 18:29 75-27-43.8 Bromoform ND ug/kg 1 08/31/10 18:29 75-25-23.8 Bromomethane ND ug/kg 1 08/31/10 18:29 74-83-93.8 2-Butanone (MEK)ND ug/kg 1 08/31/10 18:29 78-93-319.0 n-Butylbenzene ND ug/kg 1 08/31/10 18:29 104-51-83.8 sec-Butylbenzene ND ug/kg 1 08/31/10 18:29 135-98-83.8 tert-Butylbenzene ND ug/kg 1 08/31/10 18:29 98-06-63.8 Carbon disulfide ND ug/kg 1 08/31/10 18:29 75-15-07.6 Carbon tetrachloride ND ug/kg 1 08/31/10 18:29 56-23-53.8 Chlorobenzene ND ug/kg 1 08/31/10 18:29 108-90-73.8 Chloroethane ND ug/kg 1 08/31/10 18:29 75-00-33.8 Chloroform ND ug/kg 1 08/31/10 18:29 67-66-33.8 Chloromethane ND ug/kg 1 08/31/10 18:29 74-87-33.8 2-Chlorotoluene ND ug/kg 1 08/31/10 18:29 95-49-83.8 4-Chlorotoluene ND ug/kg 1 08/31/10 18:29 106-43-43.8 Dibromochloromethane ND ug/kg 1 08/31/10 18:29 124-48-13.8 1,2-Dibromoethane (EDB)ND ug/kg 1 08/31/10 18:29 106-93-43.8 Dibromomethane ND ug/kg 1 08/31/10 18:29 74-95-33.8 1,2-Dichlorobenzene ND ug/kg 1 08/31/10 18:29 95-50-13.8 1,3-Dichlorobenzene ND ug/kg 1 08/31/10 18:29 541-73-13.8 1,4-Dichlorobenzene ND ug/kg 1 08/31/10 18:29 106-46-73.8 trans-1,4-Dichloro-2-butene ND ug/kg 1 08/31/10 18:29 110-57-675.8 Dichlorodifluoromethane ND ug/kg 1 08/31/10 18:29 75-71-83.8 1,1-Dichloroethane ND ug/kg 1 08/31/10 18:29 75-34-33.8 1,2-Dichloroethane ND ug/kg 1 08/31/10 18:29 107-06-23.8 1,1-Dichloroethene ND ug/kg 1 08/31/10 18:29 75-35-43.8 cis-1,2-Dichloroethene ND ug/kg 1 08/31/10 18:29 156-59-23.8 trans-1,2-Dichloroethene ND ug/kg 1 08/31/10 18:29 156-60-53.8 1,2-Dichloropropane ND ug/kg 1 08/31/10 18:29 78-87-53.8 1,3-Dichloropropane ND ug/kg 1 08/31/10 18:29 142-28-93.8 2,2-Dichloropropane ND ug/kg 1 08/31/10 18:29 594-20-73.8 1,1-Dichloropropene ND ug/kg 1 08/31/10 18:29 563-58-63.8 cis-1,3-Dichloropropene ND ug/kg 1 08/31/10 18:29 10061-01-53.8 trans-1,3-Dichloropropene ND ug/kg 1 08/31/10 18:29 10061-02-63.8 Ethylbenzene ND ug/kg 1 08/31/10 18:29 100-41-43.8 Ethyl methacrylate ND ug/kg 1 08/31/10 18:29 97-63-27.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 53 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B102:S100114 Lab ID:5040522044 Collected:08/20/10 10:05 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV 5035A VOA Analytical Method: EPA 8260 Hexachloro-1,3-butadiene ND ug/kg 1 08/31/10 18:29 87-68-33.8 n-Hexane ND ug/kg 1 08/31/10 18:29 110-54-33.8 2-Hexanone ND ug/kg 1 08/31/10 18:29 591-78-675.8 Iodomethane ND ug/kg 1 08/31/10 18:29 74-88-475.8 Isopropylbenzene (Cumene)ND ug/kg 1 08/31/10 18:29 98-82-83.8 p-Isopropyltoluene ND ug/kg 1 08/31/10 18:29 99-87-63.8 Methylene chloride ND ug/kg 1 08/31/10 18:29 75-09-215.2 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 08/31/10 18:29 108-10-119.0 Methyl-tert-butyl ether ND ug/kg 1 08/31/10 18:29 1634-04-43.8 Naphthalene ND ug/kg 1 08/31/10 18:29 91-20-33.8 n-Propylbenzene ND ug/kg 1 08/31/10 18:29 103-65-13.8 Styrene ND ug/kg 1 08/31/10 18:29 100-42-53.8 1,1,1,2-Tetrachloroethane ND ug/kg 1 08/31/10 18:29 630-20-63.8 1,1,2,2-Tetrachloroethane ND ug/kg 1 08/31/10 18:29 79-34-53.8 Tetrachloroethene 3.8 ug/kg 1 08/31/10 18:29 127-18-43.8 Toluene ND ug/kg 1 08/31/10 18:29 108-88-33.8 1,2,3-Trichlorobenzene ND ug/kg 1 08/31/10 18:29 87-61-63.8 1,2,4-Trichlorobenzene ND ug/kg 1 08/31/10 18:29 120-82-13.8 1,1,1-Trichloroethane ND ug/kg 1 08/31/10 18:29 71-55-63.8 1,1,2-Trichloroethane ND ug/kg 1 08/31/10 18:29 79-00-53.8 Trichloroethene ND ug/kg 1 08/31/10 18:29 79-01-63.8 Trichlorofluoromethane ND ug/kg 1 08/31/10 18:29 75-69-43.8 1,2,3-Trichloropropane ND ug/kg 1 08/31/10 18:29 96-18-43.8 1,2,4-Trimethylbenzene 4.4 ug/kg 1 08/31/10 18:29 95-63-63.8 1,3,5-Trimethylbenzene ND ug/kg 1 08/31/10 18:29 108-67-83.8 Vinyl acetate ND ug/kg 1 08/31/10 18:29 108-05-475.8 Vinyl chloride ND ug/kg 1 08/31/10 18:29 75-01-43.8 Xylene (Total)ND ug/kg 1 08/31/10 18:29 1330-20-77.6 Dibromofluoromethane (S)108 %1 08/31/10 18:29 1868-53-780-124 Toluene-d8 (S)124 %1 08/31/10 18:29 2037-26-558-145 4-Bromofluorobenzene (S)73 %1 08/31/10 18:29 460-00-461-131 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.6 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 54 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B101:S005020 Lab ID:5040522045 Collected:08/20/10 10:15 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)877 mg/kg 5 08/25/10 16:5808/21/10 12:2053.1 n-Pentacosane (S)0 %5 08/25/10 16:58 629-99-2 S408/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.9 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 55 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B101:S070080 Lab ID:5040522046 Collected:08/20/10 10:30 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)746 mg/kg 5 08/25/10 21:2708/21/10 12:2055.2 n-Pentacosane (S)0 %5 08/25/10 21:27 629-99-2 S408/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.5 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 56 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:EB1:W082010 Lab ID:5040522047 Collected:08/20/10 11:00 Received:08/20/10 15:17 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3510 High End Organics (C8-C34)ND mg/L 1 08/24/10 11:3408/22/10 21:370.11 n-Pentacosane (S)92 %1 08/24/10 11:34 629-99-208/22/10 21:3740-156 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 08/31/10 19:06 67-64-1100 Acrolein ND ug/L 1 08/31/10 19:06 107-02-8100 Acrylonitrile ND ug/L 1 08/31/10 19:06 107-13-1100 Benzene