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HomeMy WebLinkAboutSB-0213 1992 EIS Summary Report re 814 818 Lafayette18 ENVIRONMENTAL ENGINEERS INC LIS ENYmONMENTAL ENGINEERS NC SUMMARY REPORT SOIL DRYWELL AND WASTE SAMPLING AND ANALYSIS AND EXCAVATION AND DISPOSAL OF SOIL 81 4/818 SOUTH LAFAYEUE BOULEVARD SOUTH BEND INDIANA FEBRUARY 1996 PREPARED FOR CITY OF SOUTH BEND DEPARTMENT OF COMMUNITY AND ECONOMIC DEVELOPMENT PREPARED BY EIS ENVIRONMENTAL ENGINEERS INC 1701 NORTH IRONWOOD DRIVE SOUTH BEND INDIANA 46635 J.C Sporleder C.P.G Stephen P.E Project Geologist President David Jeffers Project Geologist I45696JPTI\%O-% EXECUTIVE SUMMARY EIS Environmental Engineers Inc EIS of South Bend Indiana collected and analyzed samples of soil and drywells and excavated and disposed of soil from the Site located at 814/818 South Lafayette Boulevard South Bend Indiana This work addressed conditions identified in the EIS Phase Environmental Assessment for the Site dated September 22 1995 and was performed during the period of October 10 1995 through January 1996 The following summarizes the work and results Sediment from two drywells located on the east side of the Site were sampled for Volatile Organic Compounds VOC Naphthalene Toluene and Xylene were detected in each drywell However the concentration levels detected were below Indiana Department of Environmental Management IDEM Voluntary Cleanup Program VCP cleanup goals for soil from non residential site and were also below U.S Environmental Protection Agency USEPA Maximum Contaminant Levels MCL for drinking water Stained soil from two areas on the east side of the site were delineated characterized by laboratory analysis excavated and disposed at the Prairie View landfill Laboratory analysis of clearance samples collected from below the stained soil detected VOC TPH Cadmium Chromium and Lead With the exception of Toluene at one location the concentrations of VOC and TPH were below established IDEM VCP cleanup goals for soil or groundwater from non-residential site and also below USEPA MCLs for drinking water The Toluene concentration in soil at one clearance location did exceed the USEPA drinking water MCL The level of Toluene detected probably would be incapable of leaching to the groundwater in sufficient concentration to actually exceed the USEPA drinking water MCL and also did not exceed IDEM VCP cleanup goals for groundwater at non-residential site The concentrations of the Metals detected in the clearance samples did not exceed either the background mean or the background mean plus three times the standard deviation Therefore the clearance sample data indicates that the remediation with respect to the stained soil has been successfully completed 145696\RPTI\9601-96 It is noted that both the clearance and background soil sample results indicated Metal concentrations that if leached to the groundwater might be capable of exceeding established USEPA drinking water MCLs for Cadmium and Chromium and the action level for Lead The IDEM has not established VCP cleanup goal for Lead in soil however the levels of Cadmium and Chromium in soil at the Site do not exceed the IDEM VCP cleanup goals for soil at nonresidential site Also the seriousness of possible adverse impact on the groundwater at the Site would be somewhat mitigated by the availability of city water to the property and surrounding properties l45696RVfl\96Ol96 TABLE OF CONTENTS SECTION PAGE 1.0 INTRODUCTION 2.0 DRY WELL SAMPLING AND ANALYTICAL RESULTS 2.1 Drywell Sampling 2.2 Drywell Sample Analytical Results 3.0 STAINED SOIL SAMPLING ANALYSES EXCAVATION AND REMOVAL 3.1 Soil Sampling for Waste Characterization and Landfill Permitting 3.2 Soil Excavation and Landfill Disposal 4.0 SOIL CLEARANCE AND BACKGROUND SAMPLING AND ANALYTICAL RESULTS 4.1 Soil Clearance Sampling 4.2 Soil Background Sampling 4.3 Soil Clearance and Background Analytical Results TABLES TABLE PAGE 2.1 Summary of Analytical Results Dry Well Samples 4.1 Summary of Analytical Results for Volatile Organic Compounds Soil Clearance Samples 4.2 Summary of Analytical Results for Metals Soil Clearance and Background Samples 145696\RPTI\9601.96 jjj APPENDICES APPENDIX Analytical Results Original Chain-of-Custody Records Soil Sample Logs and Site Sketch showing sample locations Indiana Department of Environmental Management IDEM Special Waste Certification Application IDEM Special Waste Disposal Certification Disposal application material mailed to Prairie View landfill Letter documenting approval to dispose soil at Prairie View landfill Statement of Origin documenting the transport of excavated soil from the Site for disposal at the Prairie View landfill 145696\RPTI\9601-96 iv 1.0 INTRODUCTION On September 11 1995 EIS Environmental Engineers Inc EIS performed Phase Environmental Site Assessment at the former Miller Paint facility located at 814/818 South Lafayette Boulevard South Bend Indiana the Site The assessment report submitted September 22 1995 indicated the following conditions of concern Two drywells located on the rear east portion of the property Stained soil and residue located on the rear east portion of the property which appeared to be associated with paint materials that were used at the property In letter dated October 1995 EIS proposed that the sediment within the drywells be sampled and analyzed that the stained soil be excavated and disposed at landfill and that soil clearance background and waste characterization samples be collected and analyzed The November 1995 letter authorizing EIS to proceed was issued by Joelle Webb of the South Bend Department of Community and Economic Development During the period of October 10 1995 through January 1996 EIS performed the sampling and analyses applied for and received the required disposal permits and excavated and disposed of soil in accordance with the October 1995 proposal The following sections of this report provide summary of this work and the results l45696\RPT1\9Jl-96 2.0 DRY WELL SAMPLING AND ANALYTICAL RESULTS 2.1 Drywell Samrling The two drywell structures located on the rear east portion of the property were sampled by EIS on October 10 1995 The samples DW-1 and DW-2 consisted of sediment collected with bucket dredge from the bottom of each drywell The sample depths for drywells DW-1 and DW-2 were about seven and five feet below grade respectively The samples were submitted to the EIS laboratory for Volatile Organic Compound VOC analyses Details regarding the sample collections and locations were recorded on Sample Log and Site Sketch provided in Appendix 2.2 Drywell Sample Analytical Results The complete analytical reports for the drywell samples are provided in Appendix These results are summarized in Table 2.1 Naphthalene Toluene and Xylene were detected in the sediments collected from drywells However the detected concentrations were below established U.S Environmental Protection Agency USEPA maximum contaminant levels MCL for drinking water and below the Indiana Department of Environmental Management IDEM Voluntary Cleanup Program VCP Tier II cleanup goals for subsurface soils at non-residential sites Corresponding USEPA Drinking Water MCLs and IDEM VCP cleanup goals are provided in Table 2.1 for comparison purposes 145696\RPTI\960196 TABLE 2.1 ANALYTICAL RESULT SUMMARY DRY WELL SAMPLES USEPA Results ppm IDEM VCP DWS Cleanup Goals2 MCL3 Parameter DW-1 DW-2 ppm ppm Naphthalene 0.094 10000.00 NE5 Toluene 0.054 017 1000.00 Xylene Total 0063 0.19 1000.00 10 Notes Drywell samples DW-1 and DW-2 were collected October 10 1995 from the Site located at 814/818 South Lafayette Boulevard South Bend Indiana IDEM VCP Cleanup Goals Indiana Department of Environmental Management Voluntary Cleanup Program Tier II Cleanup Goals for Subsurface Soils Non residential Scenario February 1994 USEPA DWS MCL U.S Environmental Protection Agency Drinking Water Standard Maximum Contaminant Level May 1995 Detected but below Estimated Quantitation Limit and the result shown is an estimate NE USEPA DWS MCL has not been established 145696\RPTI\9601-96 3.0 STAINED SOIL SAMPLING ANALYSES EXCAVATION AND REMOVAL 3.1 Soil Sampling for Waste Characterization and Landfill Permitting Two separate areas of paint stained and discolored soil were observed along the east side of the Site An EIS geologist probed the stained areas with hand auger in order to delineate on visual and odor basis the vertical and lateral extent of the stained soil The first area covered approximately 81 square feet and was located near the north edge of the Site The second area covered approximately 35 square feet and was located near an east door for the on-site building The depth of staining in both areas was found to be about 0.75 to 1.5 feet below grade Soil samples were collected from three locations SC-I SC-2 and SC-3 within the larger stained area and from two locations SC-4 and SC-5 from the smaller area Both waste characterization and soil clearance samples were collected from these five locations The locations of the stained soil areas and sample locations are shown on site sketch provided in Appendix Stained soil for waste characterization analyses was collected on October 10 1995 with hand-auger from the stained interval at each of the five locations The stained soil was composited into single sample WC-1 and submitted to the EIS laboratory for waste characterization parameters for landfill disposal purposes An additional waste characterization sample WC-2 for PCB analysis for landfill disposal purposes was collected on November 16 1995 from locations adjacent to and from the same intervals as the October 10 1995 samples The complete analytical reports for the waste characterization samples are provided in Appendix These results were used to apply to IDEM for Special Waste Certification and to complete Generators Waste Profile Sheet in order to obtain permission to dispose the stained soil at the Prairie View landfill in Wyatt Indiana The Special Waste Certification Application and application fee was completed by EIS and mailed to IDEM on November 30 1995 EIS received the Special Waste Certification 145696\RPTI\9601-96 No 51083 from IDEM on January 1995 copy of the Certification is provided in Appendix Generators Waste Profile Sheet Service Agreement Waste Characterization Sample Logs and other documents required to obtain landfill approval for disposal were submitted by EIS to the Prairie View landfill on January 1996 copy of the information provided to Prairie View landfill is included in Appendix Prairie View landfill approved the disposal of soil on January 1995 letter documenting the approval to dispose is provided in Appendix 3.2 Soil Excavation and Landfill Disposal Both areas of stained soil were excavated on January 1996 The excavated soil was placed directly into truck and immediately transported to the Prairie View landfill for disposal An EIS geologist observed the excavation of all visually stained soil The resulting excavations were approximately two feet deep and were backfilled with clean sand copy of the Statement of Origin documenting the transport of excavated soil from the Site for disposal at the Prairie View landfill is provided in Appendix I4696\RVfl\9oOI.96 4.0 SOIL CLEARANCE AND BACKGROUND SAMPLING AND ANALYTICAL RESULTS 4.1 Soil Clearance Sampling As indicated in Section 3.0 soil clearance samples SC-i SC-2 SC-3 SC-4 and SC-5 were collected from five locations from two areas of stained surficial soil The clearance samples were collected from depths ranging from 1.0 to 1.5 feet below grade from unstained soils that were located immediately below the stained soil These samples were collected with hand-auger by ElS on October 10 1995 and were submitted to the EIS laboratory for VOC and Metals Total Cadmium Total Chromium and Total Lead analyses Details regarding the sample collections and locations were recorded on Sample Log and Site Sketch provided in Appendix 4.2 Soil Background Sampling EIS collected four background soil samples using hand-auger BC-i BG-2 BG-3 and BC-4 from the Site on October 10 1995 These samples were collected from an area of the Site that did not appear to have been covered by stained soil and were collected from the same soil type and at approximately the same depth as the soil clearance samples The purpose of the background samples were to obtain data regarding background metals concentrations for comparison with the clearance sample results These samples were submitted to the EIS laboratory for Metals analyses Details regarding the sample collections and locations were recorded on Sample Log and Site Sketch provided in Appendix 4.3 Soil Clearance and Background Analytical Results The complete analytical reports for the soil clearance and background samples are provided in Appendix The VOC results for the clearance samples are summarized in Table 4.1 The Metals results for the soil clearance and background samples are provided in Table 4.2 145696\RPTI\9601-96 Ca 0__9 88 Co uj ui ad Co Ca UJ C- 10 U.4 Ui Ui C-i CO Ca0E4 -to 1ow -Jo Ca Uic.Q ECOZZZZZZZZZ w_______Cot .C uJ Co t-ca0W0 aicaat CCa- II- _- Ca CO 00 Ca C-0Oacaiaz51 oWwauJ-o CO --U_CaDZZ_.Ui 5- Ca 01- TABLE 4.2 ANALYTICAL RESULT SUMMARY FOR METALS SOIL CLEARANCE AND BACKGROUND SAMPLES1 Clearance Soil Sample Results ppm Parameter SC-i SC-2 SC-3 SC-4 SC-5 Cadmium Total 1.0 1.0 1.7 1.0 1.0 Chromium Total 23.7 17.3 27.0 15.7 18.0 Lead Total 410 170 810 180 190 Background Soil Results ppm Parameter BG-i BG-2 BG-3 BG-4 Mean SD2 Mean 3xSD Cadmium Total 1.9 5.8 4.9 1.6 3.55 2.11 9.89 Chromium Total 41.4 60.6 34.4 30.0 41.6 13.51 82.13 Lead Total 160 470 580 320 382.5 182.64 930.4 Notes Soil clearance and background samples collected October 10 1995 from Site located at 814/818 South Lafayette Boulevard South Bend Indiana SD Standard Deviation Mean 3xSD Background mean plus three times the standard deviation 145696\RPTI\9601-96 As indicated in Table 4.1 several VOC and Total Petroleum Hydrocarbon TPH were detected at one or more clearance sample locations However it is noted that with the exception of Toluene at sample SC-i all detected VOC were at concentrations below IDEM VCP cleanup goals for soil or groundwater for non-residential site and also below USEPA drinking water MCLs Toluene detected at i.6 ppm at sample SC-i exceeded the USEPA drinking water MCL of i.0 ppm However it is unlikely that the Toluene in the soil at location SC-i would be capable at the concentration