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HomeMy WebLinkAboutSB-0206 1995 Phase II Soil boring Avanti SiteATEC vi FINAL REPORT Phase II Subsurface Investigation Former Avanti Property Northwest Corner of Lafayette and Sample St South Bend Indiana ATEC Project No 1-07-95-00802 Prepared For City of South Bend 1400 County-City Building South Bend Indiana Attn Ms Ann Kolata October 19 1995 ATEC Associates Inc Environmental Consultants 5150 East 65th Street Solid Hazardous Waste Site Assessments Indianapolis Indiana 46220-4871 Remedial Design Construction 317 849-4990 FAX 317 849 5260 Underground Tank Management Asbestos Surveys Analysis Hydrogeologic tnvestigati000 Monitoring Anatytical Testing Chemistry Industrial Hygiene Hazard Communication October 19 1995 Esoironmentat Audits Permitting Eoploratory Drilling Monitoring Welts Ms Ann Kolata City of South Bend 1400 County-City Building South Bend Indiana 46601 Re FINAL REPORT Phase II Subsurface Investigation Former Avanti Property NWC of Lafayette and Sample St South Bend Indiana ATEC Project No 21-07-95-00802 Dear Ms Ann Kolata ATEC Associates Inc ATEC is pleased to present the City of South Bend th this report documenting the subsurface investigation performed at the above referenced site The purpose of the study was to determine if subsurface soils have been impacted at the project site property The attached report summarizes the activities perfonned by ATEC to accomplish this objective We appreciate the opportunity to conduct this investigation and trust this report is responsive to your needs Please do not hesitate to contact the undersigned if you have any comments or questions concerning this study Sincerely ATEC ASSOCIATES INC Brad Lewis Matthew Stokes C.H.M.M Staff Environmental Scientist Senior Project Manager cc Anne Slaughter Andrew American Testing and Engineering Corporation Consulting Environ and Offices in Major U.S Cities/Since 1958 Materials Engineers TABLE OF CONTENTS 1.0 INTRODUCTION .1 2.0 FIELD ACTIVITIES 2.1 GEOPROBE SOIL SAMPLING 2.2 SECOND ROUND SOIL SAMPLING 3.0 FINDINGS 3.1 GEOLOGY 3.2 SOIL SCREENING 3.3 SOIL ANALYTICAL RESULTS 3.4 METHYLENE CHLORIDE AND TOLUENE RESULTS 4.0 CONCLUSIONS AND RECOMMENDATIONS 5.0 QUALIFICATIONS APPENDICES Appendix Field Screening Equipment Appendix Boring Logs Appendix Analytical Results PHASE 11 SUBSURFACE INVESTIGATION Former Avanti Property NWC of Lafayette and Sample St South Bend Indiana ATEC Project No 21-07-95-00802 1.0 INTRODUCTION ATEC Associates Inc ATEC was retained by the City of South Bend Indiana to perform Phase II subsurface investigation on the Former Avanti Property the project site located on the northwest corner of Lafayette and Sample Street see Figure The scope of this investigation was developed based on conversations with the client and areas of concern identified in ATECs Phase Environmental Site Assessment Borings were located to near areas of former USTs drum storage subgrade oil pits and soil staining noted during the Phase Environmental Site Assessment Sample locations B-l through B-6 were located at the east end of the former Avanti Building Room 108 This room contained several subgrade oil sumps Room 108 was also used for painting and automotive repair Sample locations B-9 through B-12 were located at the west end of the former Avanti Building This area was once used for drum storage In addition two underground storage tanks were previously located in this area Sample locations B-7 and B-8 were located within the center portion of the former building to provide complete sampling scheme across the site The scope of this Phase II subsurface investigation included advancing total of twelve GeoProbe borings The following report details the field activities laboratory results and ATECs findings relative to the project All documents concerning the investigation can be found in the appendices .- Ipe 12 12 I. ____J _L .7 II Ir-4 -- -- 13 jH _79_J ---- 91 .f 21-07-95-00802 AThC VICINITY MAP ___________ PHASE II SUBSURFACE INVESTIGATION 10-3-95FORMERAVANTIPROPERTY NORTHWEST CORNER of LAFAYETTE ST and SAMPLE ST 2000 1995 SOUTH BEND INDIANA 2.0 FIELD ACTIVITIES On September 18 and 19 1995 ATEC personnel Mr Knoel Kaneshiro ATEC Field Geologist mobilized to the project site ATEC met Mike Walker ATEC Driller to discuss boring locations and locations of utilities Prior to the start of field activities the boring locations were located and the Site Safety Plan was reviewed Figure shows the project site and relative boring locations 2.1 GeoProbe Soil Sampling On September 18 and 19 1995 ATEC personnel mobilized to the project site to collect total of 12 soil samples from 12 boring locations across the project site One soil sample from each boring for total of 12 soil samples were collected GeoProbe boring samples were designated B-l through B-l2 Borings were advanced to depth 20 ft below grade The borings were completed using GEO Scorpion van-mounted drill rig GeoProbe boring locations are shown on Figure Kansas Sampler consisting of ft in length by 2-inch diameter stainless steel rod was hydraulically driven into the subsurface soils Soil samples were collected at two foot intervals from the surface down to the bottom of each boring Between each boring the sampling equipment was decontaminated using non-phosphate detergent wash followed by tap water rinse Upon completion each bore hole was filled to the surface with non-shrink bentomte Soils from each interval were visually inspected by an ATEC scientist and classified using the Unified Soil Classification System USCS Each soil sample was placed in sealed plastic bag and later screened for the presence of hydrocarbon vapors using an H-Nu photo-ionization detector PID The PID measures total photo-ionizable vapors TPVs in the parts per million ppm range The screening procedure is outlined in Appendix complete description of the geologic materials encountered and the TPV responses are included on the boring logs in Appendix Based on field observations and TPV readings ---- MW-2 MW-1R MW-3R B9 Bi 82 B31 83 810 B-8-1 ii FORMER AVANT PROPERTY PROJECT SITE ii 812 S6 B-5 MW-4 LEGEND MONITORING WELLMW---_Wi ldentifsotisn APPROX LOCATION OF MISSING WELL SOIL BORING PROPERTY BOUNDARY 43IIMWIRMW3RREPLACEMENTWELLS 50 75 100 SCALE 100 ______21079500802 AlEC D..1g F10BORINGPLAN008028P PHASE II SUBSURFACE INVESTIGATION 101095FORMERAVANTPROPERTY NORTHWEST CORNER of LAFAYETTE ST and SAMPLE ST ___ 00 9iSOUTHBENDINDIANASIj 8KL one soil sample from each of twelve borings B-I through B-12 were collected Twelve soil samples were submitted to the ATEC laboratory for Volatile Organic Compound VOC analysis All soil samples were transported to ATECs laboratory in Indianapolis Indiana using proper quality assurance/quality control QAIQC procedures and all appropriate chain-of-custody protocols The soil samples were submitted to the ATEC laboratory for one week turn-around for verbal results 2.2 Second Round Soil Sampling Based on the results of the first round of sampling showing low levels of toluene as possible artifact ATEC remobilized to the project site to redrill three of the twelve borings to verif or discount earlier findings The three additional soil boring locations labeled B- 3-I B-8-l and B-I 1-1 corresponded to the original soil boring locations B-3 B-8 and B- 11 and are shown in Figure Soil sample collection classification and visual screening were perfonned using the same methodology described above Three soil samples were collected and submitted to the laboratory for analytical testing for toluene The three soil samples submitted to the laboratory for analysis were collected from the same depths as the original samples collected from each of the corresponding boring locations iI LI 3.0 FINDINGS 3.1 Geology Visual inspection of soil samples from borings B-i through B-i2 revealed the presence of fill material to depth of 2.0 to 3.5 ft below grade Below the fill material in these borings is moist brown silty sand In borings B-6 and B-9 four inch clay seam was encountered within the silty sand unit No groundwater was encountered in the borings Slight black staining was noted in two of the twelve borings two inch black seam was noted at approximately Ii feet below grade in boring B-I and one foot black seam was encountered in boring B-2 from to feet below grade 3.2 