ND ug/L 1 08/31/10 19:06 71-43-25.0 Bromobenzene ND ug/L 1 08/31/10 19:06 108-86-15.0 Bromochloromethane ND ug/L 1 08/31/10 19:06 74-97-55.0 Bromodichloromethane ND ug/L 1 08/31/10 19:06 75-27-45.0 Bromoform ND ug/L 1 08/31/10 19:06 75-25-25.0 Bromomethane ND ug/L 1 08/31/10 19:06 74-83-95.0 2-Butanone (MEK)ND ug/L 1 08/31/10 19:06 78-93-325.0 n-Butylbenzene ND ug/L 1 08/31/10 19:06 104-51-85.0 sec-Butylbenzene ND ug/L 1 08/31/10 19:06 135-98-85.0 tert-Butylbenzene ND ug/L 1 08/31/10 19:06 98-06-65.0 Carbon disulfide ND ug/L 1 08/31/10 19:06 75-15-010.0 Carbon tetrachloride ND ug/L 1 08/31/10 19:06 56-23-55.0 Chlorobenzene ND ug/L 1 08/31/10 19:06 108-90-75.0 Chloroethane ND ug/L 1 08/31/10 19:06 75-00-35.0 Chloroform ND ug/L 1 08/31/10 19:06 67-66-35.0 Chloromethane ND ug/L 1 08/31/10 19:06 74-87-35.0 2-Chlorotoluene ND ug/L 1 08/31/10 19:06 95-49-85.0 4-Chlorotoluene ND ug/L 1 08/31/10 19:06 106-43-45.0 Dibromochloromethane ND ug/L 1 08/31/10 19:06 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 08/31/10 19:06 106-93-45.0 Dibromomethane ND ug/L 1 08/31/10 19:06 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 08/31/10 19:06 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 08/31/10 19:06 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 08/31/10 19:06 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 08/31/10 19:06 110-57-6100 Dichlorodifluoromethane ND ug/L 1 08/31/10 19:06 75-71-85.0 1,1-Dichloroethane ND ug/L 1 08/31/10 19:06 75-34-35.0 1,2-Dichloroethane ND ug/L 1 08/31/10 19:06 107-06-25.0 1,1-Dichloroethene ND ug/L 1 08/31/10 19:06 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 08/31/10 19:06 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 08/31/10 19:06 156-60-55.0 1,2-Dichloropropane ND ug/L 1 08/31/10 19:06 78-87-55.0 1,3-Dichloropropane ND ug/L 1 08/31/10 19:06 142-28-95.0 2,2-Dichloropropane ND ug/L 1 08/31/10 19:06 594-20-75.0 1,1-Dichloropropene ND ug/L 1 08/31/10 19:06 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 08/31/10 19:06 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 08/31/10 19:06 10061-02-65.0 Ethylbenzene ND ug/L 1 08/31/10 19:06 100-41-45.0 Ethyl methacrylate ND ug/L 1 08/31/10 19:06 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 08/31/10 19:06 87-68-35.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 57 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:EB1:W082010 Lab ID:5040522047 Collected:08/20/10 11:00 Received:08/20/10 15:17 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 n-Hexane ND ug/L 1 08/31/10 19:06 110-54-35.0 2-Hexanone ND ug/L 1 08/31/10 19:06 591-78-625.0 Iodomethane ND ug/L 1 08/31/10 19:06 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 08/31/10 19:06 98-82-85.0 p-Isopropyltoluene ND ug/L 1 08/31/10 19:06 99-87-65.0 Methylene chloride ND ug/L 1 08/31/10 19:06 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/31/10 19:06 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 08/31/10 19:06 1634-04-44.0 Naphthalene ND ug/L 1 08/31/10 19:06 91-20-35.0 n-Propylbenzene ND ug/L 1 08/31/10 19:06 103-65-15.0 Styrene ND ug/L 1 08/31/10 19:06 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 08/31/10 19:06 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 08/31/10 19:06 79-34-55.0 Tetrachloroethene ND ug/L 1 08/31/10 19:06 127-18-45.0 Toluene ND ug/L 1 08/31/10 19:06 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 08/31/10 19:06 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 08/31/10 19:06 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 08/31/10 19:06 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 08/31/10 19:06 79-00-55.0 Trichloroethene ND ug/L 1 08/31/10 19:06 79-01-65.0 Trichlorofluoromethane ND ug/L 1 08/31/10 19:06 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 08/31/10 19:06 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 08/31/10 19:06 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 08/31/10 19:06 108-67-85.0 Vinyl acetate ND ug/L 1 08/31/10 19:06 108-05-410.0 Vinyl chloride ND ug/L 1 08/31/10 19:06 75-01-42.0 Xylene (Total)ND ug/L 1 08/31/10 19:06 1330-20-710.0 Dibromofluoromethane (S)99 %1 08/31/10 19:06 1868-53-780-123 4-Bromofluorobenzene (S)101 %1 08/31/10 19:06 460-00-470-126 Toluene-d8 (S)106 %1 08/31/10 19:06 2037-26-580-116 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 58 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:TRIP BLANK Lab ID:5040522048 Collected:08/19/10 08:00 Received:08/20/10 15:17 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 Acetone ND ug/L 1 08/31/10 19:44 67-64-1100 Acrolein ND ug/L 1 08/31/10 19:44 107-02-8100 Acrylonitrile ND ug/L 1 08/31/10 19:44 107-13-1100 Benzene ND ug/L 1 08/31/10 19:44 71-43-25.0 Bromobenzene ND ug/L 1 08/31/10 19:44 108-86-15.0 Bromochloromethane ND ug/L 1 08/31/10 19:44 74-97-55.0 Bromodichloromethane ND ug/L 1 08/31/10 19:44 75-27-45.0 Bromoform ND ug/L 1 08/31/10 19:44 75-25-25.0 Bromomethane ND ug/L 1 08/31/10 19:44 74-83-95.0 2-Butanone (MEK)ND ug/L 1 08/31/10 19:44 78-93-325.0 n-Butylbenzene ND ug/L 1 08/31/10 19:44 104-51-85.0 sec-Butylbenzene ND ug/L 1 08/31/10 19:44 135-98-85.0 tert-Butylbenzene ND ug/L 1 08/31/10 19:44 98-06-65.0 Carbon disulfide ND ug/L 1 08/31/10 19:44 75-15-010.0 Carbon tetrachloride ND ug/L 1 08/31/10 19:44 56-23-55.0 Chlorobenzene ND ug/L 1 08/31/10 19:44 108-90-75.0 Chloroethane ND ug/L 1 08/31/10 19:44 