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HomeMy WebLinkAboutSB-0208 2001 Grauvogel Initial Site Characterization, Heating Oil Spill Blg 69Project 2032 INITIAL SITE CHARACTERIZATION HEATING OIL SPILL 730 United Drive Studebaker Building 69 EPA Site IDINR000101006 IDEM Incident 2001-01-156 prepared for the Board of Public Works City of South Bend Indiana prepared by Grauvogel Associates Granger Indiana October2001 SAFETY HEALTH ENVIRONMENTFORD005212 jGrauvoe1 Associates November 2001 Indiana Department of lnvi roumental Management Office of Land Quality Remediation services Branch 100 North Senate Avenue P0 Box 60 15 Indianapolis IN 46206-6015 Attention Mr Gerald OCallaghari Subject Spill Incident200l-01-156 Dear Gerald Enclosed is the Initial Site Characterization for the subject incident located at 730 United Drive South Bend IN This site is located in the Studebaker Redevelopment Corridor and new Department of Public Works building is currently under construction there As we have investigated this spill on behalf of the City of South Bend it has become clearer that the material spilled was heating oil used for the former Studebaker Building 113 located to the east of the apparent tank location rather than diesel fuel or gasoline As detailed in the report the tanks was removed sometime prior to May 1986 and perhaps by Studebaker Corporation even earlier with no records The spill is located outside the 5-year time-of-travel radius of the South Bend North Weillield and is actually just outside the 10-year radius as well We found very little contamination and the contamination was limited to small area around the original tank site We also ibund evidence of chlorinated solvent plume from upgradient Based on these findings we are recommending no action response Should your review deem remediation response necessary we recommend some form of bioremediation using the existing monitoring wells lr injection points Please direct your technical review questions and correspondence to my attention at your convenience Sincerely Lawrence Gruvogel PE Cu-I CSP Enclosures Initial Site Characterization cc Littrell/South Bend 17660 Fall Creek Drive Granger Indiana 46530 219 277-4770 Project 2032 INITIAL SITE CHARACTERIZATION HEATING OIL SPILL 730 United Drive Studebaker Building 69 EPA Site ID INR0001O1006 IDEM Incident 2001-01-156 prepared for the Board of Public Works City of South Bend Indiana iI prepared by Grauvogel Associates Granger Indiana October 2001 SAFETY HEALTH ENVIRONMENTFORD005214 Project 2032 INITIAL SITE CHARACTERIZATION HEATING OIL SPILL 730 United Drive Studebaker Building 69 EPA Site ID INR000 101006 IDEM Incident 2001-01-156 prepared for the Board of Public Works City of South Bend Indiana October 2001 Prepared and Certified by 17799 STATE OF ____ Lawrence c1uoge1 PECIHCSP GratvogeI Associates ______ID 730 United Drive Heating Oil Spill ISC IDEM Incident 2001-01-156 2032 October2001 TABLE OF CONTENTS SECTION PAGE Executive Summary Ii Purpose and Methods III Chronology IV Investigation Results Geology Hydrogeology Soil Samples Groundwater Sampling Conclusions VI Recommendations VII References TABLES Spill Site Soil Sample Results Summary TPH 10 Spill Site Groundwater Sample Results Summary 11 FIGURES Former UST Site with Borings and Test Wells 12 Local Groundwater Flow at Former UST Site 13 Groundwater Contamination non-Chlorinated VOC 14 Groundwater Contamination Total SVOC 15 Groundwater Contamination Chlorinated VOC 16 Groundwater Contamination Chlorinated VOC Genera Location USGS 7.5 Quadrangle 18 1993 Plat Map 730 United Drive 19 Wellhead Protection Area Leeper Park North 20 730 United Drive Heating Oil Spill ISC IDEM IncidentN 2001-01-156 2032 October2001 EXECUTIVE SUMMARY 35-year-old heating oil spill affecting the groundwater was discovered at the site of lbrmer Studebaker Corporation UST at 730 United Drive South Bend IN formerly Studebaker Building 69 The maximum groundwater contamination concentration reported at distance of 40 downgradient from the spill from three downgradient well clusters screened from 20 to 45 below grade was 4336 igIL non-chlorinated VOC 885 tgIL SVOC and 5810 ig/L TPI-1 at 12 feet below the groundwater surface The concentrations at the groundwater surface at this same location were 15.3 jig/L non-chlorinated VOC 72 pgIL SVOC and 6260 ig/L TIH The nearest potential public health and environmental impacts from the plume are the Leeper Park municipal weUfield V2 mile north-northeast and the St Joseph River mile northeast of the spill respectively The spill is beyond the 5-year time-of-travel boundary of the weilfield and there are no private wells in the affected portion of the City Adverse impacts at these distances are not expected The No Action alternative is recommended II PURPOSE AND METHODS This report presents the details of the findings of the initial site characterization for heating oil spill at former underground storage tank UST location on Studebaker Automobile Corporation property now owned by the City of South Bend Indiana The UST was associated with operations in the former Studebaker Buildings 69 and 113 Building 69 was demolished in 2000 as part of the current construction project at the site The UST was removed sometime prior to the May 1986 registration deadline in Indiana but the party removing the tank and any records of the removal were unknown The spill site was discovered during the preliminary environmental investigation phase of the site demolition for Studebaker Building 69 730 United Drive The demolition by the City was in preparation for the construction of new Department of Public Works building and storage yard The contamination was found at UST location shown on the June 1954 general site plan for the Studebaker manufacturing pant Three other probable UST locations were included in that same investigation through interviews with long-time Studebaker employees familiar with that portion of the plant but no tanks or contamination were found at these other locations The purpose of this Initial Site Characterization was to determine the chemical constituents of the spill the extent of the spill in the soil above the groundwater table the depth and flow direction of the groundwater the constituents and extent of contamination in the groundwater the underlying hydrogeology at the site as it impacted movement of the spill in the groundwater and an estimate of the potential public health and environmental impacts of any groundwater contaminant plume detected To this end soil boring was completed at the center of the spill and three downgradient and one upgradient clusters of diameter PVC-cased and screened monitoring wells varying in depth from 25 to 45 feet were installed Three well clusters were downgradient of the spill and one was upgradient Soil sampling was done with hollow core auger and standard split spoon sampler driven ahead of the auger in one boring of each cluster Soil samples recovered from the borings at the spill were analyzed tbr total petroleum hydrocarbons TPH Soil samples collected during the monitoring well installations were screened for TPH in the field Groundwater was analyzed for total basic acidic and neutral 730 United Drive Heating Oil Spill ISC IDEM Incident200L0I-l56 _______ 2032 October 2001 semi-volatile organics SVOC total petroleum hydrocarbons TPH benzene-ethyl benzene touene-xylenes BETX and volatile organics VOC CHRONOLOGY In the process of clearing the site formerly occupied by Studebaker Buildings 69 139 and 140 for construction of the new Department of Public Works building four suspected UST sites from available records were identified and soil boring completed at each location down to the water table These preliminary borings were completed on January 2001 This work identified soil contamination at the present site groundwater sample was collected from the boring when suspected contaminated soil in close proximity to the groundwater table was discovered and this sample confirmed impact by the spill on the groundwater The spill was reported to IDEM on January 26 2001 with the receipt of the soil and groundwater sample results From previous work and research on other groundwater investigations in the area general groundwater flow direction to the northeast was anticipated On May 17-18 2001 the well clusters were installed at the locations illustrated in Figures and through The radii from the center of the spill for the well locations were established nominally at 50 and then adjusted by the proximity of the property line to the north constraints from the impending construction and the impact of other unrelated Studebaker-era contaminants on the site The first round of groundwater samples was collected on May 23 2001 second round was completed on June 25 2001 Iv INVESTIGATION RESULTS Geology The USDA Soil Survey for St Joseph County Indiana lists the soil at the spill site as Tyner loamy sand with 0%to 6%slopes Tyner soil has moderate to high permeability of 20 inches per hour in the upper and greater than 20 inches/hour below this depth This is well drained soil subject to droughtiness as result and offers little resistance to contamination movement downward to the groundwater The typical profile extends to 60 below grade The former UST location and the portion of the spill area on City property were under asphalt pavement until demolition of the site began and the plume remained under asphalt off-site The area will be repaved as part of the new construction The soil borings and other excavations on- site in connection with the demolition and construction activities gave ample evidence for the following site-specific soil profile grade 0.5 asphalt pavement 0.5 gravel roadway base 1-coal cinders bricks gravel and miscellaneous Studebaker-era debris 10 sharp change to native medium brown sand typical of Tyner at 10 11 gray brown dense silty clay 11 23 groundwater medium to coarse brown sand This profile was consistent with the Tyner classification No other silty clay lenses were encountered below 11 in any of the borings which were as deep as 45 The presence of at least thin heavily compacted silty clay layer in the borings suggests that the soil offers some resistance to surface spills and leaks above 10 below grade 730 United Drive Heating Oil Spill ISC IDEM lncident200l-0l-l56 ________ 2032 October2001 The DNR Water resources report for the St Joseph River valley reports the elevation of the Ellsworth shale bedrock underlying the area at 550 above mean sea level MSL The general grade elevation at the spill site was 722 MSL The site is shown in the glacial outwash zone of the aquifer so the remaining portion of the geologic cross-section consists of 150 of unconsQhdated sand and gravel down to the bedrock Hydrogeology The site lies within the St Joseph aquifer system which is characterized by fine to medium sand with zones of coarse sand and gravel interspersed with thin clay units of limited size.2 Soil borings and excavations at the site showed strata consistent with this information As such it is highly susceptible to groundwater contamination In the South Bend area there is clay unit layer separating the aquifer into an upper and lower water producing strata The bottom of this clay layer is at 600 to 635 MSL sloping to the northwest This layer some protection to City wells from this spill which are screened at about 200 below grade The St Joseph Aquifer has typically high transmissivity The nearest aquifer test about mile to the east reported transmissivity of 93 gallons per day per foot based on actual test data2 Thus once in the groundwater contaminants are capable of moving quickly downgradient On the same basis groundwater contaminants are more quickly diluted and dispersed once their source is eliminated As already mentioned the groundwater surface was encountered at approximately 23 below grade The actual elevation was 700.00 MSL at Well 5OSW-34 It is likely therefore that the UST did not have its bottom below the groundwater surface at any time and that the release was into the unsaturated vadose zone above the watertable In addition to this the overlying asphalt pavement at the UST location has also helped minimize the plume spread Figure illustrates the results of the groundwater surface gradient measurements completed on May 23 2001 As shown the groundwater flow direction at the spill is 11.5 east of north Thus the potential downgradient impact area of the spill plume lies to the north-northeast As can be seen from Figure this encompasses the South Bend urban area Adjacent property to the north northeast Figure is industrial land with former Studebaker buildings now used for warehousing Beyond this the railroad right-of-way and Stanley Coveleski Regional Stadium lie in the path of potential plume and beyond this more commercial and retail property The nearest residential area is public housing project 1000 feet north-northwest not directly in the path df potential plume The nearest residential area in the groundwater flow direction begins across the St Joseph River on the opposite side of downtown South Bend The nearest well supply in this urban area is the Leeper Park weilfield located just west of the St Joseph River l/2 mile north of the spill Figure These wells are screened from 75 to 100 and lie below 20 thick clay layer in the upper strata of the aquifer This clay unit is however discontinuous in the potentially affected area.4 Thus there is no geological protection from releases in the upper layer of the aquifer There are no private wells downgradient of the site between the spill and the St Joseph River 730 United Drive Heating Oil Spill ISC IDEM 1ncident200J01I56 2032 October2001 Figure presents the 1-year and 5-year time-of travel boundaries from the Leeper Park municipal wellfield designated the North Weilfield by the City The City Water Quality Engineer also indicated that the spill site is just outside the 10-year time-of travel boundary.4 Only sources within the 5-year boundary are regulated by the federal Wellhead Protection regulations This informtion supports conclusion that the potential impact from this spill on public health is small Soil Samples Soil samples were collected at intervals down to the groundwater at the center of the spill location during the initial drilling on January 2001 They were analyzed for total petroleum hydrocarbons TPH to screen for contamination from the suspected heating oil from the former UST at the location The results are shown in Table After soil contamination was found during the boring groundwater sample for BETX analysis was collected by screening the boring with diameter PVC casing and PVC slotted screen one-half into the groundwater This result is also shown in Table These results implied that spill of heating oil in the first below grade had migrated downward to the water table and accumulated on the groundwater surface During the installation of the east well cluster 56E contaminated soil was discovered The installation of well 56E-25 was completed without incident However as the auger was retrieved from the hole for 56E-35 an obvious layer of heating oil contaminated soil had been encountered at about 12 below grade above the groundwater No sample was collected Examination of the available Studebaker site maps and interviews with former employees identified this site as the terminus of previously removed piping presumably connected to the former UST The former location of the piping shows as concrete strip running from west to east from the 56E cluster in Figures and and was observable at the site There was also retaining wall formerly near this location The two wells in the cluster were separated by only so the contamination was taken as very localized deposit from this piping Groundwater Samples set of four multiple-depth monitoring wells three clusters approximately downgradient and one cluster upgradient of the confirmed spill site were designed and installed on May 17-18 2001 The location of the upgradient cluster 5OSW was set at radius of 50 to be remote from any mushroomed plume spread at the spill center and to avoid future construction activities The northeast and northwest clusters 40 NE 40 NW were located just inside the northern property line df the site at radius of 40 The eastern cluster 56E was located to avoid future construction activity at slightly greater radius of 56 All wells were drilled with hollow stem auger The casings were threaded diameter PVC with slotted PVC screens The annuli around the screens were packed with new silica screen sand and the casings then sealed with bentonite clay slurry to grade The clusters were designed as follows one well screened at the top of the water table from 20-25 below grade one well screened from 30-35 below grade for the center of the plume 4ONE one addition well screened from 40 -45 below grade 730 United Drive Heating Oil Spill ISC IDEM IiicidentTM 2001-01-156 2032 October 200 II ...The screen depths were separated by intervals to minimize interconnection effects and provide discrete data points while not missing the target plume The intent of the well placement was to intercept the contaminant plume close to its source to determine its impact With the proximity of the spill to the wells screen depths beyond 45 were not considered necessary and with the long history of pavement overlying the site the horizontal travel distance downgradient was not expected to be very great Secondly there were property line constraints 40 downgradient and the next available City property downgradient for well installation was in the right-of way to the north of this adjacent property At that distance too many other interfering plumes and sources were anticipated based upon previous work in the area to make data from this more remote location usable There was an expectation that other wells at greater radii might be needed in the future to completely characterize the plume depending on the results from these clusters Groundwater sampling as completed in two phases The initial samples were taken on May 23 2001 and analyzed for total SVOC and BETX representing the volatile organics fraction VOC The BETX results indicated the presence of xylenes and additional VOCs including chlorinated compounds so second set of samples was taken on June 25 2001 for complete and precise VOC analysis This more inclusive VOC analysis included the BETX group chlorinated compounds and the other VOCs in the EPA protocol TPH analysis was also added The findings of the sampling are summarized in Table and illustrated in Figures aiicl With the limited number of data points and the open-ended nature of the data for the plume groundwater contaminant contours were not considered appropriate Instead the concentrations keyed to their depths are shown in the figures for each of the four groups of potential contaminants non-chlorinated VOC total SVOC TPH and chlorinated VOC The individual SVOC and VOC concentrations are presented in Table while the figures give the totals only Table also lists the available regulatory values for evaluating the findings Most of these are the present Default Cleanup Criteria from the IDEM Risk Integrated System of Closure RISC for the individual compounds fot industrial locations Where IDEM has no value the Michigan DEQ Generic Cleanup Criteria for commercial/industrial sites are used For TPH the detection limit from the IDEM Tier groundwater parameters from the 1994 UST Closure Guidance Manual is used Volatiles and Chlorinated Volatiles Figure Of the 57 volatiles included in the method detectable concentrations were found for cOmpounds The trace of carbon disulfide from well 4ONW-35 35 depth was eliminated as laboratory contaminant so really only compounds were detected Of these the conglomeration reported as TPH was the greatest followed by the combined vinp-xylenes These two groups of compounds accounted for most of the plume The northeast cluster was the most affected and at this location the plume was very dilute below 35 Well cluster 5OSW reported four chlorinated volatile compounds From the groundwater surface gradient this was the presumed upgradient cluster All of the other downgradient clusters reported these same chlorinated volatiles but at lower concentrations Well 4ONW- 35 also reported ll-dichloroethane at just above the detection limit the only chlorinated volatile not reported from the upgradient cluster but at an insignificant concentration 730 United Drive Heating Oil Spill ISC IDEM Incident 2001-01-156 2032 October 2001 chlorinated compounds in the plume therefore were considered an upgradient background unassociated with the spill plume Only the non-chlorinated VOC are shown in Figure to eliminate further consideration of this upgradient plume The only VOC present above the IDEM RISC criteria was xylene and in only one well 4ONE-35 l24-trimethylbenzene exceeded the MDEQ criterion in the same well but this criterion was for aesthetics oniy taste color odor and not for health risk Overall the level of groundwater contamination based upon VOC was low Semi-Volatiles Figure Only two of the possible 