Soil Screening All soil samples collected during the investigation were screened for emission of TPVs using an TVA 1000 PID Due to the high ionization potentials for many chiorinated solvents the TVA 1000 PID was equipped with 11.6 eV lamp to better detect these constituents The screening results for soil samples from borings B-4 B-S and B-6 were all non-detect Field screening of soil samples from soil borings B-l B-2 B-3 B-iO B-il and B-l2 revealed low TPV readings throughout the borings Field screening results from B-7 B-8 and B-9 revealed slightly more elevated readings around 40 ppm throughout each of these borings The screening results for all soil samples from all twelve geoprobe borings can be found on the boring logs in Appendix 3.3 Soil Analytical Results Soil samples collected from B-I through B-12 were submitted to the ATEC laboratory for VOC testing The VOC analysis were performed on Finnigan Incos 50 GC/MS/DS system complete with Superincos Software via SW 846 Method 8240 for Purgeable Organic Compounds Note three soil samples from borings B-3-l B-8-l and B-I 1-I were collected and submitted for toluene testing The toluene analysis was performed according to the same methodology described above Analytical results from the soil samples from borings B-I through B-12 did not reveal any concentrations of VOCs other than methylene chloride and toluene Methylene chloride and toluene results are discussed in detail in Section 3.4 of this report Analytical results of the three soil samples from borings B-3-I B-8-l and B-I I-I did not reveal any concentration of toluene Table summarizes the VOC analytical results and their respective depths Table Soil Analysis Volatile Organic Compounds VOCs Former Avanti Property NWC of Lafayette and Sample Street South Bend Indiana AlEC Project No 21-07-95-00802 ____________ Sample ID Depth of Sample ft VOCs ppb Methylene Chloride ppb Toluene ppb B-I 10-12 ND ND B-2 2-3 ND 13 B-3 18-20 ND 110 8-4 18-20 ND ________ ________87 B-S 18-20 ND 29 B-6 18-20 ND 120 B-7 18-20 ND ________ ________21 B-8 18-20 ND 140 B-9 18-20 ND ____________________30 B-b 18-20 ND _________71 B-Il 10-12 ND ________ ________130 B-12 18-20 ND _________ _________92 B-3-l 18-20 NA NA ND B-8-I 18-20 NA NA ND B-Il-I 10-12 NA NA ND ND None detected above method quantitation limits NA Not analyzed Methylene chloride and toluene detected in samples Notes Methylene chloride was identified as laboratory artifact Toluene is believed to be an artifact however the source of toluene as an artifct is not Methylene Chloride and Toluene Results Analytical results from the initial round of soil sampling revealed methylene chloride and toluerie in all the samples except for the lack of toluene in Sample B-I Methylene chloride and toluene are commonly considered as laboratoiy artifact and the presence of these constituents at these concentrations are not considered attributable to the activities at the site cr adjacent properties Methylene chloride and toluene are used in various laboratory analyses and are considered laboratory artifacts Although extraction and preparation processes are all performed by trained personnel in separate rooms under vented hoods some vapors escape and are released into the laboratory atmosphere Given the extreme sensitivity of the analytical instrumentation these compounds are often detected at low levels in environmental samples The U.S EPA document Laboratory Data Validation Functional Guidelines for Evaluating Organics Analysis allows for up to ten times the concentration found in the method blank to be reported as laboratory artifact The method blank for this analysis revealed concentration of up to 12 ppb of methylene chloride thus analytical results below 120 ppb should be considered laboratory artifacts Concentrations of toluene were not identified in the method blanks for these sample results Therefore toluene concentrations in these samples could not be confirmed as the result of laboratory procedures Introduction of toluene may be the result of contaminated sample jars or other sources such as permanent marking pens or glues from tape or labels The source of toluene introduced into the samples is therefore unknown Although the source of the toluene from the initial sampling could not be determined additional soil samples B-3-l B-8-1 and B-l 1-I collected from the similar boring locations and similar depths did not reveal the presence of toluene Based on these confirming data ATEC concludes the toluene concentrations from the initial soil samples was inadvertently introduced into the samples and is not considered attributable to on-site subsurface soil conditions 4.0 CONCLUSIONS AND RECOMMENDATIONS The purpose of this investigation was to determine if the subsurface soils had been impacted by former on-site activities Based on field observations and analytical results ATEC concludes that the upper 20 ft of subsurface soils from borings B-i through B-i2 have not been impacted with volatile organic compounds Based on the findings of this study ATEC recommends no further investigation with regard to the top 20 ft of unsaturated above groundwater soils 5.0 QUALIFICATIONS Our professional services have been performed our findings obtained and our recommendations prepared in accordance with customary principles and practices in the fields of environmental science and engineering This warranty is in lieu of all other warranties either express or implied This company is not responsible for the independent conclusions opinions or recommendations made by others based on the field exploration and laboratory test data presented in this report It should be noted that all surficial environmental assessments are inherently limited in the sense that conclusions are drawn and recommendations developed from information obtained from limited research and site evaluation Subsurface conditions were not field investigated as part of this study and may differ from the conditions implied by the surficial observations Additionally the passage of time may result in change in the environmental characteristics at this site and surrounding properties The work performed in conjunction with this assessment and the data developed resulted from available information at the dates and locations given in the records searched and visible and accessible evidence on the Site Consequently this report does not warrant or guarantee that any and all problems that may exist at the site were disclosed nor does it warrant against operations or conditions present of type or at location not investigated nor against future operations or conditions 10 APPENDIX FIELD SCREENING EQUIPMENT FI-Nu ATEC used portable instrument called an H-Nu to measure TPVs emitted from the soil samples The H-Nu is equipped with small pump which continuously draws air samples into an ionization chamber which is flooded with ultra-violet light Ionization of the vapors within this chamber results in the generation of an electric current which relates to the concentration of vapors below this energy Most of the light permanent gases such as those in ambient air have ionization potentials at 12 eV or more while many organic chemicals benzene xylene toluene etc have ionization potentials below 10.5 eV For the purposes of this investigation the H-Nu was used as screening tool for the presence of photo-ionizable contaminants Following extrusion the sample was placed in plastic sample bag and the pump inlet for the H-Nu was placed in the bag for measurement The highest value recorded during this procedure was recorded on the boring logs For screening purposes ATEC relies on the calibration performed on the instrument at the factory The factory calibrates the instrument to 100 ppm benzene therefore values reported on the boring logs represent ppm as benzene In screening applications the actual numerical values recorded are of secondary importance especially since there are no established United States Environmental Protection Agency U.S EPA and the Indiana Department of Environmental Management IDEM standards for TPVs The relative magnitude of the values between sampling sites is considered to be of primary importance in screening for the presence of contaminated samples In general background levels of TPVs at an undeveloped site could range from to 25 ppm while background values