75-00-35.0 Chloroform ND ug/L 1 08/31/10 19:44 67-66-35.0 Chloromethane ND ug/L 1 08/31/10 19:44 74-87-35.0 2-Chlorotoluene ND ug/L 1 08/31/10 19:44 95-49-85.0 4-Chlorotoluene ND ug/L 1 08/31/10 19:44 106-43-45.0 Dibromochloromethane ND ug/L 1 08/31/10 19:44 124-48-15.0 1,2-Dibromoethane (EDB)ND ug/L 1 08/31/10 19:44 106-93-45.0 Dibromomethane ND ug/L 1 08/31/10 19:44 74-95-35.0 1,2-Dichlorobenzene ND ug/L 1 08/31/10 19:44 95-50-15.0 1,3-Dichlorobenzene ND ug/L 1 08/31/10 19:44 541-73-15.0 1,4-Dichlorobenzene ND ug/L 1 08/31/10 19:44 106-46-75.0 trans-1,4-Dichloro-2-butene ND ug/L 1 08/31/10 19:44 110-57-6100 Dichlorodifluoromethane ND ug/L 1 08/31/10 19:44 75-71-85.0 1,1-Dichloroethane ND ug/L 1 08/31/10 19:44 75-34-35.0 1,2-Dichloroethane ND ug/L 1 08/31/10 19:44 107-06-25.0 1,1-Dichloroethene ND ug/L 1 08/31/10 19:44 75-35-45.0 cis-1,2-Dichloroethene ND ug/L 1 08/31/10 19:44 156-59-25.0 trans-1,2-Dichloroethene ND ug/L 1 08/31/10 19:44 156-60-55.0 1,2-Dichloropropane ND ug/L 1 08/31/10 19:44 78-87-55.0 1,3-Dichloropropane ND ug/L 1 08/31/10 19:44 142-28-95.0 2,2-Dichloropropane ND ug/L 1 08/31/10 19:44 594-20-75.0 1,1-Dichloropropene ND ug/L 1 08/31/10 19:44 563-58-65.0 cis-1,3-Dichloropropene ND ug/L 1 08/31/10 19:44 10061-01-55.0 trans-1,3-Dichloropropene ND ug/L 1 08/31/10 19:44 10061-02-65.0 Ethylbenzene ND ug/L 1 08/31/10 19:44 100-41-45.0 Ethyl methacrylate ND ug/L 1 08/31/10 19:44 97-63-2100 Hexachloro-1,3-butadiene ND ug/L 1 08/31/10 19:44 87-68-35.0 n-Hexane ND ug/L 1 08/31/10 19:44 110-54-35.0 2-Hexanone ND ug/L 1 08/31/10 19:44 591-78-625.0 Iodomethane ND ug/L 1 08/31/10 19:44 74-88-410.0 Isopropylbenzene (Cumene)ND ug/L 1 08/31/10 19:44 98-82-85.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 59 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:TRIP BLANK Lab ID:5040522048 Collected:08/19/10 08:00 Received:08/20/10 15:17 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Analytical Method: EPA 8260 p-Isopropyltoluene ND ug/L 1 08/31/10 19:44 99-87-65.0 Methylene chloride ND ug/L 1 08/31/10 19:44 75-09-25.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 08/31/10 19:44 108-10-125.0 Methyl-tert-butyl ether ND ug/L 1 08/31/10 19:44 1634-04-44.0 Naphthalene ND ug/L 1 08/31/10 19:44 91-20-35.0 n-Propylbenzene ND ug/L 1 08/31/10 19:44 103-65-15.0 Styrene ND ug/L 1 08/31/10 19:44 100-42-55.0 1,1,1,2-Tetrachloroethane ND ug/L 1 08/31/10 19:44 630-20-65.0 1,1,2,2-Tetrachloroethane ND ug/L 1 08/31/10 19:44 79-34-55.0 Tetrachloroethene ND ug/L 1 08/31/10 19:44 127-18-45.0 Toluene ND ug/L 1 08/31/10 19:44 108-88-35.0 1,2,3-Trichlorobenzene ND ug/L 1 08/31/10 19:44 87-61-65.0 1,2,4-Trichlorobenzene ND ug/L 1 08/31/10 19:44 120-82-15.0 1,1,1-Trichloroethane ND ug/L 1 08/31/10 19:44 71-55-65.0 1,1,2-Trichloroethane ND ug/L 1 08/31/10 19:44 79-00-55.0 Trichloroethene ND ug/L 1 08/31/10 19:44 79-01-65.0 Trichlorofluoromethane ND ug/L 1 08/31/10 19:44 75-69-45.0 1,2,3-Trichloropropane ND ug/L 1 08/31/10 19:44 96-18-45.0 1,2,4-Trimethylbenzene ND ug/L 1 08/31/10 19:44 95-63-65.0 1,3,5-Trimethylbenzene ND ug/L 1 08/31/10 19:44 108-67-85.0 Vinyl acetate ND ug/L 1 08/31/10 19:44 108-05-410.0 Vinyl chloride ND ug/L 1 08/31/10 19:44 75-01-42.0 Xylene (Total)ND ug/L 1 08/31/10 19:44 1330-20-710.0 Dibromofluoromethane (S)98 %1 08/31/10 19:44 1868-53-780-123 4-Bromofluorobenzene (S)100 %1 08/31/10 19:44 460-00-470-126 Toluene-d8 (S)106 %1 08/31/10 19:44 2037-26-580-116 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 60 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B107:S005020 Lab ID:5040522049 Collected:08/20/10 11:10 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)218 mg/kg 1 08/25/10 16:0208/21/10 12:2010.9 n-Pentacosane (S)219 %1 08/25/10 16:02 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.0 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 61 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B107:S100120 Lab ID:5040522050 Collected:08/20/10 11:20 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)ND mg/kg 1 08/25/10 16:0908/21/10 12:2010.6 n-Pentacosane (S)88 %1 08/25/10 16:09 629-99-208/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.3 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 62 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B108:S005020 Lab ID:5040522051 Collected:08/20/10 11:25 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)182 mg/kg 1 08/25/10 16:1608/21/10 12:2010.9 n-Pentacosane (S)197 %1 08/25/10 16:16 629-99-2 4d08/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.3 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 63 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 ANALYTICAL RESULTS Pace Project No.: Project: 5040522 SBI060 Sample:SBI060:HSB-B108:S100120 Lab ID:5040522052 Collected:08/20/10 11:30 Received:08/20/10 15:17 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8015M TPH ERO Analytical Method: EPA 8015 Mod Ext Preparation Method: EPA 3546 High End Organics (C8-C34)ND mg/kg 1 08/25/10 16:2308/21/10 12:2010.8 n-Pentacosane (S)78 %1 08/25/10 16:23 629-99-208/21/10 12:2045-170 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.4 %1 08/23/10 13:250.