70 SVOCs were found in the plume The primary compound was bis 2-ethyihexyl phthalate The most heavily polluted location 40 NE-35 also reported naphthalene in both the SVOC and VOC analyses SVOCs were only detected in the downgradient wells with the northeast cluster again the most affected The level of bis 2-ethyihexyl phthalate reported equaled the RISC criterion in well 4ONW- 35 and exceeded it in well 4ONE-35 by three times Only the well in the center of the plume showed significant groundwater impact based upon SVOC results Total Petroleum Hydrocarbons TPH Figure Some overlap between the compounds included in the VOC and TPH analyses occurs notably xylenes but the TPH results did document other VOCs from the heating oil not included in the EPA VOC protocol The major component in the TPH conglomerate present in these samples was mixed xylenes So the results reported for TPH display some overlap with the VOC results TPH does indicate the presence of the spill at the groundwater surface in cluster 4ONW as well as showing the impact of the piping leak in cluster 56E The TPH results add well 4ONE-25 to the significantly impacted locations showing that portion of the spilled productis floating at the groundwater surface Well 56E-25 was only slightly impacted above the method detection limit and as discussed can be attributed to localized piping spill at that location Some additional observations were made from the data in Table The plume was comprised primarily of diesel range petroleum hydrocarbons including mixed xylenes thus confirming the heating oil UST origins of the plume The vertical extent of tl1e plume was primarily above 35 below grade At the 45 depth contaminants were detected but at three orders of magnitude less This contamination in the upper portion of the aquifer was expected with the close proximity of the well clusters to the spill The horizontal center of the plume was calculated at 11 .5 east of north from water surface elevations Figure The highest pollutant concentrations were detected in well cluster 4ONE the nearest to this flow direction as confirmation of the general plume direction The contaminants in the shallow well of the east cluster 56E was more likely associated with the presumed pipe leak at 12 below grade at this location than the UST spill because of the depth of the soil contamination So the 4ONW cluster shows some fanning of the plume to the west along the north northeasterly plume centerline 730 United Drive Heating Oil Spill ISC IDEM lncident 2001-01-156 2032 October2001 These results support the conclusion that the oniy significant groundwater impact extends at least 40 downgradient of the spill at its centerline to depth of 35 below grade which is approximately 12 below the groundwater surface elevation CQNCLUSIONS The preceding information test results and discussion support the following conclusions heating oil spill occurred from UST above the groundwater table at the approximate location shown on the Studebaker site plan the spill occurred at least IS but more likely at least 35 years prior to this investigation The spill location was capped with concrete and asphalt pavement in the intervening period and so migrated downward primarily through the influence of gravity at correspondingly slow rate The underlying urban and native soils at the site offer no impedance to the migration of the plume downward in the vadose zone and once in the groundwater the aquilŁr is capable of transmitting the contaminants rapidly downgradient The plume direction is approximately north-northeast toward the South Bend urban area and has traveled beyond the Citys property line at the site The nearest environmental and public health impacts from the plume are the St Joseph River mile northeast and the Leeper Park municipal wellfield V2 miles north- northeast of the spill respectively The spill lies outside of the regulated wellhead protection area WHPA The removal of the overlying concrete and asphalt pavement during the present construction will increase rainwater percolation through the spill and speed up the propagation of the plume VI RECOMMENDATIONS Four rernediation actions are considered applicable and feasible for this minor spill One or combination of more than one of these actions could be applied They are listed in their approximate order of increasing expense and complexity No Action No action can be justified on the basis of the limited volume of the spill the presence of other unrelated contaminant sources upgradient of the spill and the absence of downgradient public health and environmental impacts It is highly unlikely that the St Joseph River and Leeper Park weilfield will show measurable impact or degradation from this spill Likewise mitigation of this spill from the spill site will eliminate localized contamination at location with little or no environmental impact while not affecting other pollutants already in the groundwater from upgradient sources of equal impact New construction completed at the spill location has repaved the area over the spill site plus installed new drywells upgradient The nearest drywells are 30 south and 30 south- southeast of the center of the spill These structures will not materially alter the groundwater percolation through the spill since they are not located directly over the spill and previously large unpaved field was located upgradient which will now be paved and drained by drywells Thus the surface percolation situation will be returned to the 730 United Drive Heating Oil Spill ISC IDEM lncident 2001-01-156 2032 October 2001 same condition as existed at the time of the spill which will serve to retard further downward heating oil movement as occurred previously The spill location is in brownfields-type area with mitigation dictated by the IDEM Risk Integrated System of Closure RISC model As such reduced criteria compared to an unindustrialized residential locale can be applied With the exception of xylenes and bis 2ethyihexyl phthalate in the centerline well cluster existing pollutant levels are acceptable without further action hi Situ Bioremediation Enzyme and bacteria culture injection with nutrient enrichment and oxygenation at the spill site to digest these heating oil components has application to this situation Ex situ treatment i.e excavation of the contaminated soils offers no advantages over simple excavation and disposal for the amount of soil anticipated Two methods are commonly practiced with in situ treatment with and without groundwater extraction treatment and recharge The existing monitoring wells can be reused for the injections plus possible additional injection points or withdrawal points This in situ method has been established as effective with diesel and fuel oil in similarsoils It offers the advantages of minimal interference with ongoing construction at the site lower cost than excavation and dealing with the pollutant at the source The projected clean-up time is less than the recovery well option Recovery We/I well approximately 60 deep at the center of the spill would be able to reverse the localized groundwater flow and contain the plume Most of the contamination is floating at the groundwater surface The exact diameter and capacity of the well would need to be calculated based upon the characteristics of the aquifer However the volume of water is expected to be within the capacity of the nearby sanitary sewers so that discharge to the City wastewater treatment plant could be used for its disposal No effect at the wastewater plant located at the extreme northern edge of the City in terms of contaminant concentration or water volume would be expected Placement of the screen at the groundwater surface will allow recovery of the most contaminated portion oithe plume No free product is expected to be encountered This technique offers the advantages of arresting the further propagation of the plume and minimal interference with ongoing construction at the site Treatment of the wastewater generated by the well can be handled by the City with minimal increase in operating expense The main disadvantage is the slow washout of the contaminants at the source because of low solubility in water and the extended time frame for the clean-up that results contarninatedSoil Excavation Although the site of the spill has been repavecl and drained there are no structures within 30 of the spill center that would be adversely affected by excavation of contaminated soil down to the water table surface The soil borings indicate that contamination begins at about below grade and that the majority of the contamination has ponded at the water table surface at about 23 below grade Excavation to 23 would need to be done in tiers Excavation in the vadose zone would be expected to be quite localized and limited larger area would be expected at the groundwater surface 730 United Drive Heating Oil Spiti ISC DEM lncideit 2001-01 56 2032 October 200 With most of the contamination already into the groundwater as judged from the soil boring profile the effectiveness of this action will be limited but will reduce some of the potential future source for contaminants This is the highest cost alternative considered Of these options we recommend that the No Action alternative be applied on the lllowing basis There is no immediate or foreseeable public health impact downgradient This plume is only one portion of mixture of plumes including chlorinated VOC from other off-site upgradient sources and the overall benefit of remediating the plume in question would be small The second choice would be the in-situ bioremediation alternative with no groundwater extractionltreatment/recharge This has been shown effective with small releases involving groundwater in similar sandy soils It offers the highest level of reinediation with the least impact on the new construction VII REFERENCES Soil Survey for St Joseph County Indiana United States Department of Agriculture Soil Conservation Service Purdue University Agricultural Experiment Station November 1977 Water Resources Availability in the St Joseph River Basin Indiana Indiana Department of Natural Resource Water Resource Assessment 87-1 1987 Studebaker Corporation Plants Drawing WX9266 Studebaker Archives July 20 1951 Revised 6/54 interview with David Tungate Water Quality Engineer South Bend Water Works October 112001 interview with Mark Nelson St Joseph County Health Department October 11 2001 730 United Drive Heating Oil Spill ISC IDEM Incidents 2001-01-156 _________ 2032 October 2001 Table Spill Site Soil Sample Results Total Petroleum Hydrocarbons TPH 730 United Drive Building 69 Depth feet Date TPH mg/KG2 6-7.5 1/4/01 1000 12-13.5 1/4/01 450 18.5-20.0 1/12/01 47 .23.5-25.0 1/12/01 3.650 EPA/IDEM Limit 20 analyzed by EPA GC/FID protocol 8260B samples collected at presumed center of the spill as determined from historical Studebaker Automotive Corporation data II 10 730 United Drive Heating Oil Spill ISC IDEM Incident 2001-01-156 ________ 2032 October2001 rible Spill Site Groundwater Sample Results Summary Volatile Organics and Semi-Volatile Organics May 23 and June 25 2001 _____________________________________ Results ig/L ___________Indiana Monitoring Well 5OSW 56E 4ONE 4ONW RISC Screen Bottom ft 25 34 25 35 25 45 25 35 Criteria3 NON-CHLORINATED VOLATILES 6/25/01 ___ ________ benzene 99 n-butylbenzene 4.3 230 carbon disulfide 3.2 10000 ethyl benzene 10000 isopropyltoluene 4.3 46 methyl tert-butyl ether 720 naphthalene 210 2000 n-propylbenzene 26 230 toluene 20000 124-trimethylbenzene 11 200 63 135-trimethylbenzene 54 ornp-xylenes 38002 22 180 48 other compounds nd nd nd nd nd nd rid iid rid Total nd nd nd 4.3 15.3 4336 nd nd 3.2 SEMI-VOLATILES 5/23/0 ____ ____ ____ _______ bis 2-ethyihexyl phthaate 10 10 10 190 72 680 71 10 200 200 naphthalene 10 10 10 10 10 205 10 10 10 2000 68 other compounds iid nd nd nd nd nd nd rid iid Total 10 10 10 190 72 885 71 10 200 CHLORINATED VOLATILES 6/25/01 ___ _________ 11-dichloroethane 1.1 10000 c-12-dichloroethene 2.0 3.6 1.7 3.4 3.4 2.2 1000 tetrachloroethylene 1.8 3.2 1.3 1.1 1.5 3.3 2.4 2.9 55 trichloroethyleiie 21 31 4.7 15 6.8 36 11 36 200 11.1-trichioroethane 1.4 1.5 9200 Total 25 52 6.0 18 12 44 43 31 TOTAL PETROLEUM HYDROCARBONS 6/25/01 TPH I2001200120011030162601 5810 20012001 390 10006 all compounds included in EPA GC/FID protocols 8260B VOC and 8270C SVOC nd below minimum detection limit MDL refer to the laboratory report for individual MDLs BETX result 5/23/01 5650 ig/L 40 NE-35 36 j.ig/L 4ONE-45 xylenes no others detected 3IDEM Default Closure Values Table Industrial February 15 2001 MDEQ Generic Commercial/Industrial II11IIV Criteria-Drinking Water Op Memo 18 6/7/01 MDEQ Generic Commercial/Industrial IIIIJIV Cleanup Criteria aesthetics only 6IDEM Tier Groundwater Detection Limit 1994 UST Closure Guidance 11 BU1LDNG 4Nflij 40N 40 NW 56 ___50SVLZ s-- ti i- North boring and test welt location former UST LIE location 3ULDNC demolished Scale 50 ______Drawn AMG Check LWG Date 5/16/01 Iroject 2032 FigurejiFormerUSTSitewithBoringsandTestWellsGrauvogelAssociates 730 United Drive UST Spill Site 17660 FaIl Creek Drive Grangerlndlana46S3O Incident 200101-156 South Bend Indiana 12 1L5 699.80 II 321 28 699.85 40NW35 40 NE 35 699.90 88 Former UST 56 34 699.95 SpiD Location Hi 700.00 50SW34 214 Test well location angles referenced to magnetic North Groundwater surface elevations measured on 5/23/01 Elevations referenced to USGS datum Test well locations ________________________________ ________Drawn AMG Check LWG Date 6/1/01 Project 2032 FigureLocal Groundwater Flow at Former UST Site Grauvoge1 Associates 730 United Drive Bldg 69 17660 FaIl Creek Drive Granger Indiana 46530 Incident 200101156 South Bend Indiana North Building 112 Buthng84 57 723 64.6 Lr3 ._J Groundwater Flow ______ a-a-r4i _-- _627525LfI -723 -4ONW 1014635 nd 25 APh nd 45 Property Line-i 35 56 ___ 11 535 RB WALL LHdemolishedCIJRKLL 11A OFBRIS IDEBWS 4BRUSH T1 -SpiiiSite monitoring weH 13 25 concentration gIL depth Do ft Scale 140 II ________________________________ _______Drnwn AMG Check LWG Date 9/17/01 Project 2032 Groundwater Contamination Non-Chlorinated VOC Figure Grauvogel Associates 730 United Drive UST Spill Site 17660 FaIl Creek Drive Granger Indiana 46530 Incident 200101156 _____________________________Department of Public Works South Bend Indiana tNorth Building 112 Building 84 12 723 64 h__Lj Groundwater Flow __________j__ -j--4-- 7225 JJt 723 4ONW ND 25 __AIPF/7145 cotic\I\ Property Line-i 200 35 56 Spill Site TND25 724 722 190 35 L_-4 \4 .._._j______w5OSW_______J_.__ qtL demolished WALL fBRU55H oo Spill Site j\ Monitoring Well 13 25 concentration pg/L depth 00 Scale 40 ________________ ________Drawn AMG Check LWG Date 9/17/01 Project 2032 Groundwater Contamination Total SVOC Figure Grauvogel Associates 730 United Drive UST Spill Site 17660 FaIl Creek Drive Granger Indiana 46530 IncldentH 2001-01156 _______________________________Department of Public Works South Bend Indiana North Building 112 Building 84 723 646 Groundwater Flow _____ __3-._..- -40 NE 1AA 1225 LL9Y4ONW 1325 APH 4445 COVC\ Property Line1 3135 56E Spill Site 625-724 -722 p- -w__i2 25 __ ___________jl ptdemolishedCURB4LL d14 DIBRIS IDEBR/S /8RusHI oo/1jSSPillSite ii monitoring well 13 25 concentration tg/L depth -- Scale 40 ________________ ________Drawn AMG Check LWG Date 9/17/01 Project 2032 Groundwater Contamination Chlorinated VOC Figure jWGrauvogel Associates 730 United Drive UST Spill Site 17660 Fall Creek Drive Granger Indiana 46531 Incidents 200101156 ________________________________Department of Public Works South Bend Indiana North Building 112 Building 84 71 ._ Groundwater Flow /L_LL _i 7RA If -i 6260 25 jN14 723 ND2SAL/15 Property Line 390 35 723 T. 56 5OSWW ________ 12i ND 25 ___ _____________________________demolished_i_CJRB kALL 2YC BR/S DEBRIS fBRosH.I DO Spill Site monitoring wefl 13 25 concentration g/L depth CO ii __ II Scale 40 _______________________ ________Drawn AMG Check LWG Date 9/17/01 Project 2032rl\Groundwater Contamination TPH Figure GrauvogeI Associates 730 United Drive UST Spill Site 17660 FaIl Creek Drive Granger Indiana 46530 lncldent 2001-01-156 ________________________________Department of Public Works South Bend Indiana b .u r1 .-IL Ho RIf Cu --_9_MI 717 ------ .- -IL $S -- .1 CI -V TV PS sr HaL .bV F4aeg C11Seb tho SeI VV V_.V V_ ra ROAD 11 .VVV r_VV rrJP1il Fi -V I1 ro .li Thl ffexon dl VBM VV Sah0riJJVVXjjE-j-- n4oa fl tit -V VVVVrTgV Ic .. NA P1 VV if .i VV VV Vt V.rJI .- VVVV _1 VV .- 76 -----it alke Fielj- 1- Vjr VV VV VVVV VV VVV VV L_J /I-r----\.V -\i7 ti 24-raCe VVj V.7-2.Ij Monro durrIpt unroo .VVc \--.I c75 a3tl VVJ L-eseotr I44 VV _VVV ___V_ L_ Dran LWG Check LWG Date 0/4/0 Project 2032 Figure Crauvogel Associates General Location 730 United Drive 764OFaHCreekDrhe South Bend Indiana Granger Indiana 46530 LSGS 75 Quadran1e South Bend East 1991/West 1986 18 ____ 7O 35 ri Za Scale 100 Drawn AMG Check LWG Date 8/8/0 Project 2032 Figure Grauvogel Associates 1993 PIat Map 730 United Drive Studebaker Building 69 Area Gra tiger Indiana 4653 South Bend Indiana vu.ri YrInME _________ -r 5-Year Time of Travel I7 r4Y \5Wr4J 4411 Time of ____ iS4 4i ffron Spill Site JJ4 4b UI KEY North Wells Map prepared by Lawson Fischer Associates P.C from data provided by Scale 2000 Peerless Midwest Welihead Delineations Drawn LWG Check LWG Date 10/11/01 Project 2032 Figure Grauvogel Associates Welihead Protection Area 1766 Fall Creek Drive Leeper Park North Weilfield South Bend Indiana Grnger Indiana 46530 1-Year and 5-Year Time of Travel Zones 20 So cn T3on ucu 200 S\cksTPH Mct2oo dwr vactJ ii Mr Larry Grauvogel Report Date 1/19/01 Grauvogel Associates EIS Order No 010100033 17660 Fall Creek Drive EIS Sample No 073326 EIS Project No 2730-1000-01 Granger IN 46530 Tel No 277-4770 --________ Client Sample ID 32.2.6 AB Fax No 277-5281 Date Collected 1/4/01 P0 No Date Received 1/4/0 Project Name Studebaker Building 69 Collected By L.G This report presents results analysis for your samples received under our Order No above This Number is to be used in all inquiries concerning this report The EIS Sample No above as well as your Sample ID refer to the first sample in multi-sample submission DEFINITIONS RDL Reporting Detection LWnit for your sample and may include djustments for matrix interferences nd Not Detected at the RDL value If present resultis less than this value Not Detected at the numerical value shown If present result is less than this yalue Result is estimated due to matrix intØrfØrences CHAIN OF CUSTODY is enclosed if received with your sample submission DRINKING WATER CERTIFICATIONS Chemistiy C-71-02 Bacteriology 52715 NOTE Samples from Boring weresubmitted for TPHGRO but Contained only DRO Results are reported as TPHDRO even though the report lists TPHGRO HI ______ QUALITY ASSURANCE OFFICER LABORATORY DIRE OR The data in this report has been reviewed and complies with EIS Quality Control unless specifically addressed above EIS Analytical Services Inc 1701 Ironwood Drive Suite South Bend IN 46635 Tel 219-277-0707 Fax 219273-5699 SAMPLE RESULTS Page2of Iient Name Grauvogel Associates Report Date 1/1 9/01 client Project Studebaker Building 69 EIS Order No 010100033 EIS Lab Client Sample Test 1Number Description Date Parareterl LiE1i Date Analyst LMethodJ 073326 32.2.6AB 1/4/01 Moisture 11 0.1 1/5/01 LozanoS 160.3 1/4/01 TPH RO 1000 jng/kgwet 150 1/8/01 WilliamsJ 8260 073327 32.2.12 AB 1/4/01 Moisture 12 0.1 1/5/01 LozanoS 160.3 1/4/01 TPH GRO 450 mg/gwet 60 1/8/01 WilIamsJ 8260 073328 32.3.6 AB 1/4/01 Moisture 6.4 0.1 1/5/01 LozanoS 160.3 1/4/01 TPH DRO 20 mg/kgwet 20 1/8/01 CarisenS 8015 073329 32.3.12 AB 1/4/01 Moisture 8.9 0.1 1/5/01 LozanoS 160.3 1/4/01 TPH DRO 20 mg/kgwet 20 1/8/01 CarlsenS 8015 073330 32.1.6AB 1/4/01 Moisture 0.1 1/5/01 LozanoS 160.3 1/4/01 TPH DRO 20 mg/kgwet 20 1/8/01 CarisenS 8015 073331 32.1.12AB 1/4/01 Moisture 8.1 0.1 1/5/01 LozanoS 1603 1/4/01 TPH DRO 20 mg/kgwet 20 1/8/01 CartsenS 8015 II EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005239 QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010100033 QUALITY CONTROL LIMITS Methods QC Limits flormal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCAA 615 8151A 515.1 8151A 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608 /8081 8082 508 8082 22 135 40 Pesticides PCB DecachlorobiphenylDCB 608 8081A 508 8082 22 135 40 150 SOC svoc Perylene d12 525.2 70 -130 SVOC acid 2-Fluorophenol 625 8270C 8270C 21 100 25-121 SVOC acid Phenol d5 625/8270C 8270C 10-94 24-113 SVOC base/neutral Nitrobenzene d5 625/8270C 5270C 35-114 23-120 SVOC base/neutral 2-Fluorobiphenyl 625 8270C 8270C 43 116 30 115 SVOC acid 246-Tribromophenol 625 8270C 8270C 10-123 19-122 SVOC base/neutral Terphenyl d14 625 8270C 8270C 33 141 18 137 TPH Styrene 8015M 8015M 30-70 34-66 VOCIBETXITPH 12-Dichloroethane d4 624 /8260B/524.2 8260B 76-114 70-121 VOC BETX TPH Totuene d8 624 82608 524.2 82608 86-115 74-121 VOC BETX TPH BromofluorobenzØneBFB 624 8260B 524.2 82608 86 115 74 121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 073326 32.2.6 AB 8260 