at an industrial site or gasoline station could range from to 50 ppm APPENDIX BORING LOGS ATE Associates Inc SOiL BORING LOG 5150 Enat 65th Suoot Indianopol indiana 317 849-4990 Chant City of South Bend Sonag B4 Poo Subsurface Investigation job 21-07-95-00802 ntjcci i.oc.uon NW Corner of Tutt and Lafayette South Bend Indiana DRILLING and AMFUi3 INFORMATION D.ta Stmt.d 9/18/95 Hamomr Wi N/A lb. Data Cowplntad 9/18/95 Hnn.mnr map N/A to Drill Foraman Walker Spoon Saninr OD N/A in Boring Ia.pacIor Kaneshiro Rock Coca Di.N/A sono oo Boring Mathod Geoprobe Shalby Tuba OD N/A SAMPLING NOTES Boring Location 48 ft Soagh and 23 ft Eant of MW-IL_ SOIL CLASSIFICATION SURPACEEVATION ___________ Bto.n moos Clayny Silty Sand with pi.cm of brickFUJ 2.0 own madjum to con.SILTY SAND SM with 100 I-60 100 ND 60 10- 100 Inch Black .oam Ii.to nwdittm Sand balow 1511 D.cr.uutg lilt belowll 100 10 100 20.0 Bosom of Tim Boring at 20.0 It CallacOid SatiIe No.6 10-12th to VOC ___________________________________ SAMPt TYPE STAyWARD PENETRATION TEST AT COMPLETION Fr USA Ieou.ow STEM AUGERS 1W TOTAL PTO-IO86ATION VAPORS pr nas Fr GaO OEOPP.OBE IFV TorAL PLAME-IONIZATION VAPORS WATER ON RODS HA HAND AUGERS PPM PARTS WIIION ATE Associates Inc SOIL BORING LOG 5150 Earl 65th SEmI lodianapoli Indiana 317 849-4990 Client City of South Bend Boring B2 Prnoot Norm Subsurface 1nyti8ation tub 21-07-95-00802 Project Loc.lioo NW Corner of Tutt and Lafayette South Bend Indiana DIILING oral SAMPLING 1NposMnoN D.te Started 9/18/95 Hainnier Wc N/A ii. Dora Completed 9/18/95 Hammer Drop N/A in Drill Fomonee Walker Spoon Sampler OD N/A Boeing Importer Kanbiro Rock Core nm N/A AND Boring Method GeOoeobe Shelby Tubs OD N/A in SAMPLING NOTES Boeing Lecatlon 118 ft E.et and 38 ft Sonalh of WYR._._ SOIL CLASSIFICATION Lu SURFACE ELEVATION ______________ Brown momS Silty Sand with Grovel md Brick 100 s.o 100 14 Red mote medium SILTY SAND SM littl fine 2.5 2-3 inch Seam of black with Grovel material oocourgerd_3 100 100 LIght brown below 86 -- ClaywithGrevoll4-16f1 100 100 j_S 100 100 ND _____________________________________________18.0 Bottom of Teat Boeing e1 18.06 Coll.ct.d Seniple No 2.5 2-36 the VOC Iaboreteq onely. ___________________________________ SAMPL TYPE spr STANDARD PENEIAIZN TEST AT COMPLETION FT lISA HOLLOW STEM AUOEBS TPV TOTAL PHOTO.IONEL4IION V/JOBS jo 010 OBOfEOBE TPV TOTAL ASilE.IONATKN V/JOBS PT HA HAND AUOBIS PPM PASTS MILLION AT ON RODS ATE Associates Inc SOIL BORING LOG client City of South Bend B-3 Project Name Subsurface 1nvtjtion Job 21-07-9500802 pt Lo.o.NW Corn of Tuft and Lafayette South Bend Indiana DRILLING and SAMPLING INFORMATION D.teSt.n.d 9/18/95 Ilammnowt N/A lb. Dent Co.npletod 9/18/95 Hammer Drop N/A DriU WaIk Spoon S.nlor OD N/A to Bo.i..g Impeclor Kanhiro Rock Corn Di.N/A in 5pJ Boat.g Method Geoprobe Sholby Tube 00 N/A SAMPLING NOTES Eoth Location 73 ft Snih nd 58 ft MWI SOIL CLASSIFICATION SURPACEELEVATION ____________ Show.moiat Clayny Silty Sand with trot Grovel ioo NDll 2.5 Shown moag m.dwm to coat..SILTY SAND 100 ND Grovil 100 Decroa.ng SIR ioo NI belme6 100 100 ND 15-i 100 100 ND 10 100 ND __________________20.0 BoSom of Toot Doting at 20.0 ft 20-ColIeclad S.nIe No.1020forVOC.anipliag I________________________ SAMPL TYPE SFT STANDARD PERIETRATKN TEST AT COMPLETION PT lISA HOLLOW STERI AUGERS 1W TOTAL PHOTO-1ONATION VAPORS EMS FT OHO OBOPROBE TFV TOTAL FL4MB4NATION VAPORS WA ON RODS PT HA HAND AUGERS FF5.1 PArTS PMILLXN Pap of ATE Associates Inc SOIL BORING LOG 5150 E..t 65th Street lodiuoopoli b.dietrn 317 849-4990 City of South Bend Boriog B4 Prqjoot N.m Suheurface Investiation iot 21.079500802 peojeot i.oo.teon NW Cornet of Tuft and Lafayette South Bsd Indiana DRILLING end SAMPLING INFORMATION .to St.tted 9/18/95 Hammer Wt N/A lb. Date Completed 9/18/95 Hemmer Deop N/A rn DeW Foreman Walker Spoca Sampler OD N/A Boring Inigoolor IL Kaneshiio Book Core Din N/A ja.AND Boeing Method GeOBrobe Shelby Tube OD NIP in PLING NOTES Boeing Location 140 ft Soidh aad 40 ft Eand of MWJL SOIL CLASSIFICATION SURFACE ELEVATION Bewe mood CInysy Siky Send with fragm.rgsof go ND PD..L 2.5 ownmoImonmSUTYSANDSM 100 ND I-100 ND 100 ND 25 ND 190 ND CoameSanda below 12 ft 100 ND -y is 100 ND I.9100 ND 10 100 ND 20.0 Bottom of Teat Dent1 at 20.0 20 ColI.et.d Sample No.1020theVOC ___________________________________ SAMPL TYPE FTANDAID PE11ATION TEST AT COMPLETION FT HSA WOLLOW SI AUGBBS TPV TOTAL pnmO-KUZAJION VAPORS APr ORG OROPEOBE TFV TOTAL FLAME-IOtWATION VAPORS WAT ON RODSPPM PARTS PMU.LION ATE Associates Inc SOIL BORING LOG lodirnrnpoli.b.diom 317 849-4990 clorn City of South Bend oring it B5 N..OO Subaurface Investiiation Job it 21-07-95.00802 Projont Loonlion NW Corner of Tutt and Lafayette South Bend Indiana DRILLING oM SAMPLING INFORMATION oto stort..i 9/18/95 itoonmor wi N/A lb. n.t Contplnrni 9/18/95 liommor Irop N/A Drill Porn...WaIkr Spoon S.nrplrr 00 N/A .n Boring In.poctor Kanesbiro Rock Core Di.N/A j.SORrO Shelby 1\.be OD N/A in SAMPLING NCYES Booing Location _16 ft Srnelh and 78 ft Ejet of B-4 SOIL CLASSIFICATION U4 SURFACEELEVATION ____________ow rnnirnCl.y.y Silty Sorni PILL 100 ND 2.5R.I brown moint m.diorn SILTY SAND Slt 100 ND with Grovel Co..bown Satd to ft 100 ND 100 ND Co..SoM with 1mm Grovel front to lOft ND .iit ..nti below ft 100 ND 100 100 ND Vety Co...w.th Grovel below 15 ft 960 ND 10 100 ND _________________________________________20.0 20Bone.of Ton B..i at 20.0 ft Colkot.d S.nIe No.10 205 for VOC I.bo..tooy nit.Iy.n ____________________________________ SAMER TYPE STANDARD PfEr1ATION TEST AT COMPLETION PT lISA 1100.1.0W SISh AUGEBS TPV TOTAL PROTO-XIATBN VAPOES HR PT OEO OEOOIE TFV TOTAL PLAME-128rzATKne VAPORS WATER ON RODS FF HA HAND AUGEBS PPM PARTS PER MILUON P.g of ATE Associates Inc SOIL BORING LOG 5150 Eag 65th Street lotiloonpolia lodinna 317 049-4990 Client City of South Bend Bonng B6 Project Name Subsurface Investiation Job 21-07-95-00802 pct oooon NW Corner of Tuft and Lafayette South Bend Indiana DRILLING and SAMPLING INFORMATION Date Stattod 9/19/95 Hammer Wi N/A lb. Date Comploted 9/19/95 Hammer Drop N/A Deft Foreman Walker Spoon Sampler OD N/A in Boring In.poclor Kaneshiro Rook Core Din N/A rn Booing Method Ge043eObe Shelby Tub OD N/A in NOTES Boeing Lonatioc 90 ft Seselh and 12 ft of B-A SOIL CLASSIFICATION SURFACE ELEVATION It-_______________ owo molt Silty Sandy Clay with Gavel and 100 ND dobnnofBnickFIIL 30 100 ND Stow mood coat.SILTY SAND SM with Gavel I-100 ND 100 ND 550 ND Fm Sand from Ii to 13 100 ND _________________________________________14.5 inch .oem of SILTY SANDY CLAY CL at 14.5 14.7 100 ND drown mold tour.SILTY SAND SM ND Brown mold cola SILTY SAND SM with Gavel 10 100 ND 20.0 Bottom oCTet Boeing at 20.0 ft 20-ColIonted Saole No.6 10.12 for VOC ________________________ SAMPL TYPI STANDARD PENETRATION TEST AT COMPlETION FT HSA HOLLOW STEM AUGESS TPV TOTAL PIIOTO-IONIZATIOO4 VAPORS pr Fr 010 OIOPE.OEE TFV TOTAL PLAME-IONAT1ON VAPORS WAT ON RODS PT HAND AUGESS FF56 PArES PMLLION Pag of ATE Associates Inc SOIL BORING LOG SSO Los 65th SIroot bdnorpolio lodina 317 849.4960 ci __it of South Bend Boring B7 Projrt 4omn Subsurface 1nvigation Job 21-07-95-00802 Projort ooo NW Corn of Tuft and Lafayette South Bend Indiana DRILLING s.d SAMPLING INFORMATION D.n Stottod 9/19/95 Hs.onr Wi N/A lb. Dot cooiotet 9/19/95 lh.nmor Drop N/A in DriB Foroto.n Wa1k Spoon Su.lor OD N/A Boring lo.pootor Kancshiro Rook Corn Din N/A in Bonog Mithod Geogwobe SIby Tobo OD N/A in SAMPLING NOTES Boring Locsioo 122 ft Snub and 85 ft Et of M2_ SOIL CLASSIFICATION 103 SURFACE ELEVATION Boowo m.d Cloyoy Silty Bond with Grovol 00 FILL 21n.hofSiltyCloy.t2.8 100 Biowo toni md6um to nosno SILTY SAND .AVEL ioo 100 39 50 40 100 37 75 39 is 100 39 SO 40 10 i00 40 __________________20.0 Bosom of Tnt Boring .02005 20-Colbootsd Saniplo No 10208xVOC ___________________________________ SAMPLER TYPE spr STANDARD PENETRATION TEST AT COMPLETRN Fr HSA HOLLOW flER AUGERS1WTOTAL PHOTO-IONIZATION VAPORS vr nas OBO OBOWOIB1WTOTAl FLAME-IONIZATION VAPORS HA KAND AUGERS PPM PArIS PER MILLION MD M ND N p.g of ATh Associates Inc SOIL BORING LOG 5150 Ecat 65th Stowt lodnoopoLi Indiana 317 849-4990 climn ity of South Bend Boring B8 Projwt N.orr Subsurface Invtigation Job 21-07-9500802 Projwt 1ooation NW Corn of Tuft and Lafayette South Bend Indiana DRILUNO