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 64 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/20349 EPA 3510 EPA 8015 Mod Ext EPA 8015 Modified Associated Lab Samples:5040522032, 5040522047 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:470449 Associated Lab Samples:5040522032, 5040522047 Matrix:Water Analyzed High End Organics (C8-C34)mg/L ND 0.10 08/24/10 11:13 n-Pentacosane (S)%98 40-156 08/24/10 11:13 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 470450LABORATORY CONTROL SAMPLE: LCSSpike High End Organics (C8-C34)mg/L 2.12.5 83 42-136 n-Pentacosane (S)%88 40-156 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 65 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/20352 EPA 3546 EPA 8015 Mod Ext EPA 8015 Modified Associated Lab Samples:5040522001, 5040522002, 5040522003, 5040522004, 5040522005, 5040522006, 5040522007, 5040522008, 5040522009, 5040522010, 5040522011, 5040522012, 5040522013, 5040522014, 5040522015, 5040522016, 5040522017, 5040522018, 5040522019, 5040522020 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:470461 Associated Lab Samples:5040522001, 5040522002, 5040522003, 5040522004, 5040522005, 5040522006, 5040522007, 5040522008, 5040522009, 5040522010, 5040522011, 5040522012, 5040522013, 5040522014, 5040522015, 5040522016, 5040522017, 5040522018, 5040522019, 5040522020 Matrix:Solid Analyzed High End Organics (C8-C34)mg/kg ND 10.0 08/24/10 19:15 n-Pentacosane (S)%75 45-170 08/24/10 19:15 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 470462LABORATORY CONTROL SAMPLE: LCSSpike High End Organics (C8-C34)mg/kg 54.283.3 65 41-139 n-Pentacosane (S)%61 45-170 Parameter Units MS Result % Rec Limits Qual% RecConc. 470463MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5040522001 470464 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. High End Organics (C8-C34)mg/kg P689.2 -15 40-146-.2 2 2089.2667 654 667 n-Pentacosane (S)%S4045-1700 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 66 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/20353 EPA 3546 EPA 8015 Mod Ext EPA 8015 Modified Associated Lab Samples:5040522033, 5040522034, 5040522035, 5040522036, 5040522037, 5040522038, 5040522039, 5040522040, 5040522041, 5040522043, 5040522044, 5040522045, 5040522046, 5040522049, 5040522050, 5040522051, 5040522052 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:470465 Associated Lab Samples:5040522033, 5040522034, 5040522035, 5040522036, 5040522037, 5040522038, 5040522039, 5040522040, 5040522041, 5040522043, 5040522044, 5040522045, 5040522046, 5040522049, 5040522050, 5040522051, 5040522052 Matrix:Solid Analyzed High End Organics (C8-C34)mg/kg ND 10.0 08/25/10 13:54 n-Pentacosane (S)%89 45-170 08/25/10 13:54 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 470466LABORATORY CONTROL SAMPLE: LCSSpike High End Organics (C8-C34)mg/kg 56.583.3 68 41-139 n-Pentacosane (S)%76 45-170 Parameter Units MS Result % Rec Limits Qual% RecConc. 470467MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5040522033 470468 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. High End Organics (C8-C34)mg/kg P6,R188.9 -74 40-146.4 21 2088.9350 284 351 n-Pentacosane (S)%4d22345-170263 20 Parameter Units MS Result % Rec Limits Qual% RecConc. 470469MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5040522039 470470 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. High End Organics (C8-C34)mg/kg P690.5 6 40-146134 20 2090.5509 514 631 n-Pentacosane (S)%S4045-1700 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 67 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/20354 EPA 3546 EPA 8015 Mod Ext EPA 8015 Modified Associated Lab Samples:5040522021, 5040522022, 5040522023, 5040522024, 5040522025, 5040522026, 5040522027, 5040522028, 5040522029, 5040522030, 5040522031 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:470471 Associated Lab Samples:5040522021, 5040522022, 5040522023, 5040522024, 5040522025, 5040522026, 5040522027, 5040522028, 5040522029, 5040522030, 5040522031 Matrix:Solid Analyzed High End Organics (C8-C34)mg/kg ND 10.0 08/25/10 12:37 n-Pentacosane (S)%70 45-170 08/25/10 12:37 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 470472LABORATORY CONTROL SAMPLE: LCSSpike High End Organics (C8-C34)mg/kg 58.983.3 71 41-139 n-Pentacosane (S)%63 45-170 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 68 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/26363 EPA 8260 EPA 8260 8260 MSV Associated Lab Samples:5040522047, 5040522048 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:474695 Associated Lab Samples:5040522047, 5040522048 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 08/31/10 12:51 1,1,1-Trichloroethane ug/L ND 5.0 08/31/10 12:51 1,1,2,2-Tetrachloroethane ug/L ND 5.0 08/31/10 12:51 1,1,2-Trichloroethane ug/L ND 5.0 08/31/10 12:51 1,1-Dichloroethane ug/L ND 5.0 08/31/10 12:51 1,1-Dichloroethene ug/L ND 5.0 08/31/10 12:51 1,1-Dichloropropene ug/L ND 5.0 08/31/10 12:51 1,2,3-Trichlorobenzene ug/L ND 5.0 08/31/10 12:51 1,2,3-Trichloropropane ug/L ND 5.0 08/31/10 12:51 1,2,4-Trichlorobenzene ug/L ND 5.0 08/31/10 12:51 1,2,4-Trimethylbenzene ug/L ND 5.0 08/31/10 12:51 1,2-Dibromoethane (EDB)ug/L ND 5.0 08/31/10 12:51 1,2-Dichlorobenzene ug/L ND 5.0 08/31/10 12:51 1,2-Dichloroethane ug/L ND 5.0 08/31/10 12:51 1,2-Dichloropropane ug/L ND 5.0 08/31/10 12:51 1,3,5-Trimethylbenzene ug/L ND 5.0 08/31/10 12:51 1,3-Dichlorobenzene ug/L ND 5.0 08/31/10 12:51 1,3-Dichloropropane ug/L ND 5.0 08/31/10 12:51 1,4-Dichlorobenzene ug/L ND 5.0 08/31/10 12:51 2,2-Dichloropropane ug/L ND 5.0 08/31/10 12:51 2-Butanone (MEK)ug/L