Soil/Sludge/Solid 12-Dichloroethane-d4 SS 89 8260 Soil/Sludge/Solid 4-Bromofluorobenzene SS 114 8260 Soil/Sludge/Solid Toluene-d8 SS 94 073327 32.2.12 AB 8260 Soil/Sludge/Solid 12-Dichloroethane-d4SS 91 8260 Soil/Sludge/Solid 4-Bromofluorobenzene SS 114 8260 Soil/Sludge/Solid Toluene-d8 SS 101 073328 32.3.6 AB 8015 Soil/Sludge/Solid Styrene SS 65 073329 32.3.12 AB 8015 Soil/Sludge/Solid Styrene SS 60 073330 32.1.6AB 8015M Soil/Sludge/Solid StyreneSS 66 073331 32.1.12 AB 8015 Soil/Sludge/Solid StyreneSS 56 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Pagelof II QUALITY CONTROL DATA MATRIX SPIKE DUPLICATE MATRIX SPIKE MSIDMS EIS Order 010100033 EIS Lab in This Batch Comments Concerning This QC Batch QC Sample 073329 073326-073331 None Matrix Soil Test TPHDRO Quality Control Limits Back-Spike Matrix Spike Duplicate Spike RPD %R Parameter ground Amount Result Result RPD LCL IJCL LCL UCL QC Batch 20 100_j_102 --20 75 --125 QB00228 LEGEND Background Sample Result amount may be adjusted for dilution used in sample analysis Percent Recovery of Spike Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Background and Spike CHAIN OF CUSTODY RECORD PROJ NO PROJECT NAME Total dl No ______________SAMPLERS Print Name Sign JO/o3 FIELD Lab ID DATE TIME STATION LOCATION tainers __________________________________________________Type TAT Number s/rP fQ _______ort 5Jzc ____o-i5 _________733Z7 iL _______7332S tiZM IOI 733titot-f 7333O _________________i_iiiii 7333 Re ished By ignature ____ Date Time Receive nquijEs QUOTE NO igriature Dat Time Received By Signature Ship To Relinquished By Signature Date Time Received By Signature NOTES If you were issued quote number it must appear on this document Instructions area for comments are on reverse side EIS ANALYTICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE SUITE .SOUTH BEND IN 46635 Phone 2192770707 Fax 2192735 Form Ch nof--Cusody 612---97 Mr Larry Grauvogel Report Date 1/26/01 Grauvogel Associates EIS Order No 010100092 17660 Fall Creek Drive EIS Sample No 073455 EIS Project No 2730-1000-01 Granger IN 46530 Tel No 277-4770 Client Sample ID Boring2-18.5 Fax No 277-5281 Date Collected 1/12/01 P0 No Date Received 1/12/01 Project Name Studebaker Building 69 Collected By L.G This report presents results of analysis for your samples received under our Order No above This Number is to be used in all inquiries concerning this report The ELS Sample No above as well as your Sample ID refer to the first sample in multi-sample submission DEFINITIONS MDL Method Detection Limit normally achieved in the absence of interferences or other matrix difficulties RDL Reporting Detection Limit achieved in your sample If numerically greater than the MDL dilutions.were required in order to perform the analysis If numerically less than the MDL alternate techniques were employed nd Not Detected at the RDL value If present result is less than this value Not Detected at the numerical value shown If present result is less than this value Result is estimated due to matrix interferences CHAIN-OF-CUSTODY is enclosed if received with your sample submission DRINKING WATER CERTIFICATIONS Chemistry C-71-02 Bacteriology 52715 NOTE TPHGRO was requested for the Boring2 soils via your Chain-of-Custody TPH actually found is Diesel Range and results are reported as TPHDRO even though the report shows GRO _____________ QUALITY ASSURANCE OFFICER LABORATORY DIRECR The data in this report has been reviewed and complies with EIS Quality Control unless specifically addressed above EIS Analytical Services Inc 1701 lronwood Drive Suite South Bend IN 46635 Tel 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page of CLIENT SAMPLE ID Boring2 18.5 Report Date 1/26/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 073455 SAMPLE TYPE Soil/Sludge/Solid EIS Order No 010100092 Date Collected 1/12/01 Date Received 1/12/01 jTest Parameter 1ts i5n WDL Aii1 jicI1 Moisture 2.8 0.1 0.1 LozanoS 1/16/01 160.3 TPH GRO 47 mg/kgwet 30 20 WiIIiamsJ 1/18/01 8260 II EIS Analytical SeMces Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page of CLIENT SAMPLE ID Boring2 23.5 Report Date 1/26/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 073456 SAMPLE TYPE Soil/SludgelSolid EIS Order No 010100092 Date Collected 1/12/01 Date Received 1/12/01 Test Parameter Results Units RDL MDL AnaIyst Date Method Moisture 9.9 0.1 0.1 LozanoS 1/16/01 160.3 TPH GRO 3650 mg/kgwet 700 20 WilliamsJ 1/18/01 8260 EIS Analytical SeMces Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLERESULTS Page4of CLIENT SAMPLE ID Boring2 Report Date 1/26/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 073457 SAMPLE TYPE WaterNon DW EIS Order No 010100092 Date Collected 1/12/01 Date Received 1/12/01 ITest Parameter IResuIts frDL jAiiT1 Date Method BETX/MTBE Benzene nd ig/L 40 WilliamsJ 1/17/01 8260 Ethylbenzene nd pg/L 40 WilliamsJ 1/17/01 8260 Methylbutylether tert MTBE nd pg/L 80 WiiIiamsJ 1/17/01 8260 Toluene nd pg/L 40 WilliamsJ 1/17/01 8260 Xylenes Total nd pg/L 80 WilliarnsJ 1/17/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page of CLIENT SAMPLE ID Trip Blank Report Date 1/26/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 073456 SAMPLE TYPE WaterNon DW EIS Order No 010100092 Date Collected 1/12/01 Date Received 1/12/01 Parameter Results Units IRDL1 rMDL jAnalyst MØthod BETX/MTBEITPH Benzene nd pg/L WiIliamsJ 1/17/01 8260 Ethylbenzene nd pg/L WilliamsJ 1/17/01 8260 Methylbutylether tert MTBE nd pg/L WiIliamsJ 1/17/01 8260 Toluene nd pg/L WiHiamsJ 1/17/01 8260 TPH GRO nd pg/L 200 200 WiIliamsJ 1/17/01 8260 Xylenes Total nd pg/L WiIliamsJ 1/17/01 8260 HI EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010100092 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCeAA 615/8151A/515.1 8151A 15-135 Pesticides PCB 24 56-Tetrachloro-m-xyleneTCMX 608 8081 8082 508 8082 22 135 40 -150 Pesticides/PCB DecachlorobiphenylDCB 608/8081A/508 8082 22-135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625 827CC 827CC 21 100 25-121 SVOC acid Phenol d5 625/827CC 827CC 10-94 24-113 SVOC base/neutral Nitrobenzene d5 625 827CC 827CC 35-114 23 120 SVOC base/neutral 2-Fluorobiphenyl 625 827CC 827CC 43-116 30-115 SVOC acid 246-Tribromophenol 625/827CC 8270C 10 -123 19-122 SVOC base/neutral Terphenyl d14 625 827CC 8270C 33 141 18-137 TPH Styrene 8015M 8015M 30-70 34-66 VOC BETX TPH 12-Dichioroethane d4 624 8260B 524.2 826DB 76-114 70-121 VOC BETX TPH Toluene d8 624 8260B 524.2 8260B 86-115 74-121 VOCIBETX/TPH BromofluorobenzeneBFB 624/8260B/524.2 826DB 86-115 74-121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 073455 Boring2 18.5 8260 Soil/Sludge/Solid 12-Dichloroethane-d4 SS 104 8260 Soil/Sludge/Solid 4-Brornoflurobenzene SS 101 8260 Soil/Sludge/Solid Toluene-d8 SS 90 073456 Boring2 23.5 8260 Soil/Sludge/Solid 12-Dichloroethane-d4 SS 110 8260 Soil/Sludge/Solid 4-Bromofluorobenzene SS 105 8260 Soil/Sludge/Solid Toluene-d8 SS 91 073457 Boring2 8260 WaterNon DW 12-Dichloroethane-d4 SS 112 826C WaterNon DW 4-Bromoflorobenzene SS 8260 WaterNon DW Toluene-d8 SS 91 073458 Trip Blank 826Q WaterNon DW 12-Dichloroethane-d4 SS 111 8260 WaterNon DW 4-BromofluorQbenzene SS 98 8260 WaterNon DW Toluene-d8 SS 91 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Pagelof CHAIN OF CUSTODY RECORD PROJ NO PROJECT NAME 43o9 Total ________________________________________________No _______________gn 0rder ID LabFIELDtainers ID DATE TIME STATION LOCATION ______________ __________________________________ ________Type TAT Number___________PB _______________ __________________ ____________________________1z L16A4-J /rzoJ IOj Z-14U IYZ /t/i ti-___ ____________________Z________________ ushed By Signature Date Time ReceiyedBy inai EIS QUOTE NO Ship ToDateTime.Rceed By Signatu Relinquished By Signature Date Time Received By Signature NOTES If you were issued quote number it must appear on this document Instructions area for comments are on reverse side EIS ANALYTICAL SERVICES INC 1O1 NORTH IRONWOOD DRIVE SUITE .SOUTH BEND IN 46635 Phone 2192770707 Fax 2192735 Form ChainofCustody 61297 Form Completion Instructions Each slanted line represents specific container types from which specific tests are conducted Use additional record sheets if of samples or of tests exceed allotted spaces List tests per container type on the slanted lines give of containers in boxes below tests Sum all containers and place in column labeled Total No Containers For the column labeled Sample Type give brief description such as soil MW oil etc.- For column labeled TAT use one of the following Request Meaning Normal 24 weeks for written report based entirely on test complexity and number of samples week In general prior authorization is required from the lab to request day turnaround time Surcharges may or may not be appliabte depending entirely on test complexity days Must have been authorized by the Lab and increased costs muØthŁve been authorized by the client. day Must have been authorized by the Lab and increased costs must have been authorized by the client Submission Comments .1 EIS TICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE .SOUTH BEND IN 46635 Phone 219277-0707 Fax 2U 5699 Mr Larry Grauvogel Report Date 5/31/01 Grauvogel Associates EIS Order No 010500180 17660 Fall Creek Drive EIS Sample No 075606 ElSProjectNo 2730100001 Granger IN 46530 Tel No 277-4770 Client Sample ID 50 SW 10 Fax No 277-5281 Date Collected 5/17/01 P0 No Date Received 5/18/01 Project Name 730 United Drive Bldg 69 Collected By Grauvogel This report presents results of analysis for your samples received under our Order No above This Number is to be used in all inquiries concerning this report The EIS Sample No above as well as your Sample ID refer to the first sample in multi-sample submission DEFINITIONS RDL Reporting Detection Limit for ybur sample and may include adjustments for matrix interferences nd Not Detected at the RDL value If present result is less than this value Not Detected at the numerical value shown If present result is less than this value Result is estimated due to matrix interferences is enclosed if received with your sample submission DRINKING WATER CERTIFICATIONS Chemistry C-71-02 Bacteriology M-76-5 QUALITY SURANCE OFF LABORATORY DIR OR The data in this report has been reviewed and complies with EIS Quality Control unless specifically addressed above EIS Analytical Services Inc 1701 Ironwood Drive Suite South Bend IN 46635 Tel 219-277-0707 Fax 219-273-5699 Page lofFORD005251 SAMPLE RESULTS Page2of Client Name Grauvogel Associates Report Date 5/31/01 Client Project 730 United Drive Bldg 69 EIS Order No 010500180 EIS Lab Client rsarnpiel Test Numberj Description Date fTihr 5E Date Analyst Method 075606 50 Sw 10 5/17/01 Moisture%8.1 0.1 5/21/01 LozarioS 160.3 5/17/01 TPH DRO 20 mg/kgwet 20 5/22/01 CarisenS 8015 075607 50 SW 21 5/17/01 Moisture%6.5 0.1 5/21/01 LozanoS 160.3 5/17/01 TPH DRO 20 mg/kgwet 20 5/22/01 CarisenS 8015 075608 56 10 5/17/01 Moisture%10.0 0.1 5/21/01 LozanoS 160.3 5/17/01 TPH DRO 20 mg/kgwet 20 5/22/01 CarisenS 8015 075609 56 21 5/17/01 Moisture%7.8 0.1 5/21/01 LozanoS 160.3 5/17/01 TPH DRO 20 mg/kgwet 20 5/22/01 CarisenS 8015 075610 56 24 5/17/01 Moisture%5.5 0.1 5/21/01 LozanoS 160.3 5/17/01 .TPH DRO 20 .mg/kgwet 20 5/22/01 CarisenS 8015 075611 40 NW 10 5/18/01 Moisture%8.1 0.1 5/21/01 LozanoS 160.3 5/18/01 TPHDRO 20 mg/kgwet 20 5/23/01 CarisenS 8015 075612 40 NW 21 5/18/01 Moisture%11.0 0.1 5/21/01 LozanoS 160.3 5/18/01 TPHDRO 20 mg/kgwet 20 5/23/01 CarlsenS 8015M 075613 40 NE 10 5/18/01 Moisture%9.8 0.1 5/21/01 LozanoS 160.3 5/18/01 TPH DRO 21 mg/kgWet 20 5/23/01 CarisenS 8015 075614 40 NE 24 5/18/01 Moisture%10.0 0.1 5/21/01 LozanoS 160.3 5/18/01 TPH DRO 20 mg/kgwet 20 5/23/01 CarlsenS 8015M 075615 40 NW 24 5/18/01 Moisture%15.0 0.1 5/21/01 LozanoS 160.3 5/18/01 TPH DRO 20 mg/kgwet 20 5/23/01 CarisenS 8015 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE PREPARATION INFORMATION Chent Name Grauvogel Associates Report Date 5/31/01 Client Project 730 United Drive Bldg 69 EIS Order No 010500180 1iJa iii Number Description Date iiiI Completed Anaiyst Method 075606 50 Sw 10 5/17/01 Extract BETXITPH Complete 5/21/01 CarisenS 8015 075607 50 SW 21 5/17/01 Extract BETXITPH Complete 5/21/01 CarisenS 8015 075608 56 10 5/17/01 Extract BETX/TPH Complete 5/21/01 CarisenS 8015 075609 56 21 5/17/01 Extract BETX/TPH Complete 5/21/01 CarisenS 8015 075610 56 24 5/17/01 Extract BETX/TPH Complete 5/21/01 CarlsenS 8015 075611 40 NW 10 5/18/01 Extract BETXITPH Complete 5/21/01 CarisenS 8015 075612 40 NW 21 5/18/01 Extract BETX/TPH Complete 5/21/01 CarisenS 8015 075613 40 NE 10 5/18/01 Extract BETXITPI-1 Complete 5/21/01 CarlsenS 8015 075614 40 NE 24 5/18/01 Extract BETX/TPH Complete 5/21/01 CarisenS 8015 075615 40 NW 24 5/18/01 Extract BETX/TPH Complete 5121/01 CarlsenS 8015 EIS Analytical Services Inc 1701 North lronwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010500180 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenytaceticacidDCAA 615 8151A 515.1 8151A 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608 8081A 8082 508 8082 22-135 40-150 Pesticides PCB DecachlorobiphenylDCB 608 8081A 508 8082 22-135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625 8270C 8270C 21 100 25 121 SVOCacid Phenol d5 625/8270C 8270C 10-94 24-113 SVOC baselneutrai Nitrobenzene d5 625/827CC 8270C 35-114 23-120 SVOC base/neutral 2-Fluorobiphenyl 625 8270C 8270C 43-116 30-115 SVOC acid 246-Tribromophenol 625/827CC 827CC 10-123 19 122 SVOC base/neutral Terphenyl d14 625 827CC 827CC 33-141 18-137 TPH Styrene 8015M 8015M 30-70 34-66 VOC BETX TPH 2-Dichloroethane d4 624 826CB 524.2 826CB 76 114 70 121 VOC BETX TPH Toluene d8 624/ 8260B 524.2 8260B 86 115 74 121 VOC BETX TPH BromofluorobenzeneBFB 624 8260B /524.2 8260B 86-115 74 121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 075606 50 Sw io 8015 Soil/Sludge/Solid Styrene SS 52 075607 50 Sw 21 8015 Soil/Sludge/Solid Styreæe SS 51 075608 56 10 8015 Soil/Sludge/Solid Styrene SS 50 J75609 56 21 8015 Soil/Sludge/Solid Styrene SS 49 075610 56 24 8015 Soil/Sludge/Solid Styrene SSH 51 075611 40 NW 10 8015 Soil/Sludge/Solid StyreneSS 51 075612 40 NW 21 8015 Soil/Sludge/Solid Styrene SS 51 075613 40 NE 10 8015 Soil/Sludge/Solid Styrene SS 50 Q75614 40 NE 24 8015 Soil/Sludge/Solid Styrene SS 50 075615 40 NW 24 8015 Soil/Sludge/Solid Styrene SS 58 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Pagelof Ii QUALITY CONTROL DATA MATRIX SPIKE DUPLICATE MATRIX SPIKE MS/DMS EIS Order 010500180 EIS Lab in This Batch Comments Concerning This QC Batch QC Sample 075606 075606 -075615 None Matrix Soil Test TPH Diesel Range Quality Control Limits Back-Spike Matrix Spike Duplicate Spike RPD Parameter ground Amount Result Result RPD LCL UCL LCL IJCL QC Batch TPH DRO 20 40 32 80 75 --125 QB00547 LEGEND Background Sample Result Spike amount may be adjusted for dilution used in sample analysis Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Background and Spike QUALITY CONTROL DATA LABORATORY FORTIFIED METHOD BLANK LFB Matrix Lab Solvent EIS Lab With This LFB Comments Concerning This LFB Test TPH Diesel Range 075606-075615 None Prep Date See Sample Extraction Dat Run Date 5/23/01 Quality Control Limits Spike Matrix Spike Duplicate Spike RPP_L.R Parameter Amount Result Result RPD LCL UCL LCL UCL QC Batch LTPH DRO 40 33 83 80 --120 QB00547 II LEGEND The LFB may be either single spike or in dulicate and may or may not be in QC Batch with MSIDMS Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Spike and Duplicate Spike CHAIN OF CUSTODY RECORD PROJ NO PROJECT NAME Total __________________________________________No _____________ SAMPLERS Print Name Sign FIELD tainers ID of or leoAnn Con- Lab ID DATE TIME STATION LOCATION ______________ __________________________________ ________Type TAT Number Oiio f/c 1oob io.ckS O9LL tO _____25go F5c3w-S2l ____ov\O fiD ___________________ _______ ________________________73Co_____OO ID 7$c7 75JLQc3L_1L ______________ ____t300 ortriQ61a 24 ____756/o ________________________7// _______2t ____________ 4DRID bon L4ONE tQ _______7s/3 DNE-Z4 ____11O L-JJ ______75// DNWI bL1UAW 24 __Z1S Relinquished By Signtire Date Time Received By Signature EIS QUOTE NO 5//oi 1505 _____________________ Relinquished By nature Date Time Received By Signature Ship To Relinquished By Signature Date Time Received By Signature NOTES If you were issued quote number it must appear on this document Instructions area for comments are on reverse side EIS ANALYTICAL SERVICES INC 1701 NORTH IRON WOOD DRiVE SUITE .SOUTH BEND IN 46635 Phone 2192770707 Fax 2192735699 Fnrm ChainofCustody 61297 Form Completion Instructions Each slanted line represents specific container types from which specific tests are conducted Use additional record sheets if of samples or of tests exceed allotted spaces List tests per container type on the slanted lines give of containers in boxes below tests Sum all containers and place in column labeled Total No Containers For the column labeled Sample Type give brief description such as soil MW oil etc For column labeled TAT use one of the following Request Meaning Normal 24 weeks for wntten report based entirely on test complexity and number of samples week In general pnor authonzation is rŁqured froJhe lb to request day turnaround time Surcharges may or may not be appUcable depending eidireIy on test complexity days Must have been authonzed by the Lab and increaid costs musi have been authonzed by the client ----- day Must have been authorized by the Lab and increased costs must have been authorized by the dient Submission Comments ii__ EIS ICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE .SOUTH BEND IN 46635 Phone 2192770707 Fax 21 Forn of-dy Mr Larry Grauvogel Report Date 6/12/01 Grauvogel Associates EIS Order No 010500216 17660 FaIl Creek Drive EIS SampleNo 075679 EIS Project No 2730-1000-01 Granger IN 46530 Tel No 277-4770 Client Sample ID 50 SW 25 Fax No 277-5281 Date Collected 5/23/0 P0 No Date Received 5/23/01 Project Name Studebaker Building 69 Collected By L.a This report presents results of analysis for your samples received under our Order No above This Number is to be uŒed in all inquiries concerning this report The EIS Sample No above as well as yourSample ID refer to the first sample in multi-sample submission DEFINITIONS MDL Method Detection Limit normally achieved in the absence of interferences or other matrix difficulties RDL Reporting Detection Limit achieved in your sample If numerically greater than the MDL dilutions were required in order to perform the analysis If numerically less than the MDL alternate techniques were employed nd Not Detected at the RDL value If present result is less than this value Not Detected at the numerical value .shown If present result is less than this value Result is estimated due to matrix interferences CHAIN OF CUSTODY is enclosed if received with your sample submission DRINKING WATER CERTIFICATIONS Chemistry C-71-02 Bacteriology M-76-5 QUALITY ASSURANCE CER LABORATORY DIRE The data in this report has been reviewed and complies with EIS Quality Control unless specifically addressed above EIS Analytical Services Inc 1701 Ironwood Drive Suite South Bend IN 46635 Tel 219-2770707 Fax 219-273-5699 Page 1of28 SAMPLE RESULTS Page of 28 CLIENT SAMPLE ID 50 Sw 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075679 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/0 Date Received 5/23/01 ___________1AiI Date BETX Benzene nd pg/L WiIIiamsJ 5/31/01 8260 Ethylbenzene nd pgiL WiIIiamsJ 5/31/01 8260 Toluene nd pg/L WiILiamsJ 5/31/01 8260 Xylenes Total nd pgIL WiIIiarnsJ 5/31/01 8260 EIS Analytical Services Inc 1701 North lronwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Page of 28 CLIENT SAMPLE ID 50 SW 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075679 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 jTestl Parameter IResuits Units RDL 1iETI rAnalyst Date SEMIVOLATILE ORGANICS Acenaphthene nd ig/L 10 10 RoziteA 6/10/01 8270 Acenaphthylene nd pg/L 10 10 RoziteA 6/10/01 8270 Aniline nd pg/L 10 10 RoziteA 6/10/01 8270 Anthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzidine nd pg/L 50 50 RoziteA 6/10/01 8270 Benzoaanthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoapyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoghiperylene nd g/L 10 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd pgIL 10 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 50 50 RoziteA 6/10/01 8270 Benzyl alcohol nd pg/L 20 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd ig/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroethylether nd .ig/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether nd pg/L 10 10 RoziteA 6/10/01 8270 s2-ethylhexylphthalate nd JgIL 10 10 RoziteA 6/10/01 8270 Bromophenyl-phenylether nd pgfL 10 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate nd pgIL 10 10 RoziteA 6/10/01 8270 Chloro-3-methylphenol nd jg/L 10 10 RoziteA 6/10/01 8270 Chloroanhline nd pg/L 10 10 RoziteA 6/10/01 8270 Chloronaphthalene nd pg/L 10 10 RoziteA 6/10/01 8270C Chlorophenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chiorophenyl phenyl ether nd pg/L 