and SAMPLING INFORMATION BonnI 9/19/95 iiunmnrwt N/A lb. Data conktad 9/19/95 Mamma Drop N/A in Drill Pooont.n Walkft Spoon Samplor OD N/A in Boring lnoctor Kanhiro Rock Cow Din N/A Boring Mcthod GeOOrObe SaeIby Tub OD N/A in SAMPLING NOTES Boring Location 11 ft Siitdh and 78 ft Wt of MW2_ SOIL CLASSIFICATION SURFACE ELEVATION _______________ Brown moiat roam SILTY NI 100 23 100 42 M.diunt Sand tom 50 41 below 5.0 ft 100 39 j8Inoround Gravel coonon below 15 ft 100 41 10 100 40 20.0 Boon of Ton Boning .120.0 ft 20 Coll.ct.d Simple No.1020trVOC ___________________________________ SAMP1YPB sr STANDARD P8ETL4TION TEST AT COMPLEIIN FT liSA HOU.OW IrESt AUGERS TPV TOTAL POTD-IONATION VAPORS pr lw TOTAL FIAIB-IONATRN WAT ON 1005 Fl MA HAND WOER3 PSM PARTS PMILL20N ATE Associates Inc SOIL BORING LOG SISO Ee.i 6th S%owt Indaoepoh h.dign 317 849-4990 CIIOflI City of South Bend Bogt B9 Projt Nomo Subaurface 1nvtiation mb 21-07-95-00802 Pro/oct Locetion NW Corner of Tutt and Lafayette South Band Indiana DRILLING end SAMPLING INFORMATION Dete Statte 9/19/95 Hemmer wt N/A lb. DeIg Complood 9/19/95 Hemmer Drop N/A rn porem.n Walker Spoote S.ntpkr OD N/A rn Sotie lo.pector IL Kanethiro Rook Cow Dig N/A BORING AND Boeing Method GSIIOObe Shelby Tube OD N/A PLlNG NOTES Boeing Looglion _14 ft and 17 ft Sie$8h of MW- SOIL CLASSIFICATION Ill ______________________ILl-el E.O LI I- SURFACEELEVATION Brownmo4C1eyeySilIySendPlLL 100 39 3.0 100 40 Beowi moim cow.SILTY SAND SM Medium to coem below 100 44 100 40 inch Sm of SILTY SANDY CLAY CL medium to coeme SILTY SAND 100 32SMwithGravel 10 100 42 43 each Sauna SILTY SANDY CLAY CL 14.5 100 26 M-CL Stow moiR medium to Co...SILTY SAND 100 43 Medium 10 100 43 __________________20.0 BoRoin ofTed Bothg at 20.0 It 20-Collected S.nle No.10 205 Ste VOC oeenq ______ ____ SAMPI.TYB SFT STANDARD PSMETRATION TEST AT COMPtEI1ON Fr lilA HOU.OW STt AUGERS TPV TOTAL enorO-KINIZATION VAPORS NRS Fr 0110 GEOBRORR TFV TOTAL FLAME-IONIZATION VAPORS WATER ON RODS HA HAND AUGERS FEEd FAITh FMILLKN MD ATE Associates Inc SOIL BORING LOG 5150 E..t 65th Slorot btdtonnpoli Indinon 317 849-4990 City of South Bend Boin B40 Pmjtt Nomo Subawface inytigaIjon JO1t 21179500802 Loo.Uon NW Corner of Tuft and Lafayette South Bend Indiana DRILLING nnd SAMPLING INFORMATION Ioto stntoti 9/19/95 j.mmoo wt N/A u. Dot contplstod 9/19/95 Hmmco DOO9 N/A in Drin Forotono Walker Spoon 5.nipirr OD N/A Booing In.pootor Kanhiro cor Din N/A in BORING AND Boring Mothod Geoiwobe Sl.Iby Thb 01 N/A SAMPLING NOTES Boring Lanolin 26 ft and Si ft Sondli of MW.J SOIL CLASSIFICATION LU SURFACE ELEVATION tI tL _______________ moon CI.yoy FILL 100 23 100 12 100 With Omni or ft 100 19 100 .6 100 I5 100 100 10 tOO 12 ____________________20.0 Bonn of Tool Boring it 20.0 ft Cotlsctnd Sonipi No 10 20 ft kit VOC ____________________________________ SAMPL TYPE STANDARD PENETRATION TEST AT COMPLETION FT USA 1011.0w STES4 AUOESS TPV TOTAL PHOTO-IONIZATION VAPORS -.vr lIES FT 0B0 0BOtORB TFV TOTAL FLAME-IONIZATION VAPORS HA HAND AUOESB PPM PAul MILLION WAT Pg of ATE Associates Inc SOIL BORING LOG 5150 EoM 65th Stroi bdion.poli Indiono 317 849-4990 clicot City of South Bend Botiog B-il Ptojoct Noon Subaurface InvEStiftation 21-07-95-00802 Poct Location NW Corner of Tutt and Lafayette South Bend Indiana DRIWNG onI SAMPLINO INFORMATION ion Ston.ti 9/19/95 Ham.Wt N/A lb. Dot ConMbond 9/19/95 Hammoc Drop N/A Dtill Footman Walker Spoon Sairiot 00 N/A in oing in.poctor Kaneshiro Rock coot ni.N/A Booing Molbod Geeswobe Shlby Tab 00 N/A rn SAMPLING NOTES Booing Location ft id 31 ft Snili of B-10 SOIL CLASSIFICATION Ui 0.1-t-.O I- SURJtACEELEVATION UU 0.0 _______________so.m.i.t Claysy Silty S.nd 1_ 100 2.0 ow.m.i.t coame SILTY .091 SM 100 100 100 100 100 32 50 25 100 With Gcav.i b.iow 15 ft 100 10 100 10 20.0 BoO..of ToO Booing it 20.0 ft ColI.ct.d Sa.l No.6 20 VOC l.bomoooy an.ly.o ____________________________________ SAMP0 TYPE SPr STANDARD PENETRATION TEST AT COMPLETION FT NSA HOLLOW PT AUGNSS TPV TOrAI POTO-lOWAiRN VAPORS i55 050 OBOPIOBE TPV TOTAl PLAME.IONIZ.4TION VAPORS WAT ON RODS ma HAND AUONSS PPM pArES PSRMn.LHI9 P.1 of ATE Associates Inc SOIL BORING LOG %ffff 5150 65th Stroot Iodiooopoli Iodi.oo 317 849-4990 CIie.t City of South Bend Boriog 1342 Projoot N.m Subsurface Investigation lob 21-07-95.00802 projoot t.o.uo NW Corn of Tuft and Lafayette South Bend Indiana DRJLLING m.d SAMPLING INFORMATION ost sion 9/19/95 13.momr Wt N/A lb. Dm Cosipkt.d 9/19/95 H.m.m.r Drop N/A I.. C.Jl Forsmmt Walker Spoo Simplo OD N/A BO.iOg L..p.c.oo Kaneshiro Rook Coo Di.N/A Bo.iog Muthod GCOIIObe Shelby Tub OD N/A SAMPUNG MOrES Daub Looioa 48 ft So.lb md ft of B.1 SOIL CLASSIFICATION SURFACEELEVATION ______________ owt moi CI.y.y Silty 5i.I FlU oo ND 3.0 100 Show moig 0e SILTY SAND SM to.. Gavel ijo.gI.hco100Withdepd 100 100 M.diemS.nd.b.tw..nhlIol3ft 100 100 100 withuw.oo.v.Ibeloi6ft 100 ND 100 100 20.0 BoBtm of Ted Boiteg aS 20.0 ft 20-ColIect.d S.nI No.1020lbVOC I.botsteq .lys. ___________________________________SAM TYPE ar $TAND/JD PIETRATION TEST AT COMPLSTION lISA HOLLOW 1I AUGESS 1W TOTAL PHcym-WMOZATXIN VAPORS sraa usa Fr OHO OBOPROBE 1W TOTAL i1ON VAPORS FT HA HAND AUGESS PPM PASTS Pna MILLION Peg of ATE Associates Inc SOIL BORING LOG 5l50En65thSunct IndiocpoIi I..d.n 347 849-4990 Clirot City of South Be1ad Boring B-3-1 Projoct Nmc Subsurface Inveslisation me 21-07-95-00S02 Pt 1.ocaIjo NW Corner of Tuft and Lafayette South Bend Indiana tan.uro .od SPUNo INFORMATION S.ocI 10/2/95 Iimmoc Wi N/A lb. 10/2/95 I0.mm.r Drnp N/A rn Drill Pc Walker Spoo S.nl.r 00 N/A Boring io.p.ctor Kaneshiro Rock Corn Di.N/A rn Boring Mothod Geoiwobe Sb.Iby Thbn OD N/A rn SAMPLING NOTES Boring Locoioa__M ft So.h 31 ft East of MW SOD CLASSIFICATION SURFACEELEVATION ___________ Brown CI.ey Sihy S.od P11.1 2.0 Brown moUl rn.dUrn SILTY SAND Sh4 with 100 I100 100 20 10- 100 100 100 9100 Been.of Ted Boeing nI 2o.o 20.0 20 10 100 from2-3 10-12 ist 20 It Be Tolvono ____________________________________ SAMPI.RR TYPE sr srAIODARD PENErRATION TRF AT COMPLErI0N Fr HSA HOU.OW S1 AUOS 1W TOTAL PVarO-IONIZATION VAPOBS Fr OBO OBOPROBE TPV TOTAL FLAME-IONIZATION VAPOE.S WAThR ON RODS PT HA HAND AUOBES PPM PARTS PBE MILLION ATE Associates Inc SOIL BORING LOG775150E.65th SIocet Indi.n.poli Idino 317 S49-4990 Client City of South Bend Boeing B84 Project Nume Subsurface 1nvtigation mi 21-07-95-00802 Pnoct Locution NW Corn of Tutt and Lafayette South Bend Indiana DRILLING end SAMPLING INPORMATION Dnte Slanted 10/2/95 Hummer WI N/A lb. Duin Completed 10/2/95 Hummer Deep N/A in Drill Fn WaIk Spoon Sampler GD N/A in ao.j.g in.p.cut Kaniiro Rock Cone Di.N/A in Method Geoprobe Shelby Tube GD N/A in SAMPLING NOTES Boring Loention 1O ft Soudh iiI ft of MWrI_ SOIL CLASSIFICATION SURFACRELEVATION ___________ Brown mel Claysy Silty Saud and Brick PILL 100 3.0 Brown moi.t medium to coin SILTY SAND 100 58 .1 100 .10 100 BeR.n of Tent Bmieg 20.0 ft Soil .entpl.nolhseind frnm2-3 10-12 ft .120krTolvme ___________________ SAMPt TYPE SPT STANDARD PESIES1ATION TEST AT COM_PLETOON Fr NSA HOLLOW STPM AUGERS 1W TOTAL PHOTOIONIZATION VAPORS pr OBO GBOER.ORB1WTOTALFLAME-ERlAl1ON VAPORS WA ON RODS Fr HA H AUOS PPM PARTS MILLION ATE Associates Inc SOIL BORING LOG lodinnapoli li.than 317 849-4990 Client City of South Bend Bonog B-li-i Pojet Subaurface 1nvtiiation lob 21-07-95-00802 Peojeot Loorlion NW Corn of Tuft and Lafayette South Bend Indiana DRILLING and SAMPLING INFORMATION Dstn sta.te 10/2/95 Itan.mr Wt N/A lb. Data Co.oplnted 10/2/95 Hammer Drop N/A in Drill pon.Wa1k Spoon Sampler OD N/A Boring Inipecoor Kanndiiro Rook Core Din N/A BORING AND Boring Mathod GCOIWOb Shelby Tube OD N/A in SAMPLING NOtES Boring Loedion I2 ft Soaelh ii MW-SR SOIL CLASSIFICATION tel 0I-Cl-LI I- SURFACEELEVATION IL own mold Clay.y Silty Sand deb.i of Briak ioo FILL 4.0 100 Brown maid fine to m.diun SILTY SAND SM Claybalowlft 100 Tome Giavel below ft M.dinmbelow lOft 10- 100 Clay with true Gravel below 12 ft 100 20.0 20- 10 100 Bottom of Tad Bonug at 20.0 ft Sod sanipi.noU.nt.d froe.2-3ftI0-12ft and 20 It lbTolvene MMPL TYPE $PT STANDABD PtRTRAThN TEST AT COMPIZflON Fr NSA HOLLOW ST AUONSS 1W TOTAL PHOTOlONMION VAPORS AFT BBS Ft ORG OBOfRORE1WTOTAL PLAME-RHlA11ON VAPORS WAT ON RODS FT HA R pzra pMULION Pagalof APPENDIX ANALYTICAL RESULTS ATEC Associates Inc __Environmental