ND 25.0 08/31/10 12:51 2-Chlorotoluene ug/L ND 5.0 08/31/10 12:51 2-Hexanone ug/L ND 25.0 08/31/10 12:51 4-Chlorotoluene ug/L ND 5.0 08/31/10 12:51 4-Methyl-2-pentanone (MIBK)ug/L ND 25.0 08/31/10 12:51 Acetone ug/L ND 100 08/31/10 12:51 Acrolein ug/L ND 100 08/31/10 12:51 Acrylonitrile ug/L ND 100 08/31/10 12:51 Benzene ug/L ND 5.0 08/31/10 12:51 Bromobenzene ug/L ND 5.0 08/31/10 12:51 Bromochloromethane ug/L ND 5.0 08/31/10 12:51 Bromodichloromethane ug/L ND 5.0 08/31/10 12:51 Bromoform ug/L ND 5.0 08/31/10 12:51 Bromomethane ug/L ND 5.0 08/31/10 12:51 Carbon disulfide ug/L ND 10.0 08/31/10 12:51 Carbon tetrachloride ug/L ND 5.0 08/31/10 12:51 Chlorobenzene ug/L ND 5.0 08/31/10 12:51 Chloroethane ug/L ND 5.0 08/31/10 12:51 Chloroform ug/L ND 5.0 08/31/10 12:51 Chloromethane ug/L ND 5.0 08/31/10 12:51 cis-1,2-Dichloroethene ug/L ND 5.0 08/31/10 12:51 cis-1,3-Dichloropropene ug/L ND 5.0 08/31/10 12:51 Dibromochloromethane ug/L ND 5.0 08/31/10 12:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 69 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:474695 Associated Lab Samples:5040522047, 5040522048 Matrix:Water Analyzed Dibromomethane ug/L ND 5.0 08/31/10 12:51 Dichlorodifluoromethane ug/L ND 5.0 08/31/10 12:51 Ethyl methacrylate ug/L ND 100 08/31/10 12:51 Ethylbenzene ug/L ND 5.0 08/31/10 12:51 Hexachloro-1,3-butadiene ug/L ND 5.0 08/31/10 12:51 Iodomethane ug/L ND 10.0 08/31/10 12:51 Isopropylbenzene (Cumene)ug/L ND 5.0 08/31/10 12:51 Methyl-tert-butyl ether ug/L ND 4.0 08/31/10 12:51 Methylene chloride ug/L ND 5.0 08/31/10 12:51 n-Butylbenzene ug/L ND 5.0 08/31/10 12:51 n-Hexane ug/L ND 5.0 08/31/10 12:51 n-Propylbenzene ug/L ND 5.0 08/31/10 12:51 Naphthalene ug/L ND 5.0 08/31/10 12:51 p-Isopropyltoluene ug/L ND 5.0 08/31/10 12:51 sec-Butylbenzene ug/L ND 5.0 08/31/10 12:51 Styrene ug/L ND 5.0 08/31/10 12:51 tert-Butylbenzene ug/L ND 5.0 08/31/10 12:51 Tetrachloroethene ug/L ND 5.0 08/31/10 12:51 Toluene ug/L ND 5.0 08/31/10 12:51 trans-1,2-Dichloroethene ug/L ND 5.0 08/31/10 12:51 trans-1,3-Dichloropropene ug/L ND 5.0 08/31/10 12:51 trans-1,4-Dichloro-2-butene ug/L ND 100 08/31/10 12:51 Trichloroethene ug/L ND 5.0 08/31/10 12:51 Trichlorofluoromethane ug/L ND 5.0 08/31/10 12:51 Vinyl acetate ug/L ND 10.0 08/31/10 12:51 Vinyl chloride ug/L ND 2.0 08/31/10 12:51 Xylene (Total)ug/L ND 10.0 08/31/10 12:51 4-Bromofluorobenzene (S)%97 70-126 08/31/10 12:51 Dibromofluoromethane (S)%97 80-123 08/31/10 12:51 Toluene-d8 (S)%106 80-116 08/31/10 12:51 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474696LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 45.050 90 69-130 1,1,1-Trichloroethane ug/L 50.050 100 69-136 1,1,2,2-Tetrachloroethane ug/L 45.750 91 69-131 1,1,2-Trichloroethane ug/L 45.950 92 77-132 1,1-Dichloroethane ug/L 45.750 91 67-133 1,1-Dichloroethene ug/L 52.750 105 63-128 1,1-Dichloropropene ug/L 49.950 100 75-134 1,2,3-Trichlorobenzene ug/L 50.550 101 58-131 1,2,3-Trichloropropane ug/L 86.0100 86 60-131 1,2,4-Trichlorobenzene ug/L 48.750 97 60-130 1,2,4-Trimethylbenzene ug/L 44.750 89 73-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 70 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474696LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/L 46.950 94 75-126 1,2-Dichlorobenzene ug/L 46.750 93 76-124 1,2-Dichloroethane ug/L 46.850 94 69-139 1,2-Dichloropropane ug/L 45.550 91 76-129 1,3,5-Trimethylbenzene ug/L 44.950 90 74-130 1,3-Dichlorobenzene ug/L 47.750 95 76-125 1,3-Dichloropropane ug/L 45.450 91 74-126 1,4-Dichlorobenzene ug/L 46.750 93 75-122 2,2-Dichloropropane ug/L 49.650 99 53-144 2-Butanone (MEK)ug/L 300250 120 47-189 2-Chlorotoluene ug/L 47.750 95 72-128 2-Hexanone ug/L 259250 104 57-167 4-Chlorotoluene ug/L 48.750 97 73-124 4-Methyl-2-pentanone (MIBK)ug/L 221250 88 61-135 Acetone ug/L 467 L325018730-170 Acrolein ug/L 10501000 105 30-170 Acrylonitrile ug/L 8481000 85 67-136 Benzene ug/L 47.150 94 78-127 Bromobenzene ug/L 41.750 83 62-139 Bromochloromethane ug/L 46.350 93 54-162 Bromodichloromethane ug/L 46.350 93 69-133 Bromoform ug/L 43.250 86 60-127 Bromomethane ug/L 91.8 L35018430-170 Carbon disulfide ug/L 99.0100 99 58-152 Carbon tetrachloride ug/L 51.350 103 62-143 Chlorobenzene ug/L 46.450 93 75-123 Chloroethane ug/L 72.050 144 56-153 Chloroform ug/L 45.250 90 74-131 Chloromethane ug/L 54.850 110 35-147 cis-1,2-Dichloroethene ug/L 50.250 100 74-128 cis-1,3-Dichloropropene ug/L 45.550 91 58-123 Dibromochloromethane ug/L 44.250 88 66-131 Dibromomethane ug/L 46.050 92 73-133 Dichlorodifluoromethane ug/L 87.4 L35017530-170 Ethyl methacrylate ug/L 178200 89 59-138 Ethylbenzene ug/L 44.550 89 81-126 Hexachloro-1,3-butadiene ug/L 50.750 101 70-130 Iodomethane ug/L 102100 102 41-170 Isopropylbenzene (Cumene)ug/L 42.950 86 80-130 Methyl-tert-butyl ether ug/L 83.4100 83 66-147 Methylene chloride ug/L 42.250 84 32-164 n-Butylbenzene ug/L 44.250 88 68-135 n-Hexane ug/L 49.050 98 69-157 n-Propylbenzene ug/L 46.350 93 71-132 Naphthalene ug/L 48.950 98 61-135 p-Isopropyltoluene ug/L 45.350 91 66-131 sec-Butylbenzene ug/L 45.250 90 73-130 Styrene ug/L 43.250 86 74-128 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 71 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474696LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/L 36.350 73 63-117 Tetrachloroethene ug/L 45.250 90 60-119 Toluene ug/L 46.550 93 75-129 trans-1,2-Dichloroethene