10 10 RoziteA 6/10/01 8270 Chrysene nd .ig/L 10 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Di-æ-octylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dibenzoahanthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Dibenzofuran nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 12 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene13 nd pg/L 10 10 RoziteA 6/10/01 8270C Dichlorobenzene 14 nd ig/L 10 10 RoziteA 6/10/1 8270 Dichlorobenzidine 33 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorophenol 24 nd pg/L 10 10 RoziteA 6/10/01 8270 Diethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethylphenol 24 nd ii/L 10 10 RoziteA 6/10/01 8270 Thnitrophenol 24 nd pg/L 50 50 RoziteA 6/10/01 8270 initrotoluene 24 nd Jg/L 10 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 nd ig/L 10 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 nd pg/L 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page of 28 CLIENT SAMPLE ID 50 SW 34 Report Date 6/12101 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075680 SAMPLE TYPE WaterNon OW EIS Order No 010500216 Date Collected 5/23/01 Date ReCeived 5/23/01 Parameter ResuIts tlinits IMbL1 Date jj BETX Benzene nd Jg/L WilliamsJ 5/31/01 8260 Ethylbenzene .nd pg/L WilIiamsJ 5/31/01 8260 Toluene nd pg/L WilliamsJ 5/31/01 8260 Xylenes Total nd pg/L WilUarnsJ 5/31/01 8260 EIS Analytical Services Inc 1.01 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273.5699 SAMPLE RESULTS Page 4of 28 CLIENT SAMPLE ID 50 SW 25 Report Date 6/12101 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075679 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter Results Units aiyst 1Ie Fluoranthene nd pg/L 10 10 RoziteA 6/10/0 8270 Fluorene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pgIL 10 10 RoziteA 6/10/01 8270 Hexachlorobutadiene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachiorocyclopentadiene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachloroethane nd ig/L 10 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Isophorone nd pg/L 10 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Methylnaphthalene nd pg/L 10 10 RoziteA 6/10/01 8270 Methylphenol nd pgIL 10 10 RoziteA 6/10/01 8270 Methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 10 10 RziteA 6/10/01 8270 Nitroaniline nd ig/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 itrobenzene nd pgIL 10 10 RoziteA 6/10/01 8270 .iitrophenol nd pgIL 10 10 RoziteA 6/10/01 8270 Nitrophenol nd ig/L 50 50 RoziteA 6/10101 8270 .Nitroso-di-methylarnine normal nd Jg/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Pentachlorophenol nd ig/L 50 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 10 10 RoziteA 6/10/01 8270 Phenol nd pg/L .10 10 RoziteA 6/10/01 8270C Pyrene nd pg/L 10 RoziteA 6/10/01 8270 Pyridine nd pg/L 10 10 RoziteA .6/10/01 8270 Trichlorobenzene 124 nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 245 nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 246 nd pg/L 10 10 RoziteA 6/10/01 8270 II EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219.277-0707 Fax 219-273-5699 SAMPLE RESULTS age6of 28 CLIENT SAMPLE ID 50 SW 34 Report Date 6/12101 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075680 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Date SEMIVOLATILE ORGANICS Acenaphtherie nd pg/L 10 10 RoziteA 6/10101 8270 Acenaphthylene rid pg/L 10 .10 RoziteA 6/10/01 8270 Aniline rid ig/L 10 10 RoziteA 6/10/01 8270 Anthracerie nd pg/L 10 10 RoziteA 6/10/01 8270 Berizidine nd pg/L 50 50 RoziteA 6/10/01 8270 Benzoaanthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoapyrerie nd pg/L 10 10 RoziteA 6/10/01 8270 Berizobfluoranthene nd ig/L 10 10 RoziteA 6/10/01 8270 Benzoghiperylene nd ig/L 10 10 RoziteA .6/10/01 8270 Benzokfluoranthene rid iig/L 1.0 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 50 50 RoziteA 6/10/01 8270 Berizyl alcohol nd pg/L 20 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymetharie nd lJg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroethylether rid pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether nd pg/L 10 10 RoziteA 6/10/01 8270 is2-ethylhexylphthalate rid pg/L 10 10 RoziteA 6/10/01 8270 Bromophenyl-phenylether rid pg/L 10 10 RbziteA 6/10/01 8270 Butyl berizyl phthalate nd pg/L 10 RoziteA 6/10/01 8270 Chloro-3-methylpheriol rid pg/L 10 10 RoziteA 6/10/01 8270 Chloroanuline rid g/L 10 10 RoziteA 6/10/01 8270 Chloronaphthalerie rd pg/L 10 10 RoziteA 6/10/01 8270 Chlorophenol nd ig/L 10 10 RoziteA 6/10/01 8270 Chlorophenyl phenyl ether rid pg/L .10 10 RoziteA 6/10/01 8270 Chrysene rid pg/L 10 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Di-ri-octylphthalate rid pg/L 10 10 RoziteA 6/10/01 8270 Dibenzoahanthracerie nd pg/L 10 10 RoziteA 6/10/01 8270 Dibenzofuran nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 12 nd 10 10 RoziteA 6/10/01 8270 Dichloroberizene 13 rid pg/L 10 10 RoziteA 6/10/01 8270 Dichloroberizene14 nd pg/L 10 10 RoziteA 6/10/01 8270C Dichloroberizidine 33 rid iJg/L 10 10 RoziteA 6/10/01 8270 Dichlorophenol 24 nd pg/L 10 10 RoziteA 6/10/01 8270 Diethyl phthalate rid ig/L 10 10 RoziteA 6/10/01 8270 .I Dimethyl phthalate rid pg/L 10 10 RoziteA 6/10/01 8270 Dimethylpheriol 24 rid pg/L 10 10 RoziteA 6/10/01 8270 Thnitropheriol 24 rid pg/L 50 50 RoziteA 6/10/01 8270 Jinitrotoluerie 24 rid pg/L 10 10 RoziteA 6/10/01 8270 Dinitrotoluerie 26 rid ig/L 10 10 RoziteA 6/10/01 8270 Dipheriylhydrazirre 12 rid Jg/L 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page of 28 CLIENT SAMPLE ID 50 SW 34 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075680 SAMPLE TYPE WaterNon OW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter Ies Units 1RDI fAnalyst Date Fluoranthene rid pg/L 10 10 RoziteA 6/10/01 8270 Fluorene rid pg/L 10 10 RoziteA 6/10/01 8270 Hexachlorobenzene rid jg/L 10 10 RoziteA 6/10/01 8270 Hexachiorobutadiene rid pg/L 10 10 RoziteA 6/10/01 8270 Hexachlorocyclopentadiene rid pgIL 10 10 RoziteA 6/10/01 8270 Hexachioroethane nd pg/L 10 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene rid ig/L 10 10 RoziteA 6/10/01 8270 IsophOrone rid IJQ/L 10 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol rid pg/L 50 50 RoziteA 6/10/01 827 .Methylnaphthalene rid ig/L 10 10 RoziteA 6/10/01 8270 .I Methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Methylphenol nd pg/L 10 10 .RoziteA 6110/01 8270 Naphthalene nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline rid pg/L 10 10 RoziteA 6/10/01 8270 Nitroanuline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroanuline nd pg/L 10 10 RoziteA 6/10/01 8270 itrobenzene pg/L 10 10 RoziteA 6/10/01 8270 r4utropheriol nd pg/L 10 10 RziteA 6/10/01 8270 Nitrophenol rid pg/L 50 50 RoziteA 6/10/01 8270 Nitroso-di-methylamine normal nd pgIL 10 10 RoziteA 6/10/01 8270 Nitroso-di-ri-propylamine normal rid jig/L 10 10 RoziteA 6/10/0 8279 Nitroso-di-phenylamine normal rid pg/L 10 10 RoziteA 6/10/01 8270 Peritachlorophenol rid pg/L 50 59 RoziteA 6/10/01 8270 Phenanthrerie rid pglL 10 10 RoziteA 6/10/01 8270 Phenol rid .igiL 10 10 RoziteA 6/10/01 .8270 Pyrene rid pg/L 10 10 RoziteA 6/10/01 8270 Pyridine rid pg/L 10 10 RoziteA 6/10/01 8270 Trichlorobeæzene 124 rid pg/L 10 .10 RoziteA 6/10/01 8270 Trichlorophenol 245 rid pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 246 rid pg/L 10 10 RziteA 6/10/01 8270 ii EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page8of 28 CLIENT SAMPLE ID 40 NW 25 Report Date 6/1 2/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075681 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 TestiiDate BETX Benzene nd pg/L WilliamsJ 5/31/01 8260 Ethylbenzene nd pgIL WiIliamsJ 5/31/01 8260 Toluene nd pg/L WilliamsJ 5/31/01 8260 Xylenes Total nd pg/L WIliamsJ 5/31/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 2 SAMPLE RESULTS Page 9of 28 CLIENT SAMPLE ID 40 NW 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075681 SAMPLE TYPE WaterNon OW EIS Order No 010500216 Date Collected 5/23/0 Date Received 5/23/01 .St1 I1ihod1 SEMIVOLATILE ORGANICS Acenaphthene nd pg/L 10 10 RoziteA 6/10/01 8270 Acenaphthylene nd pg/L 10 10 RoziteA 6/10/01 8270 Aniline nd pg/L 10 10 RoziteA 6/10/01 8270 Anthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzidine nd pgIL 50 50 RoziteA 6/10/01 8270 Benzoaanthracene nd ig/L 10 10 RoziteA 6/10/01 8270 Benzoapyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoghiperylene nd pg/L 10 10 RoziteA 6/10/0 8270 Benzokfluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 50 50 RoziteA 6/10/01 8270 Benzyl alcohol nd Jg/L 20 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroethylether nd pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether nd pg/L 10 10 RoziteA 6/10/01 8270 is2-ethylhexylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270C Bromophenyl-phenylether nd pg/L 10 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate nd Jg/L 10 .10 RozfteA 6/10/01 8270 Chloro-3-methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chloroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 Chloronaphthalene nd ig/L 10 10 RoziteA 6/10/01 8270 Chlorophenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chiorophenyl phenyl ether nd pg/L 10 10 RozitŁA 6/10/01 8270 Chrysene nd IJg/L 10 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd igIL 10 10 RoziteA 6/10/01 8270 Di-n-octylphthalate nd pg/L 10 10 RoziteA 6/10/01 8279 Dibenzoahanthracene nd pg/L 10 10 RoziteA 6/10/0 8270 Dibenzofuran nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 12 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 13 nd pgIL 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 14 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzidine 33 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorophenol 24 nd pg/L 10 10 RoziteA 6/10/01 8270 Diethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethylphenol 24 nd pgIL 10 10 RoziteA 6/10/01 8270 initrophenol 24 nd ig/L 50 50 RoziteA 6/10/01 8270 jinitrotoluene 24 nd Jg/L 10 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 nd pg/L 10 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 nd pg/L 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 2 SAMPLE RESULTS Page 10 of 28 CLIENT SAMPLE ID 40 NW 25 Report Date 6/1 2101 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075681 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/0 Date Received 5/23/01 Test Parameter sults Us RDtI Date Fluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270 Fluorene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachioroberizene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachiorobutadiene rid igIL 10 10 RoziteA 6/10/01 8270 Hexachiorocyclopentadierie nd pgIL 10 10 RoziteA 6/10/01 8270 Hexachloroethane rid pg/L 10 10 RoziteA 6/10/01 8270 lrideno123-cdpyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Isophorone nd g/L 10 10 RoziteA 6/10/0 8270 Methyl-46-dinitropheriol nd pg/L 50 50 RoziteA 6/10/01 8270C Methylnaphthalene rid pg/L 10 10 RoziteA 6/10/01 8270 Methylphenol rid pg/L 10 10 RoziteA 6/10/01 8270 Methylphenoi4 rid pg/L 10 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 10 10 RozteA 6/10/01 8270 Nitroanuline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroanulirie rid pgIL 10 10 RoziteA 6/10/01 827CC Nitroanilirie rid pg/L 10 10 RoziteA 6/10/01 8270 itroberizerie nd ig/L 10 10 RoziteA 6/10/01 8270 .JitropherioI nd ig/L 10 i RoziteA 6/10/01 8270 Nitrophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Nitroso di methylamirie normal rid iig/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-ri-propylamine normal rid pgIL 10 10 RoziteA 6/10/01 8270 Nitroso-di-pheriylamineriorml pg/L 10 10 RoziteA 6/10/01 8270 Peritachloropheriol rid ig/L 50 50 RoziteA 6/10/01 8270 Pheriarithrerie nd pg/L 10 10 RoziteA 6/10/01 8270 Phenol nd ig/L 10 10 RoziteA 6/10/01 8270 Pyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Pyridirie nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorobenzene 124 rid pg/L 10 10 RoziteA 6/10/01 8270 Trichloropheriol 245 rid pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 246 rid pg/L 10 10 RoziteA 6/10/01 8270 .1 II EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 11 of 28 CLIENT SAMPLE ID 40 NW 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075682 3AMPLE TYPE WaterNon OW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Parameter ijFj ____________ Date BETX Benzene nd pg/L WiIIiamsJ 5/3 1/01 8260 Ethylbenzene nd pg/L WilliamsJ 5/31/01 8260 Toluene nd pgIL WiIIiamsJ 5/31/01 8260 Xylenes Total nd pg/L WiIliamsJ 5/31/01 8260 II -I EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 12 of 28 CLIENT SAMPLE ID 40 NW 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075682 SAMPLE TYPE WaterNon OW EIS Order NO 010500216 Date Collected 5/23/01 Date Received 5/23/01 Parameter iiiUnits 1i Date SEMIVOLATILE ORGANICS Acenaphthene nd pg/L 40 10 RoziteA 6/10/01 8270 Acenaphthylene nd ig/L 10 10 RoziteA 6/10/01 8270 Aniline nd Jg/L 10 10 RoziteA 6/10/01 8270 Anthracene nd pglL 10 10 RoziteA 6/10/01 8270 Benzidine nd pg/L 50 50 RoziteA 6/1 0101 8270 Benzoaanthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoapyrene nd jg/L 10 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pgL 10 10 RoziteA 6/10/01 8270 Benzoghiperylene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd pg/L 10 10 RoziteA 6/10/1 8270 Benzoic acid nd pg/L 50 50 RoziteA 6/10/01 8270 Benzyl alcohol nd ig/L 20 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd ig/L 10 10 RziteA 6/10/01 8270 Bis2 chloroethylether nd pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether nd pg/L 10 10 RoziteA 6/10/01 8270 s2 ethylhexyphthalate 200 pg/L 40 10 RoziteA 6/10/01 8270 Bromophenyl-phenylether .nd pg/L 10 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate nd ig/L 10 10 RoziteA 6/10/01 8270 Chloro-3-rnethylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chloroaniline nd pgIL 10 10 RziteA 6/10/01 8270 Chloronaphthalene nd pg/L 10 10 RoziteA 6/10/01 8270 Chlorophenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chlorophenyl phenyl ether nd pg/L 10 10 RoziteA 6/10/01 8270 Chrysene nd pg/L 10 1.0 RoziteA 6/10/01 8270 Di-n-butylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Di-n-octylphthalate nd pglL 10 10 RoziteA 6/10/01 8270 Dibenzoahanthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Dibenzofuran nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 12 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 13 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 14 nd pgIL 10 10 RoziteA 6/10/01 8270 Dichlorobenzidine 33 nd pg/L 10 10 RoziteA 6/1 0/01 8270 Dichlorophenol 24 nd pg/L 10-10 RoziteA 6/10/01 8270 Diethyl phthalate nd pgIL -10 10 RoziteA 6/10/01 8270 Dimethyl phthalate nd pgIL 10 10 RoziteA 6/10/01 8270 Dimethylphenol 24 nd pg/L 10 10 RoziteA 6/10/01 8270 Thinitrophenol 24 nd pg/L 50-50 RoziteA 6/10/01 8270 jinitrotoluene 24 nd pgIL 10 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 nd pg/L 10 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 nd pg/L 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273.5699 SAMPLE RESULTS Page 13 of 28 CLIENT SAMPLE ID 40 NW 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075682 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter tLils rtit or1 Date Fluoranthene nd pg/L 10 10 RoziteA 6/1 0/01 8270 Fluorene nd .ig/L 10 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachiorobutadiene nd pg/L 10 10 RoziteA 611 0/01 8270 Hexachiorocyciopentadiene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachioroethane nd ig/L 10 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene nd pg/L 10 10 RoziteA 6/10/01 8270 isophorone nd pg/L 10 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Methylnaphthalene nd .pg/L 10 10 RoziteA 6/10/01 8270 Methyiphenol nd pgIL 10 10 RoziteA 6/1001 8270 Methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Naphthaiene nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroanihne nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroanhline4 nd ig/L 10 10 RoziteA 6/10/01 8270 trobenzene nd pg/L 10 10 RoziteA 6/10/01 8270 .iitrophenol nd ig/L 10 10 RziteA 6/10/01 8270 Nftrophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Nitroso di methylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylamine normal nd ig/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Pentachiorophenol nd jgIL 50 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 10 10 RoziteA 6/10/01 8270 Phenol nd pgIL 10 10 RoziteA 6/10/01 8270 Pyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Pyridine nd jgIL 10 10 RoziteA 6/10/01 8270C Trichlorobenzene 124 nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenoi 245 nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 246 nd pgIL 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 14 of 28 CLIENT SAMPLE ID 40 NE 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075683 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter iiF1 LtT1 Is1 _1 Date _________ BETX Benzene nd ig/L WiIliamsJ 6/1/01 8260 Ethylbenzene nd ig/L WiIIiamsJ 6/1/01 8260 Toluene nd pg/L WilIiamsJ 6/1/01 8260 Xylenes Total nd pg/L WilliamsJ 6/1/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 2 SAMPLE RESULTS Page 15 of 28 CLIENT SAMPLE ID 40 NE 25 Report Date 6112/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075683 SAMPLE TYPE WaterNon OW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter ReSUItS Units RDL 1LI Date SEMIVOLATILE ORGANICS Aceriaphthene nd pg/L 20 10 RoziteA 6/10/01 8270 Acenaphthylene nd iJg/L 20 10 RoziteA 6/10/0 8270 Aniline nd pgIL 20 10 RoziteA 6/10/01 8270 Anthracene nd pg/L 20 10 RoziteA 6/10/01 8270 Benzidine rid pg/L 100 50 RoziteA 6/10/01 8270 Berizoaanthracene nd pg/L 20 10 RoziteA 6/10/01 8270 Berizoapyrene nd pgIL 20 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pg/L 20 10 RoziteA 6/10/01 6270 Benzoghiperylene nd pg/L 20 10 RoziteA 6/10/01 8270 Benzokfloranthene rid ig/L 20 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 100 50 RoziteA 6/10/01 8270 Benzyl alcohol nd ig/L 40 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd .ig/L 20 10 RoziteA 6/10/01 8270 Bis2-chloroethylether nd Jg/L 20 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether rid pg/L 20 10 RoziteA 6/10/01 8270 s2-ethylhexylphthalate 72 pg/L 20 10 RozitØA 6/10/01 8270 Bromophenyl-phenylether nd pg/L 20 10 RoziteA 6/10/01 8270 Butyt benzyl phthalate nd pg/L 20 10 RoziteA 6/10/01 8270 Chloro-3-methylpheriol rid pg/L 20 10 RoziteA 6/10/01 8270 Chloroanuline rid jig/L 20 10 RoziteA 6/10/01 8270 Chloronaphthalene rid pg/L 20 10 RoziteA 6/10/01 8270 Chlorophertol nd ig/L 20 10 RoziteA 6/10/01 8270 Chlorophenyl phenyl ether rid Jg/L 2 10 RoziteA 6/10/01 8270 Chrysene nd pg/L 20 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd pg/L 20 10 RoziteA 6/10/01 8270 Di-n-octylphthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Dibenzoahanthracene rid pg/L 20 10 RoziteA 6/10/01 8270 Dibenzofuran rid pg/L 20 10 RoziteA 6/10/01 8270 Dichlorobenzerie 12 rid pg/L 20 10 RoziteA 6/10/01 8270 Duchloroberizerie 13 rid pg/L 20 10 RoziteA 6/10/01 8270 Dichloroberizene 14 nd pg/L 20 10 RoziteA 6/10/01 8270 Dichloroberizidine 33 nd pg/L 20 10 RoziteA 6/10/01 8270 Dichlorophenol 24 rid pg/L 20 10 RoziteA 6/10/01 8270 Diethyl phthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Dimethyl phthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Dimethylpheriol 24 rid pg/L 20 10 RoziteA 6/10/01 8270 initropheriol 24 rid pg/L 100 50 RoziteA 6/10/01 8270 initrotoluene 24 rid pg/L 20 10 RoziteA 6/10/01 8270 Dinitrotoluerie 26 rid pg/L 20 10 RoziteA 6/10/01 8270 Dipheriylhydrazine 12 rid pg/L 20 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 16 of 26 CLIENT SAMPLE ID 40 NE 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075683 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 jTest Parameter Results UnIts RDL rr11i tDate iiidi Fluoranthene nd ig/L 20 10 RoziteA 6/10/01 8270 Fluorene nd pgIL 20 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd lJg/L 20 10 RoziteA 6/10/01 8270 Hexachiorobutadiene nd pgIL 20 10 RoziteA 6/10/01 8270 Hexachiorocycloperitadiene nd pg/L 20 10 RoziteA 6/10/01 8270 Hexachloroethane nd pg/L 20 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene nd pg/L 20 10 RoziteA 6/10/01 8270 Isophorone nd pg/L 20 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd pg/L 100 50 RoziteA 6/10/01 8270 Methylnaphthalene2 nd pg/L 20 10 RoziteA 6/10/01 8270C Methylphenol nd pg/L 20 10 RoziteA 6/10/01 8270 Methylphenol nd pg/L 20 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 20 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 20 10 RoziteA 6/10/01 8270 Nitroaniline nd pgIL 20 10 RoziteA 6/10/01 8270 NitroaniHne nd ig/L 20 10 RoziteA 6/10/01 8270 Iitrobenzene nd pg/L 20 10 RoziteA 6/10/01 8270 itrophenol nd pg/L 20 10 RoziteA 6/10/01 8270 Nitrophenol nd pg/L 100 50 RoziteA 6/10/01 8270 Nitroso-di-methylarnine normal nd pgIL 20 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylamine normal nd ig/L 20 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal nd pg/L 20 10 RoziteA 6/10/01 8270 Pentachlorophenol pd pg/L 100 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 