Consultants 5150 East 65th Street Indianapolis Indiana 462204871 Solid Hazardous Waste Site Assessments 3t7 84W4990 FAX 317 849-5260 Remedial Design Construction Underground Tank Management Asbestos Sameys Analysis Hydrogeologic Investigations Monitoring Analytical Testing Chemistry Indsutnial Hygiene Hazard Communication Enoironmeotal Audits Permitting Eoploratory Drilling Monitoring Wells September 29 1995 Brad Lewis ATEC Associates Inc 5150 65th St Indianapolis IN 46220-4871 Re Twelve Soil VOA City of South Bend ATEC Work Order Number 9509339 ATEC Project Number 21-07-9500802 Dear Mr Lewis Enclosed is thirty-one page report of results for the Organic Analyses for the twelve soil and water samples which were submitted to the ATEC Environmental/Analytical Testing Division on September 19 1995 on behalf of the City of South Bend The volatile samples were analyzed on Finnigan Incos 50 GC/MS/DS system complete with Superincos Software via SW 846 Method 8240 for Purgeable Organic Compounds Prior to analysis the system was tuned against Bromofluorobenzene and calibrated with the appropriate standard The analytical procedures are performed in accordance with the ATEC Analytical Standard Operating Procedures which are based on the methods referenced in this report These SOPs are available for your review upon request All Soil results are reported on an as received basis unless otherwise specified Any associated Quality Control information will be maintained in the Testing Division ifies copy of which can be forwarded to you upon request After thirty-day period fee will be assessed for this additional information American Testing and Engmeering Corporation Consulting Envs-o and Offices in Major US Cities/Since 1958 MaterialS Engineers Definition of LIMS Terms is included in this report for your convenience Two copies of this Analytical Report are being provided for your records Additional copies can be provided at minimum cost of $30.00 per copy It has been pleasure serving you and as always if there are any questions concerning these results or the ATEC policies please feel free to contact me Respectfully submitted ATEC ASSOCIATES INC Maiy McG -M II GC/MS Group Leader Environmental/Analytical Testing Division MMM/lam AlEC ENVIRONMENTAL DIV Order 95-09-339 5150 65TH ST Date 09/25/95 1522 Indianapolis IN 46220 Work ID City of S.B 2107-9500802 Date Received 09/19/95 Attn Bred Lewis Date CompLeted 09/25/95 Invoice Number SAMPLE IDENTIFICATION AlEC Client ATEC Client SampLe Sample SampLe SampLe ho Description Description 01 B-i 10-12 02 B-2 2-3 03 R-3 20 04 3-4 20 05 B-S 20 06 3-6 20 07 B-I 20 08 8-8 20 09 3-9 20 10 B-i020 Ii B-il 10-12 12 3-12 20 This report shalt not be reproduced except in fuLL without approval of the Laboratory Mary GILL-MaxweLl ATEC Associates REPORT Work Order 95-09-339 Received 09/19/95 REPORT COMMENTS LIMS General Definition of Terms Order Number AlEC Laboratory Identification for your sample set Please reference this number with any correspondence Sample Number ATEC Laboratory Identification for individual samples with the set Sample Description Your Sample Identification Teat Description Analytical Test Result Analytical Value Obtained Result QuaLifiers denotes less than denotes greater than N/A denotes not applicable denotes not reported denotes anstyte detected but amount present is less than the Quantitation Limit denotes analyte spiked with matrix spike compound denotes snatyte found in method blank ND not detected Units Unit of Measurement Limit Denotes Quantitation Limit Limit of reliability based the sample quantity analyzed the sample matrix and the analytical method sensitivity Analyzed Optional Field for Date Analyzed Ny Optional Field for Test Analyst AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-1 10-12 TEST CODE 8240 NAME VoLatiLe FRACTION O1A Date Time CoLLected 09/18/05 Category SOIL _______________________________ DATE .WALTZED 09/21/95 INSTRUMENT Incos RV2 DILUTION FACTOR _________________ ANALYST Rooknis VERIFIED RI McGiLL UNITS US/Kg COMMENTS Analytical Method SW 846 Mtd 8240 PRIORITY POLLUTANTS VOLATILE CONPOUNDS PARAMETER CAS RESULT LIMIT Chtoromethane 74-87-3 10 10 Bromometirane 74-83-9 10 10 Vin1t ChLoride 75-01-4 10 10 CirLoroethane 75-00-3 10 10 Methytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Digulfide 75-15-0 100 100 1.1-Oichtoroethene 75-35-4 11-Dichloroethene 75-34-3 Total 12-Dichloroethene ChLoroform 67-66-3 12-Dichtoroethane 107-06-2 2-Butanone 78-93-3 100 100 111-Trichleroethene 71-55-6 Carbon Tetrachloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bro.odlchloro.ethane 75-27-4 12-bichloroprOpene 78-87-5 Trans-i 3-Dlchtoropropene 10061-02-6 trichloroethen 79-01-6 ATEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID B-i 10-12 TEST CODE 8240 IIAME VolatiLe FRACTIOn 01A Date Time Collected 09118/95 Category SOIL Oibromochtoromethane 124-48-1 112-TricMoroethane 79-00-5 Benzene 71-43-2 is-I 3-Oichloropropene 10061-01-5 2-ChloroethyLvinytether 110-75-8 10 10 Broaoform 75-25-2 _________ 4-Methyt-2-Pentanone 108-10-i 50 50 2-HexaflOfle 591 -78-6 50 50 Tetraclnloroethane 127-18-4 122-Tatr.chtoroethane 79-34-5 TotuenC 108-88-3 Chtorobenoene 108-90-7 Ethylbenzene 100-41-4 Styrene 100-42-5 Iotat Xytenes Acroein 107-02-8 10 10 Acrytonitrite 107-13-1 100 100 Iodomethefle 74-88-4 100 100 trans i4-Dichtoro-2-butene 110-57-6 100 100 Ethyl methacryLte 97-63-2 100 100 23-Trichtoropropane 96-18-4 100 100 lrichtoroftuoromethafle 75-69-4 10 10 OichtorodifLuoromethane 75-61-8 100 100 ATEC Associates REPORT Work Order 95-09-339 Received 09119/95 SAMPLE ID 8-2 2-3 TEST CODE 8240 NAME Volatile FRACTION 02 Date Time Cottected 09/18/95 Category SOIL _______________________________ DATE ANALYZED 09122/95 INSTRUMENT Incos RV2 DILUTION FACTOR ANALYST Booknis VERIFIED BY McGiLl UNITS ug/Ka COMMENTS AnalyticaL Method SW 846 Ntd 8240 PRIORITY POLLUTANTS VOLATILE COXPOUNDS PAEANETER CAS RESULT LIMIT Chloromethane 74-87-3 10 10 Rro.omethane 74-83-9 010 10 Vinyl Chtoride 75-01-4 ID 10 Chloroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 13 Acetone 67-64-1 100 100 Carbon Disultide 75-15-0 100 100 1.1-DichLoroethene 75-35-4 11-Dichtoroethane 75-34-3 Tctal 12-Dtclitoroethene ChLoroform 67-66-3 05 12-Dichloroethene 107-06-2 2-Rutanone 78-93-3 100 100 111-Trichloroethane 71-55-6 05 Carbon Tetr.chtoride 56-23-5 _________ Vinyl Acetate 108-05-4 50 50 Bro.odichLoromethane 75-27-4 12-Dichleropropane 78-87-5 Trans-I 3-Dichtoropropene 10061-02-6 c5 Trichloroethene 79-01-6 AlEC Ammocates REPORT york Order 95-00-339 Received 09119195 SAMPLE ID 8-2 2-3 TEST CODE 8240 MANE Volatile FRACTION 02 Date Time Collected 09/18/95 Category SOIL Dibromochloromethane 124-48-1 112-Trichtoroethane 79-00-5 ______ Benzene 71-43-2 cis-1 3-Dichloropropene 10061-01-5 ______ 2-Chloroethylvinylether 110-75-8 10 10 Bromoform 75-25-2 4-Nethyl-2-Pentanone 108-10-1 50 50 2-Nexanone 591-78-6 50 50 Tetrechloroethene 127-18-4 1122-Tetrechtoroethafle 79-34-5 ________ Toluene 108-88-3 Chtorobenzene 108-90-7 Ethylbenzene 100-41-4 Styrene 100-42-5 Total Xytenes ________ Acrolein 107-02-8 10 10 Acrylonitrile 107-13-1 100 100 lodomethane 74-88-4 100 100 tr.ns 14-DtchLoro-2-butene 110-57-6 100 100 Ethy methacrytate 91-63-2 100 100 23-Trichtoropropane 96-18-4 100 100 Trichlorofluoromethane 75-69-4 10 19 Dichtorodiftuoromethane 75-61-8 100 100 AlEC Associates REPORT Work Order 95-09-339 Received 09119195 SAMPLE ID 8-3 20 TEST CODE MANE Volatile FRACTION 03A Date Time Collected 09/18/95 Category SOIL ________________________________ DATE ANALYZED 09/21/95 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Rooknis VERIFIED BY McGill UNITS ugfKg CONNECTS AnaLytical Method SW 546 Ntd 8240A PRXORITY POLLUTANTS VOLATILZ COMPOUNDS PARANETU CAS RESULT LIMIT Chtoroasetliane 74-87-3 10 10 Broisosethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chloroethane 75-00-3 10 10 Nethytene ChLoride 15-09-2 Acetone 67-64-1 100 100 Carbon Disutfide 75-15-0 100 100 11-Dichtoroethene 75-35-4 ________ 11-Dichloroethane 75-34-3 Total 12-DichEoroethene Chtorof ore 67-66-3 12-Dichtoroethane 107-06-2 2-Butanone 78-93-3 109 109 111-TrlchLoroethane 71-55-6 Carbon Tetrachloride 56-23-5 Vinyl Acetate 108-05-4 50 59 Bro.odichloromethane 75-27-4 ________ 12-Dichloropropane 78-87-5 Trans-I 3-DlchtorOpropene 10061-02-6 Trichloroethefle 79-01-6 AlEC Asaociates