ug/L 48.750 97 71-126 trans-1,3-Dichloropropene ug/L 43.950 88 54-123 trans-1,4-Dichloro-2-butene ug/L 153200 77 47-141 Trichloroethene ug/L 48.050 96 74-130 Trichlorofluoromethane ug/L 57.650 115 62-150 Vinyl acetate ug/L 127200 63 41-145 Vinyl chloride ug/L 62.250 124 55-141 Xylene (Total)ug/L 133150 89 76-132 4-Bromofluorobenzene (S)%96 70-126 Dibromofluoromethane (S)%104 80-123 Toluene-d8 (S)%98 80-116 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 72 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/26362 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:5040522039, 5040522041, 5040522042, 5040522044 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:474691 Associated Lab Samples:5040522039, 5040522041, 5040522042, 5040522044 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/31/10 12:51 1,1,1-Trichloroethane ug/kg ND 5.0 08/31/10 12:51 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/31/10 12:51 1,1,2-Trichloroethane ug/kg ND 5.0 08/31/10 12:51 1,1-Dichloroethane ug/kg ND 5.0 08/31/10 12:51 1,1-Dichloroethene ug/kg ND 5.0 08/31/10 12:51 1,1-Dichloropropene ug/kg ND 5.0 08/31/10 12:51 1,2,3-Trichlorobenzene ug/kg ND 5.0 08/31/10 12:51 1,2,3-Trichloropropane ug/kg ND 5.0 08/31/10 12:51 1,2,4-Trichlorobenzene ug/kg ND 5.0 08/31/10 12:51 1,2,4-Trimethylbenzene ug/kg ND 5.0 08/31/10 12:51 1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/31/10 12:51 1,2-Dichlorobenzene ug/kg ND 5.0 08/31/10 12:51 1,2-Dichloroethane ug/kg ND 5.0 08/31/10 12:51 1,2-Dichloropropane ug/kg ND 5.0 08/31/10 12:51 1,3,5-Trimethylbenzene ug/kg ND 5.0 08/31/10 12:51 1,3-Dichlorobenzene ug/kg ND 5.0 08/31/10 12:51 1,3-Dichloropropane ug/kg ND 5.0 08/31/10 12:51 1,4-Dichlorobenzene ug/kg ND 5.0 08/31/10 12:51 2,2-Dichloropropane ug/kg ND 5.0 08/31/10 12:51 2-Butanone (MEK)ug/kg ND 25.0 08/31/10 12:51 2-Chlorotoluene ug/kg ND 5.0 08/31/10 12:51 2-Hexanone ug/kg ND 100 08/31/10 12:51 4-Chlorotoluene ug/kg ND 5.0 08/31/10 12:51 4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 08/31/10 12:51 Acetone ug/kg ND 100 08/31/10 12:51 Acrolein ug/kg ND 100 08/31/10 12:51 Acrylonitrile ug/kg ND 100 08/31/10 12:51 Benzene ug/kg ND 5.0 08/31/10 12:51 Bromobenzene ug/kg ND 5.0 08/31/10 12:51 Bromochloromethane ug/kg ND 5.0 08/31/10 12:51 Bromodichloromethane ug/kg ND 5.0 08/31/10 12:51 Bromoform ug/kg ND 5.0 08/31/10 12:51 Bromomethane ug/kg ND 5.0 08/31/10 12:51 Carbon disulfide ug/kg ND 10.0 08/31/10 12:51 Carbon tetrachloride ug/kg ND 5.0 08/31/10 12:51 Chlorobenzene ug/kg ND 5.0 08/31/10 12:51 Chloroethane ug/kg ND 5.0 08/31/10 12:51 Chloroform ug/kg ND 5.0 08/31/10 12:51 Chloromethane ug/kg ND 5.0 08/31/10 12:51 cis-1,2-Dichloroethene ug/kg ND 5.0 08/31/10 12:51 cis-1,3-Dichloropropene ug/kg ND 5.0 08/31/10 12:51 Dibromochloromethane ug/kg ND 5.0 08/31/10 12:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 73 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:474691 Associated Lab Samples:5040522039, 5040522041, 5040522042, 5040522044 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 08/31/10 12:51 Dichlorodifluoromethane ug/kg ND 5.0 08/31/10 12:51 Ethyl methacrylate ug/kg ND 10.0 08/31/10 12:51 Ethylbenzene ug/kg ND 5.0 08/31/10 12:51 Hexachloro-1,3-butadiene ug/kg ND 5.0 08/31/10 12:51 Iodomethane ug/kg ND 100 08/31/10 12:51 Isopropylbenzene (Cumene)ug/kg ND 5.0 08/31/10 12:51 Methyl-tert-butyl ether ug/kg ND 5.0 08/31/10 12:51 Methylene chloride ug/kg ND 20.0 08/31/10 12:51 n-Butylbenzene ug/kg ND 5.0 08/31/10 12:51 n-Hexane ug/kg ND 5.0 08/31/10 12:51 n-Propylbenzene ug/kg ND 5.0 08/31/10 12:51 Naphthalene ug/kg ND 5.0 08/31/10 12:51 p-Isopropyltoluene ug/kg ND 5.0 08/31/10 12:51 sec-Butylbenzene ug/kg ND 5.0 08/31/10 12:51 Styrene ug/kg ND 5.0 08/31/10 12:51 tert-Butylbenzene ug/kg ND 5.0 08/31/10 12:51 Tetrachloroethene ug/kg ND 5.0 08/31/10 12:51 Toluene ug/kg ND 5.0 08/31/10 12:51 trans-1,2-Dichloroethene ug/kg ND 5.0 08/31/10 12:51 trans-1,3-Dichloropropene ug/kg ND 5.0 08/31/10 12:51 trans-1,4-Dichloro-2-butene ug/kg ND 100 08/31/10 12:51 Trichloroethene ug/kg ND 5.0 08/31/10 12:51 Trichlorofluoromethane ug/kg ND 5.0 08/31/10 12:51 Vinyl acetate ug/kg ND 100 08/31/10 12:51 Vinyl chloride ug/kg ND 5.0 08/31/10 12:51 Xylene (Total)ug/kg ND 10.0 08/31/10 12:51 4-Bromofluorobenzene (S)%97 61-131 08/31/10 12:51 Dibromofluoromethane (S)%97 80-124 08/31/10 12:51 Toluene-d8 (S)%106 58-145 08/31/10 12:51 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474692LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 45.050 90 65-124 1,1,1-Trichloroethane ug/kg 50.050 100 61-135 1,1,2,2-Tetrachloroethane ug/kg 45.750 91 66-124 1,1,2-Trichloroethane ug/kg 45.950 92 74-127 1,1-Dichloroethane ug/kg 45.750 91 62-132 1,1-Dichloroethene ug/kg 52.750 105 61-123 1,1-Dichloropropene ug/kg 49.950 100 74-128 1,2,3-Trichlorobenzene ug/kg 50.550 101 60-125 1,2,3-Trichloropropane ug/kg 86.0100 86 61-120 1,2,4-Trichlorobenzene ug/kg 48.750 97 58-126 1,2,4-Trimethylbenzene ug/kg 44.750 89 72-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 74 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474692LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dibromoethane (EDB)ug/kg 46.950 94 74-119 1,2-Dichlorobenzene ug/kg 46.750 93 75-117 1,2-Dichloroethane ug/kg 46.850 94 62-135 1,2-Dichloropropane ug/kg 45.550 91 74-124 1,3,5-Trimethylbenzene ug/kg 44.950 90 73-122 1,3-Dichlorobenzene