detected of leaching to the groundwater in sufficient quantities to actually exceed the drinking water MCL It should also be noted that the Toluene concentration detected at sample SC-i is below the IDEM VCP cleanup goal for groundwater at non-residential site TPH was detected at two clearance sample locations 20 ppm at SC-i and i8 ppm at SC-3 However the TPH concentrations detected are below the iOO ppm level generally used by IDEM as cleanup goal for TPH in soil Table 4.2 summarizes the Metals results for the soil clearance and background samples The background samples were required to obtain concentration of Metals in soils from areas at the Site that had not been impacted by the surface staining in order to evaluate the clearance sample results The mean standard deviation and the mean plus three times the standard deviation for the background results are provided in Table 4.2 Comparison of the clearance samples with the background data indicates the following All clearance sample results for Total Cadmium and Total Chromium are less than the background mean The clearance sample results for Total Lead are less than the background mean for samples SC-2 SC-4 and SC-5 145696RPTI\%ffl-96 The clearance sample results for Total Lead are greater than the background mean for samples SC-i and SC-3 However these results are not greater than the background mean plus three times the standard deviation suggesting that the clearance samples do not significantly exceed the background mean The above evaluation indicates that the remediation with respect to the stained soil has been successfully completed However it should be noted that both the clearance and background soil samples indicated metals concentrations that if leached to the groundwater might be capable of exceeding established USEPA drinking water MCLs of 0.005 ppm for Cadmium and 0.1 ppm for Chromium and the action level of 0.015 ppm for Lead However the levels of Cadmium and Chromium in the soil at the Site do not exceed the IDEM VCP cleanup goals for soil at non-residential site Also the seriousness of possible adverse impact on the groundwater at the Site would be somewhat mitigated by the availability of city water to the property and surrounding properties I45696\RPTI\96OI6 10 APPENDIX ANALYTICAL RESULTS ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29704 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID WC1 812/818 South Lafayette Composite Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To QUALITY CONTROL TEST RSDSPIKE MS DM5 IWO PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Ash percent 92.6 10-17-95 PovlockP Corrosivity pH SI 6.8 10-30-95 WrightC CyanideTotal rng/kgwet 10-20-95 WrhtC Flash Point Open Cup fahrenheit 201 10-31-95 WrightC Paint Fifter Liquids liquid NONE 10- 12-95 WrightC Solids Total percent 95.4 10- 16-95 PovlockP SulfideTotal mgikgwet 10-20-95 WrightC ArsenicTCLP mg/I 0.1 0.1 10-24-95 ClearN BariumTCLP mg/I 0.96 0.01 10-24-95 ClearN CadmiumTCLP mg/I 0.01 0.01 10-24-95 ClearN ChromiumTCLP mg/I 0.21 0.01 10-24-95 ClearN LeadTCLP mg/I 0.30 0.05 10-24-95 ClearN 0.40 90 90 MercuryTCLP mg/I 0.002 0.002 10-25-95 ShaneD SeleniumTCLP mg/I 0.05 0.05 10-24-95 ClearN SilverTCLP mg/I 0.01 0.01 10-24-95 ClearN HerbicidesTCLP 0-30-95 ClearB PesticidesTCLP 0-26-95 ClearB SVOCTCLP 10-27-95 GeelsS VOCTCLP 10-27-95 MyersN See Attached TCLP ORGANICS REPORT QURCER ATORYDIECT 2001 Re 5-04-94 Reded Peoe EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Orive South Bend Indiana 46635 2191277-5715 ANALYTICAL REPORT Client Report Date 11-27-95 Mr John Stark EIS Lab No 30671 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Pnority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID WC-2 Composite Sample Of Stained Soil Date Sampled 11-17-95 Date Received 11-17-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST PCB mg/kgwet 0.9 0.9 11-22-95 ClearB Extract PCB 11-20-95 ThompsonG ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations hASSOFFIcER dATORYDIEcT 2001 Rev 5-04-94 RevcI Peper EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 EIS Lab No 29704continued TEST PARAMETER UNITS RESULT DATE ANALYST Herbicide ExtractionTCLP 0-1 9-95 ThompsonG Mercury DigestionTCLP 0-24-95 Shane.D Metals Digestion ICPTCLP 10-13-95 ShaneD Pesticide ExtractionTCLP 10-19-95 ThompsonG SVOC ExtractionTCLP 10-19-95 ThompsonG TCLP Extract Formation Extraction Started 10-12-95 WrightC Extraction Completed 10-13-95 WrightC Solids Content percent 100 Sample Weight Extracted grams 150.0 Fiiter Used Whatman type GFF Initial pH SU 6.9 pH After Acid Addition SU 1.7 Extraction Fluid Used number Extraction Fluid Amount ml 3000 Extraction Fluid pH SU 4.89 Final Extract pH 8hrs SU 5.3 TCLP Extract Formation ZHE Extraction Started 10-24-95 NyeD Extraction Completed 0-25-95 NyeD Solids Content percent 100 Sample Weight Extracted grams 10.0 Fifter Used Whatmari type GF/F Extraction Fluid Used number Extraction Fluid Amount ml 200 Extraction Fluid pH SU 4.90 ADDITIONAL INFORMATION Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations Quality Control defintions are as follows %RSD Precision of replicate analysis for this sample Spike Level Parameter Spike amount in units of the result %R Matrix SpikeMS/Duplicate Matrix SpikeDMS recovery %RPD Precision of Matrix Spike recovery values Inorganic Qualty Control limits are enclosed CONCLUSION This sample is satisfactory wth respect to the analysis performed 2001 Rev 5-04-94 Recycled Papec TCLP ORGANICS REPORT SZ41LE ID NC-i REPORT DATE 11/13/95 812/818 South Lafayette Composite ZIS LAB NO 29704 --mg/i- VOLATILE ORGANICS RESULT Benzene ND 0.02 Carbon Tetrachloride ND 0.02 Chlorobenzene ND 02 Chloroform ND 0.02 4Dichlorobenzene ND 0.02 2-Dichloroethane ND 0.02 1i-Dichloroethylene ND 0.02 Methyl Ethyl Ketone ND 0.2 Tetrachloroethylene ND 0.02 Trichloroethylene ND 0.02 Vinyl Chloride ND 0.1 SEMI-VOLATILE ORGANICS o-Creaol ND 0.3 m-Cresol ND 0.1 p-Cresol ND 0.1 Total Cresols ND 0.3 24-Dinitrotoluene ND 0.1 Hexachlorobenzene ND 0.1 Rexachloro-1 3-butadiene ND 0.1 Hexachloroethane ND 0.1 Nitrobenzene ND 0.1 Pentachlorophenol ND 1.0 Pyridin ND 0.1 245-Trichlorophenol ND 1.0 246-Trichloropheno ND 0.1 PESTICIDES and HERBICIDES Chlordane ND 0.02 Endrin ND 0.001 Heptachlor and its epoxides ND 0.001 Lindane ND 0.001 Methoxychlor ND 0.001 Toxaphene ND 0.03 24D ND 0.03.3 245-TPSilvex ND 0.01 NOTES ND Not Detected at the EQL shown EQL Estimated Quantitation Limit Detection Limit Lab Form 2030 Reread 02-16-95 Reqrclad Paper ei ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29705 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client PO 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID DW-1 Drywell Sediment Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DATE ANALYST Moisture percent 26 10-16-95 SzkarlatM VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract voc 10-16-95 WilliamsJ ADDtTIONAL INFORMATION Chain-of-Custody document is enclosed Sample was ed upon receipt Batch Quality Control data is enclosed This data was generated at the time that this sample was analyzed but was performed on different sample QUA TY ASSURANC FICER LABORATORY DIRECT 2OO Rev 5-04-94 Recyclod Papec EJS ENVJRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 2191277-5715 SAMPLE ID DW-i REPORT DATE 11/13/95 Drywell Sedinent EIS LAB NO 29705 VOLATILE ORGPiNIC COMPOUNDS/PETROLEUM HYDROCARBONS Analyail Method 8021 Abreviationa and report Sample Dilution None aymbol are explained Reporting Unite ppm on the following page EQL Multiplier CCMPOUND NAME RESULT C4POUND NAME RESULT Acetone ND 0.5 t-l3-DiChlOrOpropene ND 0.10 Benzene ND 0.05 Diethyl Ether ND 0.50 Bromob.nzen ND 0.05 Ethylbenzene ND 0.05 Brcmochloromethana ND 0.05 Hezachlorobutadiene ND 0.10 Brodichloromethane ND 0.05 2-Hexanone ND 0.50 Bromoform ND 0.10 Isopropyl Benzene ND 0.10HrethanND0.25 p-Isopropyltoluene ND 0.10 n-Butyl Beflzan ND 0.10 Methylene Chloride ND 0.10 a.c-Butyl Ransena ND 0.10 Methyl Ethyl Ketone ND 0.50 tert-Butyl Benzne ND 0.10 Methyl Isobutyl Ketone ND 0.50 Carbon Tetrachlorida ND 0.10 Naphthalen 0.051 0.10 Chlorobenzene ND 0.05 n-Propyl Benzene ND 0.05 Chlorod.ibromomethane ND 0.05 Styrene ND 0.05 Chloroethzn ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 1112Tetrachloroethane ND 0.10 i-Chlorohexane ND 0.10 1122Tetrachloroethane ND 0.05 Chloroeethan ND 0.25 Tetrachloroethene ND 0.05 2-Chlorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4-Chlorotolu.n ND 0.05 Toluene 0.054 0.05 12-Dibromoethan ND 0.05 123-Trichlorobenzene ND 0.05 12-Dichlorabenzen ND 0.10 124-Trichlorobenzen ND 0.05 i3-Dichlorobenzen ND 0.10 1l1-Trichloroethan ND 0.05 14-Dichlorobenzens ND 0.10 1l2-Trichloroethane ND 0.05 Dichlorodifluoroanethan ND 0.25 Trjchloroethene ND 0.05 l-Dichlorothane ND 05 Trichlorofluoromethane ND .10 l2Dichloroethane ND 0.05 i23-Trichloropropane ND 0.25 l1-Dichloroethene ND 0.10 i12_TCTFE ND 0.10 c-12-Dichloroethene ND 0.05 l24-Triinethylbenzene ND 0.10 t-12Dichloroethene ND 0.05 l35-Trimethylbenzene ND 0.10 12-Dichloropropane ND 0.05 vinyl Chloride ND 0.10 13-Dichloropropan ND 0.10 mpxylenes 0.063 0.05 1i-Dichloropropene ND 0.10 o-lene ND 0.05 c-i 3-Dichloropropene ND 0.10 PETROLEUM HDROCABBONS PH ND 10 Lab Form 2025 Rsa.d 06-16.96 .pecl.d Paper SNPLE ID D1I-1 REPORT DATE 11/13/95 Drywell Sediment EIS IJ.B NO 29705 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Page of SURROGATE RECOVERT Method 8021 Compound Name QC Limits Recovery 12Dichloroethaned4 70 145 118 24-Dichlorotoluene 60 125 122 Toluened8 90 120 105 DEFINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected NA Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier EIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound 112-ICTFE is 112-Trichloro122-trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab Form 2025 Reabed 0695 Recyded Paper ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29706 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID DW-2 Drywell Sediment Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DATE ANALYST Moisture percent 32 10-16-95 SzkarlatM VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Sample was loed upon receipt Batch organicj Quality Control data is enclosed This data was generated at the time that this sample was analyzed but was performed on different sample AL ASS ANCE FICER LABORATORY DIRECTOR 2001 Rev 5-04-94 Recycled PaPer EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 SAMPLE ID DW-2 REPORT DATE 11/13/95 Drywell Sediment SIS LAB NO 29706 VOLATILE ORGANIC COMPOUNDS/PETROLEUZ4 HYDROCANBONS Analysia Method 8021 Ahbreviationa and report Sample Dilution None aymbola are explained Reporting Unite ppm on the following page EQL Multiplier COMPOUND NAME RESULT COMPOUND NAME RESULT Acaton ND 0.5 t-13-Dichloropropene ND 0.10 Renz.ns MD 0.05 Diethyl Ether ND 0.50 Brcaeobenzns ND 0.05 Ethylhenzene ND 0.05 Bromochioromethane ND 0.05 Hexachlorobutadiene ND 0.10 Brcmodichloromethane ND 0.05 2-Rexanone ND 0.50 Bromoform ND 0.10 Isopropyl Benzene ND 0.10 Bromomethan ND 0.25 p-Ieopropyltoluane ND 0.10 n-Butyl Benrene ND 0.10 Methylene Chloride ND 0.10 aec-Butyl Benzen ND 0.10 Methyl Ethyl Ketone ND 0.50 tert-Butyl Benzen ND 0.10 Methyl Isobutyl Ketone ND 0.50 Carbon Tetrachloride ND 0.10 Naphthalene 0.094 0.10 Chlorobenzene ND 0.05 n-Propyl Benzen ND 0.05 Chlorodibromomethane ND 0.05 Styrene ND 0.05 Chloroethane ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 l112Tetrachloroethane ND 0.10 1-Chlorohexane ND 0.10 1122-Tetrachloroethane ND 0.05 Chloromethan ND 0.25 Tetrachioroethene ND 0.05 2-Clilorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4-Chlorotoluene ND 0.05 Toluene 0.17 0.05 12-Dibromoethane ND 0.05 123-Trichlorobenzene ND 0.05 12-Dichlorobenzene ND 0.10 l24-Trichlorobenzene ND 0.05 13-Dichlorobenzene ND 0.10 111-Trichloroethane ND 0.05 14-Dichlorobenzene ND 0.10 112-Trichloroethane ND 0.05 Dichlorodifluoromethane ND 0.25 Tric1iloroethene ND 0.05 11-Dichloroethane ND 0.05 Trichlorofluoromathane ND 0.10 12-Dichlorothane ND 0.05 123-Trichloropropane ND 0.25 11-Dichloroathene ND 0.10 112_TCTFE ND 0.10 c-12-Dichloroethene ND 0.05 124-Trimethylbenzene ND 0.10 t-12-Dichloroethene ND 0.05 135-Trimethylbenzene ND 0.10 12-Dichloropropane ND 0.05 vinyl Chloride ND 0.10 13-Dichloropropane ND 0.10 mp-xylenes 0.14 0.05 11-Dichloropropene ND 0.10 o-xylene 0.050 0.05 c-i 3-Dichloropropene ND 0.10 PETROLEUM HYDROCARBONS PH ND 10 Lab Form 2025 R.aed 06-15.55 Req.cled Paper SAMPLE ID DW2 REPORT DATE 11/13/95 Drywall Sediment EIS LAB NO 29706 VOLATILE ORG.NIC COMPOUNDS/PETROLEUM HYDROCZRBONS Page of SURROGATE PECOVERI Method 8021 Compound Name QC Limits Pa Recovery 12-Dichloroathaned4 70 145 119 24-Dichlorotoluene 60 125 122 TOluened8 90 120 106 DEFINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected MR Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not requiring dilutions sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier EIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound 112-TCTFE is 112-Trichloro-122trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab Fern 2025 Reaa.d 08-1696 Recyabd Paper ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29707 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICATION Client Sample ID SC-i Clearance Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To QUALITY CONTROL TEST RSDSPIKE MS DMSRPD PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Moisture percent 6.4 10-13-95 SzkartatM CadmiumTotal mglkgwet 1.0 10-19-95 ClearN ChromiumTotal mg/kgwet 23.7 10-19-95 ClearN 18 LeadTotal mg/kgwet 410 10-19-95 ClearN 16 VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ Metals Digestion ICP 10-16-95 ShaneD ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations Quality Control definitions are as follows %RSD Precision of replicate analysis for this sample Spitce Level Parameter Spike amount in units of the result Matrix SpikeMS/Duplicate Matnx SpikeDMS recovely %RPD Precision of Matrix Spike recovery values Inorganic Quality Control limits are enclosed Batch Quality Control data is enclosed This data was generated at the time that this sample was analyzed but was perform on different sample QU ITY RAtOFFICER LABORATORY DI EC 2001 Rev 5-04-94 Recycled paper EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Dnve South Bend Indiana 46635 219/277-5715 SAWLZ ID SC-i REPORT DATE 11/13/95 Clearance Soil EIS LAB NO 29707 VOLATILE ORGANIC COMPOUNDS/PETROLEUM RYDROCARONS Analysis Method 8021 