REPORT Work Order 95-09-339 Received 09/19/95 S6PLE ID 8-3 20 TEST CODE 8240 SAME Vojetile FRACTIOW 03A Date Time CoLlected 09/18/95 Category SOIL _________Dibromochtoromethane 124-48-1 112-Trichtoroethane 79-00-5 Renzene 71-43-2 cis-1 3-Dichloropropene 10061-01-5 Z-Choroethyvinytether 110-75-8 10 10 Bromoform 75-25-2 ________ 4-Methyt-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 TetrachLoroethene 127-18-4 1122-TetrachIoroethane 79-34-5 Toun 108-88-3 110 Chtorobenzene 108-90-7 Ethytbenzene 100-41-4 Styrene 100-42-5 Tot Xytenes Acrolein 107-02-8 10 10 Acrytonitrite 107-13-1 100 100 lodomethane 74-88-4 100 100 trans 14-Dichoro-2-butene 110-57-6 100 100 Ethyl methecrytate 97-63-2 100 100 123-Trichtoropropane 96-18-4 100 100 Trichtoroftuoromethane 75-69-4 10 10 Dichlorodifluoromethane 75-61-8 100 100 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-4 20 TEST CODE 8240 lAME VoLatile FRACTION 048 Date Time ColLected 09/18/95 Category SOIL ________________________________ DATE ANALYZED 09/21/95 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Booknip VERIFIED BY MCGiLL UNITS ug/1 COMMENTS Analytical Method SW 846 Ntd 8240 PRIORITY POLLUTANTS VOLATILE COMPOUND8 PARAMETER CAS RESULT LIMIT Chloromethane 74-87-3 10 10 Rro.o.ethane 74-83-9 10 10 Vinyl ChLoride 75-01-4 10 10 Chloroeth.ne 75-00-3 olD 10 Nethytene Chloride 75-09-2 Acetone 67-64-1 109 100 Carbon Disutfide 75-15-0 100 1OD 11-DichLoroethene 75-35-4 11-Dichloroethane 75-34-3 Total 12-Dichtoroethene Chloroform 67-66-3 12-Dichloroethane 107-06-2 2-Rutanone 78-93-3 100 109 111-Trichloroethane 71-55-6 Carbon Tetrachtoride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bro.odichtoroaethan 75-27-4 12-Dichloroprop.ne 78-87-5 _________ Irene-I 3-Dlchloropropene 10061-02-6 Trichloroethene 79-01-6 AlEC Associates REPORT Uork Order 95-09-339 eceiYed 09/19/95 SAMPLE ID 8-4 20 TEST CODE 8240 NAME Volatile FRACTION 048 Date Time CoLlected 09/18/95 Category SOIL _________Dibromochloromethane 124-48-1 112-Trichloroethane 79-00-5 Beflzene 71-432 cis-1 3-Dichloropropene 10061-01-5 2-Chloroethylvinytether 110-75-8 10 10 Bromoform 75-25-2 4-Methy-2-Perttanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachloroethene 127-18-4 11 22-TetrachIoroethane 79-34-5 ToLuen 10888-3 87 Chlorobenzene 108-90-7 Ethytbenzene 100-41-4 Styrene 100-42-5 Total Xylenes Acrolein 107-02-8 10 10 Acrytonitrite 107-13-1 100 100 lodomethane 74-88-4 100 100 trans 1i.-DjchLoro-2-butene 110-57-6 dOS 100 Ethyl methacrylate 97-63-2 100 100 123-1richLoropropane 96-18-4 100 500 Trjchtorofuoro.ethane 75-69-4 10 10 Dichlorodiftuoromethane 75-61-B 500 100 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-5 20 TEST CODE 8240 NAME Volatije FRACTION 05A Date Time ColLected 09/18/95 Category SOIL ________________________________ DATE ANALYZED 09/21/05 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Booknis VERIFIED BY McGill UNITS US/KS CONMEITS Analytical Method SW 846 Mtd 8240A PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Chloromethane 74-87-3 cIt 10 Bromousethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chtoroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 100 11-DichLoroethene 75-35-4 11-Dichloroethane 75-34-3 Total 12-Dichloroethene Chloroform 67-66-3 1.2-Dichtoroethane 107-06-2 2-But.non 78-93-3 100 100 111-Trichloroethane 71-55-6 Carbon Tatrachloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bromodlchloromethane 75-27-4 12-Dichloropropane 78-87-5 Trans-i 3-Dichloropropene 10061-02-6 Trichloroethene 79-01-6 ATEC Aasociates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-5 20 TEST CODE 8240 NAME Volatile FRACTION OSA Date Time ColLected 09/18/95 Category SOIL Dibromochloromethane 124-48-1 112-Trichloroethane 79-00-5 _______ Benzene 71-43-2 do-i 3-Dichtoropropene 10061-01-5 2-ChLoroethyvinytether 110-75-8 10 10 Bromof or 75-25-2 4-Methyl-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachloroethene 127184 11 22-Tetrachloroethane 79-34-5 Totuone 108-88-3 29 Chtorobenoene 108-90-7 Ethylbenzene 100-41-4 Styrene 100-42-5 Total Dylenes Acrolein 107-02-8 10 10 AcryLonitrite 107-13-1 100 100 Iodomethane 74-88-4 100 100 trans 14-Dichoro-2-butene 110-57-6 100 100 Ethyl ethacrytate 97-63-2 100 100 1.23-Trichloropropane 96-18-4 100 100 Trichtoroftuoromethane 75-69-4 10 10 Dichlorodifluoromethane 75-61-8 100 100 AlEC Ammociates REPORT Work Order 95-09-339 Receyed 09119/95 SAMPLE ID R-6 20 TEST CODE 8240 NAME VoLatiLe FRACTION 06A Date Time CoLlected 09/19/95 Category SOIL _________________________________ DATE ANALTZED 09/21/95 INSTRUMENT Incos 8V2 DILUTION FACTOR ANALYST Booknis VERIFIED BY McGiLl UNITS uS/Kg CONENTS Analytic Method SW 846 Mtd 8240 PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Chtoromethane 74-87-3 10 10 Oro.o.ethane 74-83-9 10 10 VinyL Chloride 75-01-4 i0 10 Chloroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 100 11-Dichtoroethene 75-35-4 ii-Dichloroethane 75-34-3 Total 12-Dichtoroethene Chloroform 67-66-3 i2-Oichloroethane 107-06-2 2-Butanone 78-93-3 100 100 11Trhloroet.e _________ ________ Carbon Tetr.chtoride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bromodichloremethane 75-27-4 12-Dlchloropropane 78-87-5 Trans-i 3-Dichtoropropene 10061-02-6 Trichloroethene 79-01-6 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-6 20 TEST CODE 8240 hARE Volatile FRACTION 06A Date Time Collected 09/19/95 Category SOIL Dibromochtoromethane 124-48-1 112-Trichloroethane 79-00-5 Benzene 71-43-2 cis-I 3-Dichtoropropene 10061-01-5 2-Chtoroethylvinylether 110-75-8 10 10 Bromoform 75-25-2 4-Methy-2-Pentanone 108-10-1 50 50 2-Mexanone 591-78-6 50 50 Tetrachtoroethene 127-18-4 1122-Tetrachtoroethane 79-34-5 TohuAne 108-88-3 120 Chlorobenzene 108-90-7 Rthytbenaene 100-41-4 Styr.ne 100-42-5 Total Oytenes Acroein 107-02-8 10 10 Acrylonitrite 107-13-1 100 100 lodomethane 74-88-4 100 100 trans 14-Dichtoro-2-butene 110-57-6 100 100 Ethyl aethacrytate 97-63-2 100 100 123-Trichloropropane 96-18-4 100 100 Trichloroftuoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 8-7 20 TEST CODE 8240 NAME Volatile FRACTION 07 Date Time ColLected 09/19/95 Category SOIL _________________________________ DATE ANALYZED 09/22/95 INSTRUMENT Incos RV2 DILUTION FACTOR _________________ ANALYST Rooknis VERIFIED BY McGiLL UNITS US/ta COMMENTS __________AnaLytical Method SW 846 Mtd 8240 PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT ChLoromethane 74-87-3 10 10 Rromomethane 74-83-9 10 10 Vinyl ChLoride 75-01-4 10 10 Chtoroethane 75-00-3 10 10 Methylene Chloride 75-09-2 Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 190 11-Dichtoroetheoe 75-35-4 i1-Dichtoroethane 75-34-3 Total i2-Dichtoroethene Chloroform 67-66-3 i2-Dichloroethane 107-06-2 2-Rutanone 78-93-3 100 100 111-TrichLoroethane 71-55-6 Carbon T.trachLoride 56-23-5 Vinyl Acetate 108-05-4 50 50 Rroaodlchloro.ethane 75-27-4 12-Dichtoropropane 78-87-5 Trans-i 3-Dlchtoropropene 10061-02-6 _________ ________ Trichoro.th.ne 79-01-6 ________ ATEC Associates REPORT Uork Order 95-09-339 Received 09/19/95 SAMPLE ID 8-7 20 TEST CODE 8240 NAME Volatile FRACTION 07A Date Time Collected 09/19/95 Category SOIL __________DibromochLoromethane 124-48-1 112-TrichLoroethane 79-00-5 BenZene 71-43-2 cis-1 3-Dichtoropropene 10061-01-5 2-ChLoroethyvinytether 110-75-8 10 10 Bromofor 75-25-2 4-Nethyl-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachloroethenm 127184 122-Tetrachtoroethane 79-34-5 Totuene 108-B8-3 21 Chtorobenzene 108-90-7 Rthytbenzene 100-41-4 Styrene 100-42-5 Total Sytenes Acrolein 107-02-8 10 10 AcrylonitriLe 107-13-1 100 100 Jodomethane 74-88-4 100 100 trans 14-DichLoro-2-butene 110-57-6 100 100 Ethyl .ethacryLate 97-63-2 100 100 23-TrichLoropropane 96-18-4 100 100 Trichtorofuoromethane 75-69-4 10 10 Dichloradiftuoromethane 75-61-8 100 100 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID B-A 20 TEST CODE 8240 MANE Volatile FRACTION 08A Date Time CoLlected 09/19/95 Category SOIL _________________________________ DATE ANALYZED 09/22/95 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Booknis VERIFIED RT McGill UNITS ug/Eg COMMENTS Analytical Method SW 846 Mtd 8240A PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Chtoro.ethane 74-87-3 10 10 Rromo.ethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chloroethane 75-00-3 10 10 Netilytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Disutfide 