ug/kg 47.750 95 73-120 1,3-Dichloropropane ug/kg 45.450 91 71-122 1,4-Dichlorobenzene ug/kg 46.750 93 72-118 2,2-Dichloropropane ug/kg 49.650 99 53-136 2-Butanone (MEK)ug/kg 300250 120 33-190 2-Chlorotoluene ug/kg 47.750 95 72-122 2-Hexanone ug/kg 259250 104 44-168 4-Chlorotoluene ug/kg 48.750 97 72-120 4-Methyl-2-pentanone (MIBK)ug/kg 221250 88 58-126 Acetone ug/kg 467250 187 30-190 Acrolein ug/kg 10501000 105 30-190 Acrylonitrile ug/kg 8481000 85 65-129 Benzene ug/kg 47.150 94 76-123 Bromobenzene ug/kg 41.750 83 74-116 Bromochloromethane ug/kg 46.350 93 56-143 Bromodichloromethane ug/kg 46.350 93 67-123 Bromoform ug/kg 43.250 86 58-117 Bromomethane ug/kg 91.8 L35018447-147 Carbon disulfide ug/kg 99.0100 99 56-141 Carbon tetrachloride ug/kg 51.350 103 54-136 Chlorobenzene ug/kg 46.450 93 75-115 Chloroethane ug/kg 72.050 144 57-147 Chloroform ug/kg 45.250 90 74-123 Chloromethane ug/kg 54.850 110 31-155 cis-1,2-Dichloroethene ug/kg 50.250 100 76-119 cis-1,3-Dichloropropene ug/kg 45.550 91 56-110 Dibromochloromethane ug/kg 44.250 88 63-122 Dibromomethane ug/kg 46.050 92 70-127 Dichlorodifluoromethane ug/kg 87.4 L35017530-170 Ethyl methacrylate ug/kg 178200 89 58-126 Ethylbenzene ug/kg 44.550 89 78-121 Hexachloro-1,3-butadiene ug/kg 50.750 101 65-128 Iodomethane ug/kg 102100 102 38-173 Isopropylbenzene (Cumene)ug/kg 42.950 86 75-128 Methyl-tert-butyl ether ug/kg 83.4100 83 59-142 Methylene chloride ug/kg 42.250 84 30-170 n-Butylbenzene ug/kg 44.250 88 70-123 n-Hexane ug/kg 49.050 98 76-143 n-Propylbenzene ug/kg 46.350 93 70-126 Naphthalene ug/kg 48.950 98 60-128 p-Isopropyltoluene ug/kg 45.350 91 65-125 sec-Butylbenzene ug/kg 45.250 90 72-125 Styrene ug/kg 43.250 86 75-118 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 75 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 474692LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 36.350 73 61-114 Tetrachloroethene ug/kg 45.250 90 63-117 Toluene ug/kg 46.550 93 72-123 trans-1,2-Dichloroethene ug/kg 48.750 97 70-122 trans-1,3-Dichloropropene ug/kg 43.950 88 55-107 trans-1,4-Dichloro-2-butene ug/kg 153200 77 49-127 Trichloroethene ug/kg 48.050 96 74-121 Trichlorofluoromethane ug/kg 57.650 115 55-156 Vinyl acetate ug/kg 127200 63 46-127 Vinyl chloride ug/kg 62.250 124 50-146 Xylene (Total)ug/kg 133150 89 77-120 4-Bromofluorobenzene (S)%96 61-131 Dibromofluoromethane (S)%104 80-124 Toluene-d8 (S)%98 58-145 Parameter Units MS Result % Rec Limits Qual% RecConc. 474693MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5040522039 474694 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/kg 42.9 104 20-133103 6 2040.6ND 44.5 41.9 1,1,1-Trichloroethane ug/kg 42.9 108 27-142107 6 2040.6ND 46.4 43.7 1,1,2,2-Tetrachloroethane ug/kg 42.9 104 20-159107 3 2040.6ND 44.8 43.5 1,1,2-Trichloroethane ug/kg 42.9 111 20-155110 6 2040.6ND 47.8 44.9 1,1-Dichloroethane ug/kg 42.9 103 31-141103 6 2040.6ND 44.2 41.7 1,1-Dichloroethene ug/kg 42.9 120 23-132119 6 2040.6ND 51.4 48.5 1,1-Dichloropropene ug/kg 42.9 105 20-146104 6 2040.6ND 44.9 42.2 1,2,3-Trichlorobenzene ug/kg 42.9 67 20-14050 34 2040.6ND 28.5 20.3 1,2,3-Trichloropropane ug/kg 85.8 90 20-15384 13 2081.4ND 77.6 68.4 1,2,4-Trichlorobenzene ug/kg 42.9 69 20-12052 34 2040.6ND 29.6 21.0 1,2,4-Trimethylbenzene ug/kg 42.9 91 20-15691 5 2040.6ND 40.3 38.4 1,2-Dibromoethane (EDB)ug/kg 42.9 104 20-14399 11 2040.6ND 44.6 40.1 1,2-Dichlorobenzene ug/kg 42.9 94 20-13383 19 2040.6ND 40.5 33.6 1,2-Dichloroethane ug/kg 42.9 102 30-143100 8 2040.6ND 43.8 40.6 1,2-Dichloropropane ug/kg 42.9 102 30-14098 9 2040.6ND 43.7 39.9 1,3,5-Trimethylbenzene ug/kg 42.9 95 20-14399 1 2040.6ND 40.8 40.4 1,3-Dichlorobenzene ug/kg 42.9 94 20-13683 17 2040.6ND 40.2 33.8 1,3-Dichloropropane ug/kg 42.9 106 30-14499 12 2040.6ND 45.5 40.4 1,4-Dichlorobenzene ug/kg 42.9 91 30-13576 24 2040.6ND 39.2 30.9 2,2-Dichloropropane ug/kg 42.9 110 30-143110 6 2040.6ND 47.3 44.6 2-Butanone (MEK)ug/kg 214 131 30-190123 12 20203ND280249 2-Chlorotoluene ug/kg 42.9 102 30-170101 6 2040.6ND 43.9 41.2 2-Hexanone ug/kg 214 114 30-170107 11 20203ND244217 4-Chlorotoluene ug/kg 42.9 105 30-143102 8 2040.6ND 45.0 41.6 4-Methyl-2-pentanone (MIBK)ug/kg 214 97 30-14497 5 20203ND207196 Acetone ug/kg M021422130-180208 11 20203ND474423 Acrolein ug/kg 858 103 30-180102 7 20814ND886826 Acrylonitrile ug/kg 858 85 30-14183 7 20814ND726678 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 76 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 Parameter Units MS Result % Rec Limits Qual% RecConc. 474693MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 5040522039 474694 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Benzene ug/kg 42.9 105 50-135100 10 2040.6ND 44.9 40.7 Bromobenzene ug/kg 42.9 85 30-12575 18 2040.6ND 36.4 30.4 Bromochloromethane ug/kg 42.9 105 30-159101 9 2040.6ND 45.0 41.0 Bromodichloromethane ug/kg 42.9 102 30-14198 9 2040.6ND 43.6 39.8 Bromoform ug/kg 42.9 97 30-13595 8 2040.6ND 41.7 38.5 Bromomethane ug/kg M042.9 148 30-137240 42 2040.6ND 63.6 97.7 Carbon disulfide ug/kg 85.8 92 30-15699 2 2081.4ND 78.9 80.2 Carbon tetrachloride ug/kg 42.9 109 30-130108 6 2040.6ND 47.0 44.1 Chlorobenzene ug/kg 42.9 99 30-13791 15 2040.6ND 42.6 36.8 Chloroethane ug/kg M042.9 160 35-143157 8 2040.6ND 68.8 63.7 Chloroform ug/kg 42.9 101 30-136100 7 2040.6ND 43.5 40.5 Chloromethane ug/kg 42.9 110 28-134115 1 2040.6ND 47.2 46.7 cis-1,2-Dichloroethene