Abbreviations and report Sanple Dilution None symbols are explained Reporting Units on the following page EQL Multiplier CCPOUND NAI4E RESULT 1QJ CO.OUND NANE RESULT -Q Acetone ND 0.5 t-13-Dichloropropene ND 0.10 Benzsn ND 0.05 Diethyl Ether ND 0.50 Bromobenzene ND 0.05 Ethylbenzene 0.070 0.05 Bromochlorthan ND 0.05 Hexacblorobutadiene ND 0.10 Broodjchlorthane ND 0.05 2-Hexanone ND 0.50 BromofoEm ND 0.10 Isopropyl Benzene ND 0.10 Bromosthane ND 0.25 p-Isopropyltoluene ND 0.10 n-Butyl Beazene ND 0.10 Methylene Chloride ND 0.10 sec-Butyl Benzene ND 0.10 Methyl Ethyl Ketone ND 0.50 tartButyl Benzens ND 0.10 Methyl Isobutyl Retone 1.9 0.50 Carbon Tetrachlorids ND 0.10 Naphthalene 0.15 0.10 Chlorobenzene ND 0.05 n-Propyl Benzene ND 0.05 Chlorodibromomethana ND 0.05 Styrene ND 0.05 Chloro.thane ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 1l12Tetrachloroethane ND 0.10 1-Chlorohexane ND 0.10 1122-Tetrachloroetha.ne ND 0.05 Chloromethane ND 0.25 Tetrachloroethene ND 0.05 2Chlorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4-Chlorotoluen ND 0.05 Toluene 1.6 0.05 12-Dibromoathan ND 0.05 l23-Tricblorobenzene ND 0.05 12-Dichlorob.nzene ND 0.10 124-TrichlorObenzene ND 0.05 13-Dichlorobenzene ND 0.10 1i1-Trichloroethane ND 0.05 14Dichlorobenzene ND 0.10 112Trichloroethane ND 0.05 Dichlorodjfluoroaethane ND .25 Trichloroethene ND 05 11-Dichloroethane ND 0.05 Trichlorofluoromethan ND 0.10 12-Dichloroethane ND 0.05 123-Trichloropropane ND 0.25 11-Dichloroethene ND 0.10 112_TCTFE ND 0.10 c-12-Dichloroethene ND 0.05 124-Trimethylbenzene 0.068 0.10 t-12-Dichloroethene ND 0.05 135Trimethyibenzene 0.065 0.10 12-Dichloropropans ND 0.05 Vinyl Chloride ND 0.10 13-Dichloropropane ND 0.10 mpxylenes 0.83 0.05 11-Dichloropropane ND 0.10 o-xylene 0.56 0.05 c-l3-Dichloropropene ND 0.10 PETROLEUM HYDROCARBONSPH 20 10 Lab Form 2025 R.ab.d 06.15.56 RecyCI.d Pap.r SAMPLE ID SC-i REPORT DATE 11/13/95 Clearance Soil RIS LAB NO 29707 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Page of SURROGATE RECOVERY Method 8021 Compound Name QC Limits Recovery 12-Dichloroethaned4 70 145 92 24Dichlorotoluene 60 125 122 Toluened8 90 120 112 DEYINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected NA Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier EIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound 112-TCTTE is 112-Trichloro-122-trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab FamI 2025 Rea.ed 06-16-95 RaqcIed Paper ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29708 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID SC-2 Clearance Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 7.8 10-13-95 SzkarlatM CadmiumTotal mg/kgwet 1.0 10-19-95 ClearN ChromiumTotal mgikgwet 17.3 10-19-95 ClearN LeadTotal mglkgwet 170 10-19-95 ClearN VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ Metals Destion ICP 10-16-95 ShaneD ADDITIONAL INFORMATION Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limb DL shown DL Detection Limit and is adjusted for dilutions/concentrations Batch Ouality Control data is enclosed This data was generated at the time that this sample was analyzed but was performed on different sample QUALITY ASSORANC FICER LABORATORY DI 2001 Rev 04-94 Recyc$d Paper ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 S1WLI ID SC-2 REPORT DATE 11/13/95 Clearance Soil EIS LAN NO 29708 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Analycie Method 8021 Abbreviatione and report Sample Dilution None aymbola are explained Reporting Unit ppm on the following page EQL Multiplier COMPOUND NAME RESULT 1Q COMPOUND NAME RESULT Ac.tons ND 0.5 t-13-Dichloropropene ND 0.10 Benamns ND 0.05 Diethyl Ether ND 0.50 Bromobanz.ne ND 0.05 Ethylbenamne ND 0.05 Bromochlorom.thans ND 0.05 Eexachlorobutadiene ND 0.10 Bromodichloromethane ND 0.05 2-Rexanone ND 0.50 Bromoform ND 0.10 Icopropyl Benzene ND 0.10 Bromnomethan ND 0.25 p-I.opropyltoluene ND 0.10 n-Butyl Bennene ND 0.10 Nethylene Chloride ND 0.10 aec-Butyl Bennene ND 0.10 Methyl Ethyl Retone ND 0.50 tert-Butyl Benzene ND 0.10 Methyl Isobutyl Ketone ND 0.50 Carbon Tetrachloride ND 0.10 Naphthalene ND 0.10 Chlorobenzen ND 0.05 n-Propyl Beozene ND 0.05 Chlorodibromomnethan ND 0.05 Styrene ND 0.05 Chloroethane ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 l1l2Tetrachloroethane ND 0.10 1Chiorohezan ND 0.10 1l22-Tetrachloroethane ND 0.05 Chloromethane ND 0.25 Tetrachloroethene ND 0.05 2-Chlorotoluens ND 0.05 Tetrahydrofuran ND 0.50 4-Chlorotoluene ND 0.05 Toluene 0.052 0.05 12-Dibrcmnoethane ND 0.05 123-Trichlorobenzene ND 0.05 2Dichi.orobenzena ND 10 12 4-Trichlorobenzene ND .05 13-Dichlorobenzene ND 0.10 l11-Trichloroethane ND 0.05 4-Djchl.orobenzene ND 0.10 11 2-Trichloroethane ND 0.05 Djchlorodjfluoromethane ND .25 Trichioroethene ND 05 1-Dichioroethane ND 0.05 Trichlorofjuoromethane ND 0.10 12-Dichloroethane ND 0.05 l23-Trichloropropane ND 0.25 11-Dichloro.thene ND 0.10 112_TCTFE ND 0.10 c-12-Dichloroethen ND 0.05 124-Trimethylbenzene ND 0.10 t12-Dichloroethene ND 0.05 135-Trimethylbenzene ND 0.10 12-Dichloropropane ND 0.05 Vinyl Chloride ND 0.10 13-Dichloropropane ND 0.10 mp-xylenea 0.059 0.05 11-Dichioropropene ND 0.10 o-xylene 0.046 0.05 c-1 3-Dichioropropene ND 0.10 PETROLEUM ErDROCABBONS PH ND 10 LaD Fan 2025 Reed 06-16-95 paper SAMPLE ID SC-2 REPORT DATE 11/13/95 Clearance Soil EIS LAB NO 29708 VOLATILE ORGPNIC COMPOUNDS/PETROLEUM HYDROCARBONS Page of SURROGATE RECOVERY Method 8021 compound Name QC Limits Recovery 12Dichloroethaned4 70 145 83 24-Dich.orotolune 60 125 106 Toluened8 90 120 108 DEFINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected NE Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not r.quiring dilutions sample requires dilution th EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier EIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound 112TCTFE is 112-Trichloro-122-trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab Pom 2025 Roabid 061695 Reyded Paper ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29709 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Pnority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID SC-3 Clearance Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To QUALITY CONTROL TEST RSDSPIKE MS DMSRPD PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Moisture percent 9.9 10-13-95 SzkarlatM 4.3 CadmiumTotal mglkgwet 1.7 10-19-95 ClearN ChromiumTotal mg/kgwet 27.0 10-19-95 ClearN LeadTotal mglkgwet 810 10-19-95 ClearN VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ Metals Digesfon ICP 10-16-95 ShaneD ADDITIONAL INFORMATION Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations Quality Control definitions are as folbws %RSD Precision of replicate analysis for this sample Spike Level Parameter Spike amount in units of the result Matrix SpikeMS/Duplicate Matrix SpikeDMS recovery %RPD Precision of Matrix Spike recovery values Inorganic Quality Control limifs are enclosed Batch Quality Control data is enclosed This data was generated at the time that this sample was analyzed but was perfo different sample LAB RATORY DIR 2001 Rev 10-04-941 ReyC4ed Paper EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Dove South Bend Indiana 46635 219/277-5715 SAIULZ ID SC-3 REPORT DATE 11/13/95 Clearance Soil EIS LAB NO 29709 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Z.nalyaia Method 8021 Ahbreviationa and report Sap1e Dilution None ymbo1s are explained Reporting Units ppm on the following page EQL Multiplier COMPOUND NA1 RESULT COMPOUND NAME RESULT Acetone ND 0.5 t-l3-Dichloropropene ND 0.10 Benzene ND 0.05 Diethyl Ether ND 0.50 Bromobensene ND 0.05 Ethylbenzene ND 0.05 Bromochloromethan ND 0.05 Rexachlorobutadiene ND 0.10 Bromodichloromethan ND 0.05 2-Hezanone ND 0.50 Bromofon ND 0.10 Isopropyl Bensene ND 0.10 Bromomethane ND 0.25 p-Isopropyltoluen ND 0.10 n-Butyl Bensene ND 0.10 Methylene Chloride ND 0.10 sec-Butyl Benzene ND 0.10 Methyl Ethyl Ketone ND 0.50 tert-Butyl Benzene ND 0.10 Methyl Isobutyl Hetone ND 0.50 Carbon Tetrachloride ND 0.10 Naphthalene 0.15 0.10 Chlorobenzene ND 0.05 n-Propyl Benzene ND 0.05 Chlorodibromomethane ND 0.05 Styrene ND .05 Chloroethane ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 1ll2Tetrachloroethana ND 0.10 1-Chlorohezane ND 0.10 l122-Tetrachloroethane ND 0.05 Chloroeethane ND 0.25 Tetrachloroethene ND 0.05 2-Chlorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4Chlorotoluene ND 0.05 Toluene 0.52 0.05 12Dibromoethan ND 0.05 123Trichlorobenzene ND 0.05 12-Dichlorobenzen ND 0.10 i24-Trichlorobenzene ND 0.05 13-Dichlorobenzene ND 0.10 1ll-Trichloroethane ND 0.05 14Dichlorobenzene ND 0.10 112Trichloroethane ND 0.05 Djchlorodifluoromethane ND .25 Trichioroetkiene ND 05 lDichlorothane ND 0.05 Irichlorofluoromethane ND 0.10 12Dichlorothane ND 0.05 123-Trichloropropane ND 0.25 11-Dichlorothene ND 0.10 112-TCTFE ND 0.10 c-l2-Dichloroathene ND 0.05 124Trimethylbenzene 0.065 0.10 t12-Dichloroethene ND 0.05 135-Trimethylbenzene 0.10 12-Dichloropropan ND 0.05 Vinyl Chloride ND 0.10 13-Dichloropropane ND 0.10 mpxylenes 0.16 0.05 11-Dichloropropene ND 0.10 o-xylene 0.074 0.05 c-l3-Dichloropropene ND 0.10 PETROLEUM HVDROCABBONSPE 18 2.0 Lab Form 2025 Reeusd 06-16-95 ReycIed Paper SAMPLE ID SC-3 REPORT DATE 11/13/95 Clearance Soil 515 LAB NO 29709 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Page of SURPGATE RECOVERY Method 8021 Compound Name QC Limits Recovery 12Dichloroethaned4 70 145 84 24-Dichlorotoluene 60 125 115 Toluened8 90 120 110 DEFINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected MR Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor SQL Multiplier EIS reports do not list the adjusted SQL values Detected but below SQL and the result shown is an estimate The compound 112-TCTFE is 112-Trichloro-122trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsThle for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab Form 2025 Rmi.d 06.16-95 flecyced Paper ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29710 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Pnority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICATION Client Sample ID SC4 Clearance Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 9.7 10-13-95 SzkarlatM CadmiumTotal mg/lcgwet 1.0 10-19-95 ClearN ChrorniumTotal mg/kgwet 15.7 10-19-95 ClearN LeadTotal mg/lcgwet 180 10-19-95 ClearN VOC 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ Metals Destion ICP 10-16-95 ShaneD ADDtTIONAL INFORMATION Chain-of-Custody xument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detechon Limit and is adjusted for dilutions/concentraflons This sample was submitted br VOC Quality Control analysis Results of the Matrix Spike/Duplicate Spike are enclosed QUA ITY ASS RANCFFICER LABORATORY DIRECT 2001 Rev 5-044 Recycled Papev EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 S1LZ ID SC-4 REPORT DATE 11/13/95 Clearance Soil EIS L7B NO 29710 VOLATILE ORGP.3IC COMPOUNDS/PETROLEUM RYDROCBEONS Analysie Method 8021 Abbreviations end report Sample Dilution None symbolS are explained Reporting Unite on the following page EQL Multiplier COMPOUND NARE RESULT COMPOUND NANE RESULT Acetons ND 0.5 t-13-Dichloropropene ND 0.10 Benzens ND 0.05 Diethyl Ether ND 0.50 Rroob.nzsn ND 0.05 Ethylbenzen ND 0.05 Bromochloroethans ND 0.05 Haxacblorobutadiene ND 0.10 Rromodichlorouaethane ND 0.05 2-Hexanons ND 0.50 BrCmofO ND 0.10 Icopropyl Benzene ND 0.10 aromomethan ND 0.25 p-Isopropyltoluene ND 0.10 n-Butyl Beneen ND 0.10 Methylene Chloride ND 0.10 eeC-Butyl Benzen ND 0.10 Methyl Ethyl Xetone ND 0.50 tertButyl Bensena ND 0.10 Methyl Isobutyl Retone ND 0.50 Carbon Tetrachioride MD 0.10 Naphthalene ND 0.10 Chlerob.nzen ND 0.05 n-Propyl Benrene ND 0.05 Chlorodibromcmethane ND 0.05 Styrene ND 0.05 Chloroethane ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chlorofonn ND 0.05 11l2-Tetrachloroethane ND 0.10 1-Chlorohexan ND 0.10 1122Tetrachloroethan ND 0.05 Cbloromethan ND 0.25 Tetrachloroethene ND 0.05 2-Chlorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4Chlorotoluen ND 0.05 Toluene ND 0.05 12-Dibromoethane ND 0.05 123-Trichlorobenzene ND 0.05 12-Dichlorobenzene ND 0.10 124-Trichlorobenzene ND 0.05 13Dichlorobenzene ND 0.10 111-Trichloroethane ND 0.05 14-Dichlorobenzene ND 0.10 112Trichioroethane ND 0.05 Dichlorodifluoromethane ND 0.25 Trichloroethene MD 0.05 l1-Dichloroetbans ND 0.05 Trichlorofluorocnethan.s ND 0.10 12-Dichloro.thane ND 0.05 123-Trichloropropane ND 0.25 1l-Dichloroethens ND 0.10 1l2-TCTFE ND 0.10 c-12-Dichloroathene ND 0.05 124-Trimethylbenzene ND 0.10 t-l2-Dichloroethene ND 0.05 l35-Trinethylbenzene ND 0.10 l2-Dichloropropane ND 0.05 vinyl Chloride ND 0.10 13-Dichloropropane ND 0.10 m-fp-xylenes ND 0.05 11-Dichloropropena ND 0.10 o-xylene ND 0.05 c-13-Dichloropropene ND 0.10 PETROLEUM HYDROCARBONSPH ND 10 LsbForm 2025 Redeid 00.16-96 Recycled Paper SAMPLE ID SC-4 REPORT DATE 11/13/95 Clearance Soil EIS LAB NO 29710 VOLATILE ORGMIC COMPOUNDS/PETROLEOM HYDROCA1BONS Page of SURROGATE RZCOVERI Method 8021 Compound Name QC Limits Recovery l2Dich.oroethaned4 70 145 101 24-Dichlorotoluene 60 125 123 Toluefled8 90 120 106 DEFINITIONS ppm Parts per million milligrams per kilogram mg/kg as received ND Not Detected HR Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for samples not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor TQL Multiplier EIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound ll2-TCTFE is 112-Trichlorol22-trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids La Form 2025 Red 0516-95 Racyded Paper Øji ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29711 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICATION Client Sample ID SC-5 Clearance Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 11 10-13-95 SzkarlatM CadmiumTotal mg/kgwet 1.0 10-19-95 ClearN ChromiumTotal mg/lcgwet 18.0 10-19-95 ClearN LeadTotal mg/kgwet 190 10-19-95 ClearN voc 10-17-95 WilliamsJ See Attached ORGANICS REPORT Extract VOC 10-16-95 WilliamsJ Metals Digestion ICP 10-16-95 ShaneD ADDONAL INFORMATION Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Lime and is adjusted for dilutions/concentrations Batch Quality Control data is enclosed This data was generated at the time that this sample was analyzed but was performed on different sample QUA ITY ASS ANCE CER LABORATORY DIRECT 2001 Rev 5-04-94 Recycnd Peper EIS ENvIRONMENTAL ENGINEERS INC 1701 North ronwood Drive South Bend Indiana 46635 219/277-5715 SAMPLE SC-5 REPORT DATE 11/13/95 Clearance Soil EXS LZ4B