20 10 RoziteA 6/10/01 8270 Phenol nd pg/L 20 10 RoziteA 6/10/01 8270 Pyrene nd ig/L 20 10 RoziteA 6/10/01 8270 Pyridine nd pgIL 20 10 RoziteA 6/10/01 8270 Trichlorobenzene 124 nd ig/L 20 10 RoziteA 6/10/01 8270 Trichlorophenol 245 nd pg/L 20 10 RoziteA 6/10/01 8270 Trichlorophenol 246 nd ig/L 20 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 17 of 28 CLIENT SAMPLE ID 40 NE 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075684 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 E1 itT1 Date Methadj BETX Benzene nd pgIL 10 WiiliarnsJ 5/31/01 8260 Ethylbenzene nd g/L 10 WilliamsJ 5/31/01 8260 Toluene nd pgIL 10 .1 WilliamsJ 5/31/01 8260 Xylenes Total 5650 pg/L 20 WiliiamsJ 5/31/01 8260 II EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Pagel8of28 CLIENT SAMPLE ID 40 NE 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075684 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Parameter iiitiits 1C1 E1 Date Ewcr1 SEMIVOLATILE ORGANICS Acenaphthene nd ig/L 100 10 RoziteA 6/10/01 8270 Acenaphthylene nd pg/L 100 10 RoziteA 6/10/01 8270 Aniline nd pgIL 100 10 RoziteA 6/10/01 8270 Anthracene nd pg/L 100 10 RoziteA 6/10/01 8270 Benzidine rid Jg/L 500 50 RoziteA 6/10/01 8270 Benzoaanthracene nd pg/L 100 10 RoziteA 6/10/01 8270 Berizoapyrene nd pg/L 100 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pg/L 100 10 RoziteA 6/10/01 8270 Benzoghiperylene nd pg/L 100 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd pg/L 100 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 500 50 RoziteA 6/10/01 8270 Benzyl alcohol rid pg/L 200 20 RoziteA 6/10/01 8270 .Bis2-chloroethoxymethane nd pgIL 100 RoziteA 6/10/01 8270 Bis2-chloroethylther nd vigIL 100 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether rid ig/L 100 10 RoziteA 6/10/01 8270 s2 ethylhexylphthalate 680 pg/L 100 10 RoziteA 6/10/01 8270 dromophenyl-phenylether nd ig/L 100 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate nd pg/L 100 10 RoziteA 6/10/01 8270 Chloro-3-methylphenol nd pg/L 100 10 RoziteA 6/10/01 8270 Chloroaniline nd pg/L 100 10 RoziteA 6/1 0101 8270 Chloronaphthalene nd .pg/L 100 10 RoziteA 6/10/01 8270 Chlorophenol nd pg/L 100 10 RoziteA 6/10/01 8270 Chlorophenyl phenyl ether nd ig/L 100 10 RoziteA 6/10/01 8270 Chrysene rid pg/L 100 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd pg/L 100 10 RoziteA 6/10/01 8270 Di-ri-octylphthalate nd pg/L 100 10 RoziteA 6/10/01 8270 Dibenzoahanthracene nd pg/L 100 19 RoziteA 6/10/01 8270 Dibenzofuran nd pgiL 100 10 RozfteA 6/10/01 8270 Dichlorobenzene 12 nd pg/L 100 10 RoziteA 6/10/01 8270 Dichlorobenzene 13 nd pg/L 100 10 RoziteA 6/10/01 8270 Dichlorobenzene 14 nd pgIL 100 10 RoziteA 6/10/01 .8270 Dichlorobenzidine 33 rid pg/L 100 10 RoziteA 6/10/01 8270 Dichlorophenol 24 rid pg/L 100 10 RoziteA 6/10/01 8270 Diethyl phthalate rid Jg/L 100 10 RoziteA 6/10/01 8270 Dirnethyl phthalate ig/L 100 10 RoziteA 6/10/01 8270 Dimethylphenol 24 rid pg/L 100 10 RoziteA 6/10/01 8270 initropheriol 24 rid pgIL 500 50 RoziteA 6/10/01 8270 jinitrotoluene 24 pg/L 100 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 rid pg/L 100 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 rid pg/L 100 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 19 of 28 CLIENT SAMPLE ID 40 NE 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075684 AMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/0 Date Received 5/23/01 FTest Parameter IResults fiinits RDL Analyst jDate Fluoranthene nd .ig/L 100 10 RoziteA 6/10/01 8270 Fluorene nd pg/L 100 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pgIL 100 10 RoziteA 6/10/01 8270 Hexachlorobutadiene nd pg/L 100 10 RoziteA 6/10/01 8270 Hexachlorocyclopentadiene nd pg/L 100 10 RoziteA 6/10/01 8270 Hexachloroethane nd pg/L 100 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene nd pg/L 100 10 RoziteA 6/10/01 8270C Isophorone ig/L 100 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd .ig/L 500 50 RoziteA 6/10/01 8270 Methylnaphthalene nd pg/L 100 10 RoziteA 6/10/01 8270 Methylphenol nd pgiL IOO 10 RoziteA 6/10/01 8270 Methylphenol nd igIL 100 10 RoziteA 6/10/01 8270 Naphthalene 205 pgIL 100 10 RozitŒA 6/10/01 8270 Nitroaniline pg/L 100 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 100 10 RoziteA 6/10/01 8270 Nitroaniline nd /L 100 10 RozitØA 6/10/01 8270 iitrobenzene nd pg/L 100 10 RoziteA 6/10/01 8270.0 itrophenoI nd .pg/L 100 10 RoziteA 6/1 0/01 8270 Nitrophenol nd pg/L 500 50 RoziteA 6/10/01 8270 Nitroso-di-methylamine normal nd pg/L 100 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylamine normal nd pg/L 100 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal lJg/L 100 10 RoziteA 6/10/01 8270 Pentachlorophenol nd pg/L 500 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 100 .10 RoziteA 6/10/01 8270 Phenol nd lJg/L 100 10 RoziteA 6/10/01 8270 Pyrene nd pg/L 100 10 RoziteA 6/10/01 8270 Pyridine nd pg/L 100 10 RoziteA 6/10/01 8270 Trichlorobenzene 124 nd Jg/L 100 10 RoziteA 6/10/01 8270 Trichlorophenol 245 nd pg/L 100 10 RoziteA 6/10/01 8270 Trichorophenot 246 nd pg/L 100 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273.5699 SAMPLE RESULTS Page 20 of 28 CLIENT SAMPLE ID 40 NE 45 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075685 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter iesults MDL 1nayst Date BETX Benzene nd pg/L WiHiamsJ 6/1/01 8260 Ethylbenzene nd pgIL WillimsJ 6/1/01 8260 Toluene nd pg/L WilliamsJ 6/1/0 8260 Xylenes Total 36 pg/L WiIIiamsJ 6/1/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page2lof 28 CLIENT SAMPLE tO 40 NE 45 CLIENT PROJECT Studebaker Building 69 El Sampi No 075685 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 rmet TJ Date jj SEMIVOLATILE ORGANICS Acenaphthene rid pg/L 20 10 RoziteA 6/10/01 8270 Aceriaphthylene nd pg/L 20 10 RoziteA 6/10/01 8270 Aniline rid pg/L 20 10 RoziteA 6/10/01 8270 Arithracene nd pg/L 20 10 RoziteA 6/10/01 8270 Benzidine nd pg/L 100 50 RoziteA 6/1 0/01 8270 Benzoaanthracene nd pgIL 20 10 RoziteA 6/10/01 8270 Benzoapyrene rid pg/L 20 10 RoziteA 6/10/01 8270 Berizobfluorantherie nd pgIL 20 10 RoziteA 6/10/01 8270 Benzoghiperylene rid pg/L 20 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd pg/L 20 10 RoziteA 6/10/01 8270 Berizoic acid nd pg/L 100 50 RoziteA 6/10/01 8270 Berizyl alcohol rid pg/L 40 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd pg/L 20 10 RoziteA 6/10/01 8270 Bis2-chloroethylether rid pg/L 20 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether rid pg/L 20 10 RoziteA 6/10/01 8270 s2-ethylheylphthalate pg/L 20 10 RoziteA 6/10/01 8270 ornopheriyl-pheriylether rid pg/L 20 10 RoziteA 6/10/01 8270 Butyl berizyl phthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Chloro-3-methylphenol nd pg/L 20 10 RoziteA 6/10/01 8270 Chloroariulirie rid jiglL 20 10 RoziteA 6/10/01 8270 Chloronaphthalene rid pg/L 20 10 RoziteA 6/10/01 8270 Chloropheriol nd pg/L 20 10 RoziteA 6/10/01 8270 Chloropheriyl phenyl ether rid pg/L 20 10 RoziteA 6/10/01 8270 Chrysene nd pg/L 20 10 RozitØA 6/10/01 8270 Di-ri-butylphthalate rid pgIL 20 10 RoziteA 6/10/01 8270 Di-ri-octylphthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Diberizoaharithracerie rid pg/L 20 10 RoziteA 6/10/01 8270 Diberizofurari rid igIL 20 10 RoziteA 6/10/01 8270 Dichloroberizerie 12 pg/L 2G 10 RoziteA 6/10/01 8270 Dichloroberizerie 13 rid pg/L 20 10 RoziteA 6/10/01 8270 Dichlorobenzerie 14 rid pg/L 20 10 RoziteA 6/10/01 8270 Dichlorobenzidirie 33 rid pg/L .20 10 RoziteA 6/10/01 8270 Dichloropheriol 24 rid Jg/L 20 10 RoziteA 6/19/01 8270 Diethyl phthalate nd pg/L 20 RoziteA 6/10/01 8270 Dimethyl phthalate rid pg/L 20 10 RoziteA 6/10/01 8270 Dimethylpheriol 24 rid pgIL 20 10 RoziteA 6/10/01 8270 lnitropheriol 24 rid pgIL 100 50 RoziteA 6/10/01 8270 Jinitrotoluene 24 rid pg/L 20 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 rid pg/L 20 10 RoziteA 6/10/01 8270 Dipheriylhydrazirie 12 rid pg/L 20 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 22 of 28 CLIENT SAMPLE ID 40 NE 45 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075685 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 11 _____________ Date Fluoranthene nd pg/L 20 10 RoziteA 6/10/01 8270 Fluorerie rid pg/L 20 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pg/L 20 10 RoziteA 6/10/01 8270 Hexachlorobutadiene rid pg/L 20 10 RoziteA 6/10/01 8270 Hexachiorocyclopentadiene rid pgIL 20 10 RoziteA 6/10/01 8270 Hexachioroethane rid pg/L 20 10 RoziteA 6/10/01 8270 Indeno123-cdpyrene nd pgIL 20 10 RoziteA 6/10/01 8270 Isophorone nd pg/L 20 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd jg/L 100 50 RoziteA 6/10/01 8270 Methylnaphthalene nd pglL 20 10 RoziteA 6/10/01 8270 Methylpheriol rid pgIL 20 10 RQziteA 6/10/01 8270 Methylphenol rid pg/L 20 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 20 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 20 10 RziteA 6/10/01 8270 Nitroanuline rid pg/L 20 10 RoziteA 6/10/01 8279 Nitroanuline rid pg/L 20 10 RoziteA 6/10/01 8270 Iitrobenzene rid pg/L 20 10 RoziteA 6/10/01 8270 r4itrophenol rid ig/L 20 10 RoziteA 6/10/01 8270 Nitrophenol nd pg/L 100 50 RoziteA 6/10/01 8270 Nitroso-di-methylamine normal rid pg/L 20 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylanuine normal rid pg/L 20 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal rid pg/L 20 10 RoziteA 6/10/01 8270 Pentachioropheriol rid pg/L 100 50 RoziteA 6/10/01 8270 Phenanthrerie nd pg/L 20 10 RoziteA 6/10/01 8270 Phenol rid pg/L 20 10 RoziteA 6/10/01 8270 Pyrene rid pg/L 20 10 RoziteA 6/10/01 8270 Pyridine rid pg/L 20 10 RoziteA 6/10/01 8270 Trichloroberizene 124 rid pg/L 20 10 RoziteA 6/10/01 8270 Trichlorophenol 245 rid pg/L 20 10 RoziteA 6/10/01 8270 Trichlorophenol 246 rid pg/L 20 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 23 of 28 CLIENT SAMPLE ID 56 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075686 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Parameter ij T1 IRDL Eti iAir1 Date BETX Benzene nd pg/L WiIIiamsJ 5/31/0 8260 Ethylbenzene nd pg/L WiIliamsJ 5/31/01 8260 Toluene nd pg/L WilIiamsJ 5/31/01 8260 Xylenes Total nd pg/L WiIllamsJ 5/31/01 8260 El Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page24of 28 CLIENT SAMPLE ID 56 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075686 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter Units RDL AVIyst Date 1Mtid SEMIVOLATILE ORGANICS Acenaphthene nd pg/L 10 10 RoziteA 6/10/01 8270 Acenaphthylene nd pgIL 10 10 RoziteA 6/10/01 8270 Aniline nd pg/L 10 10 RoziteA 6/10/01 8270 Anthracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzidine nd pg/L 50 50 RoziteA 6/10/01 8270 Benzoaarithracene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoapyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzobfluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270C Benzoghiperylene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd pg/L 10 10 RoziteA 6/10/01 8270 Benzoic acid nd pg/L 50 50 RoziteA 6/10/01 8270 Benzyl alcohol nd pg/L 20 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethane nd pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroethylether nd pg/L 10 10 RoziteA 6/10/01 8270 Bis2-chloroisopropylether nd pg/L 10 10 RoziteA 6/10/01 8270 s2-ethylhexylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 i3romophenyl-phenylether nd pg/L 10 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate nd jjg/L 10 10 RoziteA 6/10/01 8270 Chloro-3-methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Chloroaniline nd pg/L 10 10 RoziteA 6/10/01 .8270 Chloronaphthalene nd pg/L 10 10 RoziteA 6/10/01 8270 Chlorophenol nd ig/L 10 10 RoziteA 6/10/01 8270 Chiorophenyl phenyl ether nd g/L 10 10 RoziteA 6/10/01 8270 Chrysene nd pg/L 10 10 RoziteA 6/10/01 8270 Di-n-butylphthalate nd igIL 10 10 RoziteA 6/10/01 8270 Di-n-octylphthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dibenzoahanthracene nd p/L 10 10 RoziteA 6/10/01 8270 Dibenzofuran nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 12 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 13 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzene 14 nd pg/L 10 10 RoziteA 6/10/01 8270 Dichlorobenzidine 33 nd pgIL 10 10 RoziteA 6/10/01 8270 Dichlorophenol 24 nd jg/L 10 10 RoziteA 6/10/01 8270 Diethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethyl phthalate nd pg/L 10 10 RoziteA 6/10/01 8270 Dimethylphenol 24 nd .igIL 10 10 RoziteA 6/10/01 8270 initrophenoI 24 nd pgIL 50 50 RoziteA 6/10/01 8270 jinitrotoluene 24 nd ig/L 10 10 RoziteA 6/10/01 8270 Dinitrotoluene 26 nd pg/L 10 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 nd pg/L 10 10 RoziteA 6/10101 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 25 of 28 CLIENT SAMPLE ID 56 25 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075686 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 rAfl Meth Fluoranthene nd Jg/L 10 10 RoziteA 6/10/01 8270 Fluorene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachiorobutadiene nd pg/L 10 10 RoziteA 6/10/01 8270 Hexachiorocyclopentadiene nd ig/L 10 10 RoziteA 6/10/01 8270 Hexachioroethane nd pg/L 10 10 RoziteA 6/10/01 8270 lndeno123-cdpyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Isophorone nd pg/L 10 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd pg/L 50 50 RoziteA 6/10/01 870 Methylnaphthalene nd jgIL 10 10 RoziteA 6/10/01 8270 Methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Methylphenol nd pg/L 10 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/01 8270 Nitroaniline nd pg/L 10 10 RoziteA 6/10/0 8270 itrobenzene nd pg/L 10 10 RoziteA 6/10/01 8270 iitrophenol nd pg/L 10 10 RoziteA 6/10/01 8270 Nitrophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Nitroso-di-methylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Njtroso-di-n-propylamine normal nd .jg/L 10 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal nd pg/L 10 10 RoziteA 6/10/01 8270 Pentachiorophenol nd pg/L 50 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 10 10 RoziteA 6/10/01 8270 Phenol nd pg/L 10 10 RoziteA 6/10/01 8270 Pyrene nd pg/L 10 10 RoziteA 6/10/01 8270 Pyridine nd pg/L 10 10 RozfteA 6/10/01 8270 Trichlorobenzene 124 pg/L 10 10 RoziteA 6/10/0 8270 Trichiorophenol 245 nd pg/L 10 10 RoziteA 6/10/01 8270 Trichlorophenol 246 nd pg/L 10 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 26 of 28 CLIENT SAMPLE ID 56 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075687 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test ameter Units RDL MDL FAnalyst pate BETX Benzene nd pg/L WilliamsJ 6/1/01 8260 Ethylbenzene nd ig/L WiIIiamsJ 6/1/0 8260 Toluene nd pg/L WiIliamsJ 6/1/01 8260 Xylenes Total nd pg/L WilIiamsJ 6/1/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 27 of 28 CLIENT SAMPLE ID 56 35 CLIENT PROJECT Studebaker Building 69 El Sample No 075687 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Test Parameter ResuIts Units DLj Anyst Date eth SEMIVOLATILE ORGANICS Aenaphthene rid pg/L 40 10 RoziteA 6/10/01 8270 Acenaphthylene nd pgIL 40 10 RoziteA 6/10/01 8270 Aniline nd pg/L 40 10 RoziteA 6/1 0/01 8270 Anthracene nd pg/L 40 10 RoziteA 6/10/01 8270 Berizidine nd pg/L 200 50 RoziteA 6/1 0/01 8270 Benzoaanthracene rid pg/L 40 10 RoziteA 6/10/01 8270 Berizoapyrene nd pg/L 40 10 RoziteA 6/10/01 8270 Benzobfluoranthene rid pg/L 40 10 RoziteA 6/10/01 8270 Benzoghiperylene nd pg/L 40 10 RoziteA 6/10/01 8270 Benzokfluoranthene nd ig/L 40 10 RoziteA 6/10/01 82700 Berizoic acid rid pg/L 200 50 RoziteA 6/10/01 8270 Berizyl alcohol nd pgIL 80 20 RoziteA 6/10/01 8270 Bis2-chloroethoxymethaæe nd pglL 40 10 RoziteA 6/10/01 8270 Bis2-chloroethylether nd pg/L 40 10 RziteA 6/10/01 8270 Bis2-chloroisopropylether rid pg/L 40 10 RoziteA 6/10/01 8270 s2-ethylhexylphthalate 190 pg/L 40 10 RoziteA 6/10/01 8270 t3romophenyl-phŁnylether nd pg/L 40 10 RoziteA 6/10/01 8270 Butyl benzyl phthalate rid pg/L 40 10 RoziteA 6/10/01 8270 Chloro-3-methylphenol rid ig/L 40 10 RoziteA 6/10/01 8270 Chloroanuline nd pg/L 40 10 RoziteA 6/10/01 8270 Chlororiaphthalene nd pg/L 40 10 RoziteA 6/10/01 8270 Chtoropheriol nd pg/L 40 10 RoziteA 6/10/01 8270 Chlorophenyl phenyl ether nd ig/L 40 10 RoziteA 6/10/01 8270 Chryserie nd .ig/L 40 10 RoziteA 6/10/01 8270 D-ri-butylphthalate rid pg/L 40 10 RoziteA 6/10/01 82700 Di-n-octylphthalate rid pg/L 40 10 RoziteA 6/10/01 8270 Dibenzoahanthracerie nd pg/L 40 10 RoziteA 6/10/01 8270 Diberizofurari nd pg/L 40 10 RoziteA 6/1 0/01 8270 Dichlorobenzene 12 rid pg/L 40 10 RoziteA 6/10/01 8270 Dichloroberizene 13 rid pg/L 40 10 RoziteA 6/10/01 8270 Dichloroberizene 14 rid pg/L 40 10 RoziteA 6/10/01 8270 Dichloroberizidirie 33 rid pg/L 40 10 RoziteA 6/10/01 8270 Dichlorophenol 24 nd pgIL 40 10 RoziteA 6/10/01 8270 Diethyl phthalate rid pg/L 40 10 RoziteA 6/10/01 8270 Dimethyl phthalate rid pg/L 40 10 RoziteA 6/10/01 8270 Dimethylphenol 24 rid pg/L 40 10 RoziteA 6/10/01 8270 initropheriol 24 rid pg/L 200 50 RoziteA 6/10/01 82700 iriitrotoluerie 24 rid pg/L 40 10 RziteA 6/10/01 82700 Dinitrotoluerie 26 rid pgIL 40 10 RoziteA 6/10/01 8270 Diphenylhydrazine 12 rid pg/L 40 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 SAMPLE RESULTS Page 28 of 28 CLIENT SAMPLE ID 56 35 Report Date 6/12/01 CLIENT PROJECT Studebaker Building 69 EIS Sample No 075687 SAMPLE TYPE WaterNon DW EIS Order No 010500216 Date Collected 5/23/01 Date Received 5/23/01 Parameter ResuIts 1Units RDL 1MDL Analyst Date Method Fluoranthene nd pg/L 40 10 RoziteA 6/10/01 8270 Fluorene pg/L 40 10 RoziteA 6/10/01 8270 Hexachlorobenzene nd pg/L 40 10 RoziteA 6/10/01 8270 Hexachiorobutadiene nd pg/L 40 10 RoziteA 6/10/01 8270 HexachlorocyclopentadiŁne nd iig/L 40 10 RoziteA 6/10/01 8270 Hexachioroetharie nd pg/L 40 10 RoziteA 6/10/01 8270 Indeno1 23-cdpyrene nd pg/L 40 10 RoziteA 6/10/01 8270 Isophorone nd lJg/L 40 10 RoziteA 6/10/01 8270 Methyl-46-dinitrophenol nd pg/L 200 50 RoziteA 6/10/01 8270 Methylnaphthalene nd pgIL 40 10 RoziteA 6/10/01 8270 Methylphenol pg/L 40 10 RoziteA 6/10/01 8270 Methylpheno nd pg/L 40 10 RoziteA 6/10/01 8270 Naphthalene nd pg/L 40 10 RziteA 6/10/01 8270C Nitroanhline nd pg/L 40 10 RozitØA 6/10/0 8270 Nitroanhline nd pg/L 40 10 RoziteA 6/10/01 8270 Nitroaniline nd ig/L 40 10 RoziteA 6/10/01 8270 ltrobenzene nd pg/L 40 .10 RozitØA 6/10/01 8270 4itrophenol rid pg/L 40 10 RoziteA 6/10/01 8270 Nitrophenol nd pg/L 200 50 RoziteA 6/10/01 8270 Nitroso-di-methylamine normal nd pg/L 40 10 RoziteA 6/10/01 8270 Nitroso-di-n-propylamine normal nd pg/L 40 10 RoziteA 6/10/01 8270 Nitroso-di-phenylamine normal nd lJg/L 40 .10 RoziteA 6/10/01 8270 Pentachiorophenol nd pg/L 200 50 RoziteA 6/10/01 8270 Phenanthrene nd pg/L 40 10 RoziteA 6/10/01 8270 Phenol nd IJg/L 40 10 RoziteA 6/10/01 8270 Pyrene nd pg/L 40 10 RoziteA 6/10/01 8270 Pyridine pg/L 40 .10 RoziteA 6/10/01 8270 Trichlorobenzene 124 nd pg/L 40 10 RoziteA 6/10/01 8270 Trichlorophenol 245 nd pg/40 10 RoziteA 6/10/01 8270 Trichlorophenol 246 nd pg/L 40 10 RoziteA 6/10/01 8270 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010500216 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCAA 615/8151A/515.1 8151k 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608 8081A 8082/508 8082 22 135 40-150 Pesticides PCB DecachlorobiphenylDCB 608/ 8081A 508 8082 22-135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625 8270C 8270C 21 100 25-121 SVOC acid Phenol d5 625/8270C 8270C 10-94 24-113 SVOC base/neutral Nitrobenzene d5 625 8270C 8270C 35 114 23-120 SVOC base/neutral 2-Fluorobiphenyl 625 8270C 8270C 43-116 30-115 SVOC acid 246-Thbromophenol 625 8270C 8270C 10-123 19-122 SVOC base/neutral Terphenyl d14 625 8270C 8270C 33 141 18-137 TPH Styrene 8015M 8015M 30-70 34 -66 VOC BETX TPH 2-Dichloroethane d4 624 8260B 524.2 8260B 76 114 70-121 VOC BETX TPH Toiuene d8 624 8260B/524.2 8260B 86 115 74 121 VOC BETX TPH BromofluorobenzeneBFB 624 8260B 524.2 826GB 86 115 74 121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 075679 50 SW 25 8260 WaterNon DW 2-DichioroŁthane-d4 SS 103 8260 WaterNon DW 4-Bromofluorobenene SS 8260 WaterNon DW Toluene-d8SS 93 075679 50 SW 25 8270 WaterNon DW Z46-Tribrmophenol SS 76 8270 WaterNon DW 2-Fluorobiphenyl SS 89 8270 WaterNon DW 2-Fluorophenol SS 75 8270 WaterNon DW Nitrobenzene-d5 SS 68 8270 WaterNon DW Phenl-d5SS 50 8270 WaterNon DW Terphenyl-d14 SS 74 075680 50 SW 34 8260 WaterNon DW 12-Dichloroethane-d4 SS 104 8260 WaterNon DW 4-Bromofluorobenzene SS 104 8260 WaterNon DW Toluene-d8 SS 90 075680 50 Sw 34 8270 WaterNon DW 246-Tribromophenol SS 71 8270 WaterNon DW 2-Fluorobiphenyl SS 87 8270 WaterNon DW 2-FluorophenolSS 69 8270 WaterNon DW Nitrobenzene-d5 SS 64 8270 WaterNon DW PhØnol-d5 SS 47 8270 WaterNon DW Terphenyl-d14 SS 71 075681 40 NW 25 8260 WaterNon DW 12-Dichloroethane-d4 SS 101 8260 WaterNon DW 4-Brornofluorobenzene SS 99 8260 WaterNon DW Toluene-d8 SS 90 075681 40 NW 25 8270 WaterNon DW 246-Tribrornophenol SS 78 8270 WaterNon DW 2-Fluorobiphenyl SS 91 8270 WaterNon DW 2-Fiuorophenol SS 75 8270 WaterNon OW Nitrobenzene-d5 SS 67 8270 WaterNon DW Phenol-d5 SS 51 8270 WaterNon DW Terphenyl-d14 SS 79 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Pagelof QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries ES Order ID 010500216 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenytaceticacidDCAA 615/ 8151A/515.1 8151k 15-135 Pesticides PCB 24 56-Tetrachloro-m-xyleneTCMX 608 8081 8082 508 8082 22 135 40-150 Pesticides PCB DecachlorobipheriylDCB 608/ 8081A 508 8082 22 135 40 150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625/ 8270C 827CC 21 100 25-121 SVOC acid Phenol d5 625/827CC 8270C 10-94 24-113 SVOC base/neutral Nitrobenzene d5 625 827CC 827CC 35 114 23-120 SVOC base/neutral 2-Fluorobiphenyl 625 827CC 827CC 43-116 30-115 SVOC acid 246-Tribromophenol 625 8270C 827CC 10-123 19-122 SVOC base/neutral Terphenyl d14 625 827CC 827CC 33 141 18-137 TPH Styrene 8015M 8015M 30-70 34-66 VOC BETX TPH 2-Dichloroethane d4 624 82608 524.2 8260B 76 114 70-121 VOC/BETX/TPH Toluened8 624/82608/524.2 82608 86-115 74-121 VOC BETX TPH BromofluorobenzeneBFB 624 8260B 524.2 8260B 86-115 74-121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 075682 40 NW 35 8260 WaterNon DW 12-DichlorOethane-d4 SS 104 8260 WaterNon OW 4-Bromofluorobenzene SS 106 8260 WaterNon DW ToluenŁ-d8 SS 94 075682 40 NW 35 8270 WaterNon OW 246-Tribromophenol SS 65 8270 WaterNon DW 2-Fluorobiphenyl SS 95 8270 WaterNon DW 2-Fluorophenol SS 59 8270 WaterNon DW Nitrobenzene-d5 SS 57 8270 WaterNon DW Phenol-d5 SS 39 8270 WaterNon DW Terphenyl-d14 SS 83 075683 40 NE 25 8260 WaterNon DW 2-DichloroŁthane-d4 SS 94 8260 WaterNon DW 4-Bromofluorobenzene SS 107 8260 WaterNon OW Toluene-dS SS 93 075683 40 NE 25 8270 WaterNon DW 246-TribromopheroI SS 80 8270 WaterNon DW 2-Fluorobiphenyl SS 92 8270 WaterNon OW 2-Fluorophenol SS 58 8270 WaterNon OW Nitrobenzene-d5 SS 65 8270 WaterNon DW Phenol-d5 SS 38 8270 WaterNon DW Terphenyl-d14 SS 80 075684 40 NE 35 8260 WaterNon DW 2-Dichloroethane-d4 SS 99 8260 WaterNon OW 4-BromofluorobenzeneSS 103 8260 WaterNon OW Toluene-d8 SS 92 075684 40 NE 35 8270 WaterNon DW 246-TrjbrornophenolSS -1 8270 WaterNon DW 2-Fluorobiphenyl SS -1 8270 WaterNon DW 2-Fluorophenol SS -1 8270 WaterNonOW Nitrobenzene-d5SS -1 8270 WaterNon DW Phenol-d5 SS -1 8270 WaterNon DW Terphenyl-d14 SS -1 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Page2of QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010500216 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCAA 615/ 8151A/515.1 8151A 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608/ 8081A 8082 508 8082 22-135 40-150 Pesticides PCB DecachlorobiphenylDCB 608/ 8081A 508 8082 22-135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOCacid 2-Fluorophenol 625/827CC 82700 21-100 25-121 SVOC acid Phenol d5 625 827CC 827CC 10-94 24 113 SVOC base/neutral Nitrobenzene d5 625 8270C 8270C 35-114 23-120 SVOC base/neutral 2-Fluorobiphenyl 625 827CC 8270C 43 116 30 115 SVOC acid 246-Tribromophenol 625 827CC 8270C 10-123 19-122 SVOC base/neutral Terphenyl d14 625 8270C 827CC 33-141 18-137 TPH Styrene 8015M 8015M 30-70 34-66 VOC/BETX TPH 12-Dichloroethane d4 624/82608/524.2 8260B 76-114 70-121 VOC/BETX TPH Toluene d8 624 82608 524.2 8260B 86 115 74 121 VOC BETX TPH BromofluorobenzeneBFB 624 8260B 524.2 8260B 86-115 74-121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 075685 40 NE 45 8260 WaterNon DW 2-Dichloroethane-d4 SS 103 8260 WaterNon DW 4-Bromofluorobenzene SS 113 8260 WaterNon DW Toluene-d8 SS 91 075685 40 NE 45 8270 WaterNon DW 246-Tribromophenol SS 68 8270 WaterNon DW 2-Fluorobiphenyl SS 88 8270 WaterNon DW 2-Fluorophenol SS 60 82700 WaterNon DW Nitrobenzene-d5 SS 65 8270 DW Phenol-d5 SS 8270 WaterNon DW Terphenyl-d14 SS 72 075686 56 25 8260 WaterNon OW 12-Dlchloroethane-d4 SS 101 8260 WaterNon DW 4-Bromofluorobenzene SS 104 8260 WaterNon DW Toluene-d8 SS 93 075686 56 25 8270 WaterNon DW 246-Tribromophenol SS 87 8270 WaterNon DW 2-Fluorobiphenyl SS 92 8270 WaterNon DW 2-Fluorophenol SS 80 8270 WaterNon OW Nitrobenzene-d5 SS 74 8270 WaterNon DW Phenol-d5 SS 55 8270 WaterNon DW Terphenyl-d14 SS 79 075687 56 35 8260 WaterNon DW 12-Dichloroethane-d4 SS 103 8260 WterNon DW 4-Bromofluorobenzene SS 114 8260 WaterNon OW Toluene-d8 SS 89 075687 56 35 8270 WaterNon DW 246-Tribromophenol SS 53 -I 8270 WaterNon DW 2-Fluorobiphenyl SS 86 8270 WaterNon DW 2-Fluorophenol SS 52 8270 WaterNonDW Nitrobenzene-d5 SS 58 8270 WaterNon OW Phenol-d5 SS 34 8270 WaterNon DW Terphenyl-d14 SS 71 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different 00 Limits SAMPLE PREPARATION INFORMATION Client Name Grauvogel Associates Report Date 6/12101 Client Project Studebaker Building 69 EIS Order No 010500216 EIS Lab Client Sample1 Description Date ii Completed AnaiysIi rui 075679 50 SW 25 5/23/01 Extract SVOC Complete 5/24/01 CartsenS 3510 075680 50 SW 34 5/23/01 Extract SVOC Complete 5/24/01 CarlsenS 3510 075681 40 NW 25 5/23/01 Extract SVOC Complete 5124/01 CarlsenS 3510 075682 40 NW 35 5/23/01 Extract SVOC Complete 5/24/01 CailsenS 3510 075683 40 NE 25 5/23101 Extract SVOC Complete 5/24/01 CarisenS 3510 075684 40 NE 35 5/23/01 Extract SVOC Complete 5/24/01 CarlsenS 3510 075685 40 NE 45 5/23/01 Extract SVOC Complete 5/24/01 CarisenS 3510 075686 56 25 5/23/01 Extract SVOC Complete 5/24/01 CarisenS 3510 075687 56 35 5/23/01 Extract SVOC Complete 5/24/01 CrlsenS 3510 EIS Analytical Services Inc 1701 North lronwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699 QUALITY CONTROL DATA MATRIX SPIKE DUPLICATE MATRIX SPIKE MS/DMS EIS Order 010500216 EIS Lab in This Batch Comments Concerning This QC Batch QC Sample 075686 075679 075687 None Matrix Groundwater Test BTEX Quality Control Limits Back-Spike Matrix Spike Duplicate Spike RPD Parameter ground Amount Result Result RPD LCL UCL LCL UCL QC Batch Benzene nd 5.7 5.8 102 5.6 98 --11 76 127 QB00599 Ethylbenzene nd 5.9 5.5 93 5.3 90 --12 75 --125 QB00599 Toluene nd 5.4 5.4 100 5.2 96 --13 76 --125 QB00599 Xylenes Total nd 11.7 11.2 96 10.7 91 --12 75 --125 0B00599 __LEGEND Background Sample Result Spike amount may be adjusted for dilution used in sample analysis Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same forthe Background and Spike QUALITY CONTROL DATA LABORATORY FORTIFIED METHOD BLANK LFB Matrix Lab Water EIS Lab With This LFB Comments Concerning This LFB Test SVOC 075679 075687 None Prep Date 5/24/01 Run Date 6/10/01 Quality Control Limits Spike Matrix_Spike Duplicate Spike ____Parameter Amount Result Result RPD LCL UCL LCL UCL QC Batch Acenaphthene 122 109 89 46 118 QBOO600 Chloro-3-methylphenol4 194 170 88 23 --97 .QBOO600 Chlorophenol 222 206 93 27 123 QBOO600 Dichlorobenzene 14 154 109 71 36 --97 QBOO600 Din itrotoluene 24 96 80 83 24 --96 0B00600 Nitrophenol4 112 56 50 10--80 0800600 Nitroso-di-n-propylamine normal 159 123 77 41 --116 QBOO600 Pentachlorophenol 255 217 85 --103 0B00600 Phenol 200 113 56 12 --110 QBOO6OO Pyrene 133 118 89 26 127 QBOO600 Trichlorobenzene 124 134 99 74 39 --98 0800600__-_______________ ___ II LEGEND The LF8 may be either single spike or in dulicate and may or may not be in QC Batch with MS/DMS Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Spike and Duplicate Spike CHAIN OF CUSTODY RECORD PROJ NO PROJECT NAME _______________________________________________________ Order ID us7-Total ________________________________________________No _______________ SAMPLERS Print Name Sign Con LAj -_-/of LabFIELDtalners DATE TIME STATION LOCATION _______ ______ _______________________________________Type TAT Number_____________________________________ L/z/tIOc%V tjiZS1 ___AI 7579 ____1gW _______7p________OO Lt -\_______75Z __________________________ ______1oo_je-_________ ______lok ______________756 jej1 Iob _____________7/95 __________________________ _____1100 __________________ Re hed By Si naturez.9zfj Date Time gure SQUOTE NO ____________________f2 ______________________________________ Time Received By Signire Ship To Relinquished By Signature Date Time Received By Signature NOTES If you were issued quote number it must appear on this document Instructions area for comments are on reverse side EIS ANALYTICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE SUITE .SOUTH BEND IN 46635 Phone 2192770707 Fax 2192735699 Form ChainofCustody 61297 Form Comnietlon Instructions Each slanted linereJresents specific container types from which specdlc tests are conducted Use additional record sheets if of samples or of tests exceed allotted paces Ust tests per cntainer type on the slanted lines give of containers in boxes below tests Sum all containers and place in column labeled Total No Containers For the column labeled Sample Type give brief description such as soil MW oil etc For column labeled TAT use one of the following Request Meaning Normal 24 weeks for written report based entirely on test complexity and number of samples week In general prior authorization is required from the lab to request day turnaround time Surcharges may or may not be applicable depending entirely on test complexity days Must have been authorized by the Lab and increased costs must have been authorized by the client day Must have been authorized by the Lab and increased costs must have been authorized by the client Submission Comments EIS ANALYTICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE SUITE .SOUTH BEND IN 46635 Phone 219277-0707 Fax 219273 Form ChainofCustody 61297 Mr Larry Grauvogel Report Date 7/6/01 Grauvogel Associates EIS Order No 010600230 17660 Fall Creek Drive EIS Sample No 076348 EIS Project No 2730-1000-01 Granger IN 46530 Tel No 277-4770 -- Client Sample ID MW 50 SW 25 Fax No 277-5281 Date Collected 6/25/01 P0 No Date Received 6/25/01 Project Name 730 United Drive Collected By Grauvogel This report presents results of analysis for your samples received under our Order No ÆbovØ This Number is to be used in all inquiries concerning this report The EIS Sample No above as well as your Sample ID refer to the first sample in multi-sample submission DEFINITIONS MDL Method Detection Limit normally achieved in the absence of Interferences or other matrix difficulties RDL Reporting Detection Limitachieved your sample If nunierically greater than the MDL dilutions were required in order to perform the analysis If numerically less than the MDL alternate techniques were employed nd Not Detected at the RDL value If present result is less than this value Not Detected at the numerical value shown If present result is less than this value Result is estimated due to matrix.interferences CHAIN OF CUSTODY is enclosed if received with your sample submission DRINKING WATER CERTIFICATIONS Chemistry C-71-02 Bacteriology M-76-5 ASSURANCE ICER LABORATORY IRECT The data in this report has been reviewed and complies with ElS Quality Control unless specifically addressed above EIS Analytical Services Inc 1701 Ironwood Drive Suite South Bend IN 46635 Tel 219-277-0707 Fax 219-273-5699 Page lof2l SAMPLE RESULTS Page 2of 21 CLIENT SAMPLE ID MW 50 SW 25 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076348 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Parameter Euits1 IT1 pate VOLATILE ORGANICS Acetone nd pg/L 10 10 WiIIiamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WiIIiamsJ 6/28/01 8260 Acrylonitrile nd pg/L 20 20 WiIIiamsJ 6/28/01 8260 Benzene nd pg/L WilliamsJ 6/28/0 8260 Bromobenzene nd pg/L WilliamsJ 6/28/0 8260 Bromochioromethane nd ig/L WiIIiamsJ 6/28/01 8260 .Bromodichloromethane nd pg/L WiIIiamsJ 6/28/01 8260 Bromoform nd pg/L WiIIiamsJ 6/28/01 8260 Bromomethane nd g/L WilIiarnsJ 6/28/01 8260 Butylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene sec nd pg/L WiUiamsJ 6/28/0 8260 Butylbenzenetert nd jg/L WilliamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilIiamsJ 6/28/01 8260 Carbon Tetrachloride nd pgIL WilliamsJ 6/28/01 8260 Chlorobenzene nd pg/L WilliamsJ 6/28/01 8260 Chloroethane nd pg/L WilliamsJ 6/28/01 8260 hloroform nd pg/L WiltiamsJ 6/28/01 8260 Chlorohexane ..nd ig/L .WiIliamsJ 6/28/01 8260 Chioromethane nd pg/L 10 10 WiIIiamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/0 8260 ChlorotoluenØ nd pg/L WiIIiamsJ 6/28/01 8260 Cyclohexanone nd pg/L 100 100 WiIIiamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 nd pg/L 30 30 WiIliarnsJ 6/28/01 8260 Dibromochloromethane nd pgIL WitIiamsJ 6/28/01 8260 Dibromoethane 12 nd pg/L WilliamsJ 6/28/01 .8260 Dibromomethane nd pg/L WiIIiarnsJ 6/28/01 8260 Dichloro-2-butene 14 nd pg/L 30 30 WiIIiamsJ 6/28/01 8260 Dichlorobenzene 12 nd pgIL WilliamsJ 6/28/01 8260 Dichlorobenzene 13 nd pg/L WiIliamsJ 6/28/01 8260 Diclilorobenzene 14 nd pg/L WilliamsJ 6/28/01 8260 Dichlorodifluoromethane nd pgiL WilliarnsJ 6/28/01 8260 Dichloroethane 11 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WilliamsJ .6/28/01 8260 Dichloroethene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene c-i 2.0 j.ig/L WilIiamsJ 6/28/01 8260 Dichloroethene t-1 nd pg/L WilIiamsJ 6/28/01 8260 Dichlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 ichloropropane 12 nd pg/L WiIliamsJ 6/28/01 8260 Lichloropropane 13 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 22 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropene 11 nd pg/L WilIiamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North lronwoodDrive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005296 SAMPLE RESULTS Page of 21 CLIENT SAMPLE ID MW 50 SW 25 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076348 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter sults Uiijts 1R1 i1 Date Method Dichloropropene c-i nd pg/L WifliamsJ 6/28/01 8260 Dichioropropene t-i3 rid g/L WilliamsJ 6/28/01 8260 Diethyl ether rid pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pgIL WilliamsJ 6/28/01 8260 Ethylbenzene nd pg/L WilliamsJ 6/28/01 8260 Heptane normal nd pg/L WiIliamsJ 6/28/01 8260 Hexachlorobutadiene nd pg/L WilliarnsJ 6/28/01 8260 Hexanone 2-rid ig/L 10 10 WilliamsJ 6/28/01 8260 lodometharie nd pg/L WilliamsJ 6/28/01 8260 lsopropylbenzene nd pg/L WiliamsJ 6/28/01 8260 Isopropyltoluene para nd pg/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WlliamsJ 6/28/01 8260 Methyl lsobutyl Ketone MIBK rid pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate rid ig/L WilliamsJ 6/28/01 8260 Methylbutylether tert MTBE nd .ig/L WilliamsJ 6/28/01 8260 Methylene chloride rid ig/L WilliamsJ 6/28/01 8260 Japhthalene rid pg/L WilliamsJ 6/28/01 8260 rropyIbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Styrene nd g/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethene .8 pg/L WilliarnsJ 6/28/01 8260 Tetrahydrofurari nd pg/L 10 10 WilliamsJ 6/28/01 8260 Toluene nd pgfL WilliamsJ 6/28/01 8260 TPH DRO/GRO nd pg/L 200 200 WilliamsJ 6/28/01 8260 Trichloroberizene 123 rid ig/L WilliamsJ 6/28/01 8260 Trichlorobenzene 124 rid pg/L WilliamsJ 6/28/01 8260 Trichloroetharie 111 rid pg/L WilliamsJ 6/28/01 8260 Trichloroetharie 112 rid pg/L WilliamsJ 6/28/01 8260 Trichloroetherie 21 pg/L WilliamsJ 6/28/01 8260 Trichlorofluoromethane rid pg/L WilliamsJ 6/28/01 8260 Trichloropropane 123 rid pg/L WilliamsJ 6/28/01 8260 Trichiorotrifluoroetharie nd pg/L WilliamsJ 6/28/0 8260 Trimethylbenzene 124 rid pg/L WilliamsJ 6/28/01 8260 Trimethylberizene 135 rid pg/L WilliamsJ 6/28/01 8260 Vinyl acetate rid pg/L 10 10 WilliamsJ 6/28/01 8260 Vinyl Chloride rid pg/L WilliamsJ 6/28/01 8260 Xylene ortho rid pg/L WilliamsJ 6/28/01 8260 yIenes meta para rid pg/L WilIiamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005297 SAMPLE RESULTS Page4of 21 CLIENT SAMPLE ID MW 50 SW 35 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076349 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test jiJits Date Method VOLATILE ORGANICS Acetone nd pgIL 10 10 WiIIiamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WilliamsJ 6/28/01 8260 Acrylonitrite rid pg/L 20 20 WilliamsJ 6/28/0 8260 Benzene nd pg/L WilIiamsJ 6/28/01 8260 Bromobenzene nd pg/L WiIliamsJ 6/28/01 8260 Bromochioromethane nd pg/L WilIiamsJ 6/28/01 8260 Brornodichloromethane nd pg/L WilIiamsJ 6/28/01 8260 Bromoform nd pg/L WiIIiamsJ 6/28/01 8260 Bromomethane nd pglL WilliamsJ 6/28/01 8260 Butylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene sec nd pgIL WilliamsJ 6/28/01 8260 Butylbenzene tert nd pg/L WilliamsJ 6/28/01 8260 Carbon disulfide nd vigIL WilliarnsJ 6/28/0 8260 Carbon Tetrachloride nd pg/L WilliamsJ 6/28/01 8260 rn Chlorobenzene nd igIL WifliamsJ 6/28/01 8260 hioroethane nd pg/L WiIIiamsJ 6/28/01 8260 chloroform nd pg/L WilliamsJ 6/28/01 8260 Chlorohexane nd pg/L WilliamsJ 6/28/01 8260 Chioromethane nd pg/L 10 10 WilliamsJ 6/28/01 8260 Chlorotoluene nd igIL WiHiamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/Q1 8260 Cyclohexanone nd pg/L 100 100 WiIIiamsJ 6/28/01 8260 Dibrorno-3-chloropropane 12 nd pg/L 30 30 WHhiamsJ 6/28/01 8260 Dibromochioromethane nd pg/L WilliamsJ 6/28/01 .8260 Dibromoethane 12 rid pg/L WilIiamsJ 6/28/01 8260 Dibromomethane nd JgIL .2 WilhiamsJ 6/28/01 8260 Dichloro-2-butene 14 rid pg/L 30 30 WilliamsJ 6/28/01 8260 Dichlorobenzene12 rid pg/L WilliamsJ 6/28/01 8260B Dichlorobenzene13 nd pg/L WiIliamsJ 6/28/01 8260 Dichlorobenzene 14 rid pg/L WilliamsJ 6/28/0 8260 Dichiorodifluoromethane rid pg/L WilliamsJ 6/28/01 8260 Dichloroethane 11 nd WilliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 nd pg/L WitliamsJ 6/28/01 8260B Dichioroethene c-12 3.6 pg/L WilliamsJ 6/28/01 8260 Dichloroethene t-12 nd .igIL WilliamsJ 6/28/01 8260 ichlorofIuoromethane nd pg/L .WilliamsJ 6/28/01 8260 Achloropropane 12 nd pg/L WifliamsJ 6/28/01 8260 Dichloropropane 13 rid pg/L WilliarnsJ 6/28/01 8260 Dichloropropane 22 rid ig/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005298 SAMPLE RESULTS age5of 21 CLIENT SAMPLE ID MW 50 SW 35 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076349 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter JResults jUnitsi RDL fMDL LAnaIyst Method Dichloropropene 11 nd pg/L WiIliamsJ 6/28/01 8260 Dichloropropene c-13 nd pgIL WilliamsJ 6/28/01 8260 Dichioropropene t-1 nd pg/L WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pg/L WilliamsJ 6/28/01 8260 Ethylbenzene nd pgIL WillimsJ 6/28/0 8260 Heptane normal nd pgIL WilliamsJ 6/28/01 8260 Hexachlorobutadiene nd pgIL WilliamsJ 6/28/01 8260 Hexanone 2-nd pg/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd pg/L WilliamsJ 6/28/01 8260 Isopropylbenzene nd pg/L WilliamsJ 6/28/01 8260 Isopropyltoluene para nd pg/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl Isobutyl Ketone MIBK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pg/L WilliamsJ 6/28/01 8260 Methylbutylether tertMTBE nd pgIL WilliamsJ 6/28/01 8260 ethylene chloride nd pg/L WiliiamsJ 6/28/0 8260 Japhthalene nd pg/L WilliamsJ 6/28/01 8260 Propylbenzenonormal nd pgIL WilliamsJ 6/28/01 860 Styrene nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 nd pg/L WifliamsJ 6/28/01 8260 Tetrachioroethene 3.2 pg/L WilliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 10 10 WilliarnsJ 6/28/01 8260B Toluene nd pg/L WilliamsJ 6/28/01 82608 TPH DRO/GRO nd ig/L 2O0 200 WiUiamsJ 6/28/01 8260 Trichlorobenzene 123 nd pg/L WilliamsJ 6/28/01 8260 Trichlorobenzene 124 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethane111 1.4 pg/L WilliamsJ 6/28/01 8260 Trichloroethane 112 nd pg/L WifliamsJ 6/28/01 8260 Trichloroethene 31 pg/L WilliamsJ 6/28/0 8260 Trichlorofluoromethane nd pgIL WilliamsJ 6/28/0 8260 Trichloropropane 123 nd pgIL WilliamsJ 6/28/01 8260 Trichlortrifluoroethane nd .1g/L WilliamsJ 6/28/01 8260 Trimethylbenzene 124 nd pgIL WilliamsJ 6/28/01 8260 Trimethylbenzene 135 nd pg/L WilliamsJ 6/28/01 8260 Vinyl acetate nd pg/L 10 10 WilliamsJ 6/28/01 8260 inyl Chloride nd pg/L WilliamsJ 6/28/0 8260 ylene ortho nd pgIL WilliamsJ 6/28/01 8260 Xylenes meta para nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219.273-5699FORD005299 SAMPLE RESULTS Page6of 21 CLIENT SAMPLE ID MW 56 25 CLIENT PROJECT 730 United Drive El Sample No 076350 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Parameter bt FDL1 Date Method VOLATILE ORGANICS Acetone nd pgIL 10 10 WiIIiamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WiHiamsJ 6/28/01 8260 Acrylonitrile rid pg/L 20 20 WlIIiamsJ 6/28/01 8260 Benzene rid ig/L WilliamsJ 6/28/01 8260 Bromobenzene rid ig/L WilIiamsJ 6/28/01 8260 Bromochioromethane nd pg/L WifflamsJ 6/28/01 8260 Bromodichioromethane nd pg/L WilliamsJ 6/28/01 8260 Bromoform nd pgIL WiliiamsJ 6/28/01 8260 Bromomethane nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene normal rid ig/L WilhiamsJ 6/28/01 8260 Butylbenzene sec rid pg/L WilhiamsJ 6/28/0 8260 Butylbenzene tert nd jig/L WilliamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilliamsJ 6/28/01 8260 Carbon Tetrachioride nd pg/L WilIiamsJ 6/28/01 8260 Chlorobenzene nd pg/L WiIliamsJ 6/28/01 8260 hioroethane nd pg/L WilliamsJ 6/28/01 826 htoroform nd pgIL WilliamsJ 6/28/0 8260 Chlbrohexane rid pg/L Wilhiamsj 6/28/01 8260 Chioromethane rid pg/L 10 10 WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Chlorotoluene pg/L WilliamsJ 6/28/0 8260 Cyclohexanone nd pgiL 100 100 WilliamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 rid pg/L 30 30 WilliamsJ 6/28/01 8260 Dibromochiorometharie nd pg/L WilliamsJ 6/28/01 8260 Dbromoethane 12 rid pg/L WilIiamsJ 6/28/01 8260 Dibromomethane nd pg/L WHhiamsJ 6/28/0 8260 Dichloro-2-butene 14 nd pg/L 30 .30 WilhiamsJ 6/28/01 8260 Dichlorobenzene 12 rid pg/L WilliarnsJ 6/28/0 8260 Dichloroberizene 13 rid pg/L WilhiamsJ 6/28/01 8260 