ug/kg 42.9 110 30-141105 10 2040.6ND 47.3 42.6 cis-1,3-Dichloropropene ug/kg 42.9 103 30-12697 12 2040.6ND 44.3 39.3 Dibromochloromethane ug/kg 42.9 100 30-12997 8 2040.6ND 42.8 39.5 Dibromomethane ug/kg 42.9 100 30-15395 10 2040.6ND 42.8 38.5 Dichlorodifluoromethane ug/kg 2d,M042.9 177 30-150177 5 2040.6ND 75.8 72.0 Ethyl methacrylate ug/kg 172 71 30-17071 6 20163ND123116 Ethylbenzene ug/kg 42.9 95 50-15092 8 2040.6ND 40.7 37.4 Hexachloro-1,3-butadiene ug/kg 42.9 57 30-13860 .08 2040.6ND 24.4 24.4 Iodomethane ug/kg 85.8 111 30-180115 2 2081.4ND 95.3 93.2 Isopropylbenzene (Cumene)ug/kg 42.9 89 50-15091 2 2040.6ND 38.0 37.1 Methyl-tert-butyl ether ug/kg 85.8 94 40-14995 4 2081.4ND 80.3 77.1 Methylene chloride ug/kg 42.9 97 30-16393 10 2040.6ND 41.7 37.9 n-Butylbenzene ug/kg 42.9 76 40-15279 1 2040.6ND 32.6 32.2 n-Hexane ug/kg 42.9 107 40-155106 6 2040.6ND 46.0 43.2 n-Propylbenzene ug/kg 42.9 97 40-170100 2 2040.6ND 41.5 40.6 Naphthalene ug/kg 42.9 74 50-12854 34 2040.6ND 33.7 24.0 p-Isopropyltoluene ug/kg 42.9 86 40-16791 .02 2040.6ND 36.8 36.8 sec-Butylbenzene ug/kg 42.9 89 40-16896 2 2040.6ND 38.1 38.9 Styrene ug/kg 42.9 89 30-14179 17 2040.6ND 38.0 32.2 tert-Butylbenzene ug/kg 42.9 76 40-14481 1 2040.6ND 32.7 33.1 Tetrachloroethene ug/kg 42.9 95 40-15597 4 2040.6ND 40.8 39.3 Toluene ug/kg 42.9 107 50-149104 8 2040.6ND 46.0 42.3 trans-1,2-Dichloroethene ug/kg 42.9 106 40-140103 9 2040.6ND 45.6 41.8 trans-1,3-Dichloropropene ug/kg 42.9 96 40-13086 17 2040.6ND 41.4 35.1 trans-1,4-Dichloro-2-butene ug/kg 172 75 30-15064 21 20163ND129105 Trichloroethene ug/kg 42.9 99 40-15397 8 2040.6ND 42.5 39.4 Trichlorofluoromethane ug/kg 42.9 123 43-140121 8 2040.6ND 52.8 49.0 Vinyl acetate ug/kg M01721230-12020 20163NDNDND Vinyl chloride ug/kg 42.9 130 36-137132 3 2040.6ND 55.7 53.8 Xylene (Total)ug/kg 128 95 50-14393 8 20122ND122113 4-Bromofluorobenzene (S)%91 61-13192 20 Dibromofluoromethane (S)%101 80-124102 20 Toluene-d8 (S)%104 58-145105 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 77 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/4970 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5040522001, 5040522002, 5040522003, 5040522004, 5040522005, 5040522006, 5040522007, 5040522008, 5040522009, 5040522010, 5040522011, 5040522013, 5040522014 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040516021 470690SAMPLE DUPLICATE: Percent Moisture %19.9 .6 520.0 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040522001 470691SAMPLE DUPLICATE: Percent Moisture %5.6 R21756.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 78 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/4971 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5040522015, 5040522016, 5040522017, 5040522018, 5040522019, 5040522020, 5040522021, 5040522022, 5040522023, 5040522024, 5040522025, 5040522026, 5040522027, 5040522028, 5040522029, 5040522030, 5040522031, 5040522033, 5040522034, 5040522035 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040522015 470693SAMPLE DUPLICATE: Percent Moisture %8.6 5 58.2 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040522033 470694SAMPLE DUPLICATE: Percent Moisture %7.5 R21756.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 79 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/4972 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5040522036, 5040522037, 5040522038, 5040522039, 5040522040, 5040522041, 5040522042, 5040522043, 5040522044, 5040522045, 5040522046, 5040522049, 5040522050, 5040522051, 5040522052 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040522036 470695SAMPLE DUPLICATE: Percent Moisture %7.3 R2956.7 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040522039 470696SAMPLE DUPLICATE: Percent Moisture %6.7 R21858.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 80 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALITY CONTROL DATA Pace Project No.: Project: 5040522 SBI060 QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/4973 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:5040522012 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040569001 471229SAMPLE DUPLICATE: Percent Moisture %8.9 1 58.8 Parameter Units Dup Result Max RPD QualifiersRPDResult 5040523012 471230SAMPLE DUPLICATE: Percent Moisture %11.2 5 510.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 81 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894 QUALIFIERS Pace Project No.: Project: 5040522 SBI060 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS Compound ND at an estimated RL of 34 ug/kg, based on the MDL. JLF 9/1/10.1d Multiple compounds are outside acceptance limits due to sample matrix. Refer to LCS for system control and data acceptability. JLF 09/01/10.2d The surrogate recovery exceeds the upper limit due to significant contribution from the target analyte. 08/25/10 EDD3d The surrogate recovery exceeds the upper limit due to significant contribution from the target analyte. 08/26/10 EDD4d Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the spike level.P6 RPD value was outside control limits.R1 RPD value was outside control limits due to matrix interferenceR2 Surrogate recovery not evaluated against control limits due to sample dilution.S4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/02/2010 11:51 AM Page 82 of 82 Pace Analytical Services, Inc. 7726 Moller Road Indianapolis, IN 46268 (317)875-5894