NO 29711 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCARBONS Analysia Method 8021 Iibbr.viationa and report 5smpie Dilution None symbols are explained Reporting Units ppm on the following page EQL Multiplier COMPOUND NSME RESULT iQJ COMPOUND NAME RESULT Acetone ND 0.5 t-13-Dichloropropene ND 0.10 Benzene ND 0.05 Diethyl Ether ND 0.50 Bromobanz.ne ND 0.05 Ethyl.benzene 0.071 0.05 Bromochjorthsne ND 0.05 Nexachlorobutadiene ND 0.10 Eromodichlorcmethane ND 0.05 2-Hezanone ND 0.50 Bromoforin ND 0.10 Isopropyl Benzene ND 0.10 Bromomathane ND 0.25 p-Iaopropyltoluene ND 0.10 n-Butyl Benzena ND 0.10 Methylene Chloride ND 0.10 sec-Butyl Hansen ND 0.10 Methyl Ethyl Xetone ND 0.50 tert-Butyl Benzene ND 0.10 Methyl Xsobutyl ICetone ND 0.50 Carbon Tetrachloride ND 0.10 Naphthalene ND 0.10 Chlorobenzene ND 0.05 n-Propyl Benzene ND 0.05 ChlorodThromomethane ND 0.05 Styrene ND 0.05 Chloroethan ND 0.25 tert-Butyl Methyl Ether ND 0.10 Chloroform ND 0.05 l112Tetrachloroethane ND 0.10 1Chlorohexane ND 0.10 ll22-Tetrachloroethane ND 0.05 Chlorothan ND 0.25 Tetrachloroethene ND 0.05 2-Cblorotoluene ND 0.05 Tetrahydrofuran ND 0.50 4Chlorotolu.ne ND 0.05 Toluene 0.20 0.05 12-Dibromoethan ND 0.05 l23Trichlorobenzene ND 0.05 l2Dichlorobenzene ND 0.10 124Trichlorobenzene ND 0.05 13Dichlorobenzene ND 0.10 111-Trichloroethane ND 0.05 14-Dichlorobenzene ND 0.10 ll2-Trichloroethane ND 0.05 Dichlorodifluoroaethane ND 0.25 Trichloroethene ND 0.05 1Dichloroethane ND .05 Trichlorofluoromethane ND 0.10 12-Dichloroethane ND 0.05 123-Trichloropropane ND 0.25 11-Dichloroethene ND 0.10 1l2_TCTFE ND 0.10 c-l 2-Dichloroathene ND 0.05 12 4-Trinethylbenzene ND 0.10 t-12-Dichloroethene ND 0.05 135-Trimethylbenzene ND 0.10 12-DichlOropropane ND 0.05 Vinyl Chloride ND 0.10 13-Dichloropropsne ND 0.10 mp-xylenes 0.32 0.05 11-Dichloropropene ND 0.10 oxylene 0.13 0.05 c-13-Dichloropropene ND 0.10 PETROLEUM HVDROCARBONSPH ND 10 LaD Form 2025 Meosed 06.16.95 Recycled Pa.r SMWLE ID SC-5 REPORT DATE 1.1/13/95 Clearance Soil RIO LRB NO 29711 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCABBONS Page of SURROGATE RECOVERY Method 8021 Compound Name QC Limits Recovery 12-Dichloroethand4 70 1.45 82 24-Dichlorotoluene 60 125 1.22 Toluened8 90 120 107 DEFINITIONS ppn Parts per million milligrams per kilogram mg/kg as received ND Not Detected NR Not Required for analysis EQL Estimated Quantitation Limit in Reporting Unite and is the Detection Limit for samples not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier HIS reports do not list the adjusted EQL values Detected but below EQL and the result shown is an estimate The compound 1l2TcTFE is 112-Trichloro--122trifluoroethane Petroleum Hydrocarbons if their presence is noted in this analysis are reported in terms of fuel oil No attempt has been made to identify the product responsible for the Petroleum Hydrocarbon response This analysis will not detect heavy distillates such as used oils motor oils hydraulic fluids Lab Form 2025 Remeed 06-18-95 Recycled Paper ANALYTICAL REPORT Client Report Date 11-13-95 MrJohnStark EISLabN0 29712 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Pflority South Bend In 46601 Chent P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICATION Client Sample ID BG-1 Background Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 52 10-13-95 SzkaflatM CadmiumTotal mg/kgwet 1.9 10-19-95 ClearN ChromiumTotal mg/kgwet 41.4 10-19-95 ClearN LeadTotal mg/kgwet 160 10-19-95 ClearN Metals Digestion ICP 0-1 6-95 ShaneD ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Um DL shown DL Detection Limit and is adjusted for dilutions/concentrations QUAU ASS ANC ICER LABORATORY DIRECTO 2001 Rev 5-04-94 EIS ENVIRONMENTAL ENGINEERS INC 1701 North roriwood Dnvo South Bond Indiana 46635 219/277-5715 ºji ANALYTICAL REPORT Client Report Date 11-13-95 MrJohn Stark EIS Lab No 29713 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID BG-2 Background Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To QUALITY CONTROL TEST RSDSPIKE MS DMSRPD PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Moisture percent 5.6 10-13-95 SzkarlatM CadmiumTotal mgllcgwet 5.8 10-19-95 ClearN 0.40 90 90 ChromiumTotal mglkgwet 60.6 10-19-95 ClearN 0.40 92 92 LeadTotal mg/lcgwet 470 10-19-95 ClearN 0.40 98 95 3.1 Metals Digestion ICP 10-16-95 ShaneD ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations Quality Control definitions are as follows %RSD Precision of replicate analysis for this sample Spike Level Parameter Spike amount in units of the result Matrix SpikeMS/Duplicale Matrix SpikeDMS recovely %RPD Precision of Matrix Spike recovery values Inorganic Quality Control limits are enclosed QUA ITY AS RANCFICER LABORATORY DIRECT 2001 Rev 5-04-94 Recyded Pepei Els ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 ANALYTICAL REPORT Client Report Date 11-13-95 MrJohnStartc EIS Lab No 29714 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID BG-3 Background Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 8.5 10-13-95 SzkailatM CadmiumTotal mglkgwet 4.9 10-19-95 ClearN ChromiumTotal mgikgwet 34.4 10-19-95 ClearN LeadTotal mg/kgwet 580 10-19-95 ClearN Metals Digestion ICP 10-16-95 ShaneD ADDITIONAL INFORMA11ON Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Umit and is adjusted for dilutions/concentrations QUA TV ASS AN FICER LABORATORY DIRECT 2001 Rev 5-04-94 Reuycied Paper EIS ENVIRONMENTAL ENGINEERS INC 1701 North lronwood Drive South Bend Indiana 46635 219/277-575 ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29715 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID BG-4 Background Soil Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST Moisture percent 6.9 10-13-95 SzkarlatM CadmiumTotal mglkgwet 1.6 10-19-95 ClearN ChromiumTotal mg/kgwet 30.0 10-19-95 ClearN LeadTotal mgIlgwet 320 10-1 9-95 ClearN Metals Digestion ICP 10-16-95 ShaneD ADDITIONAL INFORMA11ON Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations QURaR TTOYDIREC 2001 Rev 5-04-94 Recycled Paper EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-5715 º3j ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29716 Community Economic Development EIS Project No 1456-8106-95 1200 County/City Bldg 227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICATION Client Sample ID TRIP BLANK Deionized Water Date Sampled 10-09-95 Date Received 10-11-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST CadmiumTotal mg/I 0.001 0.001 10-26-95 ClearN ChromiumTotal mg/I 0.005 0.005 10-26-95 ClearN LeadTotal mg/i 0.005 0.005 10-26-95 ClearN VOC 10-17-95 WilIiams.J See Attached ORGANICS REPORT Metals Destion ICP 10-26-95 ShaneD ADDITiONAL INFORMATiON Chain-of-Custody xument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Sample containers were properly preserved per USEPA protocols Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations QUAL ASSU ANCE pTCER LABORATORY DIRECT 2001 Rev 15-04-94 Recycled Paver EIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drive South Bend Indiana 46635 219/277-575 SAMPLE ID TRIP BLANK REPORT DATE 11/13/95 Deionized Water RIS LAB NO 29716 VOLATILE ORGANIC COMPOUNDS/PETROLEUM HYDROCANBONS Analyzia Method 8021 rreviationa and report Sample Dilution None ayzabola are explained Reporting Unite ppb on the following page EQL Multiplier COMPOUND NAME RESULT EQ COMPOUND NAME RESULT QI Aceton ND 10 t-1 3Diabloropropene ND Benzen ND Diethyl Ether ND 10 Bromobenzen ND Ethylbenzene ND Bromocblorothane MD Hexachlorobutadiene ND Bromodichloromethane ND 2-Hexanone ND 10 Bromofoxm ND Isopropyl Benzene ND Broanomethane ND p-IaoprOpyltoluene ND n-Butyl Benzene ND Methylene Chloride ND aec-Butyl Benzene ND Methyl Ethyl Ketone ND 10 tert-Butyl Benzene ND Methyl Izobutyl Ketone ND 10 Carbon Tetrachloride ND Naphthalene ND Chlorobenzene ND n-Propyl Benzene ND Chlorodibromomethane ND Styrene ND Chloroethane ND tert-Butyl Methyl Ether ND Chloroform ND 1112Tetrachloroethane ND 1-Chlorohexane ND 1122-Tetrachloroethaxie ND Chloroaaethane ND Tetrachloroethene ND 2-Chlorotoluene ND Tetrahydrofuran ND 10 4-Chlorotoluene ND Toluene ND 2-Dibromoethane ND 12 3-Trichlorobenzene ND 12-Dichlorobenzene ND 124Trichlorobenzene ND 13Dichlorobenzene ND 111-Trichloroethane ND 14-Dichlorobenzene ND 112-Trichloroethane ND Dichlorodjfluoromethane ND Trichioroethene ND 1-Dichloroethane ND Trichlorofluoromethane ND 2-Dichloroethane ND 12 3-Trichioropropane ND 11-Dichloroethene ND 1l2_TCTTE ND c-12-Dichloroethene ND 124-Trimethylbenzene ND t-12-Dichloro.thene ND 135-Triniethylbenzene ND 2-Dichloropropan ND vinyl Chloride ND 13-Dichloropropane ND p-Xylenes ND 11-Dichloropropene ND o-Xylene ND c-1 3-Dichloropropene ND PETROLEUM HyDROCARBONS ND 200 Lab Form 2024 Reeaed 02.16-95 Recycled Pager WPLE ID TRIP ELMJX REPORT DATE 11/13/95 Deionized Water ZIS LB NO 29716 VOLATILE ORGANIC COMPOUNDS/PETROLEUM SIDROCARBONS Page of SURROGATE RECOVERY Method 8021 Compound Name QC Limits Recovery l2Dichloroathaned4 70 130 113 24Dichiorotoluene 70 130 99 Toluaned8 90 120 101 DESINITIONS ppb Parts per billion micrograms per liter g/l ND Not Detected MR Not Required for analysis EQL Estimated Quantitation Limit in Reporting Units and is the Detection Limit for sales not requiring dilutions If sample requires dilution the EQL shown must be multiplied by the inverse of the dilution factor EQL Multiplier HIS reports do not list the adjusted EQL value. Detected but below EQL and the result shown is an estimate The compound 1l2-TCTFE is 1l2-Trichloro-122trifluoroethana Petroleum Hydrocarbons if their presence is noted in this analysis are reported in termS of fuel oil No attempt has been made to identify the product respon.ible for the Petroleum Hydrocarbon response This analysis will not detect heavy d.istillates such as used oils motor oils hydraulic fluids Lab Form 2024 8.45.4 02.18-95 Recyc4d Paper TCLP AND HAZARDOUS WASTE CHARACTERIZATION UMITS Reference AnalytIcal Methods USEPA USEPA SW-846 USEPA USEPA SW-M6 Hazardous Waste Limit Reference Hazardous Waste Limit Reference Number Constituent Name jflgj Method Number Constituent Name JL Method VOLATILE ORGANICS TCLP METALS D018 Benzene 0.5 8260 D004 Arsenic 5.0 6010 0019 Carbon Tetrachbride 0.5 8260 0005 Banum 100.0 6010 D021 Chlorobenzene 100.0 8260 D006 Cadmium 1.0 6010 0022 Chloroform 6.0 8260 D007 Chromium 5.0 6010 D027 14-Dichlorobenzene 7.5 8260 0008 Lead 5.0 6010 0028 12-Dichloroethane 0.5 8260 D009 Mercury 0.2 7470 D029 11-Dichloroethylene 0.7 8260 0010 Selenium 1.0 6010 0035 Methyl Ethyl Ketone 200.0 8260 DOll Silver 5.0 6010 D039 Tetrachloroethylene 0.7 8260 D040 Tnchloroethylene 0.5 8260 MISCELLANEOUS D043 Vinyl Chloride 0.2 8260 0001 Ignitability 140 1010 0002 Corrosivity SU 2-12.5 9040 SEMI-VOLATILE ORGANICS 0003 Cyanide Reactivity mg/kg 250 9010 D023 o-Cresol 200.0 8270 D003 Suit ide Reactivity mg/kg 500 9030 D024 m-Cresol 200.0 8270 TCLP Extract Formation 1311 0025 p-Cresol 200.0 8270 Paint Filter Liquids Test 9095 D026 Total Cresols 200.0 8270 0030 24-Dinitrotoluene 0.13 8270 0032 Hexachlorobenzene 0.13 8270 0033 Hexachloro-13-butadiene 0.5 8270 D034 Hexachloroethane 3.0 8270 D036 Nftrobenzene 2.0 8270 D037 Pentachlorophenol 100.0 8270 0038 Pyridine 50 8270 D041 245-Trichlorophenol 400.0 8270 0042 246-Trichlorophenol 2.0 8270 PESTICIDES AND HERBICIDES 0020 Chlordane 0.03 8080 0012 Endrin 0.02 8080 0031 Heptachior and its expoxides 0.008 8080 D013 Lindane 0.4 8080 0014 Methoxychlor 10.0 8080 D015 Toxaphene 0.5 8080 0016 24-D 10.0 8150 0017 245-TP Silvex 1.0 8150 2204 Re4sed 110593 Recycled Paper REFERENCE ANALYTICAL METHODS EIS Lab No 29707-29716 Reference Used Reference Reference Test Description Test Description Acidity CaCO3 2310 305.1 Aluminum 3120 2007 6010 Alkalinity Total CaCO3 2320 310.2 Antimony 3120 2007 6010 BOD5Carbonaceous 5210B Arsenic 312GB 200.7 6010 BOD5 Soluble 5210 405.1 Barium 3120 200.7 6010 6005 Total 5210 405.1 Beryllium 31208 200.7 6010 Chloride 4500-Cl 325.3 9251 Bismuth 3111 Chlorine Residual 4500-Cl 330.5 Boron 3120 200.7 6010 COD 52200 410.4 Cadmium 3120B 200.7 6010 ColitormTotal F.Coli Screen 9222 9132 Calcium 3120 200.7 6010 Coliform Fecal 9222 Chromium 31208 200.7 6010 Coliform Chromium Hex 3500-Cr 7196 Colitorm Plate Count 9215 Cobalt 31206 200.7 6010 Cyanide Total 4500-ON 335.3 9012 Copper 31206 200.7 6010 Cyanide Reactive 7.3 Iron 3120 2007 6010 Cyanide Amenable 4500-ON 335.1 9012 Lead 3120 200.7 6010 Fluoride 4500-F 340.2 Magnesium 31206 200.7 6010 Hardness CaCO3 2340 130.1 Mercury 31128 245.1 7470 Nitrogen Ammonia 4500-NH3H 350.1 Molybdenum 31110 248.1 7480 Nitrogen Nitrate 4500-NO3F 353.2 9200 Nickel 31208 200.7 6010 Nitrogen Nitrate Nitrite 4500-NO3F 353.2 Potassium 3111 258.1 7610 Nitrogen Nitrite 4500-NO3F 353.2 Selenium 31206 200.7 6010 NitrogenOrganic 4500-NA 351.2 Silincn 31206 200.7 6010 Nitrogen Total Kjeldahl 4500-NB 351.2 Silver 3120 2007 6010 Oil GreaseFreon Extraction 5520 413.1 9070 Sodium 31208 200.7 6010 Oil GreaseHydrocarbons 5520 Thallium 31206 200.7 6010 pH 4500-MB 150.1 9040 Tm 31208 2007 6010 Phenols Total 55300 420.2 9066 Titanium 31208 200.7 6010 Phosphrous Total 4500-P 365.1 Vanadium 3111 286.1 7910 Phosphorus Ortho 4500-P 365.1 Zinc 3120 200.7 6010 Silica 4500-Si 370.1 Solids Dissolved 180C 2540 160.1 Solids Suspended 25400 1602 REFERENCES Solids Total 2540 160.3 Solids Volatile Suspended 2450 160.4 Standard Methods for the Examination of Water Solids Volatile Total 2540 160.4 and Wastewater 18th Edition Specitic Conductance 2510 120.1 9050 Methods for Chemical Analysis of Water and Sulfate 4500-SO4F 375.2 9036 Wastes EPA-60014-79-020 Suitide Total Acid Soluble 4500-SD 3762 9030 Test Methods for Evaluating Solid Waste Suitide Reactive 7.3 Physical/Chemical Methods SW-846 Surf acants MBAS 5540 425.1 Federal Register 40 CFR Parts 141 and 142 Part Surf acants CTAS 55400 Ill June 29 1989 Total Organic Carbon 5310 415.2 9060 More than one reference may be required to Total Organic Halogen 5320 9020 oumplete all tests Group Tests such as VOC BETX SVOC PCB TCLP are reported along with the appropriate Test Methods special Report Packages 2203 P011584 4-12-93 cIod Papo QUALITY CONTROL LIMITS GENERAL CHEMISTRIES/HEAVY METALS LABORATORY REPLICATE AND MATRIX SPIKE ANALYSIS Laboratory Matrix SpIke/DuplIcate Spike PameterfTest Group ReplIcate RSD %RPO COD 20 Cyanide Suitide 15 75-125 20 Inorganics-Groupi 15 80-120 20 Alkalinity Ammonia Chloride Fluoride Hardness Hex Chrome Nitrate Nitrate Nitrite Nitrite Phenols Silica Sulfate Inoiganics Group 15 BOD Dissolved Solids Oil