75-15-0 100 100 11-Dichioroethene 75-35-4 11-Dichtoroethane 75-34-3 Total i2-Dichloroethene ChLoroform 67-66-3 12-Dichloroethane 107-06-2 2-Rutanone 78-93-3 100 100 111-Trlchloroethane 11-55-6 Carbon T.trachtorld 56-23-5 Vinyl Acetate 108054 50 50 Bro.odichloromethana 75-27-4 12-DichLoropropane 78-87-5 Trans-i 3-DichLoropropene 10061-02-6 Trichloroethene 79-01-6 ATEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE 10 8-8 20 TEST CODE 8240 NAME VoLatile FRACTION 08A Date Time CoLlected 09/19/95 Category SOIL __________Oibromochoromethane 124-48-1 112-TrichLoroetharie 79-00-5 Benzene 71-43-2 cis-1 3-Dichloropropene 10061-01-5 2-Chtoroethytvinyether 110-75-8 10 10 Rromoform 75-25-2 4-Nethyl-2-Pentanone 108-10-1 50 50 2-Kexanone 591-78-6 50 50 TatrachLoroeth.ne 127-18-4 11 22-Tetrachtoroethane 79-34-5 Totuene 108-88-3 140 Chlorobenzene 108-90-7 Ethybenzene 100-41-4 Styrene 100-42-5 Total Xylenes Acrotein 107-02-8 10 10 Acrytonitrite 107-13-1 100 100 Iodo.ethane 74-88-4 100 100 trans 14-Dichloro-2-butene 110-57-6 100 100 EthyL RethacrytRte 97-63-2 100 100 123-Trichtoropropane 96-18-4 100 100 Trichloroftuoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 ATEC Associates REPORT blork Order 95-09-339 Received 09/19/95 SAMPLE ID B-S 2O TEST CODE 8240 NAME Volatile FRACTION 098 Dote Time ColLected 09/19/95 Category SOIL _________________________________ DATE ANALYZED 09/22/95 INSTRUMENT IncOS BV2 DILUTION FACTOR ANALYST Booknis VERIFIED BY McGiLl UNITS Up/Kg COMNENTS AnaLyticaL Method SW 846 Mtd 8240A PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT ChtoroNethane 74-87-3 10 10 Bromomethane 74-83-9 10 10 Vinyl ChLoride 75-01-4 10 10 Chtoroethane 75-00-3 10 10 Nethyl.ne ChLoride 75-09-2 ACetone 67-64-1 100 100 Carbon Disutfide 75-15-0 100 100 11-Dichloroethene 75-35-4 11-DichLoroothane 75-34-3 Total 12-DichLoroethene ChLoroform 67-66-3 12-Dichloroethan 107-06-2 2-Butanone 78-93-3 100 100 111-TrichLoroethane 71-55-6 Carbon Tetrachloride 56-23-5 VInyl Acetate 108-05-4 50 50 Bro.odlchloromethane 75-27-4 12-Dichloropropane 78-87-5 Trans-1 3-Dichtoropropene 10061-02-6 Trichloroethene 79-01-6 ATEC Associates REPORT york Order 95-09-339 Received 09/19/95 SAMPLE ID B-9 20 TEST CODE 8240 NAME VolatiLe FRACTION 09.A Date Time ColLected 09/19/95 Category SOIL __________Dibromochtoromethane 124-48-1 112-Trichoroethane 79-00-5 Renzene 71-43-2 cis-1 3-DichLoropropene 10061-01-5 2-Chloroethylvinytether 110-75-8 10 10 Bromoform 75-25-2 4-Methyt-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachloroethene 127-18-4 1122-Tetrachloroethane 79-34-5 Totu.n 108-88-3 30 Chlorobenzene 108-90-7 Ethybenzene 100-41-4 Styrene 100-42-5 Total Dytenes Acrolein 107-02-8 10 19 AcrytonitriLe 107-13-1 100 100 Iodo.ethane 74-88-4 100 100 trans 14-DjchLoro-2-butene 110-57-6 100 100 Ethyl methacrylate 97-63-2 100 100 23-Trichtoropropane 96-18-4 100 100 Trichtorofluoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 AlEC Amsociates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID N152O TEST CODE 8240 NAME Volatile FRACTION iSA Date Time ColLected 09/19/95 Category SOIL _______________________________ DATE ANALYZED 09/22/95 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Booknis VERIFIED BY McGilL UNITS Ug/Eg CONMEUTS Analytical Method SW 846 Ntd 8240A PRIORITY POLLUTANTSVOLATILECOMPOUNDS PARAMETER CAS RESULT LIMIT Chloro.ethane 74-87-3 10 10 Bro.o.ethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chloroethane 75-00-3 10 10 Nethyl.n ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 100 11-Dichloroethene 75-35-4 11-Dichloroethane 75-34-3 Total 12-Dichloroethene Chloroform 67-66-3 12-DIchloroeth.ne 107-06-2 2-Butenone 78-93-3 100 100 111Trichloroethane 71-55-6 ______ Carbon Tetrachloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bromodichloromethane 75-27-4 12-Dichloropropan 78-87-5 Trans-i 3-Dichloropropene 10061-02-6 Trichtoroethene 79-01-6 AlEC Associates REPORT Work Order 95-09-339 Receivedr 09/19/95 SAMPLE ID 8-1020 TEST CODE 8240 NAME VoLatiLe FRACTION iSA Date use ColLected 09/19/95 CategOry SOIL Dibromochtoromethane 124-48-1 112-Trichtoroethene 79-00-5 Benzene 71-43-2 cis-1 3-Dichtoropropene 10061-01-5 2-Chtoroethytvinyether 110-75-8 010 10 Bromoform 75-25-2 4-Methyt-2-Pentanone 108-10-1 59 50 2-Hexanone 591-78-6 50 80 Tetrachtoroethene 127-18-4 1122-Tetrachtoroethane 79-34-5 Totuene 1OR-8R-3 11 ChLorobenzene 108-90-7 Ethytbencene 100-41-4 Styrene 100-42-5 TotaL Xytenes Acrotein 107-02-8 10 10 Acrytonitrite 107-13-1 100 100 Iodoffiethane 74-88-4 100 100 trans 14-DjchLoro-2-butene 110-57-6 100 100 EthyL methacrytate 97-63-2 100 100 123-Trichtoroprop.ne 96-18-4 0100 100 Trichiorofluoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 ATEC Associatea REPORT Work Order 95-09-339 Received 09/19195 SAMPLE ID B-li flO-12 TEST CODE 8240 NAME Volatile FRACTION 11 Date Time Collected 09/19/95 Category SOIL _______________________________ DATE ANALYZED 09/22/95 INSTRUMENT Incos RV2 DILUTION FACTOR ____________________ ANALYST Rooknis VERIFIEDRT M.McGitl UNITS uB/K CONNENTS Analytical Method SW 846 Mtd 8240A PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Choro.ethane 74-87-3 10 10 Bromomethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chloroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 100 11-Dichloroethene 75-35-4 11-Dichtoroethane 75-34-3 Total 1.Z-Dichloroethene Chlorofor 67-66-3 12-Dichloroethane 107-06-2 2-Rutanone 78-93-3 100 100 111-Trichloroethane 71-55-6 Carbon T.tr.chloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Rro.odiclLoro.ethane 75-27-4 12-Dichloropropane 78-87-5 Trans-i 3-Dichloropropene 10061-02-6 Trichloroethene 79-01-6 ATEC Associates REPORT Work Order 95-09-339 Received 09119195 SAMPLE ID B-li 10-12 TEST CODE 8240 NAME Volatile FRACTION 11 Date Time ColLected 09/19/95 Category SOIL _________Dibromochloromethane 124-48-1 112-Trichloroethane 79-00-5 Benzene 71-43-2 cis-1 3-Oichloropropene 10061-01-5 2-ChLoroethyvinylether 110-75-8 10 10 Bromoform 75-25-2 4-Methyt-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachoroethene 127-18-4 1122-Tetrachloroethane 79-34-5 Tatuene 108-18-3 130 Chlorobenzene 108-90-7 Ethytb.nzene 100-41-4 Styrene 100-42-5 Total Xylenes Acrolein 107-02-8 10 10 Acrylonitrite 107-13-1 100 100 lodomethane 74-88-4 100 100 trans l4-Dichtoro-2-butene 110-57-6 100 100 EthyL methacrytate 97-63-2 100 100 123-Trichloropropane 96-18-4 100 100 Trichlorofluoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 II AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 9-12 20 TEST CODE 8240 NAME Volatile FRACTION 12 Date Time CoLlected 09/19/95 Category SOIL _____________________________ DATE ANALYZED 09/22/95 INSTRUMENT Incos BV2 DILUTION FACTOR _________________ ANALYST Booknis VERIFIED BY McGILL UNITS ug/K CONMERTS Analytical Method SW 846 Mtd 8240 PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT ChLoro.ethane 74-87-3 10 10 Bro.o.eShane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chloroethane 75-00-3 10 10 Nethytene Chtoride 75-09-2 ________ Acetone 67-64-1 100 100 Carbon Disulfide 75-15-0 100 100 i1-DichLoroethene 75-35-4 11-DichLoroethane 75-34-3 Total 12-Dichloroethene Chloroform 67-66-3 l2-DichLoroethane 107-06-2 2-Butanone 78-93-3 100 100 111-Trichtoroethane 71-55-6 Carbon Tetrachloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Bromodichloromethane 75-27-4 12-Dichtoropropane 78-87-5 Trans-i 3-Dichloroprepene 10061-02-6 TrlchLoroethene 79-01-6 iI AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID 6-12 20 TEST CODE 8240 NAME Volatile FRACTION 12A Date Tice ColLected 09/19/95 Category SOIL _________Dibromochloromethane 124-48-1 112-TrichLoroethane 79-00-5 Benzeoe 71-43-2 cis-1 3-Dichloropropene 10061-01-5 2-ChLoroethylvinytether 110-75-8 10 10 Bromoform 75-25-2 4-NethyL-2-Pentanone 108-10-1 50 SD 2-Ilesanone 591-78-6 50 50 Tetrachtoroethene 127-18-4 11 22-Tetrachloroethane 79-34-5 Totuene 1O8-R8-3 92 ChLorobenzene 108-90-7 Rthytbenzene 100-41-4 Styrene 100-42-5 Total Xylenes Acrolein 107-02-8 10 10 Acrytonitrile 107-13-1 100 100 lodomethane 74-88-4 100 100 trans 14-DichLoro-2-butene 110-57-6 100 100 Ethyl methacrylate 97-63-2 100 100 23-TrichLoropropane 96-18-4 100 100 Trichtorofluoromethane 75-69-4 10 10 EithtorodifLuoromethane 75-61-8 100 100 ATEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID Method Riank TEST CODE 8240 