Dichloroberizene 14 rid pg/L WilIiamsJ 6/28/0 8260 Dichiorodifluoromethane rid pg/L WiDiamsJ 6/28/01 8260 Dichloroethane 11 nd ig/L WilliarnsJ 6/28/01 8260 Dichloroethane 12 rid pg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 nd pg/L WilliarnsJ 6/28/01 8260 Dichioroethene c-i nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene t-12 nd pgIL WilliamsJ 6/28/01 8260 ichlorofIuoromethane rid pg/L WilliamsJ 6/28/0 8260 1chloropropane 12 rid pg/L WilliamsJ 6/28/01 8260 Dichloropropane 13 rid pg/L WilliamsJ 6/28/01 8260 Dichloropropane 22 rid igIL WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005300 SAMPLE RESULTS Page of 21 CLIENT SAMPLE ID MW 56 25 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076350 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter fiults Units Date Dichloropropene 11 nd pg/L WilliamsJ 6/28/01 -8260 Dichloropropene c-i nd pg/L WilliamsJ 6/28/01 8260 Dichloropropene t-13 nd pg/L WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WiltiamsJ 6/28/01 8260 Ethyl methacrylate nd ig/L WilliamsJ 6/28/01 8260 Ethylbenzene nd ig/L WilliamsJ 6/28/0 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachlorobutadiene nd ig/L WilliamsJ 6/28/01 8260 Hexanone 2-nd pg/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd pgIL WilliamsJ 6/28/01 8260 lsopropylbenzene nd pg/L WilliarnsJ 6/28/01 8260 Isopropyltoluene para nd pg/L WilliarnsJ 6/28/0 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilIiamsJ 6/28/01 8260 Methyl Isobutyl Ketone MIBK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pglL WilliamsJ 6/28/01 8260 Methylbutylether tert MTBE nd pg/L WilliamsJ 6/28/01 8260 lethylene chloride nd pg/L WilliamsJ 6/28/01 8260 .aphthalene nd pg/L WilliamsJ 6/28/01-8260 Propylbenzene normal hd ig/L WilliamsJ 6/28/01 8260 Styrene nd -pg/L-WilliarnsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WilliarnsJ 6/28/01 8260 Tetrachloroethane 1122 nd pg/L WilliamsJ 6/28/01 8260 Tetrachioroethene 1.3 pg/L WiIliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 10 10 WilliamsJ 6/28/01 8260 -Toluene nd ig/L WilliamsJ 6/28/01 8260 TPH DRO/GRO nd pg/L 20 200 WilliamsJ 6/28/01 8260 Trichlorobenzene 123 nd --pg/L WilliamsJ 6/28/01 8260 Trichlorobenzene 124 nd pg/L WilliamsJ 6/28/0 8260 Trichloroethane 111 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethane 112 nd pg/L WilliamsJ 6/28/01 8260 TrichloroethØne pg/L WilliamsJ 6/28/0 8260 Trichlorofluoromethane nd ig/L .2 WilliamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L WilliamsJ 6/28/91 8260 Trichlorotrifluoroethane nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 124 nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 135 nd pg/L WilliamsJ 6/28/01 8260 Vinyl acetate nd pg/L 10 10 WilliamsJ 6/28/01 8260 Vinyl Chloride nd pg/L WilliamsJ 6/28/01 8260 ylene ortho nd Jg/L WilliamsJ 6/28/01 8260 Xylenes meta para nd pg/L WilliarnsJ 6/28/0 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005301 SAMPLE RESULTS Page of 21 CLIENT SAMPLE ID MW 56 35 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076351 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter ResuIts Units RDL AnaIyst Date Md VOLATILE ORGANICS Acetone nd ig/L 10 10 WilliamsJ 6/28/01 8260 Acrolein nd ig/L 20 20 WiHiamsJ 6/28/0 8260 Acrylonitrile rid pgIL 20 20 WilIiamsJ 6/28/0 8260 Benzene nd Jg/L WilliamsJ 6/28/0 8260 Bromobenzene nd pg/L WilIiamsJ 6/28/01 8260 Bromochioromethane nd pg/L WiliiamsJ 6/28/01 8260 Bromodichioromethane nd pg/L WilliamsJ 6/28/01 8260 Bromoform nd pgIL WilUamsJ 6/28/0 8260 Bromomethane nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene normal nd pgIL WilliamsJ 6/28/01 8260 Butylbenzene sec 4.3 pg/L WiHiaæisJ 6/28/01 8260 Butylbenzene tert nd pg/L WilliamsJ 6/28/01 8260 Carbon disulfide rid pg/L WilliamsJ 6/28/0 8260 Carbon Tetrachioride nd pg/L WilliamsJ 6/28/01 8260 Chlorobenzene rid pg/L WilliamsJ 6/28/01 8260 Thioroethane rid ig/L WiIliamsJ 6/28/01 8260 chloroform nd pg/L WiIliamsJ 6/28/01 8260 Chlorohexane nd pg/L WilliamsJ 6/28/01 8260 Chloromethane nd pg/L 10 10 WiIliamsJ 6/28/01 8260 Chlorotoluene nd pgIL WiIliamsJ 6/28/01 8260 Chlorotoluene nd pgIL WiIliamsJ 6/28/01 8260 Cyclohexanone nd pgIL 100 100 WilliamsJ 6/28/01 8260 Dibromo-3-chloropropanŁ 12 nd pg/L 30 30 WilliamsJ 6/28/01 8260 Dibromochioromethane rid pg/L WiIliamsJ 6/28/01 8260 Dibrornoethane 12 rid pg/L WiIliamsJ 6/28/01 8260B Dibromomethane nd pg/L WilliamsJ 6/28/01 8260 Dichloro-2-butene 14 rid pg/L 30 30 WilIiamsJ 6/28/01 8260 Dichlorobenzene 12 nd pg/L WiIIiamsJ 6/28/01 8260 Dichlorobenzene 13 rid pg/L WilIiamsJ 6/28/0 8260 Dichlorobenzene 14 nd pg/L WilliamsJ 6/28/01 8260 Dichlorodifluoromethane nd pg/L WilliamsJ 6/28/01 8260 Dichloroethane 11 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 rid pg/L .WiIIiamsJ 6/28/01 8260 Dichioroethene c-12 1.7 pg/L WilliamsJ 6/28/01 8260 Dichioroethene t-1 nd pg/L WilliamsJ 6/28/01 8260 ichlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 ichloropropane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane13 rid ig/L WHIiamsJ 6/28/01 8260 Dichloropropane 22 rid pg/L WiIIiamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Pagegof 21 CLIENT SAMPLE ID MW 56 35 CLIENT PROJECT 730 United Drive EIS Sample No 076351 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test T1 rusI i1 Date Dichloropropene 11 nd pg/L WiDiamsJ 6/28/01 8260.B Dichioropropene c-I nd pg/L WilliamsJ 6/28/0 8260 Dichloropropene t-13 rid pg/L WiIIiamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilIiamsJ 6/28/01 8260 Ethyl methacrylate nd pg/L WilliamsJ 6/28/01 8260 Ethylbenzene nd pg/L WilliamsJ 6/28/01 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachiorobutadiene rid pg/L WilliamsJ 6/28/0 8260 Hexanone 2-nd ig/L 10 10 WillianisJ 6/28/01 8260 lodometharie nd pg/L WilliarnsJ 6/28/01 8260 Isopropylberizerie nd pg/L WilliamsJ 6/28/01 8260 Isopropyitoluene para nd pg/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliarnsJ 6/28/01 8260 Methyl Isobutyl Ketone MIBK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pg/L WilhiamsJ 6/28/01 8260 Methylbutylether tert MTBE nd pg/L WilliamsJ 6/28/01 8260 Aethylene chloride nd Jg/L WifliamsJ 6/28/01 8260 NaphthalenØ rid pg/L WilliamsJ 6/28/01 8260 Propylbenzene normal rid pg/L WilliamsJ 6/28/01 8260 Styrene nd ig/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 nd pgIL WilliamsJ 6/28/01 8260 Tetrachloroethene 1.1 pg/L WilliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 10 10 WilliamsJ 6/28/01 8260 Toluene rid pg/L WilliamsJ 6/28/0 8260 TPH DRO/GRO 1030 pg/L 200 200 WilliarnsJ 6/28/01 8260 Trichlorobenzene 123 nd pg/L WilliamsJ 6/28/0 8260 Trichloroberizerie 124 rid jg/L WilliamsJ 6/28/0 8260 Trichloroethane 111 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethane 112 rid pg/L WiUiamsJ 6/28/01 8260 Trichtoroethene 15 pg/L WitliarnsJ 6/28/01 8260 Trichlorofluoromethane nd ig/L WilliamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L WiIliamsJ 6/28/01 8260 Trichlorotrifluoroetharie rid pg/L WilliamsJ 6/28/01 8260 Trimethylberizerie 124 rid pg/L WilliamsJ 6/28/01 8260 Trimethylberizerie 135 rid pg/L WilliamsJ 6/28/01 8260 Vinyl acetate rid pg/L 10 10 WilliamsJ 6/28/01 8260 inyl Chloride rid pg/L WilliamsJ 6/28/0 8260 ylerie ortho nd pg/L WilliarnsJ 6/28/01 8260 Xylenes meta para rid pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219.277.0707 Fax SAMPLE RESULTS Page 10 of 21 CLIENT SAMPLE ID MW 40 NE 25 CLIENT PROJECT 730 United Drive Report Date 7/6/01 EIS Sample No 076352 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter Date Lei VOLATILE ORGANICS Acetone nd pg/L 10 10 WilIiamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WiIIiamsJ 6/28/01 8260 Acrylonitrile nd pg/L 20 20 WilIiamsJ 6/28/01 8260 Benzene nd pg/L WilhiamsJ 6/28/01 8260 Bromobenzene nd pg/L WiIhamsJ 6/28/01 8260 Bromochioromethane nd pgIL WiIIiamsJ 6/28/01 8260 Bromodichloromethane nd pg/L .1 WilliamsJ 6/28/01 8260 Bromoform nd pg/L WilliamsJ 6/28/01 8260 Bromomethane nd pg/L WilliamsJ 6/28/01 8260B ButylbenzØne normal nd pg/L WiIIiamsJ 6/28/01 8260 Butylbenzene sec nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene tert nd pg/L WilliamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilliamsJ 6/28/01 8260 Carbon Tetrachioride nd pg/L WilliamsJ 6/28/01 8260 Chlorobenzene nd pg/L WiIIiarnsJ 6/28/01 8260 hioroethane nd pg/L WilliamsJ 6/28/01 8260 Jhloroform nd pg/L WiIIiamsJ 6/28/01 8260 Chlorohexane nd pg/L WilhiamsJ 6/28/01 8260 Chioromethane nd pg/L 10 10 WilliamsJ 6/28/i 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Cyclohexanone nd pg/L 100 100 WilIiamsJ 6/28/01 8260 Dibromo3-chIoropropane 12 nd pg/L 30 30 WilliamsJ 6/28/01 8260 Dibromochloromethane nd Jg/L WilliamsJ 6/28/01 8260 Dibromoethane 12 nd pg/L WilliarnsJ 6/28/01 8260B Dibromomethane nd pg/L WiIIiarnsJ 6/28/01 8260 Dichloro-2-butene 14 nd pg/L 30 30 WiIliamsJ 6/28/01 8260 Dichlorobenzene 12 nd jg/L WiIIiamsJ 6/28/01 8260 Dichlorobenzene 13 nd pg/L WiIIiamsJ 6/28/01 8260 Dichlorobenzene 14 nd pgIL WilliamsJ 6/28/01 8260 Dichlorodifluoromethane nd pg/L WiIIiamsJ 6/28/0 8260 Dichloroethane 11 nd pg/L WiIliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WiIIiamsJ 6/28/0 8260 Dichloroethene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene c-12 3.4 pgIL WiIliamsJ 6/28/01 8260 Dichloroethene t-1 nd pg/L WilliamsJ 6/28/01 8260 ichlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 ichloropropane 12 nd pg/L WilliamsJ 6/28/0 8260 Dichloropropane 13 nd pg/L WiIliamsJ 6/28/01 8260 Dichloropropane 22 nd .ig/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005304 SAMPLE RESULTS age o21 CLIENT SAMPLE ID MW 40 NE 25 Report Date 7/6/0 CLIENT PROJECT 730 United Drive EIS Sample No 076352 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Parameter IResults 1ilDI Date Dichloropropene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioropropene c-i nd pg/L WiIIiamsJ 6/28/01 8260 Dichloropropene t-1 nd pg/L WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WiiliamsJ 6/28/01 8260 Ethyl methacrylate ad Jg/L WilliamsJ 6/28/01 8260 Ethylbenzene ad ig/L WilliamsJ 6/28/01 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachiorobutadiene ad pg/L WilliamsJ 6/28/01 8260 Hexanone 2-ad pg/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd pg/L WilliamsJ 6/28/0 8260 lsopropylbenzene ad pgIL WilliamsJ 6/28/01 8260 lsopropyltoluene para 4.3 pg/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketoae MEK rid pg/L 10 10 WiIIiamsJ 6/28/01 8260 Methyl isobutyl Ketone MIBK ad pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd ig/L WilliamsJ 6/28/01 8260 Methylbutylether tert MTBE ad pg/L WilliamsJ 6/28/01 8260 Aethylene chloride ad pg/L WilliamsJ 6/28/01 8260 iJaphthalene nd Jg/L WilliamsJ 6/28/01 8260 Propylbeazene normal ad pgIL WilliamsJ 6/28/01 8260 Styreae ad igIL WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 ad pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 ad pg/L .1 WilliamsJ 6/28/01 8260 Tetrachloroetheae 1.5 pg/L WilliamsJ 6/28/01 8260 Tetrahydrofuraa hd pg/L 10 10 WilliamsJ 6/28/01 8260 Toluene nd pg/L WilliamsJ 6/28/01 8260 TPH DRO/GRO 6260 pg/L 200 200 WlliamsJ 6/28/01 8260 Trichlorobenzeae 123 ad pg/L WilliamsJ 6/28/01 8260 Trichlorobenzeae 124 ad pg/L WilliamsJ 6/28/01 8260 Trichloroethaae 111 ad pg/L WilIiamsJ 6/28/01 8260 Trichloroethane 112 ad pg/L WilliamsJ 6/28/01 8260 Trichloroetheae 6.8 pg/L WilliamsJ 6/28/01 8260 Trichlorofluoromethaae ad pg/L WilliamsJ 6/28/01 8260 Trichloropropaae 123 ad pg/L WilliamsJ 6/28/01 8260 Trichlorotrifluoroethane nd pg/L WiIliamsJ 6/28/01 8260 Trirnethylbeazene 124 11 vigIL WilliamsJ 6/28/01 8260 Trimethylbeazeae 135 ad pg/L WilliamsJ 6/28/01 8260 Vinyl acetate ad pg/L 10 10 WilliamsJ 6/28/01 8260 Vinyl Chloride ad pg/L WilliamsJ 6/28/01 8260 ylene ortho ad pg/L WilliamsJ 6/28/01 8260 Xyleaes meta para nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005305 SAMPLE RESULTS Page 12 of 21 CLIENT SAMPLE ID MW 40 NE 35 CLIENT PROJECT 730 United Drive Report Date 7/6/01 EIS Sample No 076353 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01-1IijUiii 1Ibtj Date VOLATILE ORGANICS Acetone nd pg/L 100 10 WilliamsJ 6/28/01 8260 Acrolein nd pg/L 200 20 WiIIiamsJ 6/28/01 8260 Acrylonitrile nd ig/L 200 20 WilliamsJ 6/28/01 8260 Benzene nd ig/L 10 WilliamsJ 6/28/01 8260 Bromobenzene nd pg/L 10 Wifliamsj 6/28/01 8260 Bromochlorornethane nd pg/L 10 WilliamsJ 6/28/01 8260 Bromodichloromethane nd pg/L 10 WilliamsJ 6/28/01 8260 Bromoform nd pg/L 20 WiIIiamsJ 6/28/01 8260B Bromomethane nd pg/L 20 WilliamsJ 6/28/0 8260 Butylbenzene normal nd 20 WilliamsJ 6/28/0 8260 Butylbenzene sec nd pgfL 20 WilliamsJ 6/28/01 8260 Butylbenzene tert nd pg/L 20 WilliamsJ 6/28/01 8260 Carbon disulfide nd pg/L 20 WilliamsJ 6/28/01 8260 Carbon Tetrachloride æd pg/L 20 WilliamsJ 6/28/01 8260 Chlorobenzene nd pg/L 10 WilliamsJ 6/28/01 8260 horoethane nd pg/L 20 WilliamsJ 6/28/01 8260 Chloroform nd pg/L 10 WilliamsJ 6/28/01 8260 Chlorohexane .nd pg/L 20 .2 WilliamsJ 6/28/01 .8260 Chloromethane nd pgIL 100 .10 WilliarnsJ 6/28/01 8260 Chlorotoluene nd.pgIL 10 WilliarnsJ 6/28/01 8260 Chlorotoluene nd pg/L 10 6/28/01 8260 Cyclohexanone nd pg/L 1000 100 WilliamsJ 6/28/01 8260 Dibromo-3-chloropropanØ 12 nd pg/L 300 30 WilliamsJ 6/28/01 8260 Dibromochloromethane nd pgIL 10 WilliamsJ 6/28/01 8260 bibromoethane 12 nd pg/L 10 WilliamsJ 6/28/01 8260 Dibromomethane nd jg/L 20 WilliamsJ 6/28/01 8260 Dichloro-2-butene 14 nd pg/L 300 30 WiIliamsJ 6/28/01 8260 Dichlorobenzene 12 nd pg/L 20 WilliamsJ 6/28/01 82608 Dichlorobenzene 13 nd pg/L 20 WilliamsJ 6/28/01 82608 Dichlorobenzene 14 nd pgIL 20 WilliamsJ 6/28/01 8260 Dichiorodifluoromethane nd pg/L 20 WilliamsJ 6/28/01 8260 Dichloroethane 11 nd pg/L 10 WilliamsJ 6/28/01 8260 Dichloroethane 12 nd ig/L 10 WilliamsJ 6/28/01 82608 Dichloroethene 11 nd pg/L 20 WifliamsJ 6/28/01 8260 Dichloroethene c-12 nd pg/L 10 WilliamsJ 6/28/01 82608 Dichioroethene t-12 nd pg/L 10 WilliamsJ 6/28/01 8260 ichlorofluoromethane nd pg/L 50 WilliamsJ 6/28/01 8260 Jichloropropane 12 nd pg/L 10 WilliamsJ 6/28/01 8260 Dichloropropane 13 nd pg/L 20 WilliamsJ 6128/01 8260 Dichloropropane 22 nd pg/L 50 WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Pagel3of 21 CLIENT SAMPLE ID MW 40 NE 35 CLIENT PROJECT 730 United Drive Report Date 7/6/01 EIS Sample No 076353 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test1aiibtii1Date Method Dichloropropene 11 nd pg/L 20 WilliamsJ 6/28/01 8260 Dichioropropene c-13 nd pg/L 20 WilliamsJ 6/28/01 8260 Dichloropropene t-13 nd pg/L 20 .2 WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 100 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pg/L 50 WiIIiamsJ 6/28/01 8260 Ethylbenzene nd pgIL 10 WilliamsJ 6/28/01 8260 Heptane normal nd pgIL 50 WilliamsJ 6/28/01 8260 Hexachlorobutadiene nd pg/L 20 WilliamsJ 6/28/01 8260 Hexanone 2-nd pgIL 100 10 WilliamsJ 6/28/01 8260 lodomethane nd pg/L 50 WilliamsJ 6/28/01 8260 lsopropylbenzene 46 Jg/L 20 WiIliamsJ 6/28/01 8260 Isopropyltoluene para nd pg/L 20 WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 100 10 WilliamsJ 6/28/01 8260 Methyl Isobutyl KetoneMIBK nd .pg/L 100 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pg/L 50 WiIIiamsJ 6/28/01 8260 Methylbutylether tert MTBE nd igIL 20 WilliamsJ 6/28/01 8260 1ethylene chloride nd pgIL 20 WilliarnsJ 6/28/01 8260 .aphthalene 210 pg/L 20 .2 WiIIiamsJ 6/28/01 8260 Propylbenzene normal 26 pg/L 10 WiHiamsJ 6/28/01 8260 Styrene nd pg/L 10 WilliamsJ 6/28/01 8260 Tetrachloroethane 11 nd pg/L 20 WilliamsJ 6/28/0 8260 Tetrachloroethane 1122 nd pg/L 10 WilIiamsJ 6/28/01 8260 Tetrachioroethene nd Jg/L 10 WilliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 100 10 WiIliamsJ 6/28/01 8260 Toluene nd pg/L 10 WilliamsJ 6/28/01 8260 TPH DRO/GRO 5810 pg/L 2000 200 WiIliarnsJ 6/28/01 8260 Trichlorobenzene 123 nd pg/L 10 WilliamsJ 6/28/01 8260 Trichlorobenzene 124 nd pg/L 10 WilliamsJ 6/28/01 8260 Trichloroethane 111 nd pg/L 10 WilliamsJ 6/28/01 8260 Trichloroethne 112 nd ig/L 10 WilliamsJ 6/26/01 8260 Trichioroethene nd pg/L 10 WilliamsJ 6/28/01 8260 Trichiorofluoromethane nd pg/L 20 WilIiamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L 50 WilliamsJ 6/28/01 8260 Trichiorotrifluoroethane nd pg/L 20 .2 WiIliamsJ 6/28/01 8260 Trimethylbenzene 124 200 pg/L 20 WiIHamsJ 6/28/01 8260 Trimethylbenzene 135 54 pg/L 20 WilliamsJ 6/28/01 8260 Vinyl acetate nd pgIL 100 10 WiIIiamsJ 6/28/01 8260 inyl Chloride nd g/L 20 WilliamsJ 6/28/01 8260 .ylene ortho nd pg/L 10 WilliamsJ 6/28/01 8260 Xylenes meta para 3800 Jg/L 20 WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Pagel4of 21 CLIENT SAMPLE ID MW 40 NE 45 CLIENT PROJECT 730 United Drive EIS Sample No 076354 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter ResuIts jUnits 1ibt1 FA Date VOLATILE ORGANICS Acetone nd pg/L 10 10 WilliamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WilliamsJ 6/28/01 8260 Acrylonitrile nd pg/L 20 20 WilliamsJ 6/28/01 8260 Benzene nd pg/L WilIiarnsJ 6/28/01 8260 Bromobenzene nd pg/L WiIliamsJ 6/28/01 8260 Bromochloromethane nd ig/L WilliamsJ 6/28/01 8260 Bromodichioromethane nd pgIL WilliamsJ 6/28/01 8260 Bromoform nd pg/L WilliamsJ 6/28/01 8260 Bromomethane nd pg/L WilliarnsJ 6/28/01 8260 Butylbenzene normal nd pg/L WilliarrisJ 6/28/01 8260 Butylbenzene sec nd pg/L WitliamsJ 6/28/01 8260 Butylbenzene tert nd Jg/L WilIiamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilliamsJ 6/28/01 8260 Carbon Tetrachloride nd pg/L WiIIiamsJ 6/28/01 8260 Chlorobenzene nd pg/L WilliamsJ 6/28/01 826GB hioroethane nd pg/L WilliamsJ 6/28/01 8260 Chloroform nd pg/L WilIiamsJ 6/28/01 8260 Chlorohexane nd pg/L WilliamsJ 6/28/01 8260 Chioromethane nd pg/L 10 10 WilliamsJ 6/28/01 .8260 Chlorotoluene nd vigIL WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Cyclohexanone nd iig/L 100 100 WiIIiamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 nd igIL 30 30 WilliamsJ 6/28/01 8260 Dibromochloromethane nd ig/L WilliamsJ 6/28/01 8260 Dibromoethane 12 nd pg/L WilliamsJ 6/28/01 8260 Dibromomethane nd pg/L WilliamsJ 6/28/01 8260 Dichloro-2-butene 14 nd pg/L 30 30 WiIliamsJ 6/28/01 8260 Dichlorobenzene 12 nd jg/L WilliamsJ 6/28/01 8260 Dichlorobenzene 13 nd pg/L WilliamsJ 6/28/01 8260 Dichlorobenzene 14 nd pg/L WiIIiamsJ 6/28/0 8260 Dichiorodifluoromethane nd pg/L WilliamsJ 6/28/0 8260 Dichloroethane 11 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethane 12 nd jg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene c-i 3.4 pg/L WiIiamsJ 6/28/01 8260 Dichioroethene t-1 nd pg/L WilliamsJ 6/28/01 8260 ichlorofluoromethafle nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 13 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 22 nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005308 SAMPLE RESULTS Pagel5of2l CLIENT SAMPLE ID MW 40 NE 45 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076354 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter its 1U1 ii Date Dichloropropene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioropropene c-i rid pg/L WilliamsJ 6/28/01 8260 Dichloropropene t-i nd pg/L WilIiamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pgIL WilliamsJ 6/28/01 8260 Ethylbenzene nd pgIL WitliamsJ 6/28/01 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachiorobutadiene rid pgIL WilliamsJ 6/28/01 8260 Hexanone 2-nd pg/L 10 10 WillimsJ 6/28/01 8260 lodomethane nd ig/L WilliamsJ 6/28/01 8260 lsopropylbenzerie nd Jg/L WilliamsJ 6/28/01 8260 lsopropyltoluene para rid ig/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl Isobutyl Ketone MIBK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate rid pg/L WilliamsJ 6/28/01 8260 Methylbutylether tert MTBE rid pg/L WilliamsJ 6/28/01 8260 ethyene chloride nd pgIL WilliamsJ 6/28/01 8260 aphthalerie rid pg/L WilliamsJ 6/28/01 8260 .l Propylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Styrene rid pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 rid pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethene 3.3 pg/L WiHiamsJ 6/28/01 8260 Tetrahydrofuran rid pg/L 10 1.0 WilliamsJ 6/28/01 8260 Toluerie nd pg/L WilliamsJ 6/28/01 8260 TPH DRO/GRO nd pg/L 20 200 WilliamsJ 6/28/01 8260 Trichloroberizene123 rid ig/L WilliamsJ 6/28/01 8260B Trichlorobenzene 124 nd pg/L WiiliamsJ 6/28/01 8260 Trichloroethane 111 1.5 pg/L WilliamsJ 6/28/01 8260 Trichloroethane 112 rid pg/L WilliarnsJ 6/28/01 8260 Trichioroethene 36 pg/L WilliamsJ 6/28/01 8260 Tnchlorofluoromethane rid pg/L WilliamsJ 6/28/01 8260 Trichloropropane 123 rid pg/L WilliamsJ 6/28/01 8260 Trichlorotrifluoroetharie rid pg/L WilliamsJ 6/28/01 8260 Trimethylberizene 124 nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 135 nd pg/L WilliamsJ 6/28/01 8260 Vinyl acetate rid pg/L 10 10 WilliamsJ 6/28/01 8260 inyl Chloride nd ig/L WilliamsJ 6/28/01 8260 ylene ortho rid pg/L WilliamsJ 6/28/0 8260 Xylenes meta para rid .ig/L WiltiamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North lronwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Page 16 of 21 CLIENT SAMPLE ID MW 40 NW 25 CLIENT PROJECT 730 United Drive Report Date 7/6/01 EIS Sample No 076355 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Its Date IMethod VOLATILE ORGANICS Acetone nd pg/L 10 10 WiIIiamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WilliamsJ 6/28/01 8260 Acrylonitrile nd pg/L 20 20 WiIIiamsJ 6128/01 8260 Benzene nd pg/L WifliamsJ 6/28/0 8260 Bromobenzene nd pg/L WilliamsJ 6/28/01 8260 Bromochioromethane nd pg/L WiIIiamsJ 6/28/01 8260 Bromodichioromethane nd g/L WiIliamsJ 6/28/01 8260 Bromoform nd pg/L WilIiamsJ 6/28/0 8260 Bromomethane nd ig/L WifliamsJ 6/28/01 8260 Butylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene sec nd Jg/L WiIliamsJ 6/28/01 8260 Butylbenzene tert nd pg/L WiIiamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilliamsJ 6/28/01 8260 Carbon Tetrachioride nd pg/L WilIiamsJ 6/28/01 8260 Chlorobenzene nd pg/L WilIiamsJ 6/28/0.1 8260 Ioroethane nd Jg/L WilliamsJ 6/28/01 8260 Chloroform nd pg/L WilliamsJ 6/28/01 8260 Chlorohexane nd ig/L WilliamsJ 6/28/01 8260 Chioromethane nd pg/L 10 10 WUhiamsJ 6/28/01 8260 Chlorotoluene nd pgIL WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Cyclohexanone nd pg/L 100 100 WiItiamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 nd pg/L 30 30 WiUiamsJ 6/28/01 8260 Dibromochioromethane nd pgIL WilliamsJ 6/28/01 8260 Dibromoethane 12 nd g/L WilIiamsJ 6/28/01 8260 Dibromomethane nd pg/L WilliamsJ 6/28/0 8260 Dichloro-2-butene 14 nd pg/L 30 30 WilliamsJ 6/28/01 8260 Dichlorobenzene 12 nd pg/L WilIiamsJ 6/28/01 8260 Dichlorobenzene 13 nd pgIL WilhiamsJ 6/28/01 8260 Dichlorobenzene 14 nd pg/L WilliamsJ 6/28/01 8260 Dichlorodifluoromethane nd pgIL WiIIiamsJ 6/28/01 8260B Dichloroethane 11 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WilIiamsJ 6/28/01 8260 Dichloroethene 11 nd .ig/L WilliamsJ 6/28/01 8260 Dichioroethene c-i pg/L WilliamsJ 6/28/01 8260 Dichioroethene t-1 nd pg/L WiIliamsJ 6/28/01 8260 ichIorofIuoromethane nd pg/L WilIiamsJ 6/28/01 8260 Jichloropropane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 13 nd .ig/L WilliamsJ 6/28/01 8260 Dichloropropane 22 nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Page 17 of 21 CLIENT SAMPLE ID MW 40 NW 25 Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076355 SAMPLE TYPE WaterNon OW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 i-1 Pmeter liResuitsi isTj Date _________ Dichloropropene 11 nd pg/L WilIiamsJ 6I28/01 8260 Dichloropropene c-13 nd Jg/L WilliamsJ 6/28/01 8260 Dichioropropene t-1 nd pg/L WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd lJg/L WilliamsJ 6/28/01 8260 Ethylbenzene nd pg/L WilliamsJ 6/28/01 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachlorobutadiene nd pg/L WilliamsJ 6/28/01 8260 Hexanone 2-nd ig/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd ig/L WilliamsJ 6/28/01 8260 lsopropylbenzene nd pg/L WilliamsJ 6/28/01 8260 Isopropyltoluene para nd pg/L WilliamŁJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliarnsJ 6/28/01 8260 Methyl lsobutyl Ketone MIBK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pg/L WilliamsJ 6/28/01 8260 Methylbutylether tert MTBE nd pg/L WilliamsJ 6/28/0 8260 ethylene chloride nd pg/L WilliamsJ 6/28/0 8260 i4aphthalene nd pg/L WilliamsJ 6/28/01 8260 Propylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Styrene nd pg/L WillimsJ 6/28/0 8260 Tetrachloroethane 1112 nd Jg/L WilliarnsJ 6/28/01 8260 Tetrachloroethane 1122 nd pg/L WilliamsJ 6/28/01 8260 Tetrachioroethene 2.4 pg/L WilliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 10 10 WiIliamsJ 6/28/01 8260 Toluene pg/L WilliamsJ 6/28/0 8260 TPH DRO/GRO nd pg/L 200 200 WilliamsJ 6/28/01 8260 Trichlorobenzene 123 nd pg/L WilliamsJ 6/28/0 8260 Trichlorobenzene 124 nd pg/L WilliamsJ 6/28/0 8260 Trichloroethane 111 nd pg/L WilliarnsJ 6/28101 8260 Trichloroethane 112 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethene 11 pg/L WilliamsJ 6/28/01 8260 Trichlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L WilliamsJ 6/28/01 8260 Trichlorotrifluoroethane nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 124 nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 135 nd .ig/L WilliamsJ 6/28/01 8260 Vinyl acetate nd pg/L 10 10 WilliamsJ 6/28/01 8260 inyl Chloride nd pg/L WilliamsJ 6/28/0 8260 ylene ortho nd pg/L WilliamsJ 6/28/0 8260 Xylenes meta para nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax SAMPLE RESULTS Page 18 of 21 CLIENTSAMPLEID MW4O NW35 CLIENT PROJECT 730 United Drive Report Date 7/6/01 EIS Sample No 076356 3AMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25101 Date Received 6/25/01 Test Parameter jults lUnits LAii Date Method VOLATILE ORGANICS Acetone nd pg/L 10 10 WilliamsJ 6/28/01 8260 Acrolein nd 4Jg/L 20 20 WifliamsJ 6/28/01 8260 Acrylonitrile nd pg/L 20 20 WiIliamsJ 6/28/01 8260 Benzene nd pg/L WilliamsJ 6/28/0 8260 Bromobenzene nd pg/L WiIIiamsJ 6/28/01 8260 Bromochioromethane nd pg/L WilliamsJ 6/28/01 8260 Bromodichioromethane nd pg/L WilliamsJ 6/28/0 8260 Brornoform nd pg/L WilIiamsJ 6/28/01 8260 Brornomethane nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene normal nd pg/L WiIIiamsJ 6/28/01 8260 Butylbenzene sec nd pg/L WiIliamsJ 6/28/01 8260 Butylbenzene tert nd pg/L WilliamsJ 6/28/01 8260 Carbon disulfide 3.2 pg/L WilIiamsJ 6/28/01 8260 Carbon Tetrachioride nd pg/L WilliamsJ 6/28/01 8260 Chlorobenzene nd vigIL WiIllamsJ 6/28/01 8260 loroethane nd pg/L WilliamsJ 6/28/0 860 Chloroform nd .ig/L WilIiamsJ 6/28/01 8260 Chlorohexane nd pgIL WilliamsJ 6/28/01 8260 Chloromethane nd pgIL 10 10 WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Cyclohexanone nd pg/L 100 100 WilliamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 nd pgIL 30 30 WilliamsJ 6/28/01 8260 Dibromochioromethane nd ig/L WitliamsJ 6/28/01 8260 Dibromoethane 12 nd pg/L WitliamsJ 6/28/01 8260 Dibroniomethane ..nd ig/L WilliamsJ 6/28/01 8260 Dichloro-2-butene 14 nd jg/L 30 30 WilliamsJ 6/28/01 8260 Dichlorobenzene 12 nd JgIL WiIliamsJ 6/28/0 8260 Dichlorobenzene 13 nd pgIL WilliamsJ 6/28/01 8260 Dichlorobenzene 14 nd pg/L WilliamsJ 6/28/0 8260 Dichlorodifluoromethane nd ig/L WilliamsJ 6/28/01 8260 Dichloroethane 11 1.1 ig/L WilliamsJ 6/28/01 8260 Dichloroethane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene c-12 2.2 jg/L WilliamsJ 6/28/01 8260 Dichloroethene t-12 nd lJg/L WilliamsJ 6/28/01 8260 Nchlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 Jichloropropane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 13 nd gIL WilliamsJ 6/28/01 8260 Dichloropropane 22 nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005312 SAMPLE RESULTS Page 19 of 21 CLIENT SAMPLE ID MW 40 NW 35 Report Date 7/6/0 CLIENT PROJECT 730 United Drive EIS Sample No 076356 SAMPLE TYPE WaterNon OW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Parameter fResults 1Units ________ Date Method Dichloropropene 11 nd pg/L WiIIiamsJ 6/28/01 8260 Dichloropropene c-13 nd ig/L WiIIiamsJ 6/28/01 8260 Dichloropropene t-13 nd pg/L WilliamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pg/L WilliamsJ 6/28/0 8260 Ethylbenzene nd pg/L WilIiarnsJ 6/28/01 8260 Heptane normal nd ig/L WiIliamsJ 6/28/01 8260 Hexachlorobutadiene nd pg/L WilliamsJ 6/28/01 8260 Hexanone 2-nd jig/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd pg/L WilliamsJ 6/28/01 8260 lsopropytbenzene nd ig/L WilliamsJ 6/28/01 8260 lsopropyJtoluene para nd pg/L WilliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl Isobutyl Ketone MIBK nd pg/L 10 10 WiUiamsJ 6/28/01 8260 Methylmethacrylate nd pg/L WilliamsJ 6/28/01 8260 Methylbutytether tert MTBE nd pg/L WilliamsJ 6/28/01 8260 lethylene chloride nd pgIL WilliamsJ 6/28/01 8260 aphthalene nd pg/L WilliamsJ 6/28/0 8260 Propylbenzene normal nd Jg/L WilliamsJ 6/28/01 8260 Styrene nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WitIiamsJ 6/28/01 8260 Tetrachloroethane 1122 pg/L WilliamsJ 6/28/01 8260 Tetrachloroethene 2.9 pg/L WilliamsJ 6/28/01 8260 Tetrahydrofuran nd pg/L 10 10 WilIiamsJ 6/28/01 8260 Toluene nd pg/L WiliiamsJ 6/28/0 8260 TPH DRO/GRO 390 jg/L 200 200 WiIIiamsJ 6/28/01 8260 Trichlorobenzene 123 nd pg/L WilliamsJ 6/28/01 8260 Trichlorobenzene 124 nd pg/L WilliamsJ 6/28/0 8260 Trichloroethane 111 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethane 112 nd pg/L WilliarnsJ 6/28/01 8260 Trichloroethene llg/L WilliamsJ 6/28/01 8260 Trichiorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L WilliamsJ 6/28/01 8260 Trichiorotrifluoroethane nd lJg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 124 nd pg/L WiIliamsJ 6/28/0 8260 Trimethylbenzene 135 nd pg/L WilliarnsJ 6/28/01 8260 Vinyl acetate nd pg/L 10 10 WilliamsJ 6/28/01 8260 inyl ChlorideS nd pg/L WilliamsJ 6/28/01 8260 ylene ortho nd pg/L WilliamsJ 6/28/01 8260 Xylenes meta para nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005313 SAMPLE RESULTS Page 20 of 21 CLIENT SAMPLE ID Trip Blank Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076357 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/0 Date Received 6/25/01 Test _i Parameter Results iJnits RDL ibL Date Method VOLATILE ORGANICS Acetone nd jg/L 10 10 WilliamsJ 6/28/01 8260 Acrolein nd pg/L 20 20 WilliamsJ 6/28/01 8260 AcrylontriIe nd pg/L 20 20 WiltiamsJ 6/28/0 8260 Benzene nd pg/L WiIliarnsJ 6/28/01 8260 Bromobenzene nd pgIL WiIliamsJ 6/28/01 8260 Bromochioromethane rid jg/L WHhamsJ 6/28/01 8260 Bromodichloromethane rid pg/L WilliamsJ 6/28/0 8260 Bromoform nd pg/L WilliamsJ 6/28/01 8260 Bromornethane nd .ig/L WilliamsJ 6/28/01 8260 Butylbenzene normal nd pg/L WilliamsJ 6/28/01 8260 Butylbenzene sec nd pg/L .WilIiamsJ 6/28/01 8260 Butylbenzene tert nd pg/L WiHiamsJ 6/28/01 8260 Carbon disulfide nd pg/L WilliamsJ 6/28/01 8260 Carbon Tetrachlonde nd pg/L WilliamsJ 6/28/01 8260 Chlorobenzene nd pg/L WilliamsJ 6/28/0.1 8260 iloroethane nd pg/L WilliarnsJ 6/28/01 8260 Chloroform nd pg/L WflhiamsJ 6/28/01 8260 Chlorohexane nd pg/L .2 WilliamsJ 6/28/01 8260 Chioromethane nd pg/L .10 10 WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Chlorotoluene nd pg/L WilliamsJ 6/28/01 8260 Cyclohexanone rid pg/L 100 100 .WilliamsJ 6/28/01 8260 Dibromo-3-chloropropane 12 nd igfL 30 30 WilliamsJ 6/28101 8260 Dibromochloromethane rid .igIL WilliamsJ 6/28/01 8260.B Dibromoethane 12 nd pg/L WiHiarnsJ 6/28/01 8260 Dibromomethane nd pg/L WilliarnsJ 6/28/01 8260 Dichloro-2-butene 14 nd pg/L 30 30 WilliamsJ 6/28/01 8260 Dichlorobenzene 12 nd pg/L tlliamsJ 6/28/01 8260 Dichlorobenzene 13 nd pg/L WilliamsJ 6/28/0.1 8260 Dichlorobenzene 14 nd pg/L .2 WilliamsJ 6/28/01 8260 Dichiorodifluoromethane nd ig/L WilliamsJ 6/28/01 8260 Dichloroethane 11 nd pg/L WilliamsJ 6/28/01 8260 Dichioroethane 12 nd pg/L WilliamsJ 6/28/01 8260 Dichloroethene 11 nd Jg/L WilliamsJ 6/28/01 8260 Dichloroethene c-i nd pg/L WilliamsJ 6/28/01 8260 Dichioroethene t-12 nd pg/L WillianisJ 6/28/01 8260 ichIorofIuoromethane nd pg/L WillianisJ 6/28/01 8260 Jichloropropane 12 nd ig/L WilliamsJ 6/28/01 8260 Dichloropropane 13 nd pg/L WilliamsJ 6/28/01 8260 Dichloropropane 22 nd pg/L WilliamsJ 6/28/01 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005314 SAMPLE RESULTS Page 21 of 21 CLIENT SAMPLE ID Trip Blank Report Date 7/6/01 CLIENT PROJECT 730 United Drive EIS Sample No 076357 SAMPLE TYPE WaterNon DW EIS Order No 010600230 Date Collected 6/25/01 Date Received 6/25/01 Test Paraee .j Results 11 A1iF Date Dichloropropene 11 nd pg/L WilliamsJ 6/28/01 8260 Dichlropropene c-i nd pg/L WilliamsJ 6/28/01 8260 Dichioropropene t-1 nd pg/L WilHamsJ 6/28/01 8260 Diethyl ether nd pg/L 10 10 WilliamsJ 6/28/01 8260 Ethyl methacrylate nd pg/L WilliamsJ 6/28/01 8260 Ethylbenzene nd pg/L WilhamsJ 6/28/01 8260 Heptane normal nd pg/L WilliamsJ 6/28/01 8260 Hexachlorobutadiene pg/L WilIiarnsJ 6/28/01 8260 Hexanone 2-nd ig/L 10 10 WilliamsJ 6/28/01 8260 lodomethane nd pg/L WilliamsJ 6/28/01 8260 Isopropylbenzene nd jg/L WiIliamsJ 6/28/01 8260 lsopropyltoluene para nd pg/L WiIliamsJ 6/28/01 8260 Methyl Ethyl Ketone MEK nd pg/L 10 10 WilliamsJ 6/28/01 .8260 Methyl Isobutyl Ketone MIBK pg/L 10 10 WilliamsJ 6/28/01 8260 Methyl methacrylate nd pg/L WilliamsJ 6/28/0 8260 Methylbutylether tert MTBE nd pg/L WilliamsJ 6/28/01 8260 ethylene chloride nd pg/L WilliamsJ 6/28/0 8260 1aphthalene nd pg/L WilliamsJ 6/28/01 8260 Propylbenzene normal nd ig/L WilliamsJ 6/28/01 8260 Styrene nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1112 nd pg/L WilliamsJ 6/28/01 8260 Tetrachloroethane 1122 nd pgIL WilliamsJ 6/28/01 8260 Tetrachioroethene nd ig/L WilliamsJ 6/28/01 8260 Tetrahydrofuran nd ig/L 10 .10 WilliamsJ 6/28/01 8260 Toluene nd pg/L WilliarnsJ 6/28/0 8260 TPH bRO/GRO nd pg/L 200 200 WilliamsJ 6/28/01 8260 Trichlorobenzene 123 nd pgIL .1 WilliamsJ 6/28/01 8260 Trichlorobenzene 124 nd pg/L WilliamsJ 6/28/01 8260 Trichloroethane 111 nd pgIL WilliamsJ 6/28/01 8260 Trichloroethane 112 nd pgIL WilliamsJ 6/28/01 .8260 Trichioroethene nd pg/L WilliamsJ 6/28/01 8260 Trichlorofluoromethane nd pg/L WilliamsJ 6/28/01 8260 Trichloropropane 123 nd pg/L WilliamsJ 6/28/01 8260 Trichiorotrifluoroethane nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 124 nd pg/L WilliamsJ 6/28/01 8260 Trimethylbenzene 135 pgIL WilliamsJ 6/28/01 8260 Vinyl acetate nd ig/L 10 10 WilliamsJ 6/28/01 8260 Vinyl Chloride nd pg/L WilliamsJ 6/28/01 8260 ylene ortho nd pg/L WilliamsJ 6/28/01 8260 Xylenes meta para nd pg/L WilliamsJ 6/28/0 8260 EIS Analytical Services Inc 1701 North Ironwood Drive Suite South Bend IN 46635 219-277-0707 Fax 219-273-5699FORD005315 QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010600230 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCAA 615/8151A/515.1 8151A 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608 8081A 8082 508 8082 22 135 40-150 Pesticides PCB DecachlorobiphenylDCB 608 8081A 508 8082 22-135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625/8270C 8270C 21-100 25-121 SVOC acid Phenol d5 625 8270C 8270C 10-94 24 113 SVOC base/neutral Nitrobenzene d5 625 8270C 8270C 35 114 23 -120 SVOC base/neutral 2-Fluorobiphenyl 625 8270C 8270C 43 116 30 115 SVOC acid 246-Tribromophenol 625 8270C 8270C 10 123 19-122 SVOC base/neutral Terphenyl d14 625 8270C 8270C 33-141 18-137 TPH Styrene 8015M 8015M 30 70 34-66 VOC/BETX/TPH 12-Dichloroethaned4 624/8260B/524.2 8260B 76-114 70-121 VOC BETX TPH Toluene d8 624 8260B 524.2 826GB 86-115 74-121 VOC BETX TPH BromofluorobenzeneBFB 624 8260B 524.2 826GB 86-115 74-121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 076348 MW 50 Sw 25 8260 WaterNon DW 2-DichloroethanŁ-d4 SS 91 8260 WaterNon DW 4-Bromofluorobenzene SS 106 8260 WaterNon DW Toluene-d8 SS 101 076349 MW 50 SW 35 8260 WaterNon DW 2-Dichloroethane-d4 SS 95 8260 WaterNon DW 4-Bromofluorobenzene SS 106 8260 WaterNon OW Toluene-d8 SS 101 076350 MW 56 25 8260 WaterNon DW 2-Dichloroethane-d4 SS 98 8260 WaterNon OW 4-Bromofluorobenzene SS 103 8260 WaterNon DW Toluene-d8 SS 100 076351 MW 56 35 8260 WaterNon DW 2-Dichloroethane-d4 SS 94 8260 WaterNon DW 4-Brornofluorobenzene SS 111 WaterNon OW Toluene-d8 58 99 076352 MW 40 NE 25 8260 WaterNon OW 2-Dichloroethane-d4 SS 96 8260 WaterNon OW 4-Bromofiuorobenzene SS 104 8260 WaterNon DW Toluene-d8 SS 105 076353 MW 40 NE 35 8260 WaterNon OW 2-Dichloroethane-d4 SS 99 8260 WaterNon DW 4-Bromofluorobenzene SS 105 8260 WaterNon OW Toluene-d8 SS 101 076354 MW 40 NE 45 8260 WaterNon DW 2-Oichloroethane-d4 SS 99 8260 WaterNon DW 4-Bromofluorobenzene SS 102 8260 WaterNon DW Toluene-d8 SS 103 076355 MW4O NW25 8260 WaterNon DW 12-Oichloroethane-d4 SS 93 8260 WaterNon DW 4-Bromofluorobenzene SS 102 8260 WaterNon OW Toluene-d8 SS 99 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Pagelof QUALITY ASSURANCE QUALITY CONTROL DATA Method Specific Surrogate Compound Recoveries EIS Order ID 010600230 QUALITY CONTROL LIMITS Methods QC Limits Normal Test Surrogate Water Soil Water Soil Herbicides 24-DichlorophenylaceticacidDCAA 615/8151A/515.1 8151A 15-135 Pesticides PCB 2456-Tetrachloro-m-xyleneTCMX 608 8081A 8082 508 8082 22-135 40-150 Pesticides PCB DecachlorobiphenylDCB 608 8081A 508 8082 22 135 40-150 SOC svoc Perylene d12 525.2 70-130 SVOC acid 2-Fluorophenol 625 827CC 827CC 21 100 25 121 SVOC acid Phenol d5 625 827CC 827CC 10-94 24-113 SVOC base/neutral Nitrobenzene d5 625 8270C 827CC 35 114 23 120 SVOC base/neutral 2-Fluorobiphenyl 625 827CC 827CC 43 116 30 115 SVOC acid 246-Tribromophenol 625 827CC 8270C 10-123 19-122 SVOC base/neutral Terphenyl d14 625 827CC 827CC 33 141 18 137 TPH Styrene 8015M 8015M 30-70 34-66 VOC BETX TPH 2-Dichloroethane d4 624 82608 524.2 8260B 76-114 70 121 VOC/BETX/TPH Toluened8 624/8260B/524.2 82608 86-115 74-121 VOC BETX TPH BromofluorobenzeneBFB 624 82608 524.2 82608 86 115 74 121 EIS Lab No Client Sample ID Method Matrix Surrogate %Recovery 076356 MW 40 NW 35 8260 WaterNon DW 2-Dichloroethane-d4 SS 94 8260 WaterNon DW 4-Bromofluorobenzene SS 102 8260 WaterNon DW Toluene-d8 SS 101 076357 Trip Blank 82608 WaterNon DW 12-Dichloroethane-d4 SS 94 8260 HVaterNonDW 4Bromofluoroberizene SS 103 8260 WaterNon DW ToluØne-d8 SS 103 Legend -1 Surrogates diluted out -2 Surrogates not used methods with different QC Limits Page2ot QUALITY CONTROL DATA MATRIX SPIKE DUPLICATE MATRIX SPIKE MS/DMS EIS Order 010600230 EIS Lab in This Batch Comments Concerning This QC Batch QC Sample 076354 076348 076357 None Matrix Groundwater Test VOC Quality Control Limits Back-Spike Matrix_Spike Duplicate Spike RPD Parameter ground Amount Result Result RPD LCL UCL LCL UCL QC Batch Benzene nd 42 43 102 43 102 --11 76 --127 QB00650 Chlorobenzene nd 46 45 98 43 93 --13 75 --130 Q800650 Dichloroethene 11 nd 44 53 120 50 114 --14 61 --145 QB00650 Toluene nd 42 40 95 41 98 --13 76 --125 QB00650 iiiioroethene 36 41 78 102 77 100 71 --120 QB00 LEGEND Background Sample Result amount may be adjusted for dilution used in sample analysis Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Background and Spike QUALITY CONTROL DATA LABORATORY FORTIFIED METHOD BLANK LFB Matrix Lab Water EIS Lab With This LFB Comments Concerning This LFB Test VOC 076348 076357 None Prep Date See Sample Analysis Date Run Date See Sample Analysis Date Quality Control Limits Spike Matrix Spike Duplicate Spike RPO Parameter Amount Result Result RPD LCL UCL LCL IJCL QC Batch Benzene 4.9 4.7 96 76 127 QB00650 Chlorobenzerie 5.2 4.8 92 75 --130 QB00650 Dichloroethene11 5.3 5.4 102 61 --145 QBo065o Toluene 4.5 4.3 96 76 --125 QB00650 Tricoethene 4.5 4.5 100 71 --120 QB00650 LEGEND The LFB may be either single spike or in dulicate and may or may not be in QC Batch with MS/DMS Percent Recovery of Spike RPD Relative Percent Difference of the spike recoveries LCL Lower Control Limit UCL Upper Control Limit Units are normally those shown in the Analysis Report and are always the same for the Spike and Duplicate Spike CHAIN OF CUSTODY RECORD PROJ NO PROJECT NAME 13o Unec OvVe Total _______________________________________________No _______________SAMPLERS Print Name Sign FIELD tainers of __________________________________ Con Lab ID DATE TIME STATION LOCATION _______ ______________________________________________Type TAT Number___________PB _______________ __________________ O5W.26 oJZ/oi 3O SL 2-5 iJoc 23/S 6o6W6Oz5 o4O Mw 60 f5 _____73g__Oo_MW ______ o6 102-0 MW6 36 ___7C3$7___4o 4AAU3LOAZ5 11111 7C35a z6 4tj ______7C353 ____ _____________7353 _____L1O __________J2 _______________________7.357 Relinquished By Signature Date Time By EIS QUOTE NO $ignature Ship ToshedrSiqatureiDateTime Date Time Reivedy Signature1sSTature NOTES If you were issued quote number it must appear on this document Instructions area for comments are on reverse side EIS ANALYTICAL SERVICES INC 1701 NORTH IRONWOOD DRIVE SUITE .SOUTH BEND IN 46635 Phone 2192770707 Fax 219273 Form ChainofCustody 61297 Form Completion Instructions Each slanted line represents specific container types from which specific tests are conducted Use additional record sheets if of samples or of tests exceed allotted spaces List tests per container type on the slanted lines give of containers in boxes below tests Sum all containers and place in column lbeIed Total No Containers For the column labeled Sample Type give brief description such as soil MW oil etc For column labeled TAT use one of the following Reuest MeanirigL Normal 24 weeks for written report based entirely on test complexity and number of samples week In general prior authorization is required from the lab to request day turnaround time urcharges may or may not be applicable depending entirely on test complexity days MUshavØ been authorized by the Lab and increased costs must have been authorizI by the client day Must have been authorized by the Lab and increased costs must have been authorized by the client Submission Comments EIS TICAL SERVICES INC 1701 NORTH IRONW000 DRIVE .SOUTH BEND IN 46635 Phone 2192770707 Fax 21 Form CL or--Custody 12--97 DRAFT Al11 Proposed Groundwater Sampling Location accessible properties Proposed Groundwater Sampling Location right-of-way access Existing Groundwater Sampling Location Downgradient Properties Having CityAccess Proposed DirectPush 500 500 1000 Water Sampling Locations Feet for Plume Delineation DRAFT a_ -.-..- aij V- i__ .. .v a1 -l ..--Ii I- Proposed Groundwater Sampling Location accessible properties Proposed Groundwater Sampling Location iight-of-way access Existing Groundwater Downg radiant Properties Having CityAccess Proposed Direct-Push 500 500 1000 Water Sampling Locations Ft forPlume Delineation