Grease pH Specit Ic Conductance Suspended Solids Total SOlIdS Metals except Mercuiy 15 80-120 20 Mercury 15 75-125 20 TKN Phosphorus 20 80-120 25 TOH 20 75-125 25 The limits above are employed for water and solid matrices R$D is based on concentrations RPD is based on Recovery The RSD limits apply to parameters/test groups where the measured concentration is 5X Detection Limit it the measured concentration is 5X Detection Limit the RSD limit is 47%for all tests For MS1DMS if the Spike Sample yield concentrations 5X Detection Limit the RPD DC Limit 67 The individual values should contorm to the DC limits shown above 299 Pe 4-2-94 ReccIed Ppe QUALITY ASSURANCE DATA SHEET DUPLICATE MATRIX SPIKE ANALYSIS VOLATILE ORGANIC COMPOUNDSIBED Sample ID SC-4 EIS Lab No 29710 Date Analyzed 1017-95 THIS OC DATA IS APPUCABLE TO THE FOLLOWING EPA Method 8021 EIS LABORATORY NUMBERS Sample Matrix Soil 29705- 2971129776 Units ppm as received PRECISION as Relative Percent Difference ACCURACY as Matrix Spike Recovery RPD Matrix Spike %R Duplicate Spike %R Spike Background Background Matrix Spike %R Duplicate Spike %R Spike 00 Spike Back Matrix Spike Duplicate Spike QC LImfts Parameter Level %R %R RPD %R RPD Benzene 0.83 0.79 95 0.80 96 -1.0 66-142 21 Chlorobenzene 0.92 0.89 97 0.89 97 60-133 21 11-Dictiloroethene 1.00 0.85 85 0.89 89 -4.6 59-172 22 Toluene 0.84 0.78 93 0.79 94 -1.1 59-139 21 Tilchloroethene 0.80 0.78 98 0.79 99 -1.0 62-137 24 2215 Relsed 04-22-94 Royded Pape HAI OF RSCflS____Ip5 ________ ________-_tJ eocA ____ ___ RELINQUISHED DATE TiME RECEIVED BY RELiNQUISHED BY DATE TiME RECETVED Br cfocj RELiNQUISHED BY DATE TiME RECEIVED BY RELINQUISHED BY DATE TiME RECEIVED BY INTACT DWAEN MODE OF TRANSPORTATiON FiELD NOTES LS VEHICLE PUBLIC LIS ENVIRONMENTAL ENGINEtRS INC 1701 IRONW000 DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM Large Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Be Performed From This Container 40 cc vial HC1 voc TPH BETX 40 cc vial HC1 Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOD Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals H2SO4 Glass FS Oil Grease H2S04 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TKN H2S04 Glass TOH TOC 12S04 Glass Phenol NaOR Plastic Cyanide NeON-I-Zn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass LM All types of tests individual tests to be performed are to be specified on the EIS Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 ReviS 030393 _____________CHAIN OF CUSTODY RECOffIY ª1 __________oiEc NO MWE SEE REVERSE SIDE FOR INSTRUCTiONS JL/s L7.ElS LAB __DESCRIPTION _____________LiIIIIIIIII ______ __________ RELINQUISHE DATE TIME RECEI BY RELINQUISHED BY DATE TIME RECEIVED BY /10-3 ____________________________ RELINQUISHED BY DATE TIME RECEIVED BY RELINQUISHED BY DATE TIME RECEIVED BY INTAcT OAEN MODE OF 7RANSPORTA TION FIELD NOTES Els VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONWOOD DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM barge Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Re Performed From This Container 40 cc vial HC1 VOC TPH BETX 40 cc vial HC1 Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOD Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals H2SO4 Glass FS Oil Grease H2SO4 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TEN H2SO4 Glass TOH TOC H25O4 Glass Phenol NaOH Plastic Cyanide NaOHZn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass LE All types of tests individual tests to be performed are to be specified on the SIS Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 Revi 030393 -rJ CHAIN OF CUSTODY RECORD __________ ..StE REVERSE SIDE FOR INS7RUCT7ONS _DnMERYD f/FAERKS iMsm ______ ______Dw-______.7Io9___________________ /Qe rcA _____ RELINQUISH DATE TIME RECEIVED BY REUNQUISHED BY DAlI TiME RECEIVED BY SAUPLt /1-2r If S.r A44 REUNQUISIIED BY DATE T7ME RECEIVED BY RELINQUISHED BY DATE TIME RECEIVED BY INTACT vt MODE OF ThANSPORTATION FiELD NOTES tiS VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONWOOD DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM Large Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Be Performed From This Container 40 cc vial HC1 VOC TPH BETX 40 cc vial HC1 Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOO Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals 52504 Glass FS Oil Grease H2SO4 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TKN H25O4 Glass TON TOC H2SO4 Glass Phenol NaOH Plastic Cyanide NaOHZn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass LM All types of tests individual tests to be performed are to be specified on the Els Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 Res 030393 .en WVW APPENDIX ORIGINAL CHAIN-OF-CUSTODY RECORDS 46Th RIIl 1I cHAIN OF CUSTODY RECORD _________ SEE RRSE SIDE FOR INSUCflONS SRE lAB lIME OF PRIA4RY SAMPLE DESCRIPTION ///////71/i/EMARKS ________________111111 _______ ________ ________________or ________-- _________Sc--f ________ ...........__________________________ ______ ______ RELINQUISH DAlE 17ME RECEiVED BYj RELiNQUISHED 8Y DAlE liME RECEiVED BY 5A -- RELINQUISHED BY DATE TIME RECEIVED BY RELINQUISHED 0Y DATE TIME RECEIVED BY INTACT MODE OF IRANSPORTA liON FiELD NOTES Els VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONW000 DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM Large Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Be Performed From This Container 40 cc vial HC1 VOC TPH BETX 40 cc vial NC Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOD Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals H2SO4 Glass FS Oil Grease H2SO4 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TKN H2SO4 Glass TON TOC H2SO4 Glass Phenol NaOH Plastic Cyanide NaOHZn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass LM All types of tests individual tests to be performed are to be specified on the EIS Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 RV1S 030393 CHAIN OF CUSTODY RECORD _________RSE SIO FOR iNSTRUCTIONS tctLd 11 ElS LAB __________USE ONL ____10-ic p6-f iiiiiiiiii____ ___0IO9f____i3 6-____ ___ 10 _______________ ___ ____________________ ___ _________LCIc1 .- RUNQUISHED DATE TiME RECEIVED By RELINQUISHED BY DATE TiME RECEIVED BY 1O9J 5yy Lc REUNQWSHED BY DATE TIME RECEIVED BY RELINQUISHED BY DATE TIME RECEIVED BY .1NTACTH MODE OF TRANSPORTATION FIELD NOTES ETS VEHICLE PUBUC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONW000 DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM Large Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Be Performed From This Container 40 cc vial HC1 VOC TPH BETX 40 cc vial HC1 Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOD Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals H2S04 Glass FS Oil Grease H2SO4 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TEN H2SO4 Glass TOH TOC H2S04 Glass Phenol NaOH Plastic Cyanide NaOHZn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass t.M All types of tests individual tests to be performed are to be specified on the EIS Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 ROViS 030393 CHAIN OF CUSTODY RECORD __________ SEE REVERSE SIDE FOR INSTRUCTIONS ___________________iiiiiiii____ ISHED BY DATE TIME RECEIVED BY RELINQUISHED DAlE TIME RECE BYr2J2-7JE -o-q Y6 RELiNQUISHED BY DATE TIME RECEIVED BY RELINQUISHED BY DATE TIME RECEIVED BY INTAT4JBROKEN MODE OF TRANSPORTATION FIELD NOTES ElS VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONWOOD DR SOUTH BEND IN 46635 219 2775715 INSTRUCTIONS Along the slanted lines write in the Container/Preservative from the list of allowable entries given below For each sample under each container type indicate number of bottles Total bottles per sample are entered in No of Containers column Container sizes and preservative amounts are shown in the bottle displays in the prep room Substitutions may be allowable check with the lab Containers/Preservatives for various tests are shown below Following descriptions are used as required FS French Square LM Large Mouth Amber If sample is split between grab and composite bottles you can indicate this as or in the slanted lines describing the container Container/PreservativeWater Tests Which Can Be Performed From This Container 40 cc vial HC1 VOC TPH BETX 40 cc vial HC1 Ascorbic Acid Trihalomethanes where THM at site is required Unpres Plastic Acidity Alkalinity BOD Chloride Fluoride Hardness Ortho Phosphorus Silica Solids all kinds Sp Cond Sulfate Surfactants NITRATE FROM CHLORINATED WATER SOURCES ONLY Nitrite Cr6 pH HNO3 Plastic Metals H2SO4 Glass FS Oil Grease 02SO4 Plastic Ammonia COD Nitrate Nitrite Nitrate non Chlorinated Water Total Phosphorus TKN H2SO4 Glass TON TOC H2SO4 Glass Phenol NaOH Plastic Cyanide NaOHZn Plastic Sulfide Glass SVOC Glass Pesticides/PCB Glass Herbicides Preservatives differ for drinking water and other waters See bottle displays in prep room Type of Container Soil 40 cc vials VOC TPH and BETX Unpres Glass LM All types of tests individual tests to be performed are to be specified on the EI2 Laboratory Analysis Request Form If test is requested and no information is shown above check with the Laboratory 2067 ReViS 030393 APPENDIX FIELD DATA 4696RPTI\96Ol Sheet oi Project On ____ jk eick Dar4A-SAMPLE LOG Client Site Location /V//IoielIe IJZbate 0/O -95-- No of Samples Collected Container Size ______________Equipment Used cIreci9e 5d Time EIS __________ ___________________________Tyoe of Material Lab 14o Analysis RequestedSampleNoSampleLocation _____________________________________________________________ywJeu GtQI AdIIct5.s 4gIJ tc _______ VOc. _________0c __________________________________________________ DriwEll Ska.1\J is c.i .eas9-coIItT jj ________________________voc _________bJiq ___________________________________ ___________________ TCI-i.4I iesi g71 p---__________.reaS ________________________________________ .5I leuAce S.ily Ok13I.OI.S 7b7 11CC MefcilS ________Ar _____________________________ .St ItIIGTh1WIj/// _________ArCiegt 35ct.a /5 I.o-i.s /1 __________Ar ____________________________________ ___________________Jeeroe J/S4h AA 15 DL-i ao j ______________________ 27________rI ft-______________________________ _______________o.i -Ie.4CC s-S -- 5__ IAm oSC-ol ji.c ri_______ft t-ec1 ________________________________________ -ia.%q1 /1I6mIW5F5he91- _________Iu Oyet ___________________________________ ____________________Rk 6534 6-Wc e4 2-_________________iKeoe 64er ___________________________________ ____________________gKsrov63 II RIj ________________0crsOU4q Lvesjr_orr ____________________________________________ ___________ Comment WQa w4L qlr cuic\ceoniz..e HLO rn.es3meciecev7ea4c5..-W-L-.r 11ece.-19 /earawe pe -e Iz3y aftaeJe fLd Voi p.1t th rpre 4ei Collectors flame 17a.ucI JerS _____________________ Sheet _.j__L Project No _______ SOIL SAHPLE LOG Client 5A Site Location ________________ Equipment Used 1LJ 4r-No of Samples Collected __________________Container Size __________ jIq pJcIc ElS Samole No ahiple Locatioii Time Type of Material Lab No AnaLysis Reauested 4041/f f41 //e 54-c CCJ J/e5i4a/L Ii OVQ -/-gicl dAh ____________________ Comment eeA AoApeI rIr m/ TA ri iIe I/eJ Jr____________________________________ Coflectors Name OcJ lp L4 U4191144.04 tAJ SHEET OF IIiIIIIIIII PROJECT DepL Oe/g PROJECT No 9/L c5 DATE fO /0 EIS ENVIRONMENTAL ENGINEERS INC PREPARED By__________SCALE 1a/ k1C hui pe5 c.Ie3ee p1e /e/d coe jcqice Jocq/-/3yrL ecA tch ho5 coftpcsteJ W1CI 4/Q oMfie t4X-1 U-oJ r.pJr..$$-i3i co//ec1eJ -h rIipkeIcc.Qe so/.ple so/onJ w.a5 f/e/ic7 7Lec Me qii/pesicJ.e areas Rcq1 ai I/Jbt44 JtlA eqc/bQcro.J .i/e Lkcrecc.Pe1eoc/cqeasc1fecokoAo.s Sket4 6r1 Ar-PC5es Ckzra ert .tr4e 14-71p1e5a1eecln5ap/e Lj -r- defae t-.ip1e ic.-Lz -r-fe-IO5-Se5 k1Iei 41ey upIe Or 5fte J4 /-4ycf1e IcL APPENDIX INDIANA DEPARTMENTOF ENVIRONMENTAL MANAGEMENT IDEM SPECIAL WASTE CERTIFICATION APPLICATION 145696\RP1P9h4I -6 Special Waste Certification Application Cashier Room 1324 Indiana Department of Environmental Management For Office Use Univ 110 Senate Axenue Box 7060 Reviewer_______________ Indianapolis Indiana 46206-7060 Telephone 7/232-Application No _________ Generator Fee Fee 5250.00 per application PAID BY Check or Money Order Generator Information Generator Facility Location Generator Mailing .-ddress Name Address Address /OO -i4 5Lh htcACJ 6cf ek cjci L1t p/ City State Zip City State Zipi ountv 5L -5/2 County Technical Contact and Telephone Technical Contact and TelephoneLk3J-2/ EPA Identification Number Contractor Information Applicant if other than generator Proposed Disposal Site Name Er Name Pra/r hew Opp No 71-2 Address Address P.O OK __________________________/Ssc iA4e1 i9e1 C3j i.4f Vfc City State Zip City Staic Z1Pr4e4 Wuwja H4r-P11e ga -s2b-_____________________________ Technical Contact and Telephone Technical Contact and Telephone Check box if you want copy of certification e/1 Regulatory Issues Are any of the following occurring at your facility please check CERCLIS Clean-up Hazardous/Solid Waste Enforcement Corrective Atiri Air/Water Issues No Issues Other _________________________ Special Waste Certification \pplication page of List below in sectiOn the Waste Stream for which certification is being requested under this application If number of similar waste streams are being combined for certification purposes see instructions list all the waste streams included within this combination Separate applications must be submitted for each waste stream or each combination of waste streams requiring certification Wastes Information _____________________ Wastesi Names Previous Certification No _______________________________________________________________________ if applicableCoin ___________________________________________________________________________________________ __________________________________________________________________________________________________ _________________________________________________________________________________ ___________________________________________________________________________________________ _________________________________________________________________________________ ___________________________________________________________________________________________ __________________________________________________________________________________________________ ____________________________________________________________________________ 10 ____________________________________________________________________________ Antictpated annual disposal quantity Aprox Check box if this is one-time only disposal Type of disposal containers to be used .11.J SampLing and Laboratory Information Laboratory Sample Collector Name Name alJI r-c Cis Address /fJ Address i/IrA ai ti gJ City State Zip City State Zip Techntca ContacL and Teiephonc Telephone Ancii js--ys---.2-5-7/$-- /95 Special Waste Certification Application page of If certification is being requested for combination of similar waste streams under this application complete this page for each waste stream included in that combination Waste Characterization Is the waste listed hazardous waste as defined in 329 IAC 3.1 Yes No Does this waste contain PCBs or PCB items as defined in 329 IAC Yes No Physical Characteristics attach MSD Sheets if Available Physical state 5J Percent solids /C Fire explosion or spontaneous ignition hazard Yes___No_ Does this waste contain Free liquids Asbestos Solvents.g Odor None_LMiid Strong_Describe Analytical Information Sampling Date sample was collected Ii/i/$..i IqLrSample type grab___compostte Was sampline plan used Yes No_If so provide acopv if requested see instructions Is the sample representative of the waste e5 5e Results attach orieinal laboratory documentation i.e TCLP metal pesticide organics corrosivitv ignitability reactivity or other Provide QA/QC upon request Process Description attach additional pages if necessary EA1eA4 d01 cF Frnep r/1 ScI-c Qf 5e.cs caI/y 14J1J cAci1r rS .I u..1e iAe ri--iLAe frbptt1v A7L so sJe sAdu/d be ioue-I mm pseci ci i5fi7 Generator Signatures hereby certify that the information in this application is true and accurate to the best of my knowle and th waste is not hazardous waste as defined in 329 LAC 3.1 1/-.1 Stnature type or pr-mt name Date Title Prcjec4 6edoj.c EZ.S /-iiceJ- frmfr /e eero-e4 47224 7-95 Form approved by State Board of Accounts 1995 INDIANA DEPARTMENT OF ENVIRONMENTAL MANAGEMENT SPECIAL WASTE FEE TRANSMITTAL INSTRUCTIONS This form shall be used to transmit fees for all solid waste management special waste certification applications pursuant to 329 IAC 2-21-1 and is to accompany all payments Make check or money order payable to the INDIANA DEPARTMENT OF ENVIRONMENTAL MANAGEMENT Upon completion return this form the approprtate fees and the certification application to the following address CASHIER Room 1324 Indiana Department of Environmental Management 100 Senate Avenue Box 7060 Indianapolis IN 46206-7060 SECTION APPLICANTS INFORMATION Responsible Party -h mTh41LI qicj f-/ Street City Mailing Address 2y LJ\9/ State Zip Code AC-Telephone Number 4cJIcAq .J 7J Generating Facility 5iA1A eicJ Name and County Dp-cF levJom%.i 75sepA SECTION SPECIAL WASTE CERTIFICATION FEE SCHEDULE SPECIAL WASTE CERTIFICATIONS GENERATOR FEE $250.00/Application Anolications Please list all Special Waste Certification Applications being submitted with the corresponding waste streams to be certified under each Please name the waste streams exactly as they are named on the applica ion _______________________________ ___________________________________________________________ _______________________________________________________________ _______________________________________________________ _______________________________________________________________ ___________________________________________________________ Attach additional sheet if necessary TOTAL AMOUNT SUBMI1TED 12 S6 $________ Money Order No of Applications $250 TOTAL Account 2830-412600-100700 City of South Bend Community Economic Development Jon Hunt Ann Kolata Executive Director Deputy Executive Director November 17 1995 Community and Economic Development City of South Bend 1200 County-City Building South Bend Indiana 46601 EIS Environmental Engineers Inc 1701 North Ironwood Drive South Bend Indiana 46635 To Whom It May Concern This letter hereby authorizes EIS Environmental Engineers Inc on our behalf to complete sign and/or provide informationfor any Special Waste Applications Special Waste Permits Special Waste Agreements Special Waste Disposal Notifications Special Waste Letters and/or any forms related to the excavation sampling transport characterization and/or disposal of Special Waste atthe property located at 814/818 South Lafayette Blvd South Bend Indiana Sincerely Cmunity Economic Development Cy of South Bend tuttWx xih tnd tvdijxa45viil I/iSi7I lYi -1il 219i 3S-7 ci IIrnclI Buincc csiInLc Ituretu Nouinr mmci rcrriiii P1nnirri KcImim Dcc clupumccri Ktihr ci Nliriccticiii Ncmchhrmrhcmoci Xcvii lIIicilI cncIcJ Iiikc S2J cimpcv icc Iimmhcih vcmvmrc Riciccim Ix Ix mm ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29704 Community Economic Development EIS Project No 1456-8145-95 1200 County/City B1dg227 Jefferson EIS Priority South Bend In 46601 Client P.O 235-9021 CertifIcation Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDEN11FICATION Client Sample ID WC-1 812/818 South Lafayette Composite Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To QUALITY CONTROL TEST RSDSPIKE MS DMSRF PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Ash percent 92.6 10-17-95 PovlockP Corrosivity pH SU 6.8 10-30-95 WrightC CyanideTotal mgllgwet 10-20-95 WrightC Flash Point Open Cup fahrenheit 201 10-31-95 WrIghtC Paint Filteruquids liquid NONE 10-12-95 WiightC Solids Total percent 95.4 10-16-95 PovlockP SulfideTotal mg/kgwet 10-20-95 WnghtC ArsenicJCLP mg/I 0.1 0.1 10-24-95 ClearN BariumTCLP mg/i 0.96 0.01 10-24-95 ClearN CadmiumTCLP mg/I 0.01 0.01 10-24-95 ClearN ChromiumTCLP mg/i 0.21 0.01 10-24-95 ClearN LeadTCLP mg/i 0.30 0.05 10-24-95 ClearN 0.40 90 90 MercuryTCLP mg/i 0.002 0.002 10-25-95 ShaneD SeleniumTCLP mg/i 0.05 0.05 10-24-95 ClearN SilverTCLP mg/i 0.01 0.01 10-24-95 ClearN HerbicidesTCLP 10-30-95 ClearB PesticidesTCLP 10-26-95 ClearB SVOCTCLP 10-27-95 GeelsS VOCTCLP 10-27-95 MyersN See Attached TCLP ORGANICS REPORT QU ITY AS RANCFICER DI CTOR 21 Ro 5-04-94 Rdod Pop 515 ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Drwe South Bend Indiana 4F/035 219/277-5715 TCLP ORGANICS REPORT SAIWLZ ID 1-l REPORT DATI 11/13/95 $12/818 South Lafayette Compoeite RIO L7.B NO 29704 VOLATILE ORGP.NICS RESULT Banzane ND 0.02 Carbon T.tachlorjda ND 0.02 Chlorobsna.ns ND 0.02 Chlorofo ND 0.02 4Dichlorobenzen ND 0.02 2-Dichioroethan ND 0.02 1-Dichioroethylen ND 0.02 Methyl Ethyl Xeton ND 0.2 Tetrachioroetbylene ND 0.02 Trichioroethylene ND 0.02 Vinyl Chloride ND 0.1 SEMI-VOLATILE ORG3NXCS o-Cresol ND 0.1 m-Cresol ND 0.1 p-Cresol ND 0.1 Total Cresola ND 0.3 4-Din.ttrotoluane ND 0.1 Rexachlorobenzena ND 0.1 Hexachloro1 3-butadiene ND 0.1 Hezachioroathane ND 0.1 Nitrobenzene ND 0.1 Pentachiorophenol ND 1.0 Pyridin ND 0.1 2.45-Triclilorophanol ND 1.0 24 6-Trichlorophanol ND 0.1 NOTES ND Not Detected at the EQL shown EQL Estimated Quantitatjon Limit Detection Limit Lab Palm 20 R.ia.d 02-16-95 Reced Paper EIS Lab No 297oqcontlnued TEST PARAMETER RESULT DATE ANALYST Herbicide ExtractlonTCLP 10-19-95 ThompsonG Merculy DlgestionTCLP 10-24-95 ShaneD Metals Digestion ICPTCLP 10-13-95 ShaneD Pesticide ExtractionTCLP 10-19-95 ThompsonG SVOC Extraction JCLP 10-19-95 ThompsonG TCLP Extract Formation Extraction Stailed 10-12-95 WrightC Extractcn Completed 10-13-95 WrightC Solids Content percent 100 Sample Weight Extracted grams 150.0 Filter Used Whatman type GFIF InitialpH SU 6.9 pHAfterAcidAddition SU 1.7 Extraction Fluid Used number Extraction Fluid Amount ml 3000 Extraction Fluid pH SI 4.89 Final Extract pH l8hrs SU 5.3 TCLP Extract Formation ZHE Extraction Staited 10-24-95 NyeD Extraction Completed 10-25-95 NyeD Solids Content percent 100 Sample Weight Extracted grams 10.0 Filter Used Whatman type GFIF Extraction Fluid Used number Extraction Fluid Amount ml 200 Extraction Fluid pH SI 4.90 ADDITiONAL INFORMATION Chain.of-Custody ddcument is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adlusted for dilutions/concentrations Quality Control definitions are as follows %RSD Precision di replicate analysis for this sample Spike Level Parameter Spike amount in units of the result Matflx SplkeMS/Duplicate Matrix SpikeDMS recovery %RPD Precision ci Matflx Spike recovery values Inorganic Quality Control limits are enclosed CONCLUSION This sample is satisfactory with respect to the analysis performed 2l R.v 5-04-94 Recldd Pap ºji ANALYTICAL REPORT Client Report Date 11-27-95 Mr John Stark EIS Lab No 30671 Community Economic Development EIS Project No 1456-8145-95 1200 County/City B1dg227 Jefferson EIS Priority South Bend In 48601 Client P.O 235-9021 Certification Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICA11ON Client Sample ID WC-2 Composite Sample Of Stained Soil Date Sampled 11-17-95 Date Received 11-17-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST PCB mg/kgwet 0.9 0.9 11-22-95 ClearB Extract PCB 11-20-95 ThompsonG ADDfTIONAL INFORMAI1ON Chain-of-Custody ccument is enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Lime and is adjusted for dilutions/concentrations QUALITY ASSURANCE OFFICER LABORATORY DIRE OR 2001 Rev 5.04-94 Recyded Paper ENVIRONMENTAL ENGINEERS INC 701 North Ironwood Drive South Bend Indiana 46635 219/277.5715 -t CHA OF cus Too RECORD ________________ CUENT NO POJE NO CTN4.E SEE REVERSE SIDE FOR INSTRUCTIONS ___ _____________ //i io-IOS IA ii____ ____VVL.____ ___ ----itcIc ezotcA _____ REUNQUISHED DATE liME RECEIVED BY REUNQUISHED BY DAlE lIME RECEIVED BY -L-- RELINQUISHED BY DATE TIME RECEIVED BY REUNQUISHED BY DATE TIME RECEIVED BY INTACT 9BROKEN MODE OF TRANSPORTATION FIELD NOTES CN4RCF EIS VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONWOOD DR SOUTH REND IN 46635 219 2775715 CHAIN OF CUSTODY RECORD __________cur OJECT No RJEcrg4wE SEE REVERSE SIDE FOR INSTRUCTIONS EIS DESCRIP77ON ________________________ RELINQUISHED Yi Al DATE TiME RECEIVE BY RELINQUISHED BY DATE TiME RECEIVED BY jjj .-____________________-_____ RELINQUISHED BY DATE TiME RECEIVED BY RELINQUISHED BY DATE lIME RECEIVED BY .ff I4TA BROKEN MODE OF TRANSPORTATION FIELD NOTES szz US VEHICLE PUBLIC ElS ENVIRONMENTAL ENGINEERS INC 1701 IRONW000 DR SOUTH BEND IN 46635 219 2775715 Sheet Ut Project flo ____ ge11-Dcparmc3 SAHPLE LOG Client ldflam Site Location 1.oJqel/c I%14JJrA/bate ofo 9s -i.I 4cr _______________________No of Samples Collected Container Size t1IEquipmentUsedrecle 5t eeci.4\cF.Act1c4 CF EIS Samole No Sample Location Time Type of Haterial Lab No Analysis Requested 4i I1FTh 6ueJ AwcI.4 CMer tiicAij JD9 DriwEll t1 S..hcic JJ Weos Cotr jJ ______________________VOC. TCLP as ilIier_______re.e/s3ied ie it4 PraseVJIS_oil ec.277Y1__________QrCU.r _______________________________________________________Ie ias 13 LO-i.c si ii re 6ruc/74t7 VO MefqIS _________Pircr ___________________________________ ____________________CIcPuce IfIINokjLj__________..t ftr _______________________________________________________________.I Cieg-qA j-k .OI.s__________Atc _______________________________________________________________II Sc Lj ______________ ___________________ _____ _____________________aou _______________________leq1.4CC UJIit and .MOTfl1 eS-44 ____________________O1 jc _______________ _____ QnJ WF 5jAeq- __________cc.op.e _____________________________________ _____________________Rqk WC1 BgKtv63 C.o.trs S5O _______________________________ _____________________ cin4 Wcjie crr p5 _1_____________________US _________________ ___ _______OF ________ Comment 1k bm-Iqt pic-\cconec 1j10 r1aS 5qflI Uegeis pc5 fsr a...fle I...ic-I c.11ee 4tkuc/earawe 4-Pe 1-t.l5 1z3y5 aftaAe.rA Fe4 pI49 tC.hI flD 4ef. Coflectors tame Sheet _J_ Project No J3f SOIL SAHPLE LOG Client 3J-A iLJ IiJ F.IL Site Location .5 I.M iZ4/nate -c Equipment Used J/J 4r fc No of Samples Collected __________________Container Size _____________jA Fl-EIScc Sample No ithiple Locato1 Time Type of Haterlal Lab No Analysis Requested i4t qmIe /rccLc cg _______________ CeiIiq5.j scaM pie __________________________ _____________ ___ ________ Coesent aA5 eLpMeA -A4 Ad.-4.pdLIc 1J pi-_-Ic 1i--ip TA Frcn pi Iuc-cI/JecJ JiJ ex4 jA Icrz.cLr Co ec to Name Og TJ -JJj __________ih LJ.OI erCAO S.c_J_Or_L_ PROJECT sg Dept Comm 4A f.d/ PROJECT No 91 tiS S-DATE _O EIS ENVIRONMENTAL ENGINEERS INC PREPARED B__________SCALE 4lc//a Seq Eietd AJof5 ChTaCefr tIL4 c.iledre4 fro $ape UVC-/cccilo so nce /ecq//o5 ecucJt ta saflipIe 4Jas coa.j0QSeJ .so.pIc U/C- aniJ sampJr //ecleid gii o.rc -/j sI tC S./dec.rnce So.ip/C jr@I/s oJ WQ$/kc/y ic ieJec he /sccJe afca Rf944I waS 41 I/f4b fM each bac.ymu4cJ c4ae 1-Lcrco1e0cx as ficcd JepA eiraj Lcd- Ia cra er t.stpIe C/e.rac ca4l1p1s 4kThO1e oj ap/Lo redee.1pe /o-/c- AIey 41/ey SI -4 -3 Dw-I L6ND preI De.i fb@- L.da1c $ttee4 /b1A4 LaFcycHe 1vc APPENDIX IDEM SPECiAL WASTE DISPOSAL CERTIFICATION 4S6 Ih RPI IæW 96 INDIANA DEPARTMENT OF ENVIRONMENTAL MANAGEMENT We make Indiana cleaner healthier place to live EuanBayh iOONorthSenoioAveoue Governor P.O Box6OlS Kathy Prosser ianapos 462066015 taIH pI 1800451 102 Office of Solid and Hazardous Waste Management Special Waste Certification No 51083 Pursuant to 329 IAC 2-21-11 the following generator City of South Bend Dept of Community and Economic Development 8141818 South Lafayette Blvd South Bend IN 46601 has received certification from the Indiana Department of Environmental Management Office of Solid and Hazardous Waste Management for the following waste streams Soil Contaminated with Paint Residue These wastes may be disposed at any sanitary landfill specified under 329 IAC 2-21-3 as an acceptable site for the disposal of waste which is certified as special waste list of acceptable disposal sites is available from the Solid Waste Permit Section at the above address or by calling 317/232-3111 General and Special Conditions that apply to this certification are indicated on the reverse side This certification shall expire exactly years from the effective signature date below \/t\12i/3 Gregory torenz Chief Date Special Waste Permit Section Solid Waste Facilities Branch Solid and Hazardous Waste Management An Eqool Opportonty Employer Prra.don Reoyclod Pnpor General Conditions That Apply to All Special Waste Certifications The generator and/ar the hauler shall provide the landfill with copy of this certification along with advanced notification of intended disposal and provide disposal notification form with each load disposed If nuisance or pollution conditions are created immediate corrective action shall be taken Waste materials accepted under this certification shall be included