NAME Volatile FRACTION 128 Date Time CoLlected _____________Category SOIL _______________________________ DATE ANALYZED 09/21/95 INSTRUMENT Incos RV2 DILUTION FACTOR ANALYST Rooknis VERIFIED RT McGiLl OMITS ug/Eg COMMENTS AnaLytical Method SW 846 Mtd 8240 PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Chtoro.ethane 74-87-3 10 10 Rro.omethane 74-83-9 10 10 Vinyl Chloride 75-01-4 10 10 Chtoroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 12 Acetone 67-64-1 100 100 Carbon Disutfide 75-15-0 100 105 11-DichLoroethene 75-35-4 11-Dichtoroethane 75-34-3 ______ Total 12-Dichtoroethene ChLoroform 67-66-3 12-Dichloroethane 107-06-2 2-Butanone 78-93-3 100 100 111-Trichtoroethane 71-55-6 Carbon Tetrachtorlde 56-23-5 Vinyl Acetate 108-05-4 50 50 Rromodlchtoro..thane 75-27-4 12-DlchLoropropane 78-87-5 Trans-i 3-Dichtoropropene 10061-02-6 Trlchtoroethene 79-01-6 AlEC Associates REPORT Vork Order 95-09-339 Received 09/19/95 SAMPLE ID Method Blank TEST CODE 8240 NAME Volatile FRACTION Date Time Collected ______________Category SOIL _________Dibroeochloromethane 124-48-1 1l2-TrichLoroethafle 79-00-5 Benzene 71-43-2 cls-1 3-Dichloropropene 10061-01-5 2-Chloroethylvinylether 110-75-8 10 10 Broisoform 75-25-2 4-Methyl-2-Pentanone 108-10-I 50 50 2-Hexanone 591-78-6 50 50 Tetrachloroethene 127184 _________ 122-Tetrachloroethane 79-34-5 Toluene 108883 Chlorobencene 108-90-7 Ethylbeniene 100-41-4 Styrene 100-42-5 Total Oylenes Acrolein 107-02-8 10 10 Acrylonitrile 107-13-1 100 100 lodomethane 74-88-4 100 100 trans 14-Oichloro-2-butene 110-57-6 100 100 Ethyl methacrylate 97-63-2 100 100 23-Trichoropropane 96-18-4 100 100 Trichlorofluoromethane 75-69-4 10 10 Dichtorodiftuoromethane 75-61-8 100 100 AlEC Associates REPORT Work Order 95-09-339 Received 09/19/95 SAMPLE ID Method Rtank TEST CODE 8240 NAME Volatile FRACTION 12C Date Time Collected _____________Category SOIL _____________________________ DATE ANALTZED 09/22/95 INSTRUMENT Incos BV2 DILUTION FACTOR ANALYST Booknis VENIFIEDBT M.McGilI UNITS up/Kg COMMEUTS Analytical Method SW 846 Mtd 8240A PRIORITY POLLUTANTS VOLATILE COMPOUNDS PARAMETER CAS RESULT LIMIT Chloromethane 74-87-3 10 10 Bromo.ethane 74-83-9 10 10 Vinyl ChLoride 75-01-4 19 10 Chloroethane 75-00-3 10 10 Nethytene ChLoride 75-09-2 Acetone 67-64-1 100 100 Carbon DisuLfide 75-15-0 100 100 11-Dichoroethene 75-35-4 1.1-Dichloroethane 75-34-3 TotaL 1.2-DichLoroethene ChLoroform 67-66-3 12-Dithtoroethane 107-06-2 2-Butanone 78-93-3 100 100 1l1-TrichLoroathene 71-55-6 Carbon Tetrachloride 56-23-5 Vinyl Acetate 108-05-4 50 50 Broaodlchoro.ethane 75-27-4 12-Dichtoropropane 78-87-5 Trans-I 3-DlchLoropropene 10061-02-6 Trlchtoroethene 79-01-6 AlEC Associates REPORT Vork Order 95-09-339 Received 09/19/95 SAMPLE ID Method Blank TEST CODE 8240 NAME Volatije FRACTION 12C Date lice Collected _____________Category SOIL _________Dibromochloromethane 124-48-1 112-Trichloroethane 79-00-5 Beozene 71-43-2 cis-1 3-Dichloropropene 10061-01-5 .5 2-Chtoroethylvinytether 110-75-8 10 10 Bromoform 75-25-2 .5 4-Methyl-2-Pentanone 108-10-1 50 50 2-Hexanone 591-78-6 50 50 Tetrachtoroethene 127-18-4 1122-Tetrachloroethane 79-34-5 lotuene 108-88-3 Chtorobenzene 108-90-7 Ethylbenzene 100-41-4 Styrene 100-42-5 Total Xytenes Acrotein 107-02-8 10 10 Acrytonitrite 107-13-I 100 100 lodomethane 74-88-4 .100 100 trans 14-Dichtoro-2-butene 110-57-6 100 100 Ethyl methacrylate 97-63-2 .100 100 123-Trichtoropropane 96-18-4 100 100 lrichtorofluoromethane 75-69-4 10 10 Dichlorodifluoromethane 75-61-8 .100 100 ATEC Environmental Consultants DM.on of AlEC Auociates Inc 5150 East65th Street Indianapolis Indiana 46220-4871 7849-4990AX7849-4278 O7 SU3NIVINOO 3OH39IIflN ____ olaiov 03B311l4 ___ _____ 3iISOdPO3Ih I-i-___- Oc y_\c- ATEC Associates Inc __Environmental Consultants 5150 East 65th Street Indianapolis Indiana 46220-4871 Solid Hazardous Waste Site Assessments 3171 849-4990 FAX 317 8495260 Remedial Design Construction Undergroand Tank Management Asbestos Surseys Anatysis Hydrogeologic tnoestigatiOns Monitnring Analytical Testing Chemistry Industrial Hygiene Hazard Communication Enuironmentat Audits Permitting Exploratory Drilling Monitoring Welts October 1995 Brad Lewis ATEC Associates Inc 5150 65th Street Indianapolis IN 46220 Re Three Soil Toluene City of South Bend ATEC Work Order Number 9510044 ATEC Project Number 21-07-9500802 Dear Mr Lewis Enclosed is six page report of results for the Organic Analyses for the three soil samples which were submitted to the ATEC Environmental/Analytical Testing Division on October 1995 on behalf of the City of South Bend The Toluene samples were analyzed on Finnigan Incos 50 GC/MS/DS system complete with Superincos Software via SW 846 Method 8240 for Purgeable Organic Compounds Prior to analysis the system was tuned against Bromofluoro benzene and calibrated with the appropriate standard The analytical procedures are performed in accordance with the ATEC Analytical Standard Operating Procedures which are based on the methods referenced in this report These SOPs are available for your review upon request All Soil results are reported on an as received basis unless otherwise specified Any associated Quality Control information will be maintained in the Testing Division files copy of which can be forwarded to you upon request After thirty-day period fee will be assessed for this additional information American Testing and Engineering Corporation Consulting Enuiro and Offices in Major U.S Cities/Since 1958 Materials Engineers Definition of UMS Terms is included in this report for your convenience Two copies of this Analytical Report are being provided for your records Additional copies can be provided at minimum cost of $30.00 per copy It has been pleasure serving you and as always if there are any questions concerning these results or the ATEC policies please feel free to contact me Respectfully submitted ATEC ASSOCIATES INC Mary cGll-Maxwell GC/MS Group Leader Environmental/Analytical Testing Division MMM/lam ATEC Associates Inc 5150 East 65th Indianapolis IN 46220 Attn Brad Lewis Lab Proj 95100353 Date 10/06/1995 Cust Proj City of South Bend 2107-9500802 Date Received 10/03/1995DateCompleted10/04/1995 REPORT OF ANALYSIS ATEC Client ATEC Client Sample Sample Sample Sample Number Description Number Description 95-001777 8-3-1 20 9510044-1 95-001778 8-8-1 20 9510044-2 95-001779 8-11-110-12 9510044-3 95-001802 Method Blank This report shall not be reproduced except in full without approval of the Laboratory ______________ Mary McGill-Maxwell Date of Report 10/06/95 Project Number 95100353 Lab ID 95-0001777 Date Collected 10/02/95 1107 Collected By Client Date Received 10/03/95 1020 of Number Attention Brad Lewis Temperature Received on Ice ATEC Associates Inc 5150 East 65th Indianapolis IN 46220 pie Desc B-3-1 20 9510044-1 Det Test Result Unit Limit Procedure Date ICNS VOLATILES Toluene ug/Eg SW 8240 10/03/95 Date of Report 10/06/95 Project Number 95100353 Lab ID 95-0001778 Date Collected 10/02/95 1210 Collected By Client Date Received 10/03/95 1020 of NumberttentionBradLewisTemperature Received on IceATECAssociatesInc 5150 East 65th Indianapolis IN 46220 ample Desc 3-8-1 20 9510044-2 Det Test Result Unit Limit Procedure Date IC VOLATILES Toluene ug/Kg Sw 8240 10/03/95 Date of Report 10/06/95 Project Number 95100353 Lab ID 95-0001779 Date Collected 10/02/95 1240 Collected By Client Date Received 10/03/95 1020 of Number ention Brad Lewis Temperature Received on Ice ATEC Associates Inc 5150 East 65th Indianapolis IN 46220 Oample Desc B-ll-1l0-12 9510044-3 Det Test Result Unit Limit Procedure Date DR IC VOLP.TILES Toluene ug/Kg SW 8240 10/03/95 Date of Report 10/06/95 Project Number 95100353LabID95-0001802 Date Collected 10/03/95 1240 Collected By Client Date Received 10/03/95 1020 of Number Attention Brad Lewis Temperature Received on IceATECAssociatesInc 5150 East 65th Indianapolis IN 46220 plc Desc Method Blank Det Test Result Unit Limit Procedure Date ANIC CMS VOLATILES Toluene ug/Rg SW 8240 10/03/95 ATEC Environmental Consultants DMsoq of AlEC Auoclals Inc 6t 5150 East 65th Street Indianapolis Indiana 46220-4871 %o 317849-4990FAX317849-4278 NN5 --------- SH3NIYiNO3 dO8BYdflN ___ ____ aaI4IolD lbs d3iVM 3llSOdYIOO Lull Corporate Headquarters 8665 Bash Street Indianapolis IN 46256-1202 317 577-1761 FAX 311 842-7308 With Offices Nationwide