on the Special Waste Monthly Report submitted to this Office by the landfill Special Wastes may not be disposed at any landfill subject to corrective action under 329 AC 2-16-9 or at any landfill which fails to maintain compliance with 329 AC lt is the generators responsibility to properly dispose of all wastes at acceptable sites It is also the responsibility of the disposal site to notify the generators if the sites disposal status changes Any changes in the raw materials the processes generating the waste or the characteristics of the waste streams shall be reported in writing to the IDEM and the disposal site prior to further disposal If it is determined that the change is substantial this certification shall be voided by written notification from IDEM The wastes shall not contain free liquids The wastes shall not present fire or explosion hazard Special Conditions That Are Required For Disposal of the Wastes Will Be Indicated By The Reviewers Initials new TCLP shall be provided to the IDEM at the time of renewal of this certification Each waste stream shall be analyzed separately This is an intended one time only disposal If the disposal quantity sustantially exceeds the amount anticipated this Office shall be notified in accordance with General Condition Number Anticipated Disposal Quantity cubic yards CL $jer/Date cc John Stark City of South Bend Dept of Comm and Econ Dcv 1200 County-City Bldg South Bend IN 46601 Wanda Baxter-Potten ElS Environmental Engineers 1701 Ironwood Dr South Bend IN 46635 APPENDIX DISPOSAL APPLICATION PRAIRIE VIEW LANDFILL 145696\REI I\9601-Yh GENERATORS WASTE PROFILE SHEET PLEASE PRINT IN INK OR TYPE __________Waste Profile Sheet Code WMNA This form is to be used to comply with the requirements of waste agreement INSTRUCTIONS FOR COMPLETING THIS FORM ARE ATtACHED __________ Sh.d.d Ar..s For ConiracIor U.Only Decision Expiration Date Contractor Sales Rep _________________Service Agr Renewal Date A.WASTEGENERATOF\INFORMATIO1I Generator Name Snim eaa UT ef SIC Code Facility Address site of waste generation fPi_/Si.c I..w fnm HIT Blvd Generator City State/Province 8ii Jt...Ac3 Zip/Postal Code Generator USEPA/Federal 10 .4/A State/Province ID _________________ Technical Contact S4.rzr Phone 3.S 9.2 7J.._ WASTE STREAM INFORMATION See lnstp.ictiqns Name of Waste k.mAoITd ./ Process Generating Waste .5p.II /ITC.A L.fl Annual Amount/Units Apr .s t/nnSrIS Type Type Special Handling Instructions/Supplemental Information AJD4 Incidental Waste Types and Amounts AJAJP TRANSPORTATiON INFORMATION Method of Shipment Bulk Liquid Bulk Sludge Bulk Solid Drum/Box Other _______________________ Supplemental Shipping Information ___________________________________________________________________________________________ 7ai-ped Owp Yruc.k Is this DOT hazardous material No Yes If yes complete Hazard Class/ID ____________________________ Reportable Quantity/Units lb/kg Shipping Name TECHNICAL MANAGER DECISION Check One APPROVED DISAPPROVED Check if additional information is attached If Disapproved Explain If Approved Continue Management Methods Precautions Conditions or Limitations on Approval For Type Wastes Laboratory Analysis of Representative Sample Was Waived Attached It waived explain why ist Non-WMI Facility that is Approved to Manage this Waste Date _____________________ Tech Mgr Signature Name Print Date _____________________ MANAGEMENT FACILITY INFORMATION DECISION Proposed Management Facility Proposed Intermediate Transfer Facility Transporter Management Facility Gen Mgr Decision Check One APPROVED DISAPPROVED If Disapproved Explain It Approved List Precautions Conditions or Limitations on Approval General Mgr Signature Name Print Date ____________________ Turn Paae and CornDleie Side II Type Soecial Waste only comolete Part of Side 21 GENERATORS WASTE PROFILE SHEET PLEASE PRINT IN INK OR TYPE PHYSICAL CHARACTERISTICS OF WASTE See Instructions Color Does the waste have Physical State 70 F/21 Layers Specific Gravity Free Liquids r41 strong incidental odor ..Solid Semi-Solid Multi-layered .5 Yes FE No 6-k No Yes if so Liquid Powder Bi-layered Range Volume describe Othec Single Phased pH02 02-4 14.7 17-10 D1o-12.s D12.5 ORange DNA Flash Point None 40F/60C 140 99F/60 93C 200F193C Closed Cup Oen Cup CHEMICAL COMPOSITIOI RANGE IM1N-MAX Anci.ly .icc fsr1.Does the waste contain any of the following .i provide concentration if known 14 ..A NO or LESS THAN or ACTUAL _____________________________________PCBs 150 ppm ppm ___________________________________________Cyanides 30 ppm ppm ___________________________________________SuIf ides 500 ppm ppm Total __________% Please note Unless analytical results are attached the chemical composition identification should include at minimum Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver Pesticides Herbicides and any other TCLP constituents that may be present in the waste The total composition must be greater than or equal to 100%.0001%ppm or mg/I Indicate method used to determine composition if provided TCLP Total Other ______________ SAMPLING SOURCE e.g.Drum Lagoon Pit Pond Tank Vat sLa5 Rs..NeJom lOCAl 1O4 Co.14qA4.tp letI qlr REPRESENTATIVE SAMPLE CERTIFICATION Print Samplers Name Des gcrJ iS Sample Date k.7/iO/fS /1/i /95 Samplers Title is Samplers Employer if other than Generator EAJr-IA aeA 4cu J-c Zac The samplers signature certifies that any sample submitte is sentative of the waste described above pursuant to 40 CFR 261 20c or GENERATOR CERTIFICATION By signing this profile sheet the Generator certifies This waste is not Hazardous Waste as defined by USEPA or Canadian Federal regulation and/or the state/province This waste does not contain regulated radioactive materials or regulated concentrations of PCBs Polychlorinated Biphenyls The unshaded portions of this sheet and the attachments contain true and accurate descriptions of the waste material All relevant informa lion regarding known or suspected hazards in the possession of the Generator has been disclosed The Generator has read and understands the Contractors Definition of Special Waste included in Part 6.5 of the attached instructions form All types and amounts of special wastes provided in incidental amounts have been identified in section 6.6 of this form The analytical data presented herein or attached hereto were derived from testing representative sample taken in accordance with 40 CFR 261.20c or equivalent rules If any changes occur in the character waste the Generator shall notify the Contractor prior to providing the waste to the Contractor Signature Title Projinc Name lTvpe or Printl A5 tO Date Prairie View Landfill SERVICE AGREEMENT 95505 Shively Eoad NON-HAZARDOUS WASTE DISPOSAL Wyatt Indiana 46505 219/5464475 The abovenamed disposal facility and corporation are referred to herein as Facility and Contractor respectisels rCUST0MERs BILLING NAME ure.i CUSTOMERS BILLING ADDRESS Aj Ir0 Pr STATE/PROVINCE ZIP/POSTAL CODE nud1 teL Ihdizg CONTACT P4v Jef5 er PHONE NUMBER itEFERENCE BANK CONTACT PHONE NUMBER DUN BRADSTREET NA Credit nay hr esienuod to Customer after apprepri.ito credit information in loire acceptable to Contractor has been presented to and reviervod by Coierayrir Contractor man in os sole discretion require collateral depirsir tie rho tonn of cash letter itt credit or surety hondl acceptable to Contractor It Is the scsro.ssihiliii of the Customer keep said collateral deposit current Collateral deposits ishoto utilized may he adjusted when there is an iociease in disposal ioosage afluier rates Collateral deticiencier must be corrocted within 31 days of notice of required idlusimeet This is legally binding contract and Contractor agrees to provide and customer agrees to accept thc waste disposal services subject to the terms and conditions speciried in this contract ESTIMATED \iililLNT 11 WASTE fOR DlSFOSAt llnclude units e.g cubic yards pounds kilogramsl SPECIAL INSTRLCTIONSt NO FREE LIQUIDS OR DRUMS ALLOWABLE ALL LOADS MUST BE ACCOMPANIED BY DISPOSAL NOTIFICATION WITH ORIGINAL SIGNATURES ALL LOADS MUST BE TARPED DRUMS ARE ACCEPTED ON CASE BY CASE BASIS -Qk.1O-5-J INCIDENTAL SPECIAL WASTE TYPES AND .hSflUNTS LIE MS AND COsDI NSON EiERSE SIDEAND TIlE \fltCIIEI CONTRACTORS DEFINITION OF SPFCLSL WASTE IRE PARTOETHIS SfRELiIEr kiNTR\LrIR JMIiA GOrgE TERMS AND CONDITIONS OF DISPOSAL SERVICE AGREEMENT The Aereement The entire agreement of the parties for the disposal of waste the Agreement shall consist of this Service Agreement and any applicable Generators Waste Profile Sheetls Wastes Accented at Facility Customer warrants that the waste delivered to Contractor hereunder will not contain regulated quantity of any hazardous radioactive or toxic waste or substance as defined by applicable Federal state local or provincial law or regnlations Special Waste Customer acknowledges reading the attached Contractors Delinition of Special Waste dated 021921 and warrants that the waste delivered to Contractor hereunder will not contain any Special Waste unless and except as specifically described on Generators Waste Profile Sheets attached hereto or svhich Contractor later agrees to accept In svriting or 21 incidental amounts of Special Waste as listed by Customer in the Incidental Specinl asiejypesand Amounts sectvoinof ihi tnrmiThe parties may incorporate additional Special Waste as part of this Agreement if prior to delivery of such waste to Contractor Castomer has provided Generators Waste Profile Sheet for such waste and Contractor has approved disposal of such waste in writing Customer agrees to comply with precautions limitations and condition contained in Cootractoris written notice of approval of Special \Visie Rihls of Refusal/Relection Contractor has the right to refuse or reje after acceptance any toad of isastes delivered to bc Facility if the Contractor belieses the Customer has breached loris breaching its svarranites or agreements hereunder If Customer delivers ivasies in breach of any warranty or agreements herein Contractor may 0th ojg discretion either remove and dispose of ho waste and charge Customer for the costs or require Customer to promptly remc .e waste Limited l.icense to Enter Daring the term of this Agreement Customer shall have license to enter the Facility for the limited purpose 01 and only to the extent necessary for off.loading waste at the location and inthe manner directed by Contractor Except in an emergency or at the express direction of Contractor Custornerspersofdiel skull noi-leavn the immedidta siciuntv ofstheir vehicle Alter off.loading the svaste Customers personnel shall promptly leave the Facility Under no circumstances shalt Customer or its personnel engage in any scavenging of waste at the Facility Contractor may refuse to accept waste from and shall deny an entrance license to any at Customers personnel whom Contractor believes is under the inlinence of alcohol or other chemical substances Charites and Payment Unless otherwise agreed in writing by the panics hereto Customer agrees to pay Contractors posted disposal rates which may change from time to time Customer shalt be liable for all taves fees or other charges imposed apon the disposal at Customers waste by Federal state local or provincial laws and regulations Payment shall be made by Customer within ten 10 days after the date of the invoice from Contractor In the event that any payment is not made when due Contractor may terminate the Agreement Customer agrees to pay late fee for all past due payments not to exceed the maximum rate allowed by applicable law Intt This Agreement shall continue in effect until terminated by either party with or without cause upon forty.eight 48 hours notice Customers representations and svarranttes regarding the waste delivered and the mutual indemnities set forth herein shalt survive termination of this Agreement Drivers Knowledee and Authority Customer warrants that its drivers who deliver waste to the Facility have been advised by Customer of Contractors prohibition of deliveries of hazardous radioactive or toxic waste to the Facility of Contractors restrictions on delivenes of Special Waste to the Facility of the definitions ofhazardons waste and Special Waste herein provided and of the terms of this license toenier the Facility Indemnificntion Contractor agrees to indemnify save harmless and defend the Customer from and against any and alt liabilities claims penalties foilettures suits and the costs and expenses incident thereto lincluding costs of defense settlement and reasonable attorneys fees which it may hereafter incur become responsible for or pay oat as result of death or bodily injunes to any person destruction or damage to any property contamination of or adverse effects on the environment or any violation of governmental laws regnlations or orders caused solely by the negligent act negligent omission or willful misconduct of Contractors employees or its subcontractors in the performance of the Agreement Customer agrees to indemnify save harmless and defend Contractor from and against any and all liabilities claims penalties forfeitures suits and the costs and expenses incident thereto lincluding costs of defense settlement and reasonable attorneys fees which it may hereafter incur become responsible for or pay out as resalt of death or bodily injuries to any person destruction or damage to any property contamination of or adverse effects on the ensireoment or any violation of governmental laiss regulations or orders caused in whole or in part by the Customers breach of any warranty term or provision of the Agreement or any negligent act negligent omission or wittfnl misconduct of the Customer its employees or sabcontractors in the performance of he Agreement Attorneys Fees In the event of breach of the Agreement the breaching party shall pay all reasonable attorneys fees collection fees and costs of the other party incident to any aciien brought to enforce the Agreement Assienment Neither party may assign transfer or otherwise lest in any other company entity or person .snv il its rights sr obligations under the Agreement without the prior svntten consent of the other party svhich consc shall not be unreasonably wehheld provided however that Contractor may without any such prior written consent assign its rights and/or obligations under the Agreement to subsidiary or affiliate corporation Miscellaneous The Agreement shall be binding upon md shall Inure vibe honctit sI the parties hereto and their respective successors and permitted assigns The Agreement shalt he reserved by and coosirued sm accirdance with the laws at the State in which the Facility is located 02/92 INDIANA DEPARTMENT OF ENVIRONMENTAL MANEcT We make Indiana cleaner healt hier place to live Euan Bayh 100 North SenatO Avenue Governor P.O Boa 6015 Kathy Prosser India op Is da 46206 6015 ro La Fl pl 800 45 80 Office of Solid and Hazardous Waste Management Special Waste Certification No 51083 Pursuant to 329 IAC 2-21-11 the following generator City of South Bend Dept of Community and Economic Development 814/818 South Lafayette Blvd South Bend IN 46601 has received certification from the Indiana Department of Environmental Management Office of Solid and Hazardous Waste Management for the following waste streams Soil Contaminated with Paint Residue These wastes may be disposed at any sanitary landfill specified under 329 IAC 2-21-3 as an acceptable site for the disposal of waste which is certified as special waste list of acceptable disposal sites is available from the Solid Waste Permit Section at the above address or by calling 317/232-3111 General and Special Conditions that apply to this certification are indicated on the reverse side This certification shall expire exactly years from the effective signature date below 12/J/4 Greiorenz Date Special Waste Permit Section Solid Waste Facilities Branch Solid and Hazardous Waste Management An Equal Opportunity Eneployer on Reoyctod Pop.r General Conditions That Apply to All Special Waste Certifications The generator andlor the hauler shall provide the landfill with copy of this certification along with advanced notification of intended disposal and provide disposal notification form with each load disposed If nuisance or pollution conditions are created immediate corrective action shall be taken Waste materials accepted under this certification shall be included on the Special Waste Monthly Report submitted to this Office by the landfill Special Wastes may not be disposed at any landfill subject to corrective action under 329 lAG 2-16-9 or at any landfill which fails to maintain compliance with 329 IAC It is the generators responsibility to properly dispose of all wastes at acceptable sites It is also the responsibility of the disposal site to notify the generators if the sites disposal status changes Any changes in the raw materials the processes generating the waste or the characteristics of the waste streams shall be reported in writing to the IDEM and the disposal site prior to further disposal If it is determined that the chance is substantial this certification shall be voided by written notification from IDEM The wastes shall not contain free liquids The wastes shall not present fire or explosion hazard Special Conditions That Are Required For Disposal of the Wastes Will Be Indicated By The Reviewers Initials new TCLP shall be provided to the IDEM at the time of renewal of this certification Each waste stream shall be analyzed separately This is an intended one time only disposal If the disposal quantity sustantially exceeds the amount anticipated this Office shall be notified in accordance with General Condition Number Anticipated Disposal Quantity cubic yards .1 jer/Date cc John Stark City of South Bend Dept of Comm and Econ Dcv 1200 County-City Bldg South Bend IN 46601 Wanda Baxter-Potter EIS Environmental Engineers 1701 Ironwood Dr South Bend IN 46635 ANALYTICAL REPORT Client Report Date 11-13-95 Mr John Stark EIS Lab No 29704 Community Economic Development EIS Project No 1456-8145-95 1200 County/City 81dg227 Jefferson EIS Pnority South Bend In 46601 Client P.O 235-9021 Cerfication Indiana Drinking Water Certificate No C-71 -02 Invoice To SAMPLE IDENTIFICATION Client Sample ID WC-1 8121818 South Lafayette Composite Date Sampled 10-10-95 Date Received 10-11-95 Report To CLIENT Extra Report To OUAUTY CONTROL TEST RSDSPIKE MS DMSRPD PARAMETER UNITS RESULT DL DATE ANALYST LEVEL %R %R Ash percent 92.6 10-17-95 PoviockP Corrosivity pH SU 6.8 10-30-95 WrightC CyanideTotal mg/kgwet 10-20-95 WrightC Flash Point Open Cup fahrenheit 201 10-31-95 WrightC Paint Fifteruquids liquid NONE 10-12-95 WrightC Solids Total percent 95.4 10-16-95 PovloclcP SultideTotal mg/kgwet 10-20-95 WrightC ArsenicTCLP mg/I 0.1 0.1 10-24-95 ClearN BariumTCLP mg/I 0.96 0.01 10-24-95 ClearN Cadmium.TCLP mg/I 0.01 0.01 10-24-95 ClearN ChromiumTCLP mg/i 0.21 0.01 10-24-95 ClearN LeadTCLP mg/I 0.30 0.05 10-24-95 ClearN 0.40 90 90 MercwyTCLP mg/I 0.002 0002 10-25-95 ShaneD SeleniumTCLP mg/I 0.05 0.05 10-24-95 ClearN SilverTCLP mg/I 0.01 0.01 10-24-95 ClearN HerbidesTCLP 10-30-95 ClearB PesticidesTCLP 10-26-95 ClearB SVOCTCLP 10-27-95 GeelsS VOCTCLP 10-27-95 MyersN See Attached TCLP ORGANICS REPORT QUALITY ASSURANE OFFICER LABORATORY DI ECTO 2001 Rn 0-04-94 Reyod Papo ES ENVIRONMENTAL ENGINEERS INC 1701 Nor6 IronwoOd Onve Soud Bend Indiana 46635 219/277-5715 EIS Lab No 29704continued TEST PARAMETER UNITS RESULT ANALYST Herbicide ExtractionTCLP 10-19-95 ThompsonG Mercury DigestionTCLP 10-24-95 ShaneD Metals Digestion ICPTCLP 10-13-95 ShaneD Pesticide Extraction .TCLP 10-19-95 ThompsonG SVOC ExtractionTCLP 10-19-95 ThompsonG TCLP Extract Formation Extraction Started 10-12-95 WrightC Extraction Completed 10-13-95 WrightC Solids Content percent 100 Sample Weight Extracted grams 150.0 Fifter Used Whairnan type GFF Initial pH SU 6.9 pH After Acid Miition SU 1.7 Extraction fluid Used number Extraction Fluid Amount mf 3000 Extraction fluid pH SU 4.89 Final Extract pH l8hrs SU 5.3 TCLP Extract Formation ZHE Extraction Started 10-24-95 NyeD Extraction Completed 10-25-95 NyeD Solids Content percent 100 Sample Weight Extracted grams 10.0 FiRer Used Whatman type GF/F Extraction Fluid Used number Extraction Fluid Amount ml 200 Extraction Fluid pH SU 4.90 ADDITIONAL INFORMA11ON Chain-of-Custody document is enclosed Reference Analytical Methods are enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations Quality Control definitions are as follows %RSD Precision at replicate analysis for this sample Spike Level Parameter Spike amount in units of the result Matrix SpikeMS/Duplicate Matrix SpikeDMS recovery %RPD Precision of Matrix Spike recovery values Inorganic Quality Control limits are enclosed CONCLUSION This sample is satisfactory with respect to the analysis performed 2O1 Rev Poqce TCLP ORGANICS REPORT SAMPLE IIC-1 REPORT DATE 11/13/95 812/818 South Xafayetta ColEposite ZIS LAB NO 29704 g/ VOLATILE ORGABICS RZSfl.T Henaun ND 0.02 Carbon Tetrach.orid5 ND 0.02 Chlorobenzene ND 0.02 Chloroform ND 0.02 4-Dichi.orobenzene MD 0.02 2Oichloroethane ND 0.02 l-DichlOroetbylene ND 0.02 Methyl Ethyl Ratone ND 0.2 Tetrach.oroethylene MD 0.02 Trichloroethylene ND 0.02 Vinyl Chloride ND 0.1 SEMI-VOLATILE ORG7.NXCS oCreaol ND 0.1 m-Creeol ND 0.1 p-Creeol ND 0.1 Total Creeoi.3 ND 0.3 24-Dinitrotoluene ND 0.1 Hexachlorobenzene MD 0.1 Rexachloro-l 3-butadiene ND 0.1 Hexachloroethane ND 0.1 Nitrobenzena ND 0.1 Pentachlorophenol ND 1.0 Pyridine ND 0.1 245-Trichlorophenoi ND 1.0 246-Trichlorophenol ND 0.1 PESTICIDES and HERBICIDES Chlordana ND 0.02 Endrin ND 0.001 Heptachlor and its epoxides NO 0.001 Lindane NJ 0.001 Methoxychlor ND 0.001 Toxaphene ND 0.03 240 ND 0.013 245TPSilvex ND 0.01 NOTES ND Not Detected at the EQL shown EQL Estimated Quantitation Limit Detection Limit Lab Fern 2030 Reae0 100-16-95 ANALYTICAL REPORT Client Report Date 11-27-95 Mr John Stark EIS Lab No 30671 Community Economic Development EIS Project No 1456-8145-95 1200 County/City Bldg 227 Jefferson EIS Pnority South Bend In 46601 Client P.O 235-9021 CertifIcation Indiana Drinking Water Certificate No C-71-02 Invoice To SAMPLE IDENTIFICA11ON Client Sample ID WC-2 Composite Sample Of Stained Soil Date Sampled 11-17-95 Date Received 11-17-95 Report To CLIENT Extra Report To TEST PARAMETER UNITS RESULT DL DATE ANALYST PCB mg/kgwet 0.9 0.9 11-22-95 ClearB Extract PCB 11-20-95 ThompsonG ADDITIONAL INFORMATION Chain-of-Custody cument is enclosed Sample was iced upon receipt Not Detected at the Detection Limit DL shown DL Detection Limit and is adjusted for dilutions/concentrations QU LITY ASSURA OFFICER LABORATORY Dl ECTO 2r Rev 5-04th41 00004 P00 FIS ENVIRONMENTAL ENGINEERS INC 1701 North Ironwood Dnve SouA Bend Indiana 46635 2191277-5715 EDEFORINSUCflONS /0 s- pS9 ________ ____-itJc jecoto RELINQUISHED PAW TiME RECEIVED BY RELINQUISHED BY DATE TiME RECEIVED BY 1- LM-.bQt -c RELINQUISHED BY DATE TIME RECEIVED BY REUNQUISHED BY DATE TiME RECEIVED BY z$TAcTBROW4 MODE OF TRANSPORTATION FIELD NOTES VEHICLE PUBUC EIS ENVIRONMENTAL ENGINEERS INC 1701 IRONWOOD DR SOUTH BEND IN 46635 219 2775715 CHAIN OF CUSTODY RECOII WENT NQ PROJECT NO PROJECT N4ME SEE REVERSE SIDE FOR usrucnos .H.1 4Y777777777 4MPLERS USE ONLY lIME OF PRIMARY 4MPLE DESCRIPTION iAl STAIr ____ ____L4i ____ ___ ____ ___ REliNQUISHED DAIT TIME RECEI BY RELINQUISHED BY D4TE TIME RECEWED BY Isr91j/o3 _______ _______ RELiNQUISHED BY DATE flUE RECEIVED BY RELINQUISHED BY DATE TIME RECEIVED BY i..ll4T4CT MODE OF TRANSPORTATION FIELD NOTES 1/S VEHICLE PUBLIC EIS ENVIRONMENTAL ENGINtRS INC 1701 IRONW000 OR SOUTH BEND IN 46635 219 2775715 Sheet Project Hu .LSLI1 OLIk teJ DrpaIniciI SAhPLE LOG Client flflOIL uniI4f Site Location 9/i//el/a 5Jrtbace 0-10 9s IJ cpk1 _______________________No of Samples Collected Container Size I.kukftIelquipmentUseddrell9e 5ejeJDiettdie4 F.ct EIS Sample Ho Sam le Location Time Type of_Haterlal Lab Ho AnaIysiquestedQ4iJTiicerIO9raA7oVoc ________________________________________________ _____________________ 11jV1I Qacui-_____________________ ________________________o._h.iInq ______________________________________ _____________________ C.ClIqite Fo retide/scd TCL 71krAhq4iaqcqiJ..n __________2g7q_________grcg __________________ le.hAce Su4J Oqrk flre4 %pAll31L-j.c SO re Po.e/147b7 LkX Mef4LS _________IA _______________________________________________ Soji Icr.Poc If.11oii of IW$j.ip________ri fri __________________________________________________ .0lI CIcgta4JkOA.5Ijkt.a js 4.o-Lc_________Ar _______________________________________________________ olI ciqrQ4e lL44rJSThJ.5 IUOSt of uI-j ________aoo -o.i-as-.i CJe4ce .5Wtlnd ______1reCj o1 2LLc _______________ _____ OkO$l 0lOSOq fii ________________flelqs_______________________________________________ ru 1- .f6.ShS4Ji --_____________________-_-_- _______oIe caMr ____________________2M1I J6 vet -flCIIIC0ArIrco_____________________________4--S5 I4I /1G-wcjj torI1-r .-S Comment Ifac q1IpIA j.ag4e II.A_Tea inr\COAI J1J.Q eCk 5qme eUeie Tht a..ipC5 f.r afle Q-tmr 21taMLæCLd Nok5 LAI1IQ 1fr4 flD 4ef. Cofletors IIme P41I p4Cr Sheet Project t1 // SOIL SIHPLB LOC client Site Location b7zwuace 1FI Cqulpatent Used 4r cc1/ca No of Samples Collected __________________Container Size _____________ ace El-EIS Sasple Un Ltple Locatiofi Time Type of Haterlal Lab No Analysis RequestedPjjA04$ple eJ J/jrjW6--b kcJecf Oto5 QAcde-_____18_________t.-4a f1e __________cc Cowiaent j13 eoMej-p4.J jAIe r-ch icclHaOj 1prr o.149 1.I pd 5QWC ti //Jeci bJi4 Ak /UV Co ec Ia tIAme /1 __________L4/u4%Pi U-14-res AO St.sEET_j......OF__L PROJECT Dep3 Comm Oeve/ PRoJECT No 91 Lj.-9S DATE _f /O j.S EIS ENVIRONMENTAL ENGINEERS INC PREPARED ___________SCALE JJC SCQ fe Aioes i4e fros A%pIe UV cJ FhM i/rcs.dw /ccci Jrec1/y va4oue ance /ccq/soi%S ecicA ta aipe u.io Co c2sJ cztc ujo sam1oIe U/C-i 6rQuvJ .pJr.s cQG- 39 //eJeci Q.rec 4J r51 4e CtecilQnce SompIC 5Q1/5 oncJ wo$f/y 4O 4ecIecl 3y the q/rcsicJ.e area Rc.sqI was I/i%CQCi bacmc4ncI 5c4ie c.reoPeOcX 87 Cof/Cd Ce1er4 LualZ 5.iPLe c/er4 p1 5ee a1ip/. .4e1eJ 5ip/Ic4 cr /a-o-- .4 Porkiny ---fe1 ..-j-----.J.c 4/Iey jItc1s_ L6ND pr.t1 ci 8ro.4 EJ 1O .r A4 Lo.f.ycf1e City of South Bend 1S65 .i i2flfli1 Community Economic Development Jon Hunt Ann Kolata Executive Director Deputy Executive Director November 17 1995 Community and Economic Development City of South Bend 1200 County-City Building South Bend indiana 46601 EIS Environmental Engineers Inc 1701 North Ironwood Drive South Bend Indiana 46635 To Whom It May Concern This letter hereby authorizes EIS Environmental Engineers Inc on our behalf to complete sign and/or provide informationfor any Special Waste Applications Special Waste Permits Special Waste Agreements Special Waste Disposal Notifications Special Waste Letters and/or any forms related to the excavation sampling transport characterization and/or disposal of Special Waste atthe property located at 814/818 South Lafayette Blvd South Bend Indiana SOhBend 2UCini ji I3uidix iiih Bend Indiin 46BI 2B/2Sfl7I Fx 219 25-52I 110 219 23SS7 Rcjcc IIIlL1l Itureju ii I1tuint Nininci.l lriuraiii Plannri Kici IkeIu1uicnt K.ILhrvn I1.iuiiitiriner \1.znaccenl NelUhhorhjuid lcc upIIlCflt Dcrcid ik 52 Nc PIcc Ijlii einar Pcne \1 ci r- APPENDIX APPROVAL LETTER PRAIRIE VIEW LANDFILL 14%QRPII 9OOI PrairIe Vtew Recycting lsposaI Factilty P0 Box 128 15505 Shvely Road Waste Management Company Wyatt ndaria 465P5 22/546-4475 January 1996 David Jeffers EIS 1701 Ironwood Dr South Bend fN 46635 RE WMNA194556 EXP 03/31/96 State Permit 51083 EXP 12/14/00 Dear Rozite Your Contaminated Soil from City of South Bend has been approved for disposal at Prairie View RDF Listed below are the conditions under which we may accept your waste No free liquids allowed Disposal notification required with each load Thank you for choosing Prairie View RDF for your special waste disposal needs Please contact me with any questions or concerns at 219 546-4475 Sincerely yours Kd6j Snittli Kelly Smith Special waste and Division Compliance Coordinator N3TE MANAGEMENT OF iNDIANA NO APPENDIX STATEMENT OF ORIGIN DOCUMENTING THE TRANSPORT OF EXCAVATED SOIL FROM THE SITE FOR DISPOSAL AT THE PRAIRIE VIEW LANDFILL L4696\RP 1I\9Oi 16 Ill STATEMENT OF ORGIN OF SOLID WASTE WITHIN INDIANA 182084 In order to comply with the requirement sot forth in IC 13-7-22-2.7c hereby certify _____________ underoath that to the best of my knowledge the solidwaste being transported herein was /hNCA N0\ generated as follows ____ Name of Vehicle Operator Signature of VehicIOperator Date County or State Percentage Type of if other than Indiana of Load Waste /- Type of Waste Municipal Solid Waste Medical ii ill Construction Asbestos MSW -Other Ash Ill BOther ricur-uc fLU ft UYW 15 HLIJELY RUU -- LU PQftIXiU WYATT -t4 4Æ592946447 II 11111 lI CUSTOMER IH EsTNO ULUU -I -l JrnhI-lwJIII lH ill HrHr 4.r CODE 1.09 sCI9N LOAD QNTI1E AMOUNT 4. TTE